CN101947266A - Solid aromatic sobering-up agent and preparation method thereof - Google Patents
Solid aromatic sobering-up agent and preparation method thereof Download PDFInfo
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- CN101947266A CN101947266A CN2010105015185A CN201010501518A CN101947266A CN 101947266 A CN101947266 A CN 101947266A CN 2010105015185 A CN2010105015185 A CN 2010105015185A CN 201010501518 A CN201010501518 A CN 201010501518A CN 101947266 A CN101947266 A CN 101947266A
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Abstract
The invention discloses a solid aromatic sobering-up agent and a preparation method thereof. The solid aromatic sobering-up agent comprises the following components in percentage by mass: 0.75 to 1.50% of sobering-up essence, 0.50 to 1.50% of solid air refresher, 8.00 to 10.00% of efficient solubilizer, 0.40 to 0.60% of preservative and the balance of distilled water. The preparation method comprises the following four steps: preparing the sobering-up essence, solubilizing the sobering-up essence, preparing gel and mixing the sobering-up essence and the gel. In the invention, the essential oil such as anise oil is used as a component of the sobering-up essence, and the prepared solid aromatic sobering-up agent is an all-natural, nontoxic, harmless and safe product. Moreover, as the sobering-up agent comprises components such as lavender oil, the solid aromatic sobering-up agent emits fresh and soft smell of flowers and grass, which not only can purify air, but also has functions of removing fatigue, resisting depression and comforting mood; the sobering-up agent can consecutively emit pleasant aroma for 3 to 5 days and has no pollution to environment.
Description
Technical field
The invention belongs to technical field of chemistry, be specifically related to the sober up preparation method of blending technology and solid aromatic amethystic agent thereof of essence of a kind of solid aromatic.
Background technology
In China, wine is a kind of culture of the whirl of society, and spirits culture is just as cigarette is cultural, and is of long standing and well established.Drink is to merge in people's life.But wine is to tipsy, often will have certain sober up and relieve the effect of alcohol method.
At present, the product of the class of relieving the effect of alcohol on the domestic market, sober up is a lot, mainly is to be prepared into medicine (the general composite sheet medicine of RU21 peace body of the U.S., VC sheet etc.), health product (mainly being the Chinese herbal medicine Radix Puerariae, Flos Camelliae Japonicae, Herba Lycopi's root etc.).Also having some is foodstuff (Mel, Fructus Citri Limoniae, Semen phaseoli radiatis etc.).People are by taking in body Nei Laida Antialcoholic liver-protecting effect.Existing domesticly also have the floral water of use to wipe examination drunk person temple method can obviously to alleviate its signs of getting drunk.
And solid aromatic amethystic agent of the present invention is made by blending technology by several quintessence oils, and people reach and alleviate headache, dizzy, restless, nauseating, sober up effect more easily by aromatotherapy.The composition of wherein effectively sobering up has aniseed oil, Fructus Citri Limoniae oil, Mentha piperita wet goods.This product belongs to a kind of nontoxic, safety product.Show the domestic like product that also do not have.
Summary of the invention
One of purpose of the present invention is to provide a kind of solid aromatic amethystic agent.
Two of purpose of the present invention is to provide a kind of preparation method of above-mentioned a kind of solid aromatic amethystic agent.
Three of purpose of the present invention provides the essence of sobering up used in a kind of preparation method of solid aromatic amethystic agent.
Technical scheme of the present invention
A kind of solid aromatic amethystic agent, the mass percent of its contained each composition is composed as follows:
The essence 0.75%～1.50% of sobering up
Solid air freshening glue 0.50%～1.50%
Efficient solubilizing agents 8.00%～10.00%
Antiseptic 0.40%～0.60%
Surplus is a distilled water;
Efficient solubilizing agents wherein is based on nonionic, amphoteric ionic surfactant, mainly is the organic compound of alcohol, ether structure: polyoxypropylene fatty alcohol ether, polyoxyethylene aliphatic alcohol ether (12-13 alkanol polyxyethylated alcohol) etc.; Be preferably 12-13 alkanol polyxyethylated alcohol;
Solid air freshening glue wherein is macromolecular materials such as polyvinyl alcohol, hydroxypropyl emthylcellulose or modified cellulose; Be preferably modified cellulose;
Antiseptic wherein is a DMDMH(dihydroxymethyl dimethyl hydantoin) and IPBC(3-iodo-2-propynyl butyl carbamate) mixture; Be preferably that model is the product of G.P.L in the Chinese daily use chemicals industry.
The wherein said essence of sobering up comprises components such as Oleum lavandula angustifolia, oil of rosemary, eucalyptus quintessence oil, thyme oil, mentha piperita oil, Oleum Menthae Rotundifoliae, aniseed oil, people's health oil, Oleum Caryophylli, Fructus Citri Limoniae oil, laurel, hyacinthin, Oleum Pelargonii Graveolentis, coriander seed oil, Oleum Cinnamomi, antioxidant;
And the mass percent of each component described in the essence of sobering up sees Table 1:
The mass percent of each component preferably sees Table 2 in the above-mentioned described essence of sobering up:
A kind of preparation method of solid aromatic amethystic agent comprises being prepared as follows step:
(1), the sober up allotment of essence
To sober up, each component adds in the anticorrosion container (1) successively by sequence number in the essence, is stirred to 15 minutes and promptly reaches even later on;
(2), the sober up solubilising of essence
The essence of sobering up that step (1) is deployed carries out solubilising:
At first in anticorrosion container (2), add account for solid aromatic amethystic agent product gross mass (hereinafter to be referred as: product population) be 8.00～10.00% efficient solubilizing agents, be heated to 55～60 ℃, after 15 minutes, to clear; To account for product population be the deployed essence of sobering up of 0.75～1.50% step (1) to wherein adding then, after stirring 5～10 minutes with agitator, stirs, and at room temperature allows its natural cooling, promptly gets the solubilising essence of sobering up;
(3), the colloidal preparation of gel
Add in anticorrosion container (3) that to account for product population be 86.40～90.50% distilled water, for preventing that distilled water evaporates the variation that causes gross weight in the heating process, can add into accounting for product population in this process is 10.00～15.00% distilled water, heat, progressively being sprinkled into while stirring and accounting for product population is 0.50～1.50% solid air freshening glue, and heated and stirred to 85～90 ℃, after 20～30 minutes, after making powder dissolution, stop heating, its stirring is cooled to temperature about 60 ℃, promptly gets the gel colloid;
(4), sober up essence and gel and close
Add in the gel colloid of step (3) gained that to account for product population be to continue to stir after 0.40～0.60% the antiseptic, when naturally cooling to 40～50 ℃, the solubilising of slowly in the gel colloid, pouring step (2) gained into the essence of sobering up, after continuing stirred for several minute, when treating that the temperature natural cooling is got back to 30～40 ℃, stop to stir, promptly and be combined into the solid aromatic amethystic agent;
It is poured in the anticorrosion mould, allow it naturally cool to room temperature, promptly get solid aromatic amethystic agent product of the present invention.
Key character of the present invention be to sober up in the solid aromatic amethystic agent blending technology of essence.
Beneficial effect of the present invention
The present invention is the primary raw material of perfume ingredient of sobering up with aniseed oil, Fructus Citri Limoniae oil, mentha piperita oil, Herba Rosmarini Officinalis wet goods quintessence oil, and the solid aromatic amethystic agent product of gained belongs to a kind of pure natural, nontoxic, safety product.Can make solid aromatic amethystic agent of the present invention give out the fragrant fragrance of pure and fresh soft flowers and plants owing to also contain Oleum lavandula angustifolia, Herba Pelargonii Graveolentis wet goods composition in the solid aromatic amethystic agent again, not only can purify air, and the effect of driving away tired, anti-melancholy, peace show tender affection for emotion arranged, when bringing pure and fresh, fragrant fragrance of a flower gas to air, can also alleviate dizzy after drinking, headache, bring joyful, comfortable sensation to health.
Solid aromatic amethystic agent of the present invention is compared with other type products on the market, safety, to human body have no side effect, easy to carry, it is also convenient to use, and is not subject to influences such as temperature, humidity.Under conventional environment, can continue to discharge 3～5 days pleasant fragrance, also pollution-free to environment.
The specific embodiment
Below by embodiment, the present invention is further described, but do not limit the present invention.
Now use Shanghai tie up U.S. biotechnology Development Co., Ltd produce the model that provides as the product of LA01 as the solid air freshening glue in the solid aromatic amethystic agent;
The model of now using Shanghai Fine Chemical Co., Ltd of Supreme Being section to produce to provide as the product of Cosmacd N II-9 as the efficient solubilizing agents in the solid aromatic amethystic agent;
The model of now using Shanghai Fine Chemical Co., Ltd of Supreme Being section to produce to provide as the product of G.P.L as the antiseptic in the solid aromatic amethystic agent;
Now use the product B HT(2.6-ditertbutylparacresol that Shanghai traditional Chinese medicines group company produces to be provided) do
Antioxidant for the solid aromatic amethystic agent.
Embodiment 1
A kind of solid aromatic amethystic agent, the mass percent of its contained each composition is composed as follows:
Essence A 0.75% sobers up
Solid air freshening glue 0.50%
Efficient solubilizing agents 8.00%
Antiseptic 0.40%
Surplus is a distilled water 90.35%
The preparation method of above-mentioned a kind of solid aromatic amethystic agent comprises being prepared as follows step:
(1), the sober up allotment of essence A
The mass percent of each raw material sees Table 3 in the essence A example of sobering up:
According to the quality percentage composition of each component in the table 3, each component is added in the anticorrosion container (1) successively by sequence number in the table 3, be stirred to 15 minutes and promptly reach even later on;
(2), the sober up solubilising of essence A
The essence A that sobers up that step (1) is deployed carries out solubilising: add in anticorrosion container (2) at first that to account for product population be 8.00% efficient solubilizing agents, be heated to 55～60 ℃, after 15 minutes, to clear; To account for product population be 0.75% the deployed essence A that sobers up of step (1) to wherein adding then, after stirring 10 minutes with agitator, stirs, and at room temperature allows its natural cooling, promptly gets the solubilising essence A that sobers up;
(3), the colloidal preparation of gel
Add in anticorrosion container (3) that to account for product population be 90.35% distilled water, for preventing that distilled water evaporates the variation that causes gross weight in the heating process, can add into accounting for product population in this process is 15.00% distilled water, heats, and progressively being sprinkled into while stirring and accounting for product population is 0.50% solid air freshening glue, and heated and stirred to 85～90 ℃, after 30 minutes, make powder dissolution after, stop the heating, its stirring is cooled to temperature about 60 ℃, promptly gets the gel colloid;
(4), sober up essence A and gel and close
Add in the gel colloid of step (3) gained that to account for product population be to continue to stir after 0.40% the antiseptic, when naturally cooling to 40～50 ℃, the solubilising of slowly in the gel colloid, pouring step (2) gained into the essence A that sobers up, continue to stir, when treating that the temperature natural cooling is got back to 30～40 ℃, stop to stir, promptly and be combined into the solid aromatic amethystic agent.It is poured in the anticorrosion mould, allow it naturally cool to room temperature, promptly get solid aromatic amethystic agent product of the present invention.
The solid aromatic amethystic agent of above-mentioned gained has the fragrant and sweet gas of tangible fennel sweet gas and osmanthus, and blue or green fragrance of a flower fragrance is not obvious, and fragrance is not too natural, and fragrance is too single, fragrance inadequately circle and, abundant, do not send out thoroughly, outward appearance is transparent gel-form.After a period of time, fragrance weakens gradually, loses fragrance, and the colloid evaporation rate is fast.Can continue to discharge 2～3 days pleasant fragrance, sober up effect is more obvious.
Embodiment 2
A kind of solid aromatic amethystic agent, the mass percent of its contained each composition is composed as follows:
Essence B 1.50% sobers up
Solid air freshening glue 1.50%
Efficient solubilizing agents 10.00%
Antiseptic 0.60%
Surplus is a distilled water
The preparation method of above-mentioned a kind of solid aromatic amethystic agent comprises being prepared as follows step:
(1), the sober up allotment of essence B
The mass percent of each raw material sees Table 4 in the essence B example of sobering up:
According to the quality percentage composition of each component in the table 4, each component is added in the anticorrosion container (1) successively by sequence number in the table 4, be stirred to 15 minutes and promptly reach even later on;
(2), the sober up solubilising of essence B
The essence B that sobers up that step (1) is deployed carries out solubilising:
Add in anticorrosion container (2) at first that to account for product population be 10.00% efficient solubilizing agents, be heated to 55～60 ℃, after 15 minutes, to clear; To account for product population be 1.50% the deployed essence B that sobers up of step (1) to wherein adding then, after stirring 10 minutes with agitator, stirs, and at room temperature allows its natural cooling, promptly gets the solubilising essence B that sobers up;
(3), the colloidal preparation of gel
Add in anticorrosion container (3) that to account for product population be 86.40% distilled water, for preventing that distilled water evaporates the variation that causes gross weight in the heating process, can add into accounting for product population in this process is 15.00% distilled water, heats, and progressively being sprinkled into while stirring and accounting for product population is 1.50% solid air freshening glue, and heated and stirred to 85 ℃～90 ℃, after 30 minutes, make powder dissolution after, stop the heating, its stirring is cooled to temperature about 60 ℃, promptly gets the gel colloid;
(4), sober up essence B and gel and close
Add in the gel colloid of step (3) gained that to account for product population be to continue to stir after 0.60% the antiseptic, when naturally cooling to 40～50 ℃, the solubilising of slowly in the gel colloid, pouring step (2) gained into the essence B that sobers up, continue to stir, when treating that the temperature natural cooling is got back to 30～40 ℃, stop to stir, promptly and be combined into the solid aromatic amethystic agent; It is poured in the anticorrosion mould, allow it naturally cool to room temperature, promptly get solid aromatic amethystic agent product of the present invention;
The solid aromatic amethystic agent of above-mentioned gained has obviously compound with faint fragrance of a flower fragrance, slightly cool, hot fragrant and sweet gas.Fragrance is sent out thoroughly, coordination, pure and mild, mellow and full, be transparent outward appearance, and have certain gel.With the passing of time, fragrance can slowly volatilize, and still can keep fragrance preferably, and bottom note still has is with compound flower note hot sweet, really sweet, herbal, and colloidal outward appearance also can diminish over time gradually, but the state of its gel can't change.3～5 days pleasant fragrance can be continued to discharge, and sobering-up functions can be effectively reached.
Embodiment 3
A kind of solid aromatic amethystic agent, the mass percent of its contained each composition is composed as follows:
Essence C 1.13% sobers up
Solid air freshening glue 1.00%
Efficient solubilizing agents 9.00%
Antiseptic 0.50%
Surplus is a distilled water
(1), the sober up allotment of essence C
The mass percent of each raw material sees Table 5 in the essence C example of sobering up:
According to the quality percentage composition of each component in the table 5, each component is added in the anticorrosion container (1) successively by sequence number in the table 5, be stirred to 15 minutes and promptly reach even later on;
(2), the sober up solubilising of essence C
The essence C that sobers up that step (1) is deployed carries out solubilising:
Add in anticorrosion container (2) at first that to account for product population be 9.00% efficient solubilizing agents, be heated to 55～60 ℃, after 15 minutes, to clear; To account for product population be 1.13% the deployed essence C that sobers up of step (1) to wherein adding then, after stirring 10 minutes with agitator, stirs, and at room temperature allows its natural cooling, promptly gets the solubilising essence C that sobers up;
(3), the colloidal preparation of gel
Add in anticorrosion container (3) that to account for product population be 88.37% distilled water, for preventing that distilled water evaporates the variation that causes gross weight in the heating process, can add into accounting for product population in this process is 15.00% distilled water, heats, and progressively being sprinkled into while stirring and accounting for product population is 1.00% solid air freshening glue, and heated and stirred to 85～90 ℃, after 30 minutes, make powder dissolution after, stop the heating, its stirring is cooled to temperature about 60 ℃, promptly gets the gel colloid;
(4), sober up essence C and gel and close
Add in the gel colloid of step (3) gained that to account for product population be to continue to stir after 0.50% the antiseptic, when naturally cooling to 40～50 ℃, the solubilising of slowly in the gel colloid, pouring step (2) gained into the essence C that sobers up, continue to stir, when treating that the temperature natural cooling is got back to 30～40 ℃, stop to stir, promptly and be combined into the solid aromatic amethystic agent, it is poured in the anticorrosion mould, allow it naturally cool to room temperature, promptly get solid aromatic amethystic agent product of the present invention.
The solid aromatic amethystic agent of above-mentioned gained has obvious cool flavor fragrance, and the herbal breath of stronger eucalyptus quintessence oil breath of tangible penetration power and thyme oil is arranged, fragrance inadequately circle and, pure and mild, outward appearance is transparent gel-form, after a period of time, fragrance weakens, and the colloid evaporation rate is very fast.Can continue to discharge 2～3 days fragrance, sober up effect is more not obvious.
Above said content only is the basic explanation of the present invention under conceiving, and according to any equivalent transformation that technical scheme of the present invention is done, all should belong to protection scope of the present invention.
Claims (12)
1. solid aromatic amethystic agent is characterized in that the mass percent of its contained each composition is composed as follows:
The essence 0.75～1.50% of sobering up
Solid air freshening glue 0.50～1.50%
Efficient solubilizing agents 8.00～10.00%
Antiseptic 0.40～0.60%
Surplus is a distilled water;
Efficient solubilizing agents wherein is polyoxypropylene fatty alcohol ether, polyoxyethylene aliphatic alcohol ether (12-13 alkanol polyxyethylated alcohol) etc.;
Solid air freshening glue wherein is macromolecular materials such as polyvinyl alcohol, hydroxypropyl emthylcellulose or modified cellulose;
Antiseptic wherein is a DMDMH(dihydroxymethyl dimethyl hydantoin) and IPBC(3-iodo-2-propynyl butyl carbamate) mixture;
The wherein said essence of sobering up comprises components such as Oleum lavandula angustifolia, oil of rosemary, eucalyptus quintessence oil, thyme oil, mentha piperita oil, Oleum Menthae Rotundifoliae, aniseed oil, people's health oil, Oleum Caryophylli, Fructus Citri Limoniae oil, laurel, hyacinthin, Oleum Pelargonii Graveolentis, coriander seed oil, Oleum Cinnamomi, antioxidant;
And the mass percent of each component described in the essence of sobering up sees Table 1:
Described antioxidant is the BHT(2.6-ditertbutylparacresol).
2. a kind of solid aromatic amethystic agent as claimed in claim 1 is characterized in that:
Efficient solubilizing agents wherein is preferably 12-13 alkanol polyxyethylated alcohol;
Solid air freshening glue wherein is preferably modified cellulose.
3. a kind of solid aromatic amethystic agent as claimed in claim 1 or 2 is characterized in that the mass percent of its contained each composition is composed as follows:
The essence 0.75～1.50% of sobering up
Solid air freshening glue 0.50～1.50%
Efficient solubilizing agents 8.00～10.00%
Antiseptic 0.40～0.60%
Surplus is a distilled water;
Wherein said mass percent of sobering up each component described in the essence sees Table 2:
Described antioxidant is the BHT(2.6-ditertbutylparacresol).
4. a kind of solid aromatic amethystic agent as claimed in claim 1 or 2, the mass percent that it is characterized in that its contained each composition are formed and are preferably as follows:
The essence 0.75% of sobering up
Solid air freshening glue 0.50%
Efficient solubilizing agents 8.00%
Antiseptic 0.40%
Surplus is a distilled water 90.35%;
The mass percent of each raw material sees Table 3 in the wherein said essence of sobering up:
Described antioxidant is the BHT(2.6-ditertbutylparacresol).
5. a kind of solid aromatic amethystic agent as claimed in claim 1 or 2 is characterized in that the mass percent composition of its contained each composition is preferably as follows:
The essence 1.50% of sobering up
Solid air freshening glue 1.50%
Efficient solubilizing agents 10.00%
Antiseptic 0.60%
Surplus is a distilled water;
The mass percent of each raw material sees Table 4 in the wherein said essence of sobering up:
Described antioxidant is the BHT(2.6-ditertbutylparacresol).
6. a kind of solid aromatic amethystic agent as claimed in claim 1 or 2 is characterized in that the mass percent composition of its contained each composition is preferably as follows:
The essence 1.13% of sobering up
Solid air freshening glue 1.00%
Efficient solubilizing agents 9.00%
Antiseptic 0.50%
Surplus is a distilled water;
The mass percent of each raw material sees Table 5 in the wherein said essence of sobering up:
Described antioxidant is the BHT(2.6-ditertbutylparacresol).
7. the preparation method of a kind of solid aromatic amethystic agent as claimed in claim 1 or 2 is characterized in that comprising being prepared as follows step:
(1), the sober up allotment of essence
To sober up, each component adds in the anticorrosion container (1) successively in the essence, is stirred to 15 minutes and promptly reaches even later on;
(2), the sober up solubilising of essence
The essence of sobering up that step (1) is deployed carries out solubilising:
At first in anticorrosion container (2), add account for solid aromatic amethystic agent product gross mass (hereinafter to be referred as: be 8.00～10.00% efficient solubilizing agents product population), be heated to 55～60 ℃, after 15 minutes, to clear;
To account for product population be 0.75～1.50% the deployed essence of sobering up of step (1) to wherein adding then, after stirring 5～10 minutes with agitator, stirs, and at room temperature allows its natural cooling, promptly gets the solubilising essence of sobering up;
(3), the colloidal preparation of gel
Add in anticorrosion container (3) that to account for product population be 86.40～90.50% distilled water, for preventing that distilled water evaporates the variation that causes gross weight in the heating process, can add into accounting for product population in this process is 10.00～15.00% distilled water, heat, progressively being sprinkled into while stirring and accounting for product population is 0.50～1.50% solid air freshening glue, and heated and stirred to 85～90 ℃, after 20～30 minutes, after making powder dissolution, stop heating, its stirring is cooled to temperature about 60 ℃, promptly gets the gel colloid;
(4), sober up essence and gel and close
Add in the gel colloid of step (3) gained that to account for product population be to continue to stir after 0.40～0.60% the antiseptic, when naturally cooling to 40～50 ℃, the solubilising of slowly in the gel colloid, pouring step (2) gained into the essence of sobering up, after continuing stirred for several minute, when treating that the temperature natural cooling is got back to 30～40 ℃, stop to stir, promptly get the solid aromatic amethystic agent; Pour in the anticorrosion mould, allow it naturally cool to room temperature, promptly get solid aromatic amethystic agent product of the present invention.
8. the used essence of sobering up of a kind of solid aromatic amethystic agent as claimed in claim 1 or 2, the mass percent of each raw material is as follows in the essence that it is characterized in that sobering up:
Described antioxidant is the BHT(2.6-ditertbutylparacresol).
9. the essence of sobering up as claimed in claim 8, the mass percent of each raw material is formed and is preferably as follows in the essence that it is characterized in that sobering up:
Described antioxidant is the BHT(2.6-ditertbutylparacresol).
10. the essence of sobering up as claimed in claim 8, the mass percent of each raw material is formed and is preferably as follows in the essence that it is characterized in that sobering up:
Described antioxidant is the BHT(2.6-ditertbutylparacresol).
11. the essence of sobering up as claimed in claim 8, the mass percent of each raw material is formed and is preferably as follows in the essence that it is characterized in that sobering up:
Described antioxidant is the BHT(2.6-ditertbutylparacresol).
12. the essence of sobering up as claimed in claim 8, the mass percent of each raw material is formed and is preferably as follows in the essence that it is characterized in that sobering up:
Described antioxidant is the BHT(2.6-ditertbutylparacresol).
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| CN2010105015185A CN101947266A (en) | 2010-10-11 | 2010-10-11 | Solid aromatic sobering-up agent and preparation method thereof |
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| CN102978003A (en) * | 2012-12-18 | 2013-03-20 | 王洪凯 | Composite essential oil adsorbed and released by honeycomb-shaped particle base material |
| CN104107217A (en) * | 2013-04-18 | 2014-10-22 | Cj第一制糖株式会社 | Composition For Preventing Or Treating Hangover |
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| CN104027443A (en) * | 2014-06-03 | 2014-09-10 | 上海应用技术学院 | Solid aromatic anti-alcohol agent and preparation method thereof |
| CN106806927A (en) * | 2016-12-29 | 2017-06-09 | 江阴天鸿环境科技有限公司 | A kind of solid freshener of dispelling fatigue |
| CN106822966A (en) * | 2016-12-30 | 2017-06-13 | 江阴天鸿环境科技有限公司 | A kind of pure and fresh ball of the solid of rose scent |
| CN106668262A (en) * | 2017-02-17 | 2017-05-17 | 云南同方科技有限公司 | Plant essential oil compound for sobering and preparation method thereof |
| CN111544310A (en) * | 2020-05-28 | 2020-08-18 | 安徽省天助纺织科技集团股份有限公司 | Non-irritant antibacterial disinfectant wet tissue and preparation method thereof |
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