CN110302076A - A kind of moisture-keeping composition and preparation method thereof - Google Patents

A kind of moisture-keeping composition and preparation method thereof Download PDF

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Publication number
CN110302076A
CN110302076A CN201910521171.1A CN201910521171A CN110302076A CN 110302076 A CN110302076 A CN 110302076A CN 201910521171 A CN201910521171 A CN 201910521171A CN 110302076 A CN110302076 A CN 110302076A
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China
Prior art keywords
parts
moisture
keeping composition
lecithin
glycerol
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Pending
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CN201910521171.1A
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Chinese (zh)
Inventor
周国通
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Guangzhou Hailan Biotechnology Co Ltd
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Guangzhou Hailan Biotechnology Co Ltd
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Priority to CN201910521171.1A priority Critical patent/CN110302076A/en
Publication of CN110302076A publication Critical patent/CN110302076A/en
Pending legal-status Critical Current

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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34—Alcohols
    • A61K8/345—Alcohols containing more than one hydroxy group
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
    • A61K8/498—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/55—Phosphorus compounds
    • A61K8/553—Phospholipids, e.g. lecithin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/63—Steroids; Derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67—Vitamins
    • A61K8/678—Tocopherol, i.e. vitamin E
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89—Polysiloxanes
    • A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783—Angiosperms [Magnoliophyta]
    • A61K8/9789—Magnoliopsida [dicotyledons]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Emergency Medicine (AREA)
  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Biophysics (AREA)
  • Molecular Biology (AREA)
  • Dermatology (AREA)
  • Cosmetics (AREA)

Abstract

The present invention relates to cosmetic technical fields more particularly to a kind of moisture-keeping composition and preparation method thereof.This moisture-keeping composition includes following components in parts by mass: 35-55 parts of glycerol, 20-30 parts of dimethyl silicone polymer, 2-8 parts of lecithin, 3-8 parts of dipropylene glycol and 10-30 parts of water.Glycerol, dimethyl silicone polymer, lecithin and dipropylene glycol, dimethyl silicone polymer are added in the present invention can form hydrophobic thin oil film in skin surface, can reinforce skin barrier action；Lecithin is the component part of keratoderma cytolipin, supplements phosphatide, can reinforce " brick wall structure " of corneocyte, increases skin barrier；Glycerol can absorb moisture from environment, and the moisture that supplement cuticula distributes, various substances be combined with each other, cooperate, and then have good moisturizing, repair and skin sense.

Description

A kind of moisture-keeping composition and preparation method thereof
Technical field
The present invention relates to cosmetic technical fields more particularly to a kind of moisture-keeping composition and preparation method thereof.
Background technique
Currently, general cosmetics are done soon after being applied to skin surface, Bu Nengchang in cosmetic technical field Moisturizing is imitated, meanwhile, it repairs skin and pro-skin sense is also not good enough, be not able to satisfy consumer demand.
Moreover, the cosmetics for adding lecithin, since lecithin is under the conditions ofs illumination etc., easy to oxidize, Jin Erying The use for having rung product, is not able to satisfy consumer demand.
Summary of the invention
In order to solve the above technical problems, to provide a kind of moistening effect good by the present invention, while there is repair and skin Feel fabulous composition and preparation method thereof.
In order to realize technical effect of the invention, it is achieved using following technical scheme:
A kind of moisture-keeping composition, this moisture-keeping composition includes following components in parts by mass: 35-55 parts of glycerol, poly- diformazan 20-30 parts of radical siloxane, 2-8 parts of lecithin, 3-8 parts of dipropylene glycol and 10-30 parts of water.
As a further improvement, the moisture-keeping composition further includes 0.7-2.8 parts of permeation enhancers, Sodium Hyaluronate 0.3- 0.5 part and antioxidant 0.04-0.32 parts.
As a further improvement, the permeation enhancers are sodium taurocholate 0.5-2 parts and stearmide 0.2-0.8 parts, antioxygen Agent is vitamin E 0.02-0.16 parts and tea polyphenols 0.02-0.16 parts.
The present invention also provides the preparation method of moisture-keeping composition described above, preparation methods are as follows: by various components Mixing, stirring is until be uniformly mixed.
Certainly, after mixing can also in water bath ultrasonic wave 30-40 DEG C ultrasound 15-30 minutes, and then can mix It is more preferable.
The present invention also has the advantages that
1) glycerol, dimethyl silicone polymer, lecithin and dipropylene glycol are added in the present invention, dimethyl silicone polymer can be Skin surface forms hydrophobic thin oil film, can reinforce skin barrier action；Lecithin is keratoderma cytolipin Component part supplements phosphatide, can reinforce " brick wall structure " of corneocyte, increases skin barrier；Glycerol can be from environment Middle absorption moisture, the moisture that distributes of supplement cuticula, various substances be combined with each other, cooperate, so have good moisturizing, Repair and skin sense.
2) Sodium Hyaluronate, antioxidant and permeation enhancers are added in formula, and not only there is better moisturizing and other effects, And product be able to maintain more long, meanwhile, lecithin can carry antioxidant content etc. into skin, can further repair skin Skin and moisturizing.
Specific embodiment
Embodiment 1
A kind of moisture-keeping composition, this moisture-keeping composition includes following components in parts by mass: 45 parts of glycerol, poly dimethyl silicon 20 parts of oxygen alkane, 2 parts of lecithin, 3 parts of dipropylene glycol and 30 parts of water.
The moisture-keeping composition the preparation method comprises the following steps: various components are mixed, stirring is then super in water-bath until be uniformly mixed In sound wave 30-40 DEG C ultrasound 15-30 minutes.
Embodiment 2
A kind of moisture-keeping composition, this moisture-keeping composition is composed of the following components in parts by mass: 35 parts of glycerol, poly dimethyl 30 parts of siloxanes, 8 parts of lecithin, 8 parts of dipropylene glycol and 19 parts of water.
The moisture-keeping composition the preparation method comprises the following steps: various components are mixed, stirring is then super in water-bath until be uniformly mixed In sound wave 30-40 DEG C ultrasound 15-30 minutes.
Embodiment 3
A kind of moisture-keeping composition, this moisture-keeping composition is made up of in parts by mass: 55 parts of glycerol, polydimethylsiloxanes 20 parts of alkane, 7 parts of lecithin, 8 parts of dipropylene glycol and 10 parts of water.
The moisture-keeping composition the preparation method comprises the following steps: various components are mixed, stirring is then super in water-bath until be uniformly mixed In sound wave 30-40 DEG C ultrasound 15-30 minutes.
Embodiment 4
A kind of moisture-keeping composition, this moisture-keeping composition is composed of the following components in parts by mass: 45 parts of glycerol, poly dimethyl 20 parts of siloxanes, 2 parts of lecithin, 3 parts of dipropylene glycol, 30 parts of water, 0.7 part of permeation enhancers, 0.3 part of Sodium Hyaluronate and anti-oxidant 0.04 part of agent；Wherein, permeation enhancers are 0.5 part of sodium taurocholate and 0.2 part of stearmide, antioxidant be 0.02 part of vitamin E and 0.02 part of tea polyphenols.
The moisture-keeping composition the preparation method comprises the following steps: various components are mixed, stirring is then super in water-bath until be uniformly mixed In sound wave 30-40 DEG C ultrasound 15-30 minutes.
Embodiment 5
A kind of moisture-keeping composition, this moisture-keeping composition includes following components in parts by mass: 35 parts of glycerol, poly dimethyl silicon 30 parts of oxygen alkane, 8 parts of lecithin, 8 parts of dipropylene glycol, 19 parts of water, 2.8 parts of permeation enhancers, 0.5 part of Sodium Hyaluronate and antioxidant 0.32 part, wherein permeation enhancers are 2 parts and 0.8 part of stearmide of sodium taurocholate, and antioxidant is that 0.16 part of vitamin E and tea are more 0.16 part of phenol.
The moisture-keeping composition the preparation method comprises the following steps: various components are mixed, stirring is then super in water-bath until be uniformly mixed In sound wave 30-40 DEG C ultrasound 15-30 minutes.
It should be understood that mixing various components in embodiment 1-3, stirring is until be uniformly mixed.1) may is that will gather Dimethyl siloxane and lecithin are uniformly mixed, and obtain mixture A；2) glycerol and dipropylene glycol are poured into water, are stirred It is uniformly mixed, obtains mixture B, then be slowly added to be uniformly mixed in mixture A by mixture B.
Various components are mixed in embodiment 4-5, stirring is until be uniformly mixed.May is that 1) by dimethyl silicone polymer, Lecithin, permeation enhancers and antioxidant are uniformly mixed, and obtain mixture A；2) by glycerol, dipropylene glycol Sodium Hyaluronate It is poured into water, is uniformly mixed, obtain mixture B, then be slowly added to be uniformly mixed in mixture A by mixture B ?.
Application effect test:
1, the holding time tests:
A: product is placed in clear vial, room temperature, place a period of time after, 1) observation product colour variation, color It is divided into 1,1.5,2,2.5,3,3.5 and 4 grade, and 1-4 grades, color gradually turns yellow (i.e. 1 grade of color is most light, and 4 grades of colors are most yellow)；2) 8mL is taken, with 1500 revs/min, is centrifuged 5 minutes, the deposited phenomenon of observation centrifugation bottom of the tube, experimental result is shown in Table 1.
Table 1
In addition, if embodiment 4 or 5, not adding vitamin E or tea polyphenols (other compositions for the data in table 1 With preparation method and embodiment 4 or 5) as, it places 15 days after being centrifuged without precipitating, has precipitating after placing centrifugation in 40 days, place Precipitating is also had after centrifugation in 85 days.
Centrifugation be product generally in it is uniformly mixed in the state of be centrifuged.
Illustrate after being added to permeation enhancers, Sodium Hyaluronate and antioxidant, can significantly improve in the case where there is illumination condition The resting period of product is still able to maintain original form after product is placed 85 days, and product is enabled preferably to be applied to illumination Under the conditions of, produce unexpected technical effect.
Meanwhile if product is placed in light-shielding container (such as shading bucket), room temperature, after placing 85 days, embodiment 1-5's Product colour is almost unchanged, and centrifugation is also generated without precipitating, illustrates this product in light-shielding container, can be good at protecting for a long time It deposits.
2, skin sensing examination:
Using the Essence of the prior art, the moisture-keeping composition of the present invention of Essence gross mass 1% or 3%, stirring are added (and/or 30-35 DEG C ultrasound 15-30 minutes) is uniformly mixed, and product is uniformly applied to surface (5 people of (hand) skin Test, data are the average value of test), experimental result is shown in Table 2.
Table 2
Note: numerical value is that skin sense is felt, apply the feeling of descendant, worst is 0, preferably 100.
By experiment as can be seen that product of the present invention can improve the skin sense of Essence well, it is added to permeation enhancers, thoroughly After bright matter acid sodium and antioxidant, effect is more preferable.
3, moistening effect is tested
Using the Essence of the prior art, the moisture-keeping composition of the present invention of Essence gross mass 3% is added, is uniformly mixed, Then be applied to hand skin surface (every place's test area be 5*5cm2, sample size is 0.2 gram), test the table of hand skin Face (temperature is 20 DEG C, humidity 40%-60%) water content, water content are divided into 1-5 grades, and 5 grades of water content highests, 1 grade contains Water is minimum (selection 5 people test, data are the average value of test).
Table 3
Note: 1) embodiment 6 is that embodiment 4 is added without permeation enhancers, other compositions and preparation method and embodiment 4 one Sample；Embodiment 7 is that embodiment 4 is added without hyaluronic acid, and other compositions and preparation method are in the same manner as in Example 4.
Further illustrate, product of the invention that there is good moistening effect.Permeation enhancers, hyaluronic acid, lecithin etc. It can mutually cooperate with, so that moisture content reaches still very high, and water lock effect is good, produces unexpected after smearing after 4 hours Technical effect.This may be that permeation enhancers can help lecithin to permeate, while carry hyaluronic acid and vitamin E etc. together Into the inside of skin, and then being capable of long-time moisturizing.
Wherein, prior art Essence the preparation method comprises the following steps:
1), 2 portions of trehaloses, 3 parts of antierythrites, 0.5 part of xanthan gum and 2 parts of glycerol are added in 75 parts of deionized waters；
2) stirring and dissolving after, being heated to 81-85 DEG C, cools to 35-39 DEG C of 3 parts of Flos Hibisci Mutabilis extracts of addition and 0.2 part sweet Oxalic acid dipotassium, stirs evenly；
3), with citric acid, PH to 5-6 adjusting, 0.2 portion of preservative is added --- uride stirs evenly in.
It should be noted that dimethyl silicone polymer of the present invention can choose viscosity (25 DEG C) between 400-800cps, It enables to product more stable when being arranged so that, is not likely to produce precipitating.
Lecithin is also possible to hydrolecithin, in this way, can save the longer time when being added without antioxidant.
Certainly, No. CAS of each substance can also be table 4 with INCI.
Table 4
Chinese INCI title No. CAS
Dimethyl silicone polymer DIMETHICONE 9006-65-9；63148-62-9；9016-00-6
Lecithin LECITHIN 8002-43-5；8030-76-0；93685-90-6
Dipropylene glycol DIPROPYLENE GLYCOL 110-98-5；25265-71-8
It is also that there is good skin sense after use meanwhile by products application of the invention in smoothing toner either facial mask And moisture retention.
As described above, is only a preferred embodiment of the present invention, when the range that cannot limit implementation of the invention with this, I.e. generally according to simple equivalent changes and modifications made by content documented by the claims in the present invention and description of the invention, all still Belong within the claims in the present invention scope.In addition, abstract part and title, which are intended merely to auxiliary patent document, searches it With the interest field being not intended to limit the invention.

Claims (4)

1. a kind of moisture-keeping composition, which is characterized in that this moisture-keeping composition includes following components in parts by mass: glycerol 35-55 Part, 20-30 parts of dimethyl silicone polymer, 2-8 parts of lecithin, 3-8 parts of dipropylene glycol and 10-30 parts of water.
2. moisture-keeping composition as described in claim 1, which is characterized in that the moisture-keeping composition further includes permeation enhancers 0.7- 2.8 parts, 0.3-0.5 parts of Sodium Hyaluronate and 0.04-0.32 parts of antioxidant.
3. moisture-keeping composition as described in claim 1, which is characterized in that the permeation enhancers are for sodium taurocholate 0.5-2 parts and hard 0.2-0.8 parts of acyl amine, antioxidant is vitamin E 0.02-0.16 parts and tea polyphenols 0.02-0.16 parts.
4. the preparation method of the moisture-keeping composition as described in claim 1-3, which is characterized in that mix various components, stir Until being uniformly mixed.
CN201910521171.1A 2019-06-17 2019-06-17 A kind of moisture-keeping composition and preparation method thereof Pending CN110302076A (en)

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102319199A (en) * 2011-09-07 2012-01-18 珠海姗拉娜化妆品有限公司 Natural long-acting moisture-keeping essence and preparation method thereof
CN102362843A (en) * 2011-10-24 2012-02-29 浙江工业大学 Tea seed oil skin oil and preparation method thereof
KR20140120159A (en) * 2013-04-02 2014-10-13 주식회사 엘지생활건강 Cosmetic composition of pump spray type with composing silicone composition for improving spray angle
CN105534823A (en) * 2016-01-26 2016-05-04 四川程立农业科技有限公司 Tea polyphenols cosmetics
CN108186540A (en) * 2018-03-17 2018-06-22 霍振荣 A kind of body lotion for preventing cutis laxa
CN109394642A (en) * 2018-12-03 2019-03-01 杭州恩格生物医疗科技有限公司 A kind of anti-inflammatory skin care item and preparation method thereof of releiving

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102319199A (en) * 2011-09-07 2012-01-18 珠海姗拉娜化妆品有限公司 Natural long-acting moisture-keeping essence and preparation method thereof
CN102362843A (en) * 2011-10-24 2012-02-29 浙江工业大学 Tea seed oil skin oil and preparation method thereof
KR20140120159A (en) * 2013-04-02 2014-10-13 주식회사 엘지생활건강 Cosmetic composition of pump spray type with composing silicone composition for improving spray angle
CN105534823A (en) * 2016-01-26 2016-05-04 四川程立农业科技有限公司 Tea polyphenols cosmetics
CN108186540A (en) * 2018-03-17 2018-06-22 霍振荣 A kind of body lotion for preventing cutis laxa
CN109394642A (en) * 2018-12-03 2019-03-01 杭州恩格生物医疗科技有限公司 A kind of anti-inflammatory skin care item and preparation method thereof of releiving

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