CN102178629B - Silybum marianum essential oil skin-care cream and preparation method thereof - Google Patents
Silybum marianum essential oil skin-care cream and preparation method thereof Download PDFInfo
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- CN102178629B CN102178629B CN2011100979333A CN201110097933A CN102178629B CN 102178629 B CN102178629 B CN 102178629B CN 2011100979333 A CN2011100979333 A CN 2011100979333A CN 201110097933 A CN201110097933 A CN 201110097933A CN 102178629 B CN102178629 B CN 102178629B
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Abstract
The invention discloses silybum marianum essential oil skin-care cream and a preparation method thereof. The formula of the silybum marianum essential oil skin-care cream comprises 5-15 parts of silybum marianum essential oil, 2-4 parts of glycerin monostearate (GMS), 6-13 parts of stearic acid, 4-9 parts of white Vaseline, 6-13 parts of liquid paraffin, 5-15 parts of glycerol, 10-18 parts of urea and 70-90 parts of deionized water. The preparation method of the silybum marianum essential oil skin-care cream comprises the following steps: respectively heating oil-phase raw materials and water-phase raw materials to 70-80 DEG C, and stirring at the temperature of 70-80 DEG C and the pressure of 1-1.3atm (standard atmospheric pressure) to obtain oil-phase material and water-phase material; stirring the oil-phase material and the water-phase material to form emulsion under heat insulation condition; and cooling to 45 DEG C, adding perfume materials, stirring, cooling to below 35 DEG C and finally discharging. The skin-care cream has the advantages of promoting metastasis, preserving heat, nourishing skin, and preventing frostbite and healing chaps without side effects, is particularly suitable for a person with dry and rough skin and skin peeling on hands and feet.
Description
Technical field
The present invention relates to a kind of cosmetics and preparation method thereof, is a kind of silybum marianum essential oil skin-care cream and preparation method thereof specifically.
Background technology
Be seen everywhere in the market for xerosis cutis, coarse, the peel cosmetics of phenomenon of skin brothers, although also can have effect, but the weak effect that moisturizing, control are chapped, multipotency kept about 1 hour, and then skin can recover again former state, so just needed repeatedly to smear again, thereby increase the use amount of cosmetics, increased cost.And existing cosmetics much have side effect, and the somebody tends to occur buccal redness, flowing water, pruritus, dermatitis equivalent damage face or causes skin allergic reaction after using, and will make like this skin become even worse.
Herba Silybi mariani has another name called that water flies Phasiana, Silybum marianum Gaertn is Compositae Silybum plant.Formal name used at school (Silybum marianum CL, Gaertn.) be biennial or the annual herb plant.Originate in Mediterranean, wild distribution is also arranged on the western grass in Asia.All there are cultivation in existing Europe, Asia, Africa, South and North America.
Silybum Marianum Gaertn Seed Oil claims " kangaroo oil " (Kangal oil) abroad, and edible and sunflower seed oil, safflower oil are similar.The units such as the 4th pharmaceutical factory, institute for drug control, Wuhan, botanical garden, Xi'an made animal toxicity experiment, nutritional test and edible through Guangzhou at home, proved nontoxicly, had higher nutritive value; Again through many people repeatedly for many years, edible through the new Cao Zhen resident in Dongtai city particularly is all without abnormal response.But because the present large multiplex 95 type oil presses of liquefaction equipment of China, material loading, discharge, remove impurity etc. are all manually carried out; The machine oil expression is only through natural sedimentation, and the oil product acid number is high, and the gastronomical process oil smoke is large, and edible flavor is poor; Machine presses cake and can not directly eat because solvent is high through carrying the oil that reclaims after element is carried in plain workshop, can only sell as iundustrial oil, has caused very large waste.
Summary of the invention
Goal of the invention: in order to overcome the deficiencies in the prior art, the object of the present invention is to provide a kind ofly can enhance metabolism, preserving moisture and protecting skin, the antifreeze silybum marianum essential oil skin-care cream that more splits, has no side effect.
Another object of the present invention is to provide a kind of preparation method of silybum marianum essential oil skin-care cream.
Technical scheme: in order to solve the problems of the technologies described above, the technical solution adopted in the present invention is:
A kind of silybum marianum essential oil skin-care cream, comprise following component, the prescription of each component is as follows: 5-15 part Herba Silybi mariani quintessence oil, 2-4 part monoglyceride, 6-13 part stearic acid, 4-9 part white vaseline, 6-13 part white oil, 5-15 part glycerol, 10-18 part carbamide, 70-90 part deionized water more than are mass fraction.
Optimization formula is: according to the mass fraction, and 10 parts of Herba Silybi mariani quintessence oils, 3 parts of monoglycerides, 8 parts of stearic acid, 7 parts of white vaseline, 10 parts of white oils, 9 parts of glycerol, 15 parts of carbamide, 80 parts of deionized waters.
In order to solve above-mentioned another purpose, the technical solution adopted in the present invention is: the preparation method of described silybum marianum essential oil skin-care cream, the method comprises the steps:
(1) accurately take by weighing each component according to prescription, for subsequent use;
(2) Herba Silybi mariani quintessence oil, monoglyceride, stearic acid, white vaseline, white oil are joined in the oil phase stirred tank, are heated to 70-80 ℃, 1 to-1.3 standard atmosphere depress and 70-80 ℃ of insulated and stirred to the fusing, namely obtain oil phase material;
(3) deionized water, glycerol, carbamide are joined in the water stirred tank, be warmed to 70-80 ℃, depress and in the dissolving of 70-80 ℃ of insulated and stirred, obtain the water material at 1 to-1.3 standard atmosphere;
(4) under the insulated and stirred oil phase material and water material are joined in the emulsifying kettle, depress and became the uniformly emulsify shape at 70-80 ℃ of insulated and stirred 10-20 minute at 1 to-1.3 standard atmosphere;
Allocate the spice of 0.1-0.3 mass parts when (5) then being cooled to 45 ℃ into and depress stirring 5-10 minute at 1 to-1.3 standard atmosphere, be cooled to 35 ℃ again and obtain semi-finished product with bottom discharge, semi-finished product namely obtain described silybum marianum essential oil skin-care cream through after the assay was approved.
The time of preferably, stirring in the step (3) is 5-10 minute.
The Herba Silybi mariani quintessence oil is to obtain the Herba Silybi mariani crude oil through the twice pressing cold-press from Compositae Silybum plant seed among the present invention, and the Herba Silybi mariani crude oil obtains the Herba Silybi mariani quintessence oil by refine again.
Wherein, the Herba Silybi mariani quintessence oil contains up to the linoleic plus oleic acid more than 80%, and linoleic acid is that human body can not synthesize.The research discovery, cholesterol must after linoleic acid is combined, could turn round and metabolism in vivo normally.If the shortage linoleic acid, cholesterol will be combined with some satisfied fatty acid, and dysbolismus occurs, and under the blood vessel wall deposition, progressively forms atherosclerosis, causes cardiovascular and cerebrovascular disease.Linoleic acid is unique essential fatty acid of generally acknowledging.Extremely paying attention to because linoleic acid can reduce blood cholesterol levels, and prevention of arterial is atherosis, can play the softening skin blood capillary, promote skin metabolism, is the desirable material of beauty and skin care.
Contained unsaturated fatty acids such as linoleic plus oleic acid in the Herba Silybi mariani quintessence oil are drying oil preferably, iodine value higher (93.12 ~ 127.5%), and it has good moisture retention and durability, and is long-acting obviously to the moisturizing effect of skin.
Also contain silymarin in the Herba Silybi mariani quintessence oil, the phenolic hydroxyl group of silymarin provides hydrogen atom and powerful antioxidation is arranged.They have the removing Characteristics of Free Radicals Produced, inhibition of lipid peroxidation, and direct Scavenger of ROS, to anti peroxidation of lipid, the flowability of keeping cell membrane has obvious effect to removal skin keratin, wrinkle removing stricture of vagina, defying age.
Also contain abundant aminoacid, vitamin and the abundant trace element such as Fe, Se in the Herba Silybi mariani quintessence oil, obvious to skin nourishing effect.
Beneficial effect: compared with prior art, advantage of the present invention is: owing to having adopted the Herba Silybi mariani quintessence oil, contain unsaturated fatty acid more than 80% and an amount of aminoacid, trace element and vitamin in the Herba Silybi mariani quintessence oil, can improve the circulation of subcutaneous capillary, promote the metabolism of human skin cell's tissue, have powerful oxidation resistance and enhancing immunity effect; Carbamide has the effect of removing the epiderm skin horny layer and keeping skin moisturizing.Thereby goods had enhance metabolism, preserving moisture and protecting skin, antifreezely more split; Can effectively prevent chapping, preventing chilblain, anti peroxidation of lipid, radioprotective, removing free radical, antidotal health care.Be particularly suitable for xerosis cutis, coarse, the people of skin brothers decortication uses, and can make the long-term maintenance of skin soft and moist careful, and be free from side effects.Adopt this preparation method can be the fully synthetic skin ﹠ complexion improving cream of making of Herba Silybi mariani quintessence oil and other skin protection raw materials, thereby improve the utilization rate of Herba Silybi mariani quintessence oil.
The specific embodiment
The present invention is further described below by specific embodiment and accompanying drawing; should be pointed out that for the person of ordinary skill of the art, under the prerequisite that does not break away from the principle of the invention; can also make some modification and improvement, these also should be considered as belonging to protection scope of the present invention.
Embodiment 1: according to the mass fraction, accurately taking by weighing 10 parts of Herba Silybi mariani quintessence oils, 3 parts of monoglycerides, 8 parts of stearic acid, 7 parts of white vaseline, 10 parts of white oils joins in the oil phase stirred tank, be heated to 70-80 ℃, and depress at 70-80 ℃, 1 to-1.3 standard atmosphere and to stir fusing in 5-15 minute and obtain oil phase material; Accurately take by weighing 9 parts of glycerol, 15 parts of carbamide, 80 parts of deionized waters and join in the water stirred tank, be warmed to 70-80 ℃ and depress at 1 to-1.3 standard atmosphere and to stir dissolving in 5-10 minute; Under the insulated and stirred oil phase material and water material are joined in the emulsifying kettle, depress 70-80 ℃ of insulated and stirred 10-20 minute one-tenth uniformly emulsify shape at 1 to-1.3 standard atmosphere, allocate the spice of 0.1 mass parts when then being cooled to 45 ℃ into and depress stirring 5-10 minute at 1 to-1.3 standard atmosphere, be cooled to again 35 ℃ with bottom discharge, store to storage tank, carry out the qualified rear packing of the inspection of semifinished product and namely form the silybum marianum essential oil skin-care cream finished product.
The Herba Silybi mariani quintessence oil is to obtain the Herba Silybi mariani crude oil through the twice pressing cold-press from Compositae Silybum plant seed among the present invention, and the Herba Silybi mariani crude oil obtains the Herba Silybi mariani quintessence oil by refine again.
Wherein, the Herba Silybi mariani quintessence oil contains up to the unsaturated fatty acids such as linoleic plus oleic acid more than 80%, also contains silymarin, and abundant aminoacid, vitamin and the abundant trace element such as Fe, Se.
This silybum marianum essential oil skin-care cream is tested according to following standard: the guide rule of GB/T1.1-2000 cosmetic standard; The basic regulations of GB/T 11-1993 Standard compilation; GB 5296.3 " Instructions for use of products of consumer interest cosmetics universal tag "; GB 5296.3 Instructions for use of products of consumer interest cosmetics universal tags; The mensuration of GB/T 13531.1 cosmetics universal test method pH value; QB/T 1684 cosmetics inspection rules; QB/T 1685 cosmetic product packaging external appearance requirements; QB/T 2286-1997 moisturizer; JJF 1070-2000 Metrolgy Inspection of Products in Prepackages rule; State Bureau of Technical Supervision makes quantification packing commodity metrological supervision regulation [1995] No. 43; Defend the method prison and send out [2002] No. 229 cosmetics health standards; Regulation among the GB/T 13531.1; 5.7 regulations among the QB/T 2286-1997; 6.1.1 regulation among the JJF 1070-2000; GB 5296.3; QB/T 1685.
Embodiment 2: according to the mass fraction, accurately take by weighing 5 parts of Herba Silybi mariani quintessence oils, 2 parts of monoglycerides, 6 parts of stearic acid, 4 parts of white vaseline, 6 parts of white oils and join in the oil phase stirred tank, be heated to 70-80 ℃ and depress at 1 to-1.3 standard atmosphere and to stir fusing in 5-15 minute; Accurately take by weighing 5 parts of glycerol, 10 parts of carbamide, 70 parts of deionized waters and join in the water stirred tank, be warmed to 70-80 ℃ and depress at 1 to-1.3 standard atmosphere and to stir dissolving in 5-10 minute; Under the insulated and stirred oil phase material and water material are joined in the emulsifying kettle, depress 70-80 ℃ of insulated and stirred 10-20 minute one-tenth uniformly emulsify shape at 1 to-1.3 standard atmosphere, allocate 0.2 part spice when then being cooled to 45 ℃ into and depress stirring 5-10 minute at 1 to-1.3 standard atmosphere, be cooled to again 35 ℃ with bottom discharge, store to storage tank, carry out the qualified rear packing of the inspection of semifinished product and namely form the silybum marianum essential oil skin-care cream finished product.
Embodiment 3: according to the mass fraction, accurately take by weighing 15 parts of Herba Silybi mariani quintessence oils, 4 parts of monoglycerides, 13 parts of stearic acid, 9 parts of white vaseline, 13 parts of white oils and join in the oil phase stirred tank, be heated to 70-80 ℃ and depress at 1 to-1.3 standard atmosphere and to stir fusing in 5-15 minute; Accurately take by weighing 15 parts of glycerol, 18 parts of carbamide, 90 parts of deionized waters and join in the water stirred tank, be warmed to 70-80 ℃ and depress at 1 to-1.3 standard atmosphere and to stir dissolving in 5-10 minute; Under the insulated and stirred oil phase material and water material are joined in the emulsifying kettle, depress 70-80 ℃ of insulated and stirred 10-20 minute one-tenth uniformly emulsify shape at 1 to-1.3 standard atmosphere, allocate 0.3 part spice when then being cooled to 45 ℃ into and depress stirring 5-10 minute at 1 to-1.3 standard atmosphere, be cooled to again 35 ℃ with bottom discharge, store to storage tank, carry out the qualified rear packing of the inspection of semifinished product and namely form the silybum marianum essential oil skin-care cream finished product.
Claims (4)
1. silybum marianum essential oil skin-care cream, it is characterized in that comprising following component, the prescription of each component is as follows: 5-15 part Herba Silybi mariani quintessence oil, 2-4 part monoglyceride, 6-13 part stearic acid, 4-9 part white vaseline, 6-13 part liquid paraffin, 5-15 part glycerol, 10-18 part carbamide, 70-90 part deionized water, 0.1-0.3 the spice of mass fraction more than is mass fraction.
2. a kind of silybum marianum essential oil skin-care cream according to claim 1, it is characterized in that, according to the mass fraction, 10 parts of Herba Silybi mariani quintessence oils, 3 parts of monoglycerides, 8 parts of stearic acid, 7 parts of white vaseline, 10 parts of liquid paraffin, 9 parts of glycerol, 15 parts of carbamide, 80 parts of deionized waters, 0.1 part of spice.
3. the preparation method of a silybum marianum essential oil skin-care cream claimed in claim 1 is characterized in that the method comprises the steps:
(1) accurately take by weighing each component according to prescription, for subsequent use;
(2) Herba Silybi mariani quintessence oil, monoglyceride, stearic acid, white vaseline, liquid paraffin are joined in the oil phase stirred tank, are heated to 70-80 ℃, 1 to-1.3 standard atmosphere depress and 70-80 ℃ of insulated and stirred to the fusing, namely obtain oil phase material;
(3) deionized water, glycerol, carbamide are joined in the water stirred tank, be warmed to 70-80 ℃, depress and in the dissolving of 70-80 ℃ of insulated and stirred, obtain the water material at 1 to-1.3 standard atmosphere;
(4) under the insulated and stirred oil phase material and water material are joined in the emulsifying kettle, depress and became the uniformly emulsify shape at 70-80 ℃ of insulated and stirred 10-20 minute at 1 to-1.3 standard atmosphere;
Allocate the spice of 0.1-0.3 mass fraction when (5) then being cooled to 45 ℃ into and depress stirring 5-10 minute at 1 to-1.3 standard atmosphere, be cooled to 35 ℃ again and obtain semi-finished product with bottom discharge, semi-finished product namely obtain described silybum marianum essential oil skin-care cream through check and packing after reaching the national cosmetic relevant criterion.
4. the preparation method of silybum marianum essential oil skin-care cream according to claim 3 is characterized in that, the time of stirring in the step (3) is 5-10 minute.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011100979333A CN102178629B (en) | 2011-04-19 | 2011-04-19 | Silybum marianum essential oil skin-care cream and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN2011100979333A CN102178629B (en) | 2011-04-19 | 2011-04-19 | Silybum marianum essential oil skin-care cream and preparation method thereof |
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| CN102178629A CN102178629A (en) | 2011-09-14 |
| CN102178629B true CN102178629B (en) | 2013-03-06 |
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| CN108158912B (en) * | 2018-03-21 | 2020-08-28 | 胡莹姝 | Silybum marianum gel for removing acne and repairing scars and preparation method thereof |
| CN108721173A (en) * | 2018-08-17 | 2018-11-02 | 四川自然菲科技有限公司 | A kind of anti-aging type eye cream quickly absorbed |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3869442D1 (en) * | 1987-01-19 | 1992-04-30 | Rochas Parfums | COSMETIC OR DERMATOLOGICAL PREPARATIONS CONTAINING AN EXTRACT OF THE FRUIT OF THE SILYBUM MARIANUM WITH A HIGH SYLIMARINE CONTENT WITH ESSENTIAL FATTY ACIDS. |
| JP4063443B2 (en) * | 1999-04-07 | 2008-03-19 | 花王株式会社 | Whitening cosmetics |
| FR2809008B1 (en) * | 2000-05-19 | 2006-07-28 | Sarl I De Zica | COSMETIC COMPOSITION COMPRISING CERAMIDES ASSOCIATED WITH SILYMARIN |
| CZ294004B6 (en) * | 2001-03-12 | 2004-09-15 | Irel Spol. S R.O. | Therapeutic and cosmetic compositions for topic application |
| TWI256893B (en) * | 2003-03-25 | 2006-06-21 | Fancl Corp | Composition for promoting production of type I collagen and/or elastin |
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Application publication date: 20110914 Assignee: ZHENJIANG YIXIN BIOENGINEERING TECHNOLOGY CO.,LTD. Assignor: Dou Jianguo Contract record no.: 2014320000458 Denomination of invention: Silybum marianum essential oil skin-care cream and preparation method thereof Granted publication date: 20130306 License type: Exclusive License Record date: 20140528 |
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