CN112006942A - Essential oil composition and application thereof - Google Patents
Essential oil composition and application thereof Download PDFInfo
- Publication number
- CN112006942A CN112006942A CN201910460011.0A CN201910460011A CN112006942A CN 112006942 A CN112006942 A CN 112006942A CN 201910460011 A CN201910460011 A CN 201910460011A CN 112006942 A CN112006942 A CN 112006942A
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- Prior art keywords
- oil
- seed oil
- essential
- skin
- essential oil
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- 230000001105 regulatory effect Effects 0.000 description 1
- 238000000518 rheometry Methods 0.000 description 1
- 235000003441 saturated fatty acids Nutrition 0.000 description 1
- 230000037307 sensitive skin Effects 0.000 description 1
- 230000008313 sensitization Effects 0.000 description 1
- 239000008159 sesame oil Substances 0.000 description 1
- 235000011803 sesame oil Nutrition 0.000 description 1
- 229920002545 silicone oil Polymers 0.000 description 1
- 230000037394 skin elasticity Effects 0.000 description 1
- 230000036556 skin irritation Effects 0.000 description 1
- 231100000475 skin irritation Toxicity 0.000 description 1
- 230000005808 skin problem Effects 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 239000003549 soybean oil Substances 0.000 description 1
- 239000008117 stearic acid Substances 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 230000037072 sun protection Effects 0.000 description 1
- 235000020238 sunflower seed Nutrition 0.000 description 1
- 238000003815 supercritical carbon dioxide extraction Methods 0.000 description 1
- 230000009747 swallowing Effects 0.000 description 1
- 235000019640 taste Nutrition 0.000 description 1
- 230000009967 tasteless effect Effects 0.000 description 1
- 239000002562 thickening agent Substances 0.000 description 1
- 229960000984 tocofersolan Drugs 0.000 description 1
- 235000019149 tocopherols Nutrition 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 238000002137 ultrasound extraction Methods 0.000 description 1
- -1 vitamin E compound Chemical class 0.000 description 1
- 235000020234 walnut Nutrition 0.000 description 1
- 239000010497 wheat germ oil Substances 0.000 description 1
- 230000002087 whitening effect Effects 0.000 description 1
- 230000037314 wound repair Effects 0.000 description 1
- 235000004835 α-tocopherol Nutrition 0.000 description 1
- 239000002076 α-tocopherol Substances 0.000 description 1
- 235000007680 β-tocopherol Nutrition 0.000 description 1
- 239000011590 β-tocopherol Substances 0.000 description 1
- 239000002478 γ-tocopherol Substances 0.000 description 1
- QUEDXNHFTDJVIY-UHFFFAOYSA-N γ-tocopherol Chemical class OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1 QUEDXNHFTDJVIY-UHFFFAOYSA-N 0.000 description 1
- QUEDXNHFTDJVIY-DQCZWYHMSA-N γ-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1 QUEDXNHFTDJVIY-DQCZWYHMSA-N 0.000 description 1
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/115—Fatty acids or derivatives thereof; Fats or oils
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/11—Encapsulated compositions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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Abstract
The invention discloses an essential oil composition and application thereof. The invention firstly discloses an essential oil composition which comprises the following components in percentage by weight: 0.001-99% of the seed oil of the Indian fruit, 0.001-99% of the seed oil of the purple perilla and 0.001-99% of the sesame seed oil. The vegetable oil composition is prepared into soft capsule cosmetics or foods, can prevent oil from oxidative deterioration, and can supplement oil by supplementing unsaturated fatty acids of three vegetable oils to enhance essential linolenic acid to balance and supplement oil, keep skin soft, fine, smooth and compact, keep hair smooth and bright, supplement dietary nutrition, and maintain health.
Description
Technical Field
The invention relates to the technical field of cosmetics and foods, in particular to a natural essential oil composition and application thereof.
Background
Essential oil is a pure oil-based cosmetic system and plays a role in supplementing oil in the skin or hair care process. The essential oil can be divided into I type and II type according to the formula. Wherein the type I is mainly mineral oil; the II type takes synthetic grease or natural grease as a substrate, and is compounded with other natural grease and essential oil, so that the oil is supplemented, the skin care effects of relieving, helping sleep, removing acnes and the like are increased, and the hair care effects of improving carding, softening, luster and the like are improved.
The type I essential oil is an enclosed humectant, is greasy in skin feel, is easy to block pores, causes blackheads, comes from petrochemical industry, such as mineral oil, silicone oil and the like, and is not beneficial to environmental protection; the II type essential oil is popular with consumers increasingly due to natural raw materials, multi-source edible plants, ecological environmental protection, multiple effects, health and safety, and becomes a mainstream product in the current market.
Investigation of the uk Mintel GNPD global new product database revealed that there was a global total of 781 skin care essential oil products marketed to date including body care (645sku), face/neck care (87sku), suit (17sku), hand/nail care (14sku), sun protection (9sku), lip care (3sku), foot care (3sku), disarmed water (1sku), eye care (1 sku). As can be seen, skin oils are currently used mainly in two major areas, body care and face/neck care.
The essential oil has a simple formula, mainly comprises vegetable oil and natural essential oil, and is mostly non-linolenic mixed oil on the market. Deep analysis of a 87-model facial natural essential oil formula shows that the main 10 types of plant oil raw materials comprise avocado oil, wild soybean oil, sunflower seed oil, hazelnut seed oil, jojoba seed oil, meadowfoam seed oil, macadamia nut seed oil, rosa canina fruit oil, castor bean oil and cashew nut oil. These vegetable fats and oils generally contain two saturated fatty acids, C16:0Palmitic acid Palmitic acid and C18:0Stearic acid Stearic acid, and 1 Monounsaturated fatty acid (MUFA), C18:1n-9 Oleic acid (Oleic acid), and 1 polyunsaturated fatty acid (PUFA), C18:2n-6 Linoleic acid (linolic acid). Since linoleic acid and another PUFA, Linolenic acid (Linolenic acid), are necessary for the formation of the epidermal lipid barrier and for healthy body functions, Linolenic acid, which is an essential omega-3 essential polyunsaturated fatty acid, is relatively lacking in current mainstream essential oil formulations.
Because saturated fatty acid is difficult to absorb, the skin feels greasy or sticky, pores are easy to block, acne is induced, the skin is not suitable for oily skin, and polyunsaturated fatty acid is easy to absorb, low in residue and fresh and cool in skin feel, has the anti-inflammatory and soothing effects and is suitable for various skin types and sensitive skin, the essential oil is selected from vegetable oil raw materials, and particularly needs to be further strengthened by linolenic acid type grease to balance the polyunsaturated fatty acid, so that the skin care and health care value is improved. According to investigation, only a few vegetable oils and fats in nature, such as purple perilla seed oil, Indian fruit seed oil, linseed oil and the like, contain higher contents of C18:3n-3 alpha-linolenic acid and C18:3n-6 gamma-linolenic acid.
Once rich in polyunsaturated fatty acids, essential oils tend to deteriorate by oxidation. The higher the polyunsaturated fatty acid content, the higher the skin care value, but the greater the difficulty of the antioxidant technology. In order to prevent the oxidation of oil, chemical antioxidants or natural antioxidants are often added into the formula of the essential oil, but the addition is not an ideal scheme.
Vitamin E acetate (tocopheryl acetate), 2, 6-di-tert-butyl-4-methylphenol (butylated hydroxytoluene (BHT)), and the like, which are common chemical antioxidants for essential oils. The vitamin E acetate can resist grease oxidation, and has the effects of moistening and preserving skin, protecting ultraviolet ray and the like. According to the safety evaluation report of the american society for cosmetics and perfumery (CTFA) cosmetic ingredient examination (CIR) panel, tocopheryl acetate has a potential risk of skin sensitization and carcinogenesis (Photo-carcinogenesis), and contains Methyl-hydroquinone (Methyl-hydroquinone) as a synthetic raw material. BHT has toxicity to liver, lung and kidney at high dose or in long-term use, has no established carcinogenicity or anticancer activity, and can cause skin irritation and sensitization. Based on potential health risks, the global environment working group EWG scored tocopherol acetate and BHT as 3 and 4 points, respectively.
In order to prevent the oxidation of the grease, the second method is to add natural antioxidants such as Vitamin A (VA), Vitamin E (VE) and wheat germ oil into the formula of the essential oil, and the natural antioxidants are rich in VE and dihydroxy-gamma-ferulic acid phytosterol ester, so that the antioxidant effect can be partially replaced, but the grease cannot be sufficiently prevented from being oxidized and deteriorated by using the natural antioxidants alone, and other technologies are still required to be combined for application.
For 2016, the cosmetics in foreign countries have come into new dosage forms of external essential oil soft capsules or Ampoules (Ampoules), and gradually receive industrial attention. The essential oil wrapped by the soft capsule is mature and feasible in preparation technology, can effectively isolate air, prevent oil from oxidative deterioration, improve the stability of the product and prolong the shelf life, becomes an antioxidant technology and a new formulation of the essential oil with a very promising prospect, and is suitable for a linolenic acid type essential oil product with higher antioxidant technical requirements.
At present, the beauty oil soft capsule is still used as an oral food preparation formulation in China, such as an astaxanthin tea seed oil capsule-201611041965.0; walnut hemp oil health food-201010236464.4; vitamin E compound capsule-200710068178. X. Secondly, the microcapsule is used as an intermediate raw material of food or cosmetics instead of a product formulation, such as a peony seed oil microcapsule, a preparation method and application thereof-201410195444.5; a coenzyme Q10 microcapsule, its preparation method and application-201110406600.4; a cosmetic-201410029596.8 containing mosquito repellent composition microcapsule is provided.
In recent years, soft capsule cosmetics begin to gradually appear in China, but no patent technology of external essential oil soft capsules exists. 201710336305.3 provides a skin caring capsule, which breaks the packaging form of conventional cosmetics and is packaged in disposable capsule. The oily or dry product can be packaged with gelatin, and the water-soluble product can be packaged with waterproof material (such as plastic). For ease of use, a twist-off seal may be left at one end of the capsule. 201810539888.4-provides a capsule essence and a method for preparing the same.
In a word, the essential oil gradually takes natural vegetable oil as the main product flow, and the industry needs a healthier and safer antioxidant technology and a new formulation product of linolenic acid type essential oil so as to solve the problems that the vegetable oil is easy to oxidize and deteriorate and has insufficient nutritional performance.
Disclosure of Invention
One of the purposes of the invention is to provide a essence oil composition.
The second object of the present invention is to provide the use of the above composition.
In order to achieve the purpose, the invention adopts the following technical scheme: the invention provides an essential oil composition which comprises the following components in percentage by weight: 0.001-99% of the seed oil of the Indian fruit, 0.001-99% of the seed oil of the purple perilla and 0.001-99% of the sesame seed oil.
Preferably, the composition comprises the following components in percentage by weight: 0.1 to 50 percent of the seed oil of the Indian fruit, 0.1 to 50 percent of the perilla seed oil and 0.1 to 50 percent of the sesame seed oil.
Preferably, the composition comprises the following components in percentage by weight: 1-40% of the seed oil of the Indian fruit, 1-40% of the seed oil of the purple perilla and 1-40% of the sesame seed oil.
The invention further provides application of the composition in preparing external soft capsule cosmetics and internal soft capsule foods.
The invention further provides a skin-care and hair-care soft capsule cosmetic which is characterized by comprising the following components in percentage by weight: 0.001-99% of the adductor seed oil, 0.001-99% of the perilla seed oil, 0.001-99% of the sesame seed oil and the balance of cosmetic auxiliary materials.
Preferably, the cosmetic comprises the following components in percentage by weight: 0.1 to 50 percent of the seed oil of the Indian fruit, 0.1 to 50 percent of the perilla seed oil, 0.1 to 50 percent of the sesame seed oil and the balance of cosmetic auxiliary materials.
Preferably, the cosmetic comprises the following components in percentage by weight: 1-40% of the seed oil of the Indian fruit, 1-40% of the seed oil of the purple perilla and 1-40% of the sesame seed oil.
The invention further provides an oral soft capsule food which is characterized by comprising the following components in percentage by weight: 0.001-99% of the adductor seed oil, 0.001-99% of the perilla seed oil, 0.001-99% of the sesame seed oil and the balance of cosmetic auxiliary materials.
Preferably, the soft capsule food comprises the following components in percentage by weight: 0.1 to 50 percent of the seed oil of the Indian fruit, 0.1 to 50 percent of the perilla seed oil, 0.1 to 50 percent of the sesame seed oil and the balance of cosmetic auxiliary materials.
Preferably, the soft capsule food comprises the following components in percentage by weight: 1-40% of the seed oil of the Indian fruit, 1-40% of the seed oil of the purple perilla and 1-40% of the sesame seed oil.
The soft capsule cosmetics or soft capsule food auxiliary materials are natural, edible and high-purity cosmetics or food auxiliary materials, such as a solvent, natural grease, a chelating agent, an emulsifier, a humectant, a thickener, a solubilizer, an emollient, a rheology regulator, an antioxidant, a whitening agent, an anti-aging agent, a conditioner, a soothing agent and the like, and are prepared into soft capsule cosmetics or soft capsule food according to a certain proportion. Non-food-grade cosmetic auxiliary materials are not applied to the preparation of soft capsules.
The essential oil composition developed based on the technology has the following advantages:
1) linolenic acid type essential oil can balance and supplement omega 3, omega 6 and omega 9 fatty acid of skin or hair;
2) contains natural antioxidant, and can prevent oxidative deterioration of essential oil to a certain extent;
3) the skin care product is dry oil, is fresh and easy to absorb, has no greasy skin feel and no stickiness in hair feel, is mild and low in stimulation, and is suitable for various skin types and hair types;
4) has multiple skin and hair care effects such as moistening and repairing, and nutrition and health promotion effects.
The essential oil soft capsule developed based on the technology further has the following advantages and characteristics:
1) the dosage form is novel, beautiful and sanitary: the air can be effectively isolated, the oxidative deterioration of oil is prevented, the freshness of essential oil is kept, the stability of the product is improved, the shelf life is prolonged, and particularly, the product is kept fresh and guaranteed after being opened;
2) the large package and the small package are organically combined, so that the storage is convenient, and the bag is convenient to carry in a small amount of outdoor travel;
3) comprehensive use: the full-food-grade cosmetic or food can be combined with oral administration and external application, has multiple functions, and realizes comprehensive beauty and health care.
In addition, the cosmetic or food developed based on the composition of the invention has the formula without adding essence, chemical pigment, chemical antioxidant, mineral oil petrolatum and allergen; and the formula is edible, all natural and high in purity (EWG score is less than or equal to 2 points).
The essential oil of the invention, including the crabapple seed oil, the perilla seed oil and the sesame seed oil, can be prepared by adopting pharmaceutical technology, such as supercritical carbon dioxide extraction, low-temperature cold pressing, ultrasonic/microwave extraction, organic solvent extraction and other methods, or traditional heating reflux, cold soaking, percolation, distillation and other methods, and can also be a vegetable oil product with standard and quantitative unsaturated fatty acid on the market, such as crabapple seed oil with 95 percent of total unsaturated fatty acid and the like.
The essential oil comprises the crabapple seed oil, the perilla seed oil and the sesame seed oil which are all cosmetic raw materials and food raw materials approved by China.
The Plukenetia VOLUBILIS or Plukenetia VOLUBILIS SEED OIL, is golden yellow amber OIL, is native to south America, and has been eaten by local residents for more than 3000 years to keep skin soft, help wound repair, and prevent and treat insect bite and microbial infection and other skin problems in tropical areas. The alpha-Linolenic acid (Linolenic acid) content in the plukenetia volubilis linneo oil is more than 42%, the total unsaturated fatty acid accounts for more than 92% of the fat content, the plukenetia volubilis linneo oil mainly comprises Linolenic acid (42% -60%), oleic acid (8% -15%) and linoleic acid (25% -40%), can balance omega 3, omega 6 and omega 9 fatty acids, is easy to absorb into dry oil, is beneficial to balancing and supplementing skin grease, has fresh skin feel, can moisten skin and resist aging, protects hair, and prevents hair from breaking and branching. The high content of polyunsaturated fatty acids in the embelia americana oil makes it very easily oxidisable even in mild environments, and has a certain degree of self-oxidation resistance due to the presence of type 4 tocopherols including alpha-tocopherol (vitamin E), beta-tocopherol, gamma-tocopherol (>100ppm) and-tocopherol (>60 ppm). The crabapple oil, with an EWG score of 1, has been marketed globally for 1637 products, including 866 skin care products and 534 hair products, in the beauty and personal care areas. In the field of food, the crabapple seed oil is a new resource food approved by China, and has health-care functions of reducing fat, resisting depression and the like.
Perilla (Perilla frutescens) SEED OIL, British name Perilla frutescens SEED OIL, is a light yellow vegetable OIL obtained by cold pressing Perilla frutescens SEEDs, has mild smell, is rich in essential fatty acids, mainly omega 3 alpha-linolenic acid (C18:3n-3), usually 50% -60%, and is slightly higher than the crabapple SEED OIL. Also a dry oil, has refreshing and non-greasy skin feeling, and has healing, anti-aging, soothing, moisturizing and skin caring properties. Perilla seed oil, with an EWG score of 1, has been marketed globally to date under item 577 in the beauty and personal care areas, including skin care products (473sku) and hair products (16 sku). In the food field, 36 dietary supplement products are sold on the market all over the world and are used for strengthening brain, protecting eyes, resisting oxidation, protecting heart blood vessels and the like.
SESAME (SESAMUM INDICUM) SEED OIL, known as SESAMUM INDICUM (SESAME) SEED OIL, is a colorless or yellow transparent vegetable OIL extracted from SESAME SEEDs and has a fragrant smell. The sesame seed oil mainly contains oleic acid and linoleic acid, and the linolenic acid content is low. Sesame seed oil has strong oxidation resistance, stability and long shelf life, and contains natural vitamins A and E and antioxidant unsaponifiable matters which are lacked in part of vegetable oil, such as Sesamin (Sesamin), Sesamol (Sesamol), Sesamolin (Sesamolin) and the like. Sesame seed oil, with an EWG score of 1, is a universal personal care oil. In the fields of beauty treatment and personal care, the natural essence, the skin conditioner and the hair conditioner are used, and 11,908 types of products containing sesame seed oil are sold on the market globally so far, including skin care products (8,301sku) and hair products (1,412 sku). Sesame oil is recommended for essential oil natural antioxidants due to its antioxidant activity. Good skin feeling, easy penetration and absorption, moistening, purifying/detoxifying and regenerating/repairing, and can restore moisture and skin elasticity, moisturize and resist aging. In the food field, 79 dietary supplement products are sold on the market globally and are used for regulating immunity, slimming, protecting cardiovascular system, resisting oxidation, protecting vision, strengthening brain, supplementing energy, assisting digestion and the like.
Drawings
Fig. 1 shows a essence oil soft capsule prepared in an embodiment of the present invention.
Detailed Description
The invention is further illustrated by the following examples. The following examples present representative gel preparations and associated test data. It must be noted that the following examples are intended to illustrate the invention and are not intended to limit it. The simple increase and decrease of the formula raw materials and the process improvement of the invention according to the essence of the invention belong to the protection scope of the invention.
Example 1 preparation and application of essential oil soft capsule cosmetic of the present invention
The formula of the essence oil is as follows:
the formula of the soft capsule rubber is as follows:
| # | ingredient name | Proportion (%) |
| 1 | Gelatin | 40.82％ |
| 2 | Glycerol | 18.36％ |
| 3 | Purified water | 40.82％ |
| Total up to | 100％ |
The process flow comprises the following steps:
1) preparing essential oil: uniformly mixing lavender oil and the same amount of camellia seed oil, adding the same amount of camellia seed oil into the mixture, uniformly mixing the mixture again, finally adding the same amount of camellia seed oil into the mixture, uniformly mixing the mixture with the sesame seed oil and the sea buckthorn seed oil, putting the mixture, the rest camellia seed oil, the rest perilla seed oil, the rest plukenetia volubilis linneo oil (the nectarine seed oil) and the rest tocopherol (vitamin E) into a pot, stirring for 1 hour, emulsifying and homogenizing for 30 minutes, vacuumizing until no bubbles exist, detecting quality parameters, and discharging for later use after the mixture is qualified.
2) Preparing soft capsules: assembling a soft capsule pelleting press, adjusting process parameters and pressing the gelatin-glycerol soft capsule. The thickness of the rubber is controlled between 0.80mm and 0.90mm, and the viscosity of the rubber solution is controlled between 18000 and 22000 CPa. The content of the essence oil is 0.42-0.45 g/grain.
3) And (3) capsule shaping and drying: and (5) carrying out drying operation, and detecting the weight and the hardness of the product in the process.
4) Rejecting unqualified products: and selecting and discarding the abnormal pills, the adhesion pills, the bubble pills, the leakage pills and other unqualified products.
5) Packaging: aluminum-plastic or bottling and boxing.
And (3) stability investigation:
sample placement conditions: temperature 38 ± 1 ℃, relative humidity: 75 percent; after continuous 3-month inspection, the inspected items including sense, loading deviation, peroxide value, acid value, total number of bacterial colonies, coliform group, mould and yeast are qualified, and the result meets the requirement of product quality standard; the product has stable quality according to the detection result of the stability test.
Skin feel trial for consumers:
10 female consumers, 25-50 years old, participated in a single experience of skin feel for the product (see figure 1), with the following test results: the soft capsule is light yellow in appearance, transparent and oily, has crystal and moist texture, is fragrant in essence oil after a capsule handle is opened, is easy to smear and spread, is fresh, non-sticky, non-greasy, easy to absorb and low in residue, and finally has insignificant oily feeling, soft, moist and bright skin. The skin types are not irritant and sensitive.
Example 2 preparation and application of essence oil soft capsule cosmetic of the invention
The formula of the essence oil is as follows:
| # | name of raw materials | Input proportion | Use of |
| 1 | Perilla seed oil | 40％ | Hair conditioning agent |
| 2 | Mega fruit oil (Indian fruit seed oil) | 40％ | Hair conditioning agent |
| 3 | Sesame seed oil | 19％ | Hair conditioning agent |
| 4 | Tocopherol (vitamin E) | 1％ | Antioxidant agent |
| Total up to | 100％ |
The formula of the soft capsule rubber is as follows:
| # | ingredient name | Proportion (%) |
| 1 | Gelatin | 40.82％ |
| 2 | Glycerol | 18.36％ |
| 3 | Purified water | 40.82％ |
| Total up to | 100％ |
The process flow comprises the following steps:
1) preparing essential oil: adding oleum Sesami, Perilla seed oil, MEIGUOGUO oil, and tocopherol (vitamin E) into a pot, stirring for 1 hr, emulsifying and homogenizing for 30 min, vacuumizing until no bubble is formed, detecting quality parameters, and discharging after qualified.
2) Preparing soft capsules: assembling a soft capsule pelleting press, adjusting process parameters and pressing the gelatin-glycerol soft capsule. The thickness of the rubber is controlled between 0.80mm and 0.90mm, and the viscosity of the rubber solution is controlled between 18000 and 22000 CPa. The content of the essence oil is 0.42-0.45 g/grain.
3) And (3) capsule shaping and drying: and (5) carrying out drying operation, and detecting the weight and the hardness of the product in the process.
4) Rejecting unqualified products: and selecting and discarding the abnormal pills, the adhesion pills, the bubble pills, the leakage pills and other unqualified products.
5) Packaging: aluminum-plastic or bottling and boxing.
And (3) stability investigation:
sample placement conditions: temperature 38 ± 1 ℃, relative humidity: 75 percent; after continuous 3-month inspection, the inspected items including sense, loading deviation, peroxide value, acid value, total number of bacterial colonies, coliform group, mould and yeast are qualified, and the result meets the requirement of product quality standard; the product has stable quality according to the detection result of the stability test.
And (3) hair care trial of consumers:
10 female consumers, 25-50 years old, participated in the single experience of hair care of the essential oil, and the test results are as follows: the soft capsule has light golden yellow appearance, transparent oil shape, crystal and moist texture, after the capsule handle is opened, the essential oil has faint scent and is easy to smear, and after the soft and moist soft capsule is smeared, the hair is soft, moist, bright, smooth and easy to comb. Can be used for multiple times to improve hair breakage and split.
Example 3 preparation and application of essence oil soft capsule cosmetic of the invention
The formula of the essence oil is as follows:
| # | name of raw materials | Input proportion |
| 1 | Perilla seed oil | 10％ |
| 2 | Mega fruit oil (Indian fruit seed oil) | 50％ |
| 3 | Sesame seed oil | 40％ |
| Total up to | 100％ |
The formula of the soft capsule rubber is as follows:
| # | ingredient name | Proportion (%) |
| 1 | Gelatin | 40.82％ |
| 2 | Glycerol | 18.36％ |
| 3 | Purified water | 40.82％ |
| Total up to | 100％ |
The preparation process flow comprises the following steps:
1) preparing essential oil: adding oleum Sesami, Perilla seed oil, and MEIGUOGUO oil (Plukenetia volubilis seed oil) into a pot, stirring for 1 hr, emulsifying and homogenizing for 30 min, vacuumizing until no bubble is formed, detecting quality parameters, and discharging after qualified.
2) Preparing soft capsules: assembling a soft capsule pelleting press, adjusting process parameters and pressing the gelatin-glycerol soft capsule. The thickness of the rubber is controlled between 0.80mm and 0.90mm, and the viscosity of the rubber solution is controlled between 18000 and 22000 CPa. The content of the essence oil is 0.42-0.45 g/grain.
3) And (3) capsule shaping and drying: and (5) carrying out drying operation, and detecting the weight and the hardness of the product in the process.
4) Rejecting unqualified products: and selecting and discarding the abnormal pills, the adhesion pills, the bubble pills, the leakage pills and other unqualified products.
5) Packaging: aluminum-plastic or bottling and boxing.
And (3) stability investigation:
sample placement conditions: temperature 38 ± 1 ℃, relative humidity: 75 percent; after continuous 3-month inspection, the inspected items including sense, loading deviation, peroxide value, acid value, total number of bacterial colonies, coliform group, mould and yeast are qualified, and the result meets the requirement of product quality standard; the product has stable quality according to the detection result of the stability test.
The consumer tastes out:
10 female consumers, 25-50 years old, took part in the single experience of the mouthfeel of the essential oil soft capsule food. 1 capsule is taken orally, is tasteless and is easy to swallow; after swallowing, there is no gastrointestinal discomfort. Can be used as dietary supplement of linolenic acid, and is beneficial for skin and health.
Claims (6)
1. A essence oil composition for cosmetics and foods, comprising: 0.001-99% of the seed oil of the Indian fruit, 0.001-99% of the seed oil of the purple perilla and 0.001-99% of the sesame seed oil.
2. The essential oil composition of claim 1, which comprises: 0.1 to 50 percent of the seed oil of the Indian fruit, 0.1 to 50 percent of the perilla seed oil and 0.1 to 50 percent of the sesame seed oil.
3. The essential oil composition of claim 1, which comprises: 1-40% of the seed oil of the Indian fruit, 1-40% of the seed oil of the purple perilla and 1-40% of the sesame seed oil.
4. The composition according to any one of claims 1 to 3, which can be mixed with other cosmetic raw materials to make into soft capsule cosmetic for skin care of face, body, hands and feet.
5. The composition according to any one of claims 1 to 3, which can be formulated into a soft capsule cosmetic for hair care products in combination with other cosmetic raw materials.
6. The composition according to any one of claims 1 to 3, optionally in combination with other food materials, for the preparation of a soft gelatin capsule food for nutritional dietary supplementation.
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| CN201910460011.0A CN112006942A (en) | 2019-05-30 | 2019-05-30 | Essential oil composition and application thereof |
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| CN201910460011.0A CN112006942A (en) | 2019-05-30 | 2019-05-30 | Essential oil composition and application thereof |
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| CN112006942A true CN112006942A (en) | 2020-12-01 |
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| CN201910460011.0A Pending CN112006942A (en) | 2019-05-30 | 2019-05-30 | Essential oil composition and application thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113057911A (en) * | 2021-04-12 | 2021-07-02 | 杭州易蓬科技有限公司 | Skin care composition with water resistance and antibacterial effect |
| CN114917158A (en) * | 2022-05-25 | 2022-08-19 | 云南西草资源开发有限公司 | Anti-aging essence containing micro-molecule plukenetia volubilis linneo oil with permeation promoting technology and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN113057911A (en) * | 2021-04-12 | 2021-07-02 | 杭州易蓬科技有限公司 | Skin care composition with water resistance and antibacterial effect |
| CN114917158A (en) * | 2022-05-25 | 2022-08-19 | 云南西草资源开发有限公司 | Anti-aging essence containing micro-molecule plukenetia volubilis linneo oil with permeation promoting technology and preparation method thereof |
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Application publication date: 20201201 |