CN102362843B - Tea seed oil skin oil and preparation method thereof - Google Patents
Tea seed oil skin oil and preparation method thereof Download PDFInfo
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- CN102362843B CN102362843B CN2011103253022A CN201110325302A CN102362843B CN 102362843 B CN102362843 B CN 102362843B CN 2011103253022 A CN2011103253022 A CN 2011103253022A CN 201110325302 A CN201110325302 A CN 201110325302A CN 102362843 B CN102362843 B CN 102362843B
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Abstract
The invention provides tea seed oil skin oil and a preparation method thereof. The tea skin oil is prepared from the following components in weight proportion: 85-95% of tea seed oil subjected to short path distillation processing, 0.5-1% of flowery essential oil and 4.5-15% of ester; the invention gives full play to natural resources in China and provides a beautifying skin oil which adopts no industrial chemicals, is nutrient to skin of human body and is easy to be absorbed by skin. Main raw materials of a product in the invention are separated by adopting a short path distillation pure physical means, contain pure natural substance, has no toxic or side effect to human body and is applicable to people in various age groups, the product is rich in natural vitamin E and tea polyphenol, no antioxidant is required to be added, the natural vitamin E and the tea polypheonl can realize synergistic antioxidation, and quality guarantee period can be effectively prolonged.
Description
(1) technical field
The present invention relates to a kind of tea seed oil skin oil and preparation method thereof.
(2) background technology
Along with people's living standard improves day by day, more and more to the demand of beauty treatment, skin protection, people's the propensity to consume more and more tends to pursue nutrition, natural plant extracts is the cosmetics of raw material.The cosmetics that existing market is sold much contain synthetics, and solvent easily produces chemical reaction and zest is large to skin, thereby causes skin lesion.A lot of skin protection oil also are formulated as basis other materials of interpolation take white oil on the market, are difficult for for skin absorbs skin being had certain stimulation.
Tea-seed oil is green tea oil (Green tea seed oil), being different from Camellia oil, is take the Folium Camelliae sinensis tree seeds as raw material, the green health vegetable oil that extract, containing abundant unsaturated fatty acid, vitamin E and tea polyphenols, is non-drying, cold oils and fats.Tea-seed oil is rich in unit/polybasic unsaturated fatty acid and reaches 82%, can the regulation of skin permeability, reduce the loss of moisture, increase the skin moisturizing effect, human body skin also is easy to absorb, can keep nutrition, moisture and elasticity to skin, improve the degeneration of keratodermatitis, be good skin protection and wetting agent; Natural Vitamin E reaches 0.5% up to 200mg/L, tea polyphenols, is higher than the content in the general Camellia oil far away, has very strong antioxidation, need not to add any antioxidant, can effectively stop product " to become sour ", and is more healthy and safe.Can protect the body tissue biomembrane to exempt from that free radical is attacked and oxidation has significant protection radiation resistance, skin nursing is had good result, especially suitable to high-end cosmetic material.
Although Oleum Camelliae is used in the cosmetics already, food stage tea-seed oil acid number is about 0.5mgKOH/g, and is faint yellow about peroxide value 7mmol/kg, and obvious Camellia oil abnormal smells from the patient is arranged.Because acid number and peroxide value are higher, when being used for preparing cosmetics, the peroxide in the Camellia oil has zest, the higher shelf-life that may affect product of acid number to skin, and its color and abnormal smells from the patient can affect outward appearance and the sense of taste of product.
(3) summary of the invention
The object of the invention provides a kind of skin care item take tea-seed oil as main component and preparation method thereof.
The technical solution used in the present invention is:
A kind of tea seed oil skin oil, made by the component that the quality proportioning is following:
Tea-seed oil 85～95% through the distillation processing
Rose Absolute 0.5～1%
Ester 4.5～15%
The described tea-seed oil of processing through distillation obtains by the following method:
Get commercially available tea-seed oil and carry out the distillation first time, 160～170 ℃ of vapo(u)rizing temperatures, operating pressure 0.01～0.05mmHg, 80～85 ℃ of feeding temperatures, rotating speed 100～200r/min; Get the debris of for the first time distillation and partly carry out the distillation second time, 200～220 ℃ of vapo(u)rizing temperatures, operating pressure 0.01～0.04mmHg, 80～85 ℃ of feeding temperatures, rotating speed 100～200r/min gets the condensed fluid that distills away for the second time, is the described tea-seed oil of processing through distillation;
First step short-path distillation mainly is to remove the light molecular substance such as minute residual hydro carbons, solvent, fatty acid, and it mainly is to remove the weight molecule materials such as pigment, crystal that the second step short-path distillation is processed.The tea-seed oil acid value that processed through two step distillations this moment is less than 0.08mgKOH/g, and peroxide value is less than 0.4mmol/Kg, and appearance colorless is sparkling and crystal-clear transparent.
Described Ester is isopropyl palmitate or isopropyl myristate, and Ester can promote skin to absorb, and improves product spread and breathability, reduces viscosity and greasy feeling.Described Rose Absolute is distillation extraction obtains from corresponding plant flowers plants essential oil, and fragrance is pure, and skin is had no stimulation and certain opsonic action is arranged.
The present invention with the commercially available tea-seed oil of routine after two steps, short-path distillations were processed, hydro carbons, solvent, fatty acid and pigment had both been removed, vitamin E and tea polyphenols isoreactivity material in the tea-seed oil have been kept as far as possible again, for the preparation of skin protection oil, far away than good in the effect aspect the skin nursing before processing.
Described Rose Absolute is Flos Rosae Rugosae quintessence oil, Fructus Gardeniae quintessence oil or jasmin quintessence oil.
Preferably, described tea seed oil skin oil makes as follows:
(1) gets commercially available tea-seed oil and carry out the distillation first time, 160～170 ℃ of vapo(u)rizing temperatures, operating pressure 0.02mmHg, 80 ℃ of feeding temperatures, rotating speed 150r/min;
The debris of (2) getting for the first time distillation remnants is partly carried out the distillation second time, 200～220 ℃ of vapo(u)rizing temperatures, operating pressure 0.01mmHg, 80 ℃ of feeding temperatures, rotating speed 150r/min;
(3) getting the quality proportioning is condensed fluid, Flos Rosae Rugosae quintessence oil and the isopropyl palmitate that 90%: 0.8%: 9.2% tea-seed oil distills out for the second time, and mixing preparation is even, namely gets described tea seed oil skin oil.
The invention still further relates to the preparation method of described tea seed oil skin oil, described method comprises:
(1) gets commercially available tea-seed oil and carry out the distillation first time, 160～170 ℃ of vapo(u)rizing temperatures, operating pressure 0.01～0.05mmHg, 80～85 ℃ of feeding temperatures, rotating speed 100～200r/min;
The debris of (2) getting for the first time distillation remnants is partly carried out the distillation second time, 200～220 ℃ of vapo(u)rizing temperatures, operating pressure 0.01～0.04mmHg, 80～85 ℃ of feeding temperatures, rotating speed 100～200r/min;
(3) get the condensed fluid that tea-seed oil distills out for the second time, adding Rose Absolute and Ester mixing preparation are even, namely get described tea seed oil skin oil; Described condensed fluid, Rose Absolute and Ester quality consumption proportion are 85～95%: 0.5～1%: 4.5～15%; Described Ester is isopropyl palmitate or isopropyl myristate.
The present invention gives full play to China's natural resources, and a kind of industrial chemicals, nutritious to human body skin that do not have is provided, the skin protection that easily is absorbed by the skin oil.Product primary raw material of the present invention adopts the pure physical means of short-path distillation to separate, contain pure natural substance, human body is had no side effect, be suitable for the each age group crowd and use, product self is rich in natural Vitamin E and tea polyphenols, need not to add antioxidant, both can play the antioxidation of Synergistic (referring to publication Folium Camelliae sinensis " synergism of tea polyphenols and other antioxidant ", 2000,26 (2)), can effectively prolong the shelf-life of product.
(4) specific embodiment
The present invention is described further below in conjunction with specific embodiment, but protection scope of the present invention is not limited in this:
Embodiment 1: tea-seed oil is processed
1, first step short-path distillation is processed: the tea-seed oil of 1000g (Kingsoft, Jinhua oils and fats company limited) raw material, 160～170 ℃ of vapo(u)rizing temperatures, operating pressure 0.02mmHg, 80 ℃ of feeding temperatures, rotating speed 150r/min.Obtained component comprise the condensed fluid that distills away and and remaining debris, remaining debris mainly contains sweet three esters, part DAG, vitamin E, sterol and part weight molecule material, light component mainly contains the light molecular substance such as fatty acid, solvent, through the gas chromatography-mass spectrography analysis, fatty acid purity reaches 98%.
2, the second step short-path distillation is processed: get the debris part of the short-path distillation remnants first time as this time raw material.200～220 ℃ of vapo(u)rizing temperatures, operating pressure 0.01mmHg, 80 ℃ of feeding temperatures, rotating speed 150r/min.Obtained component comprise the condensed fluid that distills away and and remaining debris, remaining debris mainly contains the part weight molecule materials such as pigment, solid content, the condensed fluid that distills away is altogether about 650g, mainly contain the light molecular substance such as glyceride, vitamin E, sterol and tea polyphenols, wherein the vitamin E mass content is about 0.06%, the tea polyphenols mass content is about 0.32%, and acid value is less than 0.08mgKOH/g, and peroxide value is less than 0.4mmol/Kg, appearance colorless is sparkling and crystal-clear transparent.
Embodiment 2: the allotment of skin protection oil
Compositions in weight percentage is: the tea-seed oil (the condensed fluid part of distilling away for the second time) after for the second time short-path distillation processing of embodiment 1: 90%; Flos Rosae Rugosae quintessence oil (Zhejiang 99 red rose Science and Technology Ltd.s) 0.8%; Ester: isopropyl palmitate 9.2%, the three carries out mixing preparation, and evenly rear packing namely obtains product, and shelf life of products reached more than 24 months.
Skin protection oil of the present invention is fine and smooth, and feel is cunning, and spreadability is good, more easily absorbs, and the Flos Rosae Rugosae flavor is arranged.Often use, to the skin nonirritant, can nourish moist skin, represent skin soft and smooth moist.
Embodiment 3: the allotment of skin protection oil
Compositions in weight percentage is: the tea-seed oil (the condensed fluid part of distilling away for the second time) after for the second time short-path distillation processing of embodiment 1: 88%; Jasmin quintessence oil (Ji'an City Qingyuan District east natural perfume material oil refinery) 1%; Ester: isopropyl myristate 11%, the three carries out mixing preparation, and evenly rear packing namely obtains product, and shelf life of products reached more than 24 months.
Skin protection oil feel of the present invention is fine and smooth, lubricious, and moisture-keeping efficacy has the Flos Jasmini Sambac flavor, makes skin smooth tender, pale beautiful, can keep out free radical injury, prevents that skin moisture content runs off.
Embodiment 4: the allotment of skin protection oil
Compositions in weight percentage is: the tea-seed oil (the condensed fluid part of distilling away for the second time) after for the second time short-path distillation processing of embodiment 1: 95%; Fructus Gardeniae quintessence oil (Shaanxi natural flower aroma biotechnology development corporation, Ltd.) 0.5%; Ester: isopropyl palmitate 4.5%, the three carries out mixing preparation, and evenly rear packing namely obtains product, and shelf life of products reached more than 24 months.
Skin protection oil of the present invention is fine and smooth, and spreadability is good, more easily absorbs, and the Flos Gardeniae flavor is arranged.To the skin nonirritant, can nourish moist skin.
Embodiment 5: the allotment of skin protection oil
Compositions in weight percentage is: the tea-seed oil (the condensed fluid part of distilling away for the second time) after for the second time short-path distillation processing of embodiment 1: 92%; Flos Rosae Rugosae quintessence oil (Zhejiang 99 red rose Science and Technology Ltd.s) 1%; Ester: isopropyl palmitate or isopropyl myristate 7%, the three carries out mixing preparation, and evenly rear packing namely obtains product, and shelf life of products reached more than 24 months.
Skin protection oil feel of the present invention is cunning, and spreadability is good, and the Flos Rosae Rugosae flavor is arranged.To the skin nonirritant, can nourish moist skin, represent skin soft and smooth moist.
Embodiment 6:
Skin care item oil for embodiment 2 obtains in the middle of peroxide value (POV value) determination experiment, after oven, is significantly less than the blank value, embodies better oxidation resistance.Skin protection oil removes in the test at free radical, and wherein the ultra-oxygen anion free radical clearance rate reaches more than 85%, is within the specific limits significant dose-effect relationship, can alleviate in a way skin damage, makes skin look more glossy, and vigor is arranged.
Claims (4)
1. tea seed oil skin oil, made by the component that the quality proportioning is following:
Tea-seed oil 85 ~ 95% through the distillation processing
Rose Absolute 0.5 ~ 1%
Ester 4.5 ~ 15%
Above-mentioned three kinds of constituent mass percentage ratio sums are 100%;
The described tea-seed oil of processing through distillation obtains by the following method:
Get tea-seed oil and carry out the distillation first time, 160 ~ 170 ℃ of vapo(u)rizing temperatures, operating pressure 0.02 mmHg, 80 ℃ of feeding temperatures, rotating speed 150r/min; Get the debris of for the first time distillation remnants and partly carry out the distillation second time, 200 ~ 220 ℃ of vapo(u)rizing temperatures, operating pressure 0.01 mmHg, 80 ℃ of feeding temperatures, rotating speed 150 r/min get the condensed fluid that distills away for the second time, are the described tea-seed oil of processing through distillation;
Described Ester is isopropyl palmitate or isopropyl myristate.
2. tea seed oil skin oil as claimed in claim 1 is characterized in that described Rose Absolute is Flos Rosae Rugosae quintessence oil, Fructus Gardeniae quintessence oil or jasmin quintessence oil.
3. tea seed oil skin oil as claimed in claim 1 is characterized in that described tea seed oil skin oil makes as follows:
(1) gets tea-seed oil and carry out the distillation first time, 160 ~ 170 ℃ of vapo(u)rizing temperatures, operating pressure 0.02 mmHg, 80 ℃ of feeding temperatures, rotating speed 150 r/min;
(2) get and distill for the first time debris and partly carry out second time and distill 200 ~ 220 ℃ of vapo(u)rizing temperatures, operating pressure 0.01 mmHg, 80 ℃ of feeding temperatures, rotating speed 150 r/min;
(3) getting the quality proportioning is condensed fluid, Flos Rosae Rugosae quintessence oil and the isopropyl palmitate that the tea-seed oil of 90%:0.8%:9.2% distills out for the second time, and mixing preparation is even, namely gets described tea seed oil skin oil.
4. the preparation method of the described tea seed oil skin oil of claim 1, described method comprises:
(1) gets tea-seed oil and carry out the distillation first time, 160 ~ 170 ℃ of vapo(u)rizing temperatures, operating pressure 0.02mmHg, 80 ℃ of feeding temperatures, rotating speed 150 r/min;
(2) get and distill for the first time debris and partly carry out second time and distill 200 ~ 220 ℃ of vapo(u)rizing temperatures, operating pressure 0.01 mmHg, 80 ℃ of feeding temperatures, rotating speed 150 r/min;
(3) get the condensed fluid that tea-seed oil distills out for the second time, adding Rose Absolute and Ester mixing preparation are even, namely get described tea seed oil skin oil; Described condensed fluid, Rose Absolute and Ester quality consumption proportion are 85 ~ 95%:0.5 ~ 1%:4.5 ~ 15%; Above-mentioned three kinds of constituent mass percentage ratio sums are 100%; Described Ester is isopropyl palmitate or isopropyl myristate.
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| CN2011103253022A CN102362843B (en) | 2011-10-24 | 2011-10-24 | Tea seed oil skin oil and preparation method thereof |
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| CN2011103253022A CN102362843B (en) | 2011-10-24 | 2011-10-24 | Tea seed oil skin oil and preparation method thereof |
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| CN102362843A CN102362843A (en) | 2012-02-29 |
| CN102362843B true CN102362843B (en) | 2013-01-23 |
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Families Citing this family (3)
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| CN102885753B (en) * | 2012-11-06 | 2014-05-28 | 广西三江源源茶业有限公司 | Refining-free natural tea seed skincare oil and preparation method thereof |
| CN105377263B (en) * | 2013-07-11 | 2020-05-29 | 株式会社爱茉莉太平洋 | Antioxidant or skin whitening composition containing 21-O-angeloyltheasapogenol E3 derived from green tea seed |
| CN110302076A (en) * | 2019-06-17 | 2019-10-08 | 广州海岚生物科技有限公司 | A kind of moisture-keeping composition and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1372921A (en) * | 2002-03-18 | 2002-10-09 | 黄宝生 | Face-beautifying camellia seed oil with natural flower fragrance |
| CN101717691A (en) * | 2009-10-30 | 2010-06-02 | 华南理工大学 | Method for refining cosmetic camellia oil by adopting short-path distillation |
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- 2011-10-24 CN CN2011103253022A patent/CN102362843B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1372921A (en) * | 2002-03-18 | 2002-10-09 | 黄宝生 | Face-beautifying camellia seed oil with natural flower fragrance |
| CN101717691A (en) * | 2009-10-30 | 2010-06-02 | 华南理工大学 | Method for refining cosmetic camellia oil by adopting short-path distillation |
Non-Patent Citations (2)
| Title |
|---|
| 肖婷 等.茶籽油的精制方法研究进展.《广东化工》.2007,第34卷(第3期),第46页. |
| 茶籽油的精制方法研究进展;肖婷 等;《广东化工》;20070331;第34卷(第3期);第46页 * |
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