CN113749957A - Frosted powder mist texture composition, preparation method and application thereof, and lip glaze - Google Patents

Frosted powder mist texture composition, preparation method and application thereof, and lip glaze Download PDF

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Publication number
CN113749957A
CN113749957A CN202111181594.7A CN202111181594A CN113749957A CN 113749957 A CN113749957 A CN 113749957A CN 202111181594 A CN202111181594 A CN 202111181594A CN 113749957 A CN113749957 A CN 113749957A
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mist
frosted
polymethylsilsesquioxane
mica
texture composition
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CN113749957B (en
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何益飞
刘静华
刘媛甜
肖懿宇
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Guangzhou Jiyan Cosmetics Technology Co Ltd
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Guangzhou Jiyan Cosmetics Technology Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/58Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
    • A61K8/585Organosilicon compounds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/26Aluminium; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89Polysiloxanes
    • A61K8/891Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89Polysiloxanes
    • A61K8/895Polysiloxanes containing silicon bound to unsaturated aliphatic groups, e.g. vinyl dimethicone
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/02Preparations containing skin colorants, e.g. pigments
    • A61Q1/04Preparations containing skin colorants, e.g. pigments for lips
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/02Preparations containing skin colorants, e.g. pigments
    • A61Q1/04Preparations containing skin colorants, e.g. pigments for lips
    • A61Q1/06Lipsticks
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/001Preparations for care of the lips

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  • Life Sciences & Earth Sciences (AREA)
  • Public Health (AREA)
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  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
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  • Birds (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Dermatology (AREA)
  • Cosmetics (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Abstract

The invention provides a frosted powder mist texture composition, a preparation method and application thereof and lip glaze, and particularly relates to the technical field of daily cosmetics. The frosted mist texture composition provided by the invention comprises cyclopentadimethylsiloxane, polymethylsilsesquioxane, polydimethylsiloxane/vinyl polydimethylsiloxane crosspolymer and mica. Wherein the mass ratio of the cyclopentadimethylsiloxane, the polymethylsilsesquioxane, the polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer and the mica is (10-50): (1-20): (1-20): (1-20). The reticular cross-linked structure of the powder in the frosted powder mist texture composition can well lock the cyclopentadimethylsiloxane, the residence time of the cyclopentadimethylsiloxane on the skin is prolonged, the longer skin moistening effect is achieved, the velvet effect, the moistening degree and the lasting degree of the cosmetics are synergistically improved, and the product has the light and thin powder mist texture of the frosted powder.

Description

Frosted powder mist texture composition, preparation method and application thereof, and lip glaze
Technical Field
The invention relates to the technical field of daily cosmetics, in particular to a frosted powder mist texture composition, a preparation method and application thereof and lip glaze.
Background
The makeup effect of the frost and the mist makes the makeup face look hazy and soft, brings high-grade makeup feeling compared with the water makeup effect, and is deeply loved by consumers. A great number of powder mist cosmetic products on the market have a plurality of defects, which are particularly characterized by large coating resistance, heavy weight and no lightness, and the phenomena of dry drawing, wrinkle development and dry scrap peeling.
In view of the above, the present invention is particularly proposed.
Disclosure of Invention
One of the purposes of the invention is to provide a frosted powder mist texture composition to relieve the technical problems of large application resistance, heavy weight and light weight, dry drawing and wrinkle development and dry scrap and skin peeling of cosmetics in the prior art.
The second purpose of the present invention is to provide a method for preparing a frosted mist texture composition, which has the advantages of simple preparation process, large treatment capacity, suitability for mass production and low cost.
The invention also aims to provide the application of the frosted mist texture composition, which provides a better soft mist makeup feeling for a lip makeup product and is suitable for large-scale popularization and application.
The fourth purpose of the invention is to provide a lip glaze which has velvet effect, good moistening degree and durability and light and thin powder fog texture of frosted powder.
In order to solve the technical problems, the invention adopts the following technical scheme:
in a first aspect of the invention, a frosted mist texture composition is provided comprising cyclopentadimethylsiloxane, polymethylsilsesquioxane, dimethicone/vinyl dimethicone crosspolymer, and mica.
Optionally, the cyclopentadimethylsiloxane, the polymethylsilsesquioxane, the dimethicone/vinyl dimethicone crosspolymer, and the mica are in a mass ratio of (10-50): (1-20): (1-20): (1-20).
Preferably, the weight ratio of the cyclopentadimethylsiloxane, the polymethylsilsesquioxane, the dimethicone/vinyl dimethicone crosspolymer, and the mica is (15-25): (2-5):(2-5): (4-9).
Preferably, the weight ratio of the cyclopentadimethylsiloxane, the polymethylsilsesquioxane, the dimethicone/vinyl dimethicone crosspolymer, and the mica is (12-18): (3-4): (3-6): (3-4).
Optionally, the cyclopentadecyldimethicone, the polymethylsilsesquioxane, the dimethicone/vinyl dimethicone crosspolymer, and the mica are in a mass ratio of 18:3:3: 4.
Optionally, the cyclopentadecyldimethicone, polymethylsilsesquioxane, dimethicone/vinyl dimethicone crosspolymer, and mica are in a mass ratio of 12:4:6: 3.
The second aspect of the present invention provides a method for preparing the frosted mist texture composition, wherein the cyclopentadimethylsiloxane, the polymethylsilsesquioxane, the dimethicone/vinyl dimethicone crosspolymer, and the mica are uniformly mixed to obtain the frosted mist texture composition.
In a third aspect of the present invention, there is provided the use of said frosted mist texture composition in cosmetics.
Optionally, the frosted mist texture composition is present in the cosmetic in an amount of 15-60% by mass.
Preferably, the content of the frosted mist texture composition in the cosmetic is 25-40% by mass.
Preferably, the cosmetic comprises a lip cosmetic.
Preferably, the lip cosmetic comprises lipstick or lip gloss.
In a fourth aspect, the present invention provides a lip glaze comprising the frosted mist texture composition of the first aspect or the frosted mist texture composition prepared by the preparation method of the second aspect.
Preferably, at least one of an emollient, a filling powder, and a colorant is further included.
Optionally, the emollient comprises a first emollient and a second emollient.
Optionally, an additive is also included.
Preferably, the additive comprises a perfume and/or a preservative.
The invention has at least the following beneficial effects:
according to the frosted powder mist texture composition provided by the invention, polymethylsilsesquioxane and polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer have good dispersibility in cyclopentadimethylsiloxane, and the reticular cross-linked structure of the powder can well lock cyclopentadimethylsiloxane and prolong the residence time of cyclopentadimethylsiloxane on skin, so that a longer-term skin moistening effect is achieved, the velvet effect, the moistening degree and the persistence of cosmetics are synergistically improved, and the product has the light and thin powder mist texture of frosted powder.
The preparation method of the frosted mist texture composition provided by the invention has the advantages of simple preparation process, large treatment capacity, suitability for mass production and low cost.
The application of the cream mist texture composition in cosmetics provides better soft mist makeup feeling for the cosmetics, improves the high-grade makeup feeling and better meets the requirements of consumers.
The lip glaze provided by the invention has a velvet effect, is long in moisture and durable, and is not pulled dry after being smeared, so that the lip makeup has a light and thin powder mist makeup feeling.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention clearer, the technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention. The components of embodiments of the present invention may be arranged and designed in a wide variety of different configurations.
According to a first aspect of the present invention there is provided a frosted mist texture composition comprising cyclopentadimethylsiloxane, polymethylsilsesquioxane, a dimethicone/vinyl dimethicone crosspolymer and mica.
According to the cream mist texture composition provided by the invention, cyclopentadimethylsiloxane is used as an emollient, so that the cream mist texture composition has good ductility and air permeability, can be well attached to skin, and achieves a good emollient effect. However, cyclopentadimethylsiloxane has a high volatility, and gradually volatilizes with the increase of the application time on the skin, so that the effect of moisturizing the skin cannot be achieved for a long time. Polymethyl silsesquioxane and polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer are used as spherical powder, so that smooth and silky feeling can be brought to products, the texture on the surface of skin can be filled, a good soft-focus effect is achieved, and good lubricating and silky feeling is provided, but the silky powder can cause adverse effects such as uneven coloring, faint coloring and the like on products with more pigment toner. Mica as flaky powder can be tightly attached to the surface of skin to play a good color fixing role, but the mica has the phenomena of poor ductility and dryness when being used alone. The polymethylsilsesquioxane and the polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer have good dispersibility in cyclopentadimethylsiloxane, and the reticular cross-linked structure of the powder can well lock the cyclopentadimethylsiloxane and prolong the residence time of the cyclopentadimethylsiloxane on the skin, so that a longer-term skin moistening effect is achieved, the velvet effect, the moistening degree and the persistence of cosmetics are synergistically improved, and the product has the light and thin powder fog texture of frosted powder.
Cyclopenta-dimethyl silicone polymer is colorless, odorless and volatile, and can be added into essence, lotion, foundation make-up, pre-make-up emulsion and hair conditioner to give smooth and silky feeling. Cyclopenta-polydimethylsiloxane is of high molecular weight and is easily volatilized and cannot be absorbed by skin.
Polymethylsilsesquioxane enhances the spreadability and smoothness of the cosmetic, adding gloss to it. The emulsion skin care formula is used for improving smooth skin feeling, glossiness, powder feeling and soft light effect, and the formula presents a fine porcelain appearance, and the proper content can prevent agglomeration, smooth the surface and improve the touch feeling.
The dimethicone/vinyl dimethicone crosspolymer is non-toxic and imparts a silky feel to the product, but this silky feel is not maintained for long periods of time and also reduces the absorption of other ingredients.
Mica belongs to natural mineral, has luster, and can be made into matte shape. The cosmetic is mainly used as a coloring agent, so that the brightness of the cosmetic is increased, and the texture and the touch of the skin are increased after the cosmetic is used. Mica is not absorbed by skin, and is mineral substance which causes no harm to skin, and is mainly used for enhancing the shiny visual effect of cosmetics.
Optionally, the cyclopentadimethylsiloxane, the polymethylsilsesquioxane, the dimethicone/vinyl dimethicone crosspolymer, and the mica are in a mass ratio of (10-50): (1-20): (1-20): (1-20).
In some embodiments of the invention, the mass ratio of cyclopentadimethylsiloxane, polymethylsilsesquioxane, dimethicone/vinyl dimethicone crosspolymer, and mica is typically, but not limited to, 10: 1: 1: 1. 20: 1: 1: 1. 30: 1: 1: 1. 40: 1: 1: 1. 50: 1: 1: 1. 10: 2:2: 2. 20:2:2: 2. 10: 10: 10: 10. 20: 20: 20: 20. 10: 20: 20: 20. 30: 20: 20: 20. 40: 20: 20: 20 or 50: 20: 20: 20.
preferably, the weight ratio of the cyclopentadimethylsiloxane, the polymethylsilsesquioxane, the dimethicone/vinyl dimethicone crosspolymer, and the mica is (15-25): (2-5):(2-5): (4-9).
In some preferred embodiments of the invention, the mass ratio of cyclopentadimethylsiloxane, polymethylsilsesquioxane, dimethicone/vinyl dimethicone crosspolymer, and mica is typically, but not limited to, 15:2:2:4, 25:5:5:9, 20:3:3:6, 25:5:5:5, 20:2:2:4, 20:5:5:5, 20: 4:4:4 or 18:4: 4:4.
Preferably, the weight ratio of the cyclopentadimethylsiloxane, the polymethylsilsesquioxane, the dimethicone/vinyl dimethicone crosspolymer, and the mica is (12-18): (3-4): (3-6): (3-4).
In some preferred embodiments of the invention, the mass ratio of cyclopentadimethylsiloxane, polymethylsilsesquioxane, dimethicone/vinyl dimethicone crosspolymer, and mica is typically, but not limited to, 12:3:3:3, 18:4:6:4, 12:4:4:4, 12:4:6:4, 13:4:4:4, 16:4:4:4, 18:4:4:4, or 16:4:6: 4.
Optionally, the cyclopentadecyldimethicone, the polymethylsilsesquioxane, the dimethicone/vinyl dimethicone crosspolymer, and the mica are in a mass ratio of 18:3:3: 4.
Optionally, the cyclopentadecyldimethicone, polymethylsilsesquioxane, dimethicone/vinyl dimethicone crosspolymer, and mica are in a mass ratio of 12:4:6: 3.
According to the second aspect of the present invention, the preparation method of the cream mist texture composition comprises uniformly mixing the cyclopentadimethylsiloxane, the polymethylsilsesquioxane, the dimethicone/vinyl dimethicone crosspolymer, and the mica to obtain the cream mist texture composition.
The preparation method of the frosted mist texture composition provided by the invention has the advantages of simple preparation process, large treatment capacity, suitability for mass production and low cost.
The use of said frosted mist texture composition provided according to the third aspect of the present invention in cosmetics.
The application of the cream mist texture composition in cosmetics provides better soft mist makeup feeling for the cosmetics, improves the high-grade makeup feeling and better meets the requirements of consumers.
Optionally, the frosted mist texture composition is present in the cosmetic in an amount of 15-60% by mass.
In some embodiments of the present invention, the content of the frosted mist texture composition in the cosmetic is typically, but not limited to, 15%, 20%, 25%, 30%, 35%, 40%, 45%, 50%, 55%, or 60% by mass.
Preferably, the content of the frosted mist texture composition in the cosmetic is 25-40% by mass.
In some preferred embodiments of the present invention, the content of the frosted mist texture composition in the cosmetic is typically, but not limited to, 25%, 30%, 35% or 40% by mass.
Preferably, the cosmetic comprises a lip cosmetic.
Preferably, the lip cosmetic comprises lipstick or lip gloss.
In some embodiments of the invention, the lip cosmetic is typically, but not limited to, lipstick or lip gloss.
According to a fourth aspect of the present invention, there is provided a lip glaze comprising the frosted mist texture composition of the first aspect or the frosted mist texture composition prepared by the preparation method of the second aspect.
The lip glaze provided by the invention has a velvet effect, is long in moisture and durable, and is not pulled dry after being smeared, so that the lip makeup has a light and thin powder mist makeup feeling.
Preferably, at least one of an emollient, a filling powder, and a colorant is further included.
Optionally, the emollient comprises a first emollient and a second emollient.
In some embodiments of the invention, the first emollient is typically, but not limited to, VP/hexadecene copolymer or isododecane.
In some embodiments of the invention, the second emollient is typically, but not limited to, polydimethylsiloxane crosspolymer, caprylyl glycol, tocopheryl acetate, or polyglyceryl-2 triisostearate.
Optionally, the lip glaze further comprises filler powder.
In some embodiments of the invention, the filler powder is typically, but not limited to, silica, a methyl methacrylate crosspolymer, or talc.
Optionally, the lip glaze further comprises a colorant.
In some embodiments of the present invention, the colorant is typically, but not limited to, CI 77491, CI15850, CI 77492, or CI 77499.
Optionally, an additive is also included.
Preferably, the additive comprises a perfume and/or a preservative.
In some embodiments of the invention, the preservative is typically, but not limited to, phenoxyethanol.
Embodiments of the present invention will be described in detail below with reference to examples, but those skilled in the art will appreciate that the following examples are only illustrative of the present invention and should not be construed as limiting the scope of the present invention.
The specifications and types of the raw materials used in the examples and comparative examples of the present invention are shown in the following table 1, and those who do not indicate specific conditions are performed according to the conventional conditions or conditions suggested by the manufacturer.
TABLE 1 raw material specification and model table
Figure BDA0003297462030000081
Example 1
This example provides a frosted mist texture composition comprising the following components: 18kg of cyclopenta dimethyl silicone polymer, 3kg of polymethylsilsesquioxane, 3kg of polydimethylsiloxane/vinyl dimethyl silicone cross-linked polymer and 6kg of mica.
Example 2
This example provides a frosted mist texture composition comprising the following components: 12kg of cyclopentadimethylsiloxane, 6kg of polymethylsilsesquioxane, 5kg of polydimethylsiloxane/vinyl polydimethylsiloxane crosspolymer and 3kg of mica.
Example 3
This example provides a frosted mist texture composition comprising the following components: 25kg of cyclopenta dimethyl silicone polymer, 2kg of polymethylsilsesquioxane, 2kg of polydimethylsiloxane/vinyl dimethyl silicone cross-linked polymer and 1kg of mica.
Example 4
This example provides a frosted mist texture composition comprising the following components: 18kg of cyclopenta dimethyl silicone polymer, 3kg of polymethylsilsesquioxane, 3kg of polydimethylsiloxane/vinyl dimethyl silicone cross-linked polymer and 4kg of mica.
Example 5
This example provides a frosted mist texture composition comprising the following components: 12kg of cyclopenta dimethyl silicone polymer, 4kg of polymethylsilsesquioxane, 6kg of dimethyl silicone polymer/vinyl dimethyl silicone polymer cross-linked polymer and 3kg of mica.
Example 6
This example provides a frosted mist texture composition comprising the following components: 10kg of cyclopenta dimethyl silicone polymer, 1kg of polymethylsilsesquioxane, 1kg of polydimethylsiloxane/vinyl dimethyl silicone cross-linked polymer and 1kg of mica.
Example 7
This example provides a frosted mist texture composition comprising the following components: 10kg of cyclopenta dimethyl silicone polymer, 20kg of polymethylsilsesquioxane, 20kg of polydimethylsiloxane/vinyl dimethyl silicone cross-linked polymer and 20kg of mica.
Example 8
This example provides a frosted mist texture composition comprising the following components: 50kg of cyclopenta dimethyl silicone polymer, 1kg of polymethylsilsesquioxane, 1kg of polydimethylsiloxane/vinyl dimethyl silicone cross-linked polymer and 1kg of mica.
Example 9
This example provides a frosted mist texture composition comprising the following components: 50kg of cyclopentasiloxane, 20kg of polymethylsilsesquioxane, 20kg of polydimethylsiloxane/vinyl polydimethylsiloxane crosspolymer and 20kg of mica.
Example 10
This example provides a lip glaze comprising the frosted mist texture composition provided in example 1, and 1kg of VP/hexadecene copolymer, 9.53kg of isododecane, 35.2kg of polydimethylsiloxane, 6.8kg of polydimethylsiloxane crosspolymer, 0.175kg of octylglycol, 0.2kg of tocopherol acetate, 6kg of polyglycerol-2 triisostearate, 2.5kg of silica, 2kg of methyl methacrylate crosspolymer, 0.067kg of talc, 2.314kg of CI 77491, 1.36kg of CI15850, 0.922kg of CI 77492, 0.357kg of CI 77499, 0.325kg of phenoxyethanol, and 0.05kg of essence.
Example 11
This example provides a lip glaze comprising the frosted mist texture composition provided in example 2, and 5kg of VP/hexadecene copolymer, 10.31kg of isododecane, 35.2kg of polydimethylsiloxane, 6.8kg of polydimethylsiloxane crosspolymer, 0.162kg of octylglycol, 0.2kg of tocopherol acetate, 6kg of polyglycerol-2 triisostearate, 2kg of methyl methacrylate crosspolymer, 3kg of talc, 2.314kg of CI 77491, 1.36kg of CI15850, 0.922kg of CI 77492, 0.357kg of CI 77499, 0.325kg of phenoxyethanol, and 0.05kg of essence.
Example 12
This example provides a lip glaze comprising the frosted mist texture composition provided in example 3, and 1kg of VP/hexadecene copolymer, 10kg of isododecane, 35kg of polydimethylsiloxane, 7kg of polydimethylsiloxane crosspolymer, 0.2kg of octylene glycol, 0.2kg of tocopherol acetate, 6kg of polyglycerol-2 triisostearate, 2.5kg of silica, 2kg of methyl methacrylate crosspolymer, 0.5kg of talc, 2.5kg of CI 77491, 1.3kg of CI15850, 0.9kg of CI 77492, 0.4kg of CI 77499, 0.4kg of phenoxyethanol, and 0.1kg of perfume.
Examples 13 to 18
This example provides a lip glaze comprising the frosted mist texture compositions of examples 4-9, respectively, and the remaining components and amounts are the same as in example 10 and will not be described herein.
Comparative example 1
The comparative example provides a lip glaze comprising the following components: 1kg of VP/hexadecene copolymer, 10kg of isododecane, 35kg of polydimethylsiloxane, 7kg of polydimethylsiloxane crosspolymer, 0.2kg of octanethyl glycol, 0.2kg of tocopherol acetate, 6kg of polyglycerol-2 triisostearate, 6kg of polydimethylsiloxane/vinyl polydimethylsiloxane crosspolymer, 21kg of cyclopentadimethylsiloxane, 3kg of polymethylsilsesquioxane, 2kg of methyl methacrylate crosspolymer, 3kg of talc, 2.5kg of CI 77491, 1.3kg of CI15850, 0.9kg of CI 77492, 0.4kg of CI 77499, 0.4kg of phenoxyethanol and 0.1kg of essence.
Comparative example 2
The lip glaze provided by the comparative example is different from that provided by the comparative example 1 in that 18kg of cyclopentadimethylsiloxane, 6kg of mica, no polymethylsilsesquioxane, 2.5kg of silica and 0.5kg of talcum powder are adopted, and the rest of raw materials and preparation steps are the same as those in the comparative example 1 and are not repeated.
Comparative example 3
This comparative example provides a lip glaze which is different from comparative example 1 in that no polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer, 18kg of cyclopentadimethylsiloxane, 6kg of mica, 6kg of polymethylsilsesquioxane, 2.5kg of silica and 0.5kg of talc are present, and the rest of the raw materials and the preparation steps are the same as in comparative example 1 and are not described again.
Comparative example 4
This comparative example provides a lip glaze, which is different from comparative example 1 in that 9kg of polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer, 12kg of mica, 9kg of polymethylsilsesquioxane, 2.5kg of silica and 0.5kg of talc are used, and the rest of the raw materials and the preparation steps are the same as those in comparative example 1 and are not repeated.
Comparative example 5
This comparative example provides a lip glaze which differs from comparative example 1 in that 9kg of PDMS/vinyl PDMS crosslinked polymer, no mica, no polymethylsilsesquioxane, 2.5kg of silica and 0.5kg of talc are used, and the remaining raw materials and preparation steps are the same as in comparative example 1 and are not described again.
Comparative example 6
The lip glaze provided by the comparative example is different from comparative example 1 in that no polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer, no mica, 9kg of polymethylsilsesquioxane, 2.5kg of silica and 0.5kg of talcum powder are provided, and the rest of raw materials and preparation steps are the same as those of comparative example 1 and are not repeated.
Comparative example 7
The lip glaze provided by the comparative example is different from comparative example 1 in that 9kg of polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer, 9kg of mica, no polymethylsilsesquioxane, 2.5kg of silica and 0.5kg of talcum powder are contained, and the rest of raw materials and preparation steps are the same as those in comparative example 1 and are not repeated.
Test example 1
The lip enamels obtained in examples 10 to 18 and comparative examples 1 to 7 were subjected to a durability effect test.
60 women with daily cosmetic habits of healthy volunteers are selected, and the age is 20-40 years old. The above examples 10-18 and comparative examples 1-7 were applied to the lip skin of volunteers in groups randomly divided into 6 groups of 9-10 persons, and the lip skin of volunteers was examined after 2 hours, and the change in lip color was measured using a spectrocolorimeter (the difference in skin color after 2 hours of use of the product from before use, Δ L, smaller Δ L indicates more color remained on the lips and higher color, i.e., better durability). Specific test results are shown in table 2.
TABLE 2 durability Performance data sheet
Change of lip color Δ L
Example 10 1.7
Example 11 2.0
Example 12 1.9
Example 13 0.7
Example 14 1.1
Example 15 1.9
Example 16 1.6
Example 17 1.8
Example 18 1.3
Comparative example 1 1.7
Comparative example 2 2.3
Comparative example 3 2.2
Comparative example 4 2.7
Comparative example 5 2.5
Comparative example 6 3
Comparative example 7 2
As can be seen from Table 2, the lip color change data of examples 10-18 are smaller than those of comparative examples 1-7, and the lip colors of examples 10-18 have more residual colors and better persistence. Meanwhile, the composition containing the cyclopentadimethyl siloxane, the polymethylsilsesquioxane, the polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer and the mica has the effect of improving the durability in the formula of the lip glaze product. Of these, examples 13 and 14 are the best in durability, as can be seen in cyclopentadimethylsiloxane, polymethylsilsesquioxane, dimethicone/vinyl dimethicone crosspolymer, and mica at (12-18): (3-4): (3-6): the best effect can be achieved when the ratio is (3-4).
Test example 2
The lip enamels obtained in examples 10 to 18 and comparative examples 1 to 7 were subjected to sensory testing.
60 women with daily cosmetic habits of healthy volunteers are selected, and the age is 20-40 years old. The lip enamels obtained in examples 10 to 18 and comparative examples 1 to 7 were subjected to sensory testing. The test dimensions are: velvet fog feeling, moisture degree, and light and thin feeling were evaluated on a scale of 5, with 5 being very excellent, 4 being excellent, 3 being general, 2 being poor, and 1 being poor. The scores were averaged over 60 volunteers and the results are shown in table 3.
TABLE 3 sensory data sheet
Figure BDA0003297462030000141
Figure BDA0003297462030000151
As can be seen from Table 3, the sensory data of examples 10 to 18 are better than those of comparative examples 1 to 7, and examples 10 to 18 are better in velvet, moisturizing, light and thin dimensions. Meanwhile, the composition containing the cyclopentadienylene dimethyl siloxane, the polymethylsilsesquioxane, the polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer and the mica has the effects of enhancing velvet effect, improving moisture and maintaining light and thin makeup feeling in the formula of the lip glaze product. Of these, examples 13 and 14 perform best, and it can be seen that the cross-linked polymers of cyclopentadimethicone, polymethylsilsesquioxane, dimethicone/vinyl dimethicone and mica are described in (12-18): (3-4): (3-6): the best effect can be achieved when the ratio is (3-4).
The frosted mist texture composition provided by the invention enables lip glaze to have a high-grade velvet effect and good moistening degree and durability, enables products to have the light and thin mist texture of frosted powder, and improves the high-grade look of makeup.
The above examples of the present invention are merely examples for clearly illustrating the present invention and are not intended to limit the embodiments of the present invention. Other variations and modifications will be apparent to persons skilled in the art in light of the above description. Any modification, equivalent replacement, and improvement made within the spirit and principle of the present invention should be included in the protection scope of the claims of the present invention.

Claims (10)

1. A frosted mist texture composition comprising cyclopentadimethylsiloxane, polymethylsilsesquioxane, dimethicone/vinyl dimethicone crosspolymer, and mica.
2. The frosted mist texture composition of claim 1, wherein the weight ratio of cyclopentadimethylsiloxane, polymethylsilsesquioxane, the dimethicone/vinyl dimethicone crosspolymer, and mica is 10-50: 1-20: 1-20: 1 to 20;
preferably, the weight ratio of the cyclopentadimethylsiloxane, the polymethylsilsesquioxane, the dimethicone/vinyl dimethicone crosspolymer, and the mica is (15-25): (2-5):(2-5): (4-9).
3. The frosted mist texture composition of claim 1, wherein the weight ratio of cyclopentadimethylsiloxane, polymethylsilsesquioxane, the dimethicone/vinyl dimethicone crosspolymer, and mica is (12-18): (3-4): (3-6): (3-4);
preferably, the weight ratio of the cyclopentadimethylsiloxane, the polymethylsilsesquioxane, the dimethicone/vinyl dimethicone crosspolymer, and the mica is 18:3:3: 4.
4. The frosted mist texture composition of claim 1, wherein the weight ratio of cyclopentadimethylsiloxane, polymethylsilsesquioxane, the dimethicone/vinyl dimethicone crosspolymer, and mica is 12:4:6: 3.
5. The method of preparing a frosted mist texture composition according to any of claims 1-4, wherein the cyclopentadimethylsiloxane, the polymethylsilsesquioxane, the dimethicone/vinyl dimethicone crosspolymer, and the mica are mixed uniformly to obtain the frosted mist texture composition.
6. Use of the frosted mist texture composition according to any of claims 1-4 in cosmetics.
7. The use according to claim 6, wherein the frosted mist texture composition is present in the cosmetic in an amount of 15-60% by weight;
preferably, the content of the frosted mist texture composition in the cosmetic is 25-40% by mass.
8. A lip glaze comprising the frosted mist texture composition of any one of claims 1 to 4 or the frosted mist texture composition prepared by the preparation method of claim 5.
9. The lip glaze according to claim 8, further comprising at least one of an emollient, a filling powder, and a coloring agent;
preferably, the emollient comprises a first emollient and a second emollient.
10. The lip glaze of claim 8, further comprising an additive;
preferably, the additive comprises a perfume and/or a preservative.
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