CN106729863B - High-elastic moisturizing solid scent and preparation method thereof - Google Patents

High-elastic moisturizing solid scent and preparation method thereof Download PDF

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Publication number
CN106729863B
CN106729863B CN201710132345.6A CN201710132345A CN106729863B CN 106729863 B CN106729863 B CN 106729863B CN 201710132345 A CN201710132345 A CN 201710132345A CN 106729863 B CN106729863 B CN 106729863B
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solid aromatherapy
essential oil
elastic
aromatherapy
preparation
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CN106729863A (en
Inventor
李建强
李玉
吴转璋
余文婷
施雪凤
杨俭
郭玉娇
曹会选
李建红
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Nanchang Yanpu Optoelectronic Precision Instrument Co ltd
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East China Institute of Technology
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00Disinfection, sterilisation or deodorisation of air
    • A61L9/01Deodorant compositions
    • A61L9/012Deodorant compositions characterised by being in a special form, e.g. gels, emulsions
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00Disinfection, sterilisation or deodorisation of air
    • A61L9/01Deodorant compositions
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00Disinfection, sterilisation or deodorisation of air
    • A61L9/01Deodorant compositions
    • A61L9/013Deodorant compositions containing animal or plant extracts, or vegetable material
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L2209/00Aspects relating to disinfection, sterilisation or deodorisation of air
    • A61L2209/20Method-related aspects
    • A61L2209/21Use of chemical compounds for treating air or the like

Abstract

The invention discloses a kind of high-elastic moisturizing solid aromatherapy and preparation method thereof, the high-elastic moisturizing solid aromatherapy includes by weight percentage: carragheen 2.0%~3.0%;Moisturizer 2.2%~2.8%;Methyl hydroxybenzoate 0.05%~0.10%;Nipasol 0.01~0.05%;Essential oil 0.08%~1.50%;Remaining is water.Solid aromatherapy surface smoothness of the invention is good, and in air, after one month, moulding is still three-dimensional, and only volume reduces than before, still keeps good fragrance for exposure;The formula and preparation process that the present invention passes through optimization solid aromatherapy, solid aromatherapy to make has good surface smoothness, moisture retention and elasticity, make the appearance looks elegant of product, fragrance is more lasting, and solid aromatherapy is unlikely to deform and cracks in transport and use process.

Description

High-elastic moisturizing solid scent and preparation method thereof
Technical field
The invention belongs to daily necessities chemical field, it is related to a kind of champignon and preparation method thereof, more specifically, is related to one kind High-elastic moisturizing solid scent and preparation method thereof.
Background technique
Champignon can effectively improve the air quality in closing and semiclosed environment, remove the air peculiar smell in environment, Make air delicate fragrance, builds the atmosphere of a comfortable delicate fragrance.
Most of existing solid aromatherapy increases the viscosity and curing degree of gel by adding salts substances, mainly logical Addition such as calcium chloride salts substances are crossed to adjust the degree of gelation of gel, thus there is easy dehydration and be also easy to produce bubble etc. Situation, manufactured solid aromatherapy may be unsatisfactory in terms of surface flatness, moisture retention and elasticity.Surface flatness is good, makes The appearance looks elegant of product;Good moisture retention makes fragrance more lasting;Good elasticity, solid aromatherapy are being transported and were being used It is unlikely to deform and cracks in journey.
Chinese patent ZL201110405139.0 discloses a kind of solid aromatherapy, in terms of composition weight, comprising 0.8%~ 1.5% emulsifier, 2%~3% heat preserving agent, 0.3%~0.8% stabilizer, 1.2%~1.8% coagulator, 0.05%~0.12% preservative, 3%~8% soap base, 1.5%~3% agar main body, 3%~5% plant essence Oil and 3%~8% charcoal, wherein emulsifier is rilanit special, and heat preserving agent is dipropylene glycol, and stabilizer is polyoxyethylene or card Wave resin series, coagulator are gypsum, and preservative is potassium sorbate, and soap base is sodium soap.Due to using active carbon, solid Champignon is black, unsightly;The degree of gelation of gel is adjusted using gypsum, thus there is easy dehydration and is also easy to produce gas Situations such as bubble.
Therefore, for solid aromatherapy, people have been devoted to improve formula and preparation process, to provide good surface light The solid aromatherapy of slip, moisture retention and elasticity.
Summary of the invention
Therefore, in order to overcome the drawbacks described above of existing solid scent, the purpose of the present invention is to provide one kind have it is good Surface smoothness, moisture retention and elasticity high-elastic moisturizing solid aromatherapy.
Another object of the present invention is to provide the preparation methods of above-mentioned high-elastic moisturizing solid aromatherapy.
According to an aspect of the present invention, high-elastic moisturizing solid aromatherapy of the invention includes by weight percentage:
According to another aspect of the present invention, the preparation method of high-elastic moisturizing solid aromatherapy of the invention, steps are as follows:
Methyl hydroxybenzoate (Methylparaben), Nipasol (Propylparaben) and essential oil are pressed into above-mentioned weight hundred Divide than sampling, mixes them uniformly, obtain uniform essential oil preservative mixed solution;
At 65 DEG C~75 DEG C, carragheen is dissolved in water, moisturizer is added after being completely dissolved, uniformly mixes, obtains Carrageenan solutions;
At 65 DEG C~75 DEG C, essential oil preservative mixed solution obtained above is added in carrageenan solutions, sufficiently After mixing, pour into mold;Then it is cooled and shaped, obtains solid aromatherapy.
Beneficial effect
The present invention passes through the formula and preparation process of optimization solid aromatherapy, for example, preservative methyl hydroxybenzoate and oxybenzene third Ester is used cooperatively, and can be better protected from mildew, be addled, and eliminating peculiar smell keeps fragrance more longlasting, enables essential oil more good dissolving In carrageenan solutions;Moisturizer dipropylene glycol can extend the service life of solid aromatherapy well;Temperature is controlled in preparation Degree and stirring generate bubble to avoid air is entered, so that the solid aromatherapy made has good surface smoothness, moisturizing Property and elasticity, make the appearance looks elegant of product, fragrance is more lasting, and solid aromatherapy is unlikely to deform and opens in transport and use process It splits.
Specific embodiment
In the following, high-elastic moisturizing solid aromatherapy and preparation method thereof of the invention is more specifically described.
According to an aspect of the present invention, high-elastic moisturizing solid aromatherapy of the invention includes by weight percentage:
In preferred embodiments, high-elastic moisturizing solid aromatherapy of the invention includes by weight percentage:
In the present invention, the carragheen is preferably K-type carragheen, and K-type carragheen can play coagulator and stabilizer Effect, it is dissolved in water at high temperature as gel solution, is cooled to half solid fraction at room temperature, can there is good fixed effect, And uniform and smooth, water-retaining property is excellent, has high resiliency, and the service life and transport for being conducive to extend champignon save, stability It is good.Preferably, the K-type carragheen selects the produced green new carragheen of Zhengzhou Wan Jiahui food additives.
The moisturizer is polyol humectant, can extend the service life of solid aromatherapy well;Preferably, institute Stating moisturizer is dipropylene glycol.
Methyl hydroxybenzoate (Methylparaben, i.e. methyl p-hydroxybenzoate), Nipasol (Propylparaben, i.e., Propylparaben) it is used as preservative, nontoxic, zero stimulation effectively extends the service life of champignon, prevents mould Become, addle.Methyl hydroxybenzoate and Nipasol are used cooperatively, and can not only play the role of preservative, and fragrance can be made more to hold Long, essential oil is enable preferably to be dissolved in carrageenan solutions.
The essential oil is natural plant essential oil, and green, health can effectively remove foreign flavor indoors, distribute pure and fresh fragrance, It relieves fatigue, builds comfortable pure and fresh atmosphere.Preferably, the essential oil is the pure and fresh flax of KD50254, KD20085 vanilla perfume Essence etc..
High-elastic moisturizing solid aromatherapy of the invention is as needed, can also include ethyl alcohol.The ethyl alcohol is fine solvent, energy Peculiar smell in carragheen is enough eliminated, keeps fragrance more pure and fresh, content is preferably 0.30%~0.80%.
In addition, high-elastic moisturizing solid aromatherapy of the invention is as needed, it can also include pigment, by weight percentage, The content of pigment is preferably 0.001%~0.002%.
According to another aspect of the present invention, the preparation method of high-elastic moisturizing solid aromatherapy of the invention, steps are as follows:
Methyl hydroxybenzoate, Nipasol and essential oil are sampled by above-mentioned weight percent, them is mixed uniformly, obtains Even essential oil preservative mixed solution;
At 65 DEG C~75 DEG C, carragheen is dissolved in water, moisturizer is added after being completely dissolved, uniformly mixes, obtains Carrageenan solutions;
At 65 DEG C~75 DEG C, essential oil preservative mixed solution obtained above is added in carrageenan solutions, sufficiently After mixing, pour into mold;Then it is cooled and shaped, obtains solid aromatherapy.
In the preparation process in accordance with the present invention, it needs to be slowly stirred in the preparation of essential oil preservative mixed solution, to avoid Bubble is generated into air.
In the preparation of carrageenan solutions, temperature is controlled in 65 DEG C~75 DEG C, is uniformly mixed using stirring, is stirred Speed is 350 (r/min), generates bubble to avoid enter into air as far as possible.Specifically, it removes ionized water and is heated to 65 DEG C~75 DEG C, it is slowly added to K-type carragheen, stir about 40 minutes or so or longer time, is completely dissolved to K-type carragheen, moisturizing is added Agent dipropylene glycol continues stir about 20 minutes or the longer time, obtains carrageenan solutions.
At 65 DEG C~75 DEG C, essential oil preservative mixed solution, carrageenan solutions and ethyl alcohol are sufficiently mixed, mixed Time about 20min or longer time.
In addition, in the preparation process in accordance with the present invention, as needed, when preparing carrageenan solutions, pigment colour can be mixed into Powder adds guarantor for example, first in water by pigment dissolved, carragheen being then added at 65 DEG C~75 DEG C, making it dissolve Humectant uniformly mixes, obtains carrageenan solutions.
By the following examples technical solution that the present invention is further explained, but following embodiment should not be construed as to this hair The limitation of bright protection scope.
Embodiment 1
The composition of high-elastic moisturizing solid aromatherapy
It takes methyl hydroxybenzoate 0.16g, Nipasol 0.07g, essential oil 2.56g to be put into a container, is uniformly mixed, directly It is completely dissolved to preservative, it is spare to obtain essential oil preservative mixed solution.
It removes ionized water 218g and is heated to 70 DEG C, be added toner (famille rose 60) 0.0024g, stir about 2-3 minutes is to complete Fully dissolved is slowly added to 5.83gK type carragheen when water temperature reaches 70 DEG C, stir about 40 minutes or so, complete to K-type carragheen Moisturizer dipropylene glycol 5.83g is added in fully dissolved, continues stir about 20 minutes, obtains carrageenan solutions.This process temperature is kept At 70 DEG C or so, mixing speed control is 350 (r/min).
It is at 70 DEG C or so, essential oil preservative mixed solution, carrageenan solutions and ethyl alcohol 1.52g obtained is sufficiently mixed It closes, stir about 20min is poured into mold, is cooled to room temperature, and is formed, is obtained solid aromatherapy.
Embodiment 2
The composition of high-elastic moisturizing solid aromatherapy
It takes methyl hydroxybenzoate 0.15g, Nipasol 0.05g, essential oil 3g to be put into a container, is uniformly mixed, until Preservative is completely dissolved, and it is spare to obtain essence preservative mixed solution.
It removes ionized water 233.54g and is heated to 70 DEG C, toner (PMS2985C brilliant blue) 0.0025g is added, stir about 2-3 divides Clock is to being completely dissolved, and when water temperature reaches 70 DEG C, is slowly added to 6g K-type carragheen, and stir about 40 minutes or so, to K-type OK a karaoke club Glue is completely dissolved, and dipropylene glycol 6g is added, and is continued stir about 20 minutes, is obtained carrageenan solutions.This process temperature is maintained at 70 DEG C or so, mixing speed control is 350 (r/min).
It is at 70 DEG C or so, essential oil preservative mixed solution, carrageenan solutions and ethyl alcohol 1.25g obtained is sufficiently mixed It closes, stir about 20min is poured into mold, is cooled to room temperature, and is formed, is obtained solid aromatherapy.
Solid aromatherapy surface smoothness made from embodiment 1 and embodiment 2 is good, exposes in air, after one month, moulding Still three-dimensional, only volume reduces than before, still keeps good fragrance.

Claims (6)

1. a kind of high-elastic moisturizing solid aromatherapy includes by weight percentage:
Wherein, the carragheen is K-type carragheen, and the moisturizer is dipropylene glycol.
2. high-elastic moisturizing solid aromatherapy as described in claim 1, characterized in that by weight percentage, the high-elastic moisturizing Solid aromatherapy includes:
3. high-elastic moisturizing solid aromatherapy as claimed in claim 2, characterized in that the high-elastic moisturizing solid aromatherapy also includes face Material, by weight percentage, the content of the pigment are 0.001%~0.002%.
4. high-elastic moisturizing solid aromatherapy as claimed any one in claims 1 to 3, characterized in that the essential oil is plant Natural perfume essential oil.
5. the preparation method of high-elastic moisturizing solid aromatherapy as described in claim 1, steps are as follows:
Methyl hydroxybenzoate, Nipasol and essential oil are sampled according to their own weight percent, them is mixed uniformly, obtains To uniform essential oil preservative mixed solution;
At 65 DEG C~75 DEG C, carragheen is dissolved in water, moisturizer is added after being completely dissolved, uniformly mixes, obtains OK a karaoke club Sol solution;
At 65 DEG C~75 DEG C, in the presence of ethyl alcohol, OK a karaoke club peptization is added in essential oil preservative mixed solution obtained above In liquid, after being sufficiently mixed, pour into mold;Then it is cooled and shaped, obtains solid aromatherapy.
6. the preparation method of high-elastic moisturizing solid aromatherapy as claimed in claim 5, characterized in that in the preparation of carrageenan solutions In, stirring rate 350r/min, mixing time is 40 minutes or more, so that carragheen is completely dissolved;It is added after being completely dissolved Moisturizer stirring 20 minutes or more, obtains carrageenan solutions.
CN201710132345.6A 2017-03-07 2017-03-07 High-elastic moisturizing solid scent and preparation method thereof Active CN106729863B (en)

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Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110651798B (en) * 2018-06-29 2021-04-13 东华理工大学 Pure natural mosquito-repellent solid aromatherapy and preparation method thereof
CN109260492B (en) * 2018-09-28 2021-02-09 广东爱车小屋电子商务科技有限公司 Solid air freshener and preparation method thereof
CN109701062B (en) * 2019-01-21 2020-12-11 东华理工大学 Antistatic solid champignon and static eliminator comprising same
CN112023101A (en) * 2020-09-10 2020-12-04 苏州花仙子环保科技有限公司 Air freshener composition
CN113384733B (en) * 2021-06-29 2023-02-10 湖北瑞晟生物有限责任公司 Herbal aromatic solid aromatherapy

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1662586A (en) * 2002-06-19 2005-08-31 昭和电工株式会社 Hydrous gel and production process and use of the hydrous gel
CN101954107A (en) * 2010-10-11 2011-01-26 上海应用技术学院 Solid aromatic sleep aid and preparation method thereof
CN102441185A (en) * 2011-12-08 2012-05-09 李舜丽 Solid champignon
CN105193672A (en) * 2015-10-29 2015-12-30 苏建华 Cell regeneration and restoration essence and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1662586A (en) * 2002-06-19 2005-08-31 昭和电工株式会社 Hydrous gel and production process and use of the hydrous gel
CN101954107A (en) * 2010-10-11 2011-01-26 上海应用技术学院 Solid aromatic sleep aid and preparation method thereof
CN102441185A (en) * 2011-12-08 2012-05-09 李舜丽 Solid champignon
CN105193672A (en) * 2015-10-29 2015-12-30 苏建华 Cell regeneration and restoration essence and preparation method thereof

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Effective date of registration: 20231228

Address after: Room 301, Unit 1, Building 2, Ganghang Community, No. 393 Kaifa Road, Liantang Town, Nanchang County, Nanchang City, Jiangxi Province, 330000

Patentee after: Nanchang Yanpu Optoelectronic Precision Instrument Co.,Ltd.

Address before: 344000 No. 56, Xuefu Road, Fuzhou, Jiangxi

Patentee before: EAST CHINA INSTITUTE OF TECHNOLOGY

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