CN104306259B - A kind of pure natural skin care oil without preservative and compound essence and preparation method thereof - Google Patents
A kind of pure natural skin care oil without preservative and compound essence and preparation method thereof Download PDFInfo
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- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a kind of pure natural skin care oil without preservative and compound essence and preparation method thereof, the skin care oil is mainly using the plant flowers and plants with beauty functions, high-quality tea-seed oil and natural VE as raw material, without preservative and compound essence, preparation process no chemical residues, the active ingredient do not destroyed in raw material, product has pure natural characteristic, and performance is stable, lasting.Methods described technique is simple, and no chemical residues are easy to utilize.
Description
Technical field
The invention belongs to skin care field, it is related to a kind of pure natural skin care oil and its system without preservative and compound essence
Preparation Method.
Technical background
Grease has been rooted in the hearts of the people as the part in fashionable life, and in fields such as skin care, beauty, health cares, application is wide
It is general, particularly high-end beauty and skin care market, for the requirement also more and more higher of raw material.
Tea-seed oil is as being one of China's most ancient woody edible vegetable oil.Its aliphatic acid constitutes the king's in similar oil
Olive oil, with very high nutritive value.Its main fatty acid is monounsaturated fatty acids oleic acid, and content is typically more than 80%.
It is very beneficial for skin absorption, has experiment to show that it can protect skin-nourishing, improve skin texture, be a kind of non-convention
The cosmetic base oil thought.But tea-seed oil has a kind of distinctive strong smell of tea-seed oil, the smell during skin care oil is made
It is very difficult to remove, influences the sense organ of skin care oil, limit its popularization and application.
Existing most cosmetic skin care oils are mainly constituted with base oil, essential oil, other chemical constituents.Such as patent
02112769.7 introduces method, and simple mixing is completed.Find that this stabilized with mixture is poor by practice.Essential oil fragrance is kept
Time is short.In addition, essential oil is expensive, in the market counterfeit and shoddy goods are more, and often contain compound essence in essential oil, essential oil
There is chemical residual in preparation process so that the quality of skin care oil cannot be ensured well.
The content of the invention
In view of the above-mentioned problems, the invention provides a kind of pure natural skin care oil without preservative and compound essence.The shield
Skin oil is mainly using the plant flowers and plants with beauty functions, high-quality tea-seed oil and natural VE as raw material, without preservative
And compound essence, preparation process no chemical residues, the active ingredient do not destroyed in raw material, product has pure natural characteristic, and property
Can be stable, lasting.
The present invention is achieved through the following technical solutions：
A kind of pure natural skin care oil without preservative and compound essence, it is characterised in that containing tea-seed oil, with fragrance
And the oil-soluble extract and natural VE of the natural plants tissue with beauty functions.Tea-seed oil nutrition is enriched, single
Unsaturated fatty acid content is high, containing camellia is sweet, Phospholipids and soap is sweet, vitamin E, tannin etc., is very beneficial for skin absorption, energy
Skin-nourishing is enough protected, improves skin texture.The present invention utilize its good oxidation resistance, and by with natural complex
E coordinates, and on the premise of not adding preservative agent, also ensure that product has lasting stability.In addition, by using natural plant
The oil-soluble extract of thing tissue, it is to avoid by the way of base oil is mixed with essential oil, preparation process no chemical residues are not destroyed
Active ingredient in raw material, product has pure natural characteristic, and can effectively cover the distinctive smell of tea-seed oil.
As optional, natural plants tissue and tea-seed oil and natural VE with beauty functions are used for raw material,
Directly extract the active ingredient in natural plants tissue to obtain skin care oil product with tea-seed oil, preparation process no chemical residues,
Without artificial additive, with preferably pure natural.
As optional, in above-mentioned pure natural skin care oil, the natural plants group with fragrance and with beauty functions
It is woven at least one of rose, lavandulae flos, lavender, pot marigold, Jasmine.
As optional, in above-mentioned pure natural skin care oil, the proportioning of the component by mass is tea-seed oil：1000 parts,
0.5-5 parts of oil-soluble extract, the natural VE of natural plants tissue：0.5 ~ 1.5 part.
As optional, in above-mentioned pure natural skin care oil, the tea-seed oil is high-quality tea-seed oil, and its acid value is less than 0.5,
Colourless free from extraneous odour.
Present invention also offers a kind of preparation method of above-mentioned pure natural skin care oil, comprise the following steps:
（1）Tea-seed oil is added in reactor, natural VE is added, under inert protective atmosphere, it is heated with stirring to 40 ~
75℃；
（2）Add and temperature is maintained under the natural plants tissue powder with fragrance and with beauty functions, inert protective atmosphere
Degree stirring 2 ~ 10 hours；
（3）Savory spilling is treated, cooling is stood, then carries out separation of solid and liquid, gained liquid phase part produces skin care oil product.
Obtained active ingredient is extracted in product from corresponding natural plants tissue and accounts for natural plants tissue powder stock quality
0.5-5%。
As optional, in above-mentioned preparation method, above-mentioned inert protective atmosphere is that nitrogen is protected or helium protection.
As optional, in above-mentioned preparation method, the proportioning of each raw material in parts by mass is tea-seed oil：1000 parts, naturally
Plant tissue powder：20 ~ 100 parts, natural VE:0.5 ~ 1.5 part.
As optional, in above-mentioned preparation method, the natural plants tissue powder is prepared in accordance with the following methods：Selection tool
Plants savory and with certain beauty functions, carry out dedusting, impurity elimination（Only leave the plant tissue with effect and fragrance）、
Crushed after being dried.
As optional, in above-mentioned preparation method, the tea-seed oil is prepared in accordance with the following methods：Selected pollution-free oil tea
Seed, shells, hydraulic pressure squeezing, by physical deacidification, decolouring, the processing of deodorization procedures.Using cold press mode of shelling, heating behaviour is not required to
Make simple, and natural constituent will not be destroyed.It can be obtained by membrane filtration, charcoal absorption progress depickling, decolouring, deodorization procedures
The acid value obtained is less than 0.5, the high-quality tea-seed oil of colourless free from extraneous odour, and chemical residual is all not present in whole preparation process, it is ensured that
The pure natural characteristic of tea-seed oil.
As optional, in above-mentioned preparation method, the separation of solid and liquid operation is specially first filtered, then to filtering
Solid constituent be centrifuged, then the liquid phase of obtained liquid phase with being filtrated to get will be centrifuged merge, and produce skin care oil product.
As optional, in above-mentioned preparation method, by step（3）In obtained skin care oil sealing preserve, then according to production
Product demand, different batches of product is mixed.It can consider purposes and fragrance, acid value, the mistake of product during mixing seasoning
The indexs such as oxidation number.Preferably, the acid value of controllable product is below 3.0, peroxide value is below 10.
Preparation method of the present invention may include sorting, crushing, heating, immersion, filtering, centrifugation, seasoning（The step
Suddenly to be optional）Etc. process, preparation technology is simple, can obtain skin care oil product pure natural and with lasting stability.According to root
According to the difference of raw material, can obtain with whitening, it is antibacterial, repair wounded tissue, softening skin, increase elasticity of skin, prevent skin
The skin care oil for the effects such as drying.
All features disclosed in this specification, or disclosed all methods or during the step of, except mutually exclusive
Feature and/or step beyond, can combine in any way.
Beneficial effects of the present invention：
The present invention utilizes its good oxidation resistance, and by coordinating with natural VE, in the premise of not adding preservative agent
Under, it also ensure that product has lasting stability.In addition, by using the oil-soluble extract of natural plants tissue, keeping away
Exempt from by the way of base oil is mixed with essential oil, preparation process no chemical residues, the active ingredient do not destroyed in raw material, product tool
There is pure natural characteristic, and can effectively cover the distinctive smell of tea-seed oil.
Preparation method of the present invention may include sorting, crushing, heating, immersion, filtering, centrifugation, seasoning（The step
Suddenly to be optional）Etc. process, preparation technology is simple, can obtain skin care oil product pure natural and with lasting stability.According to root
According to the difference of raw material, can obtain with whitening, it is antibacterial, repair wounded tissue, softening skin, increase elasticity of skin, prevent skin
The skin care oil for the effects such as drying.
Embodiment：
The above of embodiment by the following examples again to the present invention is described in further detail.But
The scope that this should not be interpreted as to above-mentioned theme of the invention is only limitted to following example.The spiritual and original of the present invention is not being departed from
Any modification made within then, and the equivalent substitution made according to ordinary skill knowledge and customary means or change
Enter, all should include within the scope of the present invention.It is raw materials used in following examples to buy from the market.Wherein institute
Commercially available high-quality tea-seed oil can be used by stating tea-seed oil, it would however also be possible to employ the tea-seed oil prepared by the following method.
High-quality tea-seed oil preparation example
Selected pollution-free tea seed, shells, and crushes, hydraulic pressure squeezing, obtains the low first squeezing tea oil of lighter color, acid value, then pass through
Cross the processing of physical deacidification, decolouring, deodorization procedures.As optional, the physical deacidification, decolouring, deodorization procedures are specially first right
Tea-seed oil carries out membrane filtration and then is carrying out charcoal absorption.The preferred fenestra aperture of membrane filtration is less than or equal in 10 microns
Hollow fiber film, such as polysulfones or polyether sulfone hollow fiber ultrafiltration film.The preferred specific surface area of activated carbon is more than or equal to 800m2/ g activity
Charcoal.This method is used to obtain high-quality tea-seed oil of the acid value for 0.2 colorless and odorless.By the aperture and the work that adjust filter membrane
The high-quality tea-seed oil that acid value is respectively a series of 0.5,0.4,0.3 colorless and odorless has successfully been made in the specific surface area of property carbon.
The Rose Essentielle skin care oil of embodiment 1
Selected rose, the flower base of a fruit is removed, crushed after being dried is standby, will be homemade featured according to the method for the invention
Acid value be added to for the tea-seed oil 10kg of 0.2 colorless and odorless in reactor, add 0.008kg natural VEs, be passed through nitrogen
Gas, starts stirring, chuck heating, when temperature reaches 50 DEG C, adds 1.0kg Flos Rosae Rugosas pollens, continues to stir, temperature control 55 ±
5 DEG C, maintain 4 hours, be separated by filtration when product.The product gives off a strong fragrance, the micro- Huang of color and luster, is applied on skin and absorbs fast, stays
The fragrant time is long.Acid value is below 3.0, and peroxide value is below 10, and product stability is good, and long shelf-life was up to 30 months.
Rose liposoluble constituent is mainly the volatile oil compositions with aromatic odor, and these components have regulating qi-flowing for relieving pain,
Improvement Peripheral Microcirculation effect promoting blood circulation and removing blood stasis, there is Flavonoid substances in addition, can remove free radical, remove pigementation work
With.In skin care oil of the present invention, it under the osmosis of tea-seed oil, can be very good to improve skin, realize crease-resistant, guarantor
Wet, skin whitening effect.In order to verify effect of product, 10 volunteers are have chosen daily respectively on the left side of every volunteer
The back of the hand smears product described in the present embodiment（It is used as experimental group）, smeared in right hand the back of the hand and use base oil and rose in the prior art
The skin care oil that Rose Absolute is mixed with（As a control group）, it is continuous to smear two weeks, as a result show the skin of experimental group and control group
Skin situation makes moderate progress before not smearing, and the crease-resistant of experimental group, moisturizing, whitening effect are significantly better than control group.
Embodiment 2
Selected rose, the flower base of a fruit is removed, crushed after being dried is standby, by the tea that featured acid value is 0.5 colorless and odorless
Seed oil 10kg is added in reactor, is added 0.005kg natural VEs, is passed through nitrogen, starts stirring, and temperature is worked as in chuck heating
Degree reaches 70 DEG C, adds 0.3kg Flos Rosae Rugosas pollens, continues to stir, and temperature control is maintained 2 hours, is separated by filtration at 70 ± 5 DEG C
To product.The product gives off a strong fragrance, the micro- Huang of color and luster, is applied on skin and absorbs fast, fragrance remaining time is long.Properties of product and embodiment
Product is suitable described in 1.
The lavender of embodiment 3 perfume skin care oil
Selected lavender, removes chalk dust removing and debris, and crushed after being dried is standby, is 0.2 colorless and odorless by featured acid value
Tea-seed oil 10kg be added in reactor, add 0.01kg natural VEs, be passed through nitrogen, start stirring, chuck is heated,
When temperature reaches 45 DEG C, 0.5kg lavender powders are added, continue to stir, temperature control is maintained 6 hours at 45 ± 5 DEG C, filtering
Separation waits until product.The product has stronger lavender fragrant, the micro- Huang of color and luster, is applied on skin and absorbs fast, fragrance remaining time
It is long.And product stability is good, long shelf-life was up to 30 months.
Lavender has fragrant medicinal herbs " good reputation, waved containing substantial amounts of fragrant camphor tree esters and linalool class fragrance in its bud
Hair oil composition, these compositions, which have, promotes cytothesis, the effect such as antibacterial, analgesia, in addition also containing the liposoluble sweet-scented osmanthus of energy
The components such as careless element, this compound is also the effect with anti-inflammation.The contrast experiment confirmation similar with embodiment, this implementation
Lavender flavor type skin care oil described in example has effects that promotion cytothesis and antibacterial necessarily, and combination property is better than existing
The skin care oil being mixed with technology using base oil and lavender oil oil.
The pot marigold of embodiment 4 perfume skin care oil
Selected pot marigold, removes the flower base of a fruit and dust, and crushed after being dried is standby, is 0.2 colorless and odorless by featured acid value
Tea-seed oil 10kg be added in reactor, add 0.012kg natural VEs, be passed through nitrogen, start stirring, chuck is heated,
When temperature reaches 60 DEG C, 0.8kg pot marigold powder is added, continues to stir, temperature control is maintained 10 hours at 60 ± 5 DEG C, filtering point
From when product.The product fragrance is simple and elegant, and color and luster is slightly yellow, is applied on skin and absorbs fast, fragrance remaining time is long.And product stability
Good, long shelf-life was up to 30 months.
Its armaticity volatile matter lemon alkenes of pot marigold have anticancer, and triterpene compound has anti-inflammatory and accelerates wound to be cured
The effect of conjunction.The contrast experiment similar with embodiment confirms that the pot marigold odor type skin care oil described in the present embodiment has certain
Effect of anti-inflammatory and accelerating wound healing, and combination property is better than in the prior art using base oil and the mixing of pot marigold essential oil
The skin care oil of preparation.
The jasmin skin care oil of embodiment 5
Selected Jasmine, removes chalk dust removing and debris, and crushed after being dried is standby, is 0.2 colorless and odorless by featured acid value
Tea-seed oil 10kg be added in reactor, add 0.015kg natural VEs, be passed through nitrogen, start stirring, chuck is heated,
When temperature reaches 50 DEG C, 0.7kg jasmine pollen is added, continues to stir, temperature control is maintained 10 hours at 50 ± 5 DEG C, filtering point
From when product.The product gives off a strong fragrance, pale yellow, is applied on skin and absorbs fast, fragrance remaining time is long.And product stability
Good, long shelf-life was up to 30 months.
Its pleasant aroma of Jasmine, key component is phenmethylol and its esters, jasmone, linalool, benzoic acid virtue
The components such as camphor tree alcohol ester, have effects that stable mood, eliminate anxiety, refresh oneself and recover from fatigue.Other Jasmine polysaccharide component has anti-sense
The effects such as dye, solution sore.The contrast experiment similar with embodiment confirms that the jasmine fragrance skin care oil described in the present embodiment has
Certain stable mood, eliminate it is nervous, refresh oneself recover from fatigue and anti-infective solution sore effect, and combination property is better than existing skill
The skin care oil being mixed with art using base oil and jasmin essential oil.
The hybrid modulation of embodiment 6
According to product demand, the product chosen in embodiment 1-5 is mixed, and obtaining has mixing odor type and a variety of functions
A series of skin care oil products.The finger such as purposes and fragrance, acid value, peroxide value of product can be considered during mixing seasoning
Mark.
The preferred embodiments of the present invention are the foregoing is only, are merely illustrative for the purpose of the present invention, and it is nonrestrictive；
Those of ordinary skill in the art understand that can carry out many to it in the spirit and scope that the claims in the present invention are limited changes
Become, modification, or even equivalent change, but fall within protection scope of the present invention.
Claims (8)
1. a kind of pure natural skin care oil without preservative and compound essence, it is characterised in that containing tea-seed oil, with fragrance simultaneously
The oil-soluble extract and natural VE of natural plants tissue with beauty functions, give birth to through adding natural dimension in tea-seed oil
Plain E steps, inertia protection and heating stepses and natural plants tissue immerse tea-seed oil step and obtained；Its component matching somebody with somebody by mass
Than for tea-seed oil：1000 parts, 0.5-5 parts of oil-soluble extract, the natural VE of natural plants tissue：0.5 ~ 1.5 part；
Its preparation method comprises the following steps：
（1）Tea-seed oil is added in reactor, adds under natural VE, inert protective atmosphere, is heated with stirring to 40 ~ 75 DEG C；
（2）Adding under the natural plants tissue powder with fragrance and with beauty functions, inert protective atmosphere maintains temperature to stir
Mix 2 ~ 10 hours；
（3）Savory spilling is treated, cooling is stood, then carries out separation of solid and liquid, gained liquid phase part produces skin care oil product.
2. a kind of pure natural skin care oil without preservative and compound essence according to claim 1, it is characterised in that institute
State the natural plants with fragrance and with beauty functions and be organized as rose, lavandulae flos, lavender, pot marigold, Jasmine
At least one of.
3. a kind of pure natural skin care oil without preservative and compound essence according to claim 1, it is characterised in that institute
Tea-seed oil acid value is stated less than 0.5, colourless free from extraneous odour.
4. a kind of pure natural skin care oil without preservative and compound essence according to claim 1, it is characterised in that each
The proportioning of raw material in parts by mass is tea-seed oil：1000 parts, natural plants tissue powder：20 ~ 100 parts, natural VE:0.5
~ 1.5 parts.
5. a kind of pure natural skin care oil without preservative and compound essence according to claim 1, it is characterised in that institute
Natural plants tissue powder is stated to prepare in accordance with the following methods：Plant of the selection with fragrance and with certain beauty functions, is carried out
Dedusting, impurity elimination, crushed after being dried.
6. a kind of pure natural skin care oil without preservative and compound essence according to claim 1, it is characterised in that institute
Tea-seed oil is stated to prepare in accordance with the following methods：Selected pollution-free tea seed, shells, hydraulic pressure squeezing, by physical deacidification, decolouring, takes off
The processing of smelly process.
7. a kind of pure natural skin care oil without preservative and compound essence according to claim 1, it is characterised in that institute
State separation of solid and liquid operation specially first to be filtered, then the solid constituent filtered is centrifuged, then centrifugation is obtained
Liquid phase merge with the liquid phase being filtrated to get, produce skin care oil product.
8. a kind of pure natural skin care oil without preservative and compound essence according to claim 1, it is characterised in that will
Step（3）In obtained skin care oil sealing preserve, then according to product demand, different batches of product is mixed.
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| CN201410566967.6A CN104306259B (en) | 2014-10-23 | 2014-10-23 | A kind of pure natural skin care oil without preservative and compound essence and preparation method thereof |
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| CN104306259B true CN104306259B (en) | 2017-08-25 |
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| CN107802524A (en) * | 2017-12-08 | 2018-03-16 | 广州若羽臣科技股份有限公司 | A kind of skin care oil |
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| FR2763843B1 (en) * | 1997-05-30 | 1999-08-20 | Marie Pratt | COMPOSITION HAVING PARTICULARLY ANTI-AGING SKIN ACTION |
| CN101305974B (en) * | 2008-07-11 | 2010-04-14 | 广东新大地生物科技股份有限公司 | Camellia oil preparation method for cosmetics |
| CN102688171B (en) * | 2012-06-18 | 2013-10-30 | 陈小锋 | Infant skin care oil and preparation method thereof |
| CN102908268B (en) * | 2012-10-19 | 2014-11-05 | 伊国群 | Camellia type skin care solution |
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Denomination of invention: Pure natural skin oil containing no preservative and synthesized essence and preparation method of pure natural skin oil Effective date of registration: 20200722 Granted publication date: 20170825 Pledgee: Ya'an Rural Commercial Bank Co.,Ltd. Pledgor: YA'AN TAISHI BIOLOGICAL SCIENCE AND TECHNOLOGY Co.,Ltd. Registration number: Y2020510000076 |