CN104306259A - Pure natural skin oil containing no preservative and synthesized essence and preparation method of pure natural skin oil - Google Patents
Pure natural skin oil containing no preservative and synthesized essence and preparation method of pure natural skin oil Download PDFInfo
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Abstract
The invention discloses pure natural skin oil containing no preservative and synthesized essence and a preparation method of the pure natural skin oil. The skin oil mainly adopts plant flowers, high-quality tea seed oil and natural vitamin E as raw materials and contains no preservative and synthesized essence, the preparation process has no chemical residue, the active ingredients in the raw materials are not damaged, and the product has pure natural characteristics and is stable and lasting in performance. The method is simple in process, free from chemical residue and convenient to popularize to use.
Description
Technical field
The invention belongs to skin care field, relate to a kind of not containing pure natural skin care oil and preparation method thereof of antiseptic and compound essence.
Technical background
Oils and fats, as the part in fashionable life, is rooted in the hearts of the people, and be widely used in fields such as skin protection, beauty treatment, health cares, particularly high-end beauty and skin care market, the requirement for raw material is also more and more higher.
Oleum Camelliae is as being one of the most ancient woody edible vegetable oil of China.Its fatty acid forms the olive oil of the king in similar oil, has very high nutritive value.Its main fatty acid is monounsaturated fatty acid oleic acid, and content is generally more than 80%.Be very beneficial for skin to absorb, it can protect skin-nourishing to have experiment to show, improves skin texture, is a kind of ideal cosmetic base oil.But Oleum Camelliae has the distinctive strong abnormal smells from the patient of a kind of Oleum Camelliae, in the process making skin care oil, abnormal smells from the patient is difficult to remove, and affects the sense organ of skin care oil, limits it and apply.
Existing most cosmetic skin care oil is mainly with base oil, quintessence oil, other chemical constituents composition.As patent 02112769.7 introduction method, simply mix.Find that this stabilized with mixture is poor through practice.The quintessence oil fragrance retention time is short.In addition, quintessence oil is expensive, and on market, counterfeit and shoddy goods are more, and normal containing compound essence in quintessence oil, there is chemical residual, make the quality of skin care oil can not get good guarantee in the preparation process of quintessence oil.
Summary of the invention
For the problems referred to above, the invention provides a kind of pure natural skin care oil not containing antiseptic and compound essence.This skin care oil is mainly to have the plant flowers and plants of beauty functions, high-quality Oleum Camelliae and natural Vitamin E for raw material, not containing antiseptic and compound essence, preparation process, without chemical residual, does not destroy the effective ingredient in raw material, product has pure natural characteristic, and stable performance, lasting.
The present invention is achieved through the following technical solutions:
Containing a pure natural skin care oil for antiseptic and compound essence, it is characterized in that, containing Oleum Camelliae, there is fragrance and there is oil-soluble extract and the natural Vitamin E of the natural plants tissue of beauty functions.Oleum Camelliae nutrition is enriched, and monounsaturated fatty acid content is high, phospholipid sweet containing Flos Camelliae Japonicae and soap is sweet, vitamin E, tannin etc., is very beneficial for skin and absorbs, can protect skin-nourishing, improve skin texture.The present invention utilizes its good oxidation resistance, and by coordinating with natural Vitamin E, under the prerequisite of not adding preservative agent, also can ensure that product has lasting stability.In addition, by adopting the oil-soluble extract of natural plants tissue, the mode adopting base oil to mix with quintessence oil is avoided, preparation process is without chemical residual, do not destroy the effective ingredient in raw material, product has pure natural characteristic, and effectively can cover the distinctive abnormal smells from the patient of Oleum Camelliae.
As optional, adopt that to have the natural plants tissue of beauty functions and Oleum Camelliae and natural Vitamin E be raw material, effective ingredient in direct Oleum Camelliae lixiviate natural plants tissue obtains skin care oil product, preparation process is without chemical residual, not containing artificial additive, there is better pure natural.
As optional, in above-mentioned pure natural skin care oil, described in there is fragrance and the natural plants with beauty functions is organized as at least one in Flos Rosae Rugosae, lavender flower, lavandula angustifolia, Calendula officinalis, Flos Jasmini Sambac.
As optional, in above-mentioned pure natural skin care oil, described component proportioning is by mass Oleum Camelliae: 1000 parts, oil-soluble extract 0.5-5 part of natural plants tissue, natural Vitamin E: 0.5 ~ 1.5 part.
As optional, in above-mentioned pure natural skin care oil, described Oleum Camelliae is high-quality Oleum Camelliae, and its acid value is less than 0.5, colourless free from extraneous odour.
Present invention also offers a kind of preparation method of above-mentioned pure natural skin care oil, comprise the following steps:
(1) Oleum Camelliae is added in reactor, add natural Vitamin E, under inert protective atmosphere, be heated with stirring to 40 ~ 75 DEG C;
(2) add and have fragrance and the natural plants with beauty functions organizes powder, under inert protective atmosphere, holding temperature stirs 2 ~ 10 hours;
(3) treat savory spilling, leave standstill cooling, then carry out solid-liquid separation, namely gained liquid phase part obtains skin care oil product.The effective ingredient that in product, lixiviate obtains from corresponding natural plants tissue accounts for the 0.5-5% of natural plants tissue powder powder stock quality.
As optional, in above-mentioned preparation method, above-mentioned inert protective atmosphere is nitrogen protection or helium protection.
As optional, in above-mentioned preparation method, each raw material is Oleum Camelliae by the proportioning of mass parts: 1000 parts, natural plants organizes powder: 20 ~ 100 parts, natural Vitamin E: 0.5 ~ 1.5 part.
As optional, in above-mentioned preparation method, described natural plants organizes powder to prepare in accordance with the following methods: select to have fragrance and the plant with certain beauty functions, carry out dedusting, roguing (only leaving the plant tissue with effect and fragrance), crushed after being dried.
As optional, in above-mentioned preparation method, described Oleum Camelliae is prepared in accordance with the following methods: selected pollution-free Semen Camelliae, shells, and hydraulic pressure squeezes, through the process of physical deacidification, decolouring, deodorization procedures.Employing is shelled cold pressing mode, does not need heating operation simple, and can not destroy natural constituent.Carry out deacidification by membrane filtration, activated carbon adsorption, decolouring, the obtainable acid value of deodorization procedures be less than 0.5, the high-quality Oleum Camelliae of colourless free from extraneous odour, and there is not chemical residual in whole preparation process, ensure that the pure natural characteristic of Oleum Camelliae.
As optional, in above-mentioned preparation method, described solid-liquid separation operation is specially first filters, and then carries out centrifugalize to the solid constituent of filtering, then the liquid phase that the centrifugal liquid phase obtained and filtration obtain is merged, obtain skin care oil product.
As optional, in above-mentioned preparation method, skin care oil obtained in step (3) sealing is preserved, then according to product demand, different batches product is mixed.The indexs such as the purposes of product and fragrance, acid value, peroxide value can be considered during mixing seasoning.As preferably, can control the acid value of product below 3.0, peroxide value is below 10.
Preparation method of the present invention can comprise select materials, pulverize, heat, soak, filter, centrifugalize, the operation such as seasoning (this step is optional), preparation technology is simple, can obtain pure natural and have the skin care oil product of lasting stability.According to the difference according to raw material, can obtain have whitening, antibacterial, repair wounded tissue, softening skin, the skin care oil that increases elasticity of skin, prevent the effects such as xerosis cutis.
All features disclosed in this description, or the step in disclosed all methods or process, except mutually exclusive feature and/or step, all can combine by any way.
Beneficial effect of the present invention:
The present invention utilizes its good oxidation resistance, and by coordinating with natural Vitamin E, under the prerequisite of not adding preservative agent, also can ensure that product has lasting stability.In addition, by adopting the oil-soluble extract of natural plants tissue, the mode adopting base oil to mix with quintessence oil is avoided, preparation process is without chemical residual, do not destroy the effective ingredient in raw material, product has pure natural characteristic, and effectively can cover the distinctive abnormal smells from the patient of Oleum Camelliae.
Preparation method of the present invention can comprise select materials, pulverize, heat, soak, filter, centrifugalize, the operation such as seasoning (this step is optional), preparation technology is simple, can obtain pure natural and have the skin care oil product of lasting stability.According to the difference according to raw material, can obtain have whitening, antibacterial, repair wounded tissue, softening skin, the skin care oil that increases elasticity of skin, prevent the effects such as xerosis cutis.
detailed description of the invention:
Detailed description of the invention is by the following examples described in further detail foregoing of the present invention again.But this should be interpreted as that the scope of the above-mentioned theme of the present invention is only limitted to following example.Not departing from any amendment made within the spirit and principles in the present invention, and the equivalent replacement made according to ordinary skill knowledge and customary means or improvement, all should be included in protection scope of the present invention.Raw materials usedly in following examples all can to buy from the market.Wherein said Oleum Camelliae can adopt commercially available high-quality Oleum Camelliae, also can adopt the Oleum Camelliae prepared by the following method.
high-quality Oleum Camelliae preparation example
Selected pollution-free Semen Camelliae, shells, and pulverizes, and hydraulic pressure squeezes, and obtains lighter color, first squeezing Oleum Camelliae that acid value is low, then through the process of physical deacidification, decolouring, deodorization procedures.As optional, described physical deacidification, decolouring, deodorization procedures are specially first carries out membrane filtration to Oleum Camelliae and is then carrying out activated carbon adsorption.The preferred fenestra aperture of described membrane filtration is less than or equal to the hollow-fibre membrane of 10 microns, as polysulfones or polyether sulfone hollow fiber ultrafiltration film.The preferred specific surface area of described active carbon is more than or equal to 800m
2the active carbon of/g.Adopt the method can obtain the high-quality Oleum Camelliae that acid value is 0.2 colorless and odorless.The high-quality Oleum Camelliae that acid value is respectively a series of colorless and odorless of 0.5,0.4,0.3 has successfully been obtained by the adjustment aperture of filter membrane and the specific surface area of activated carbon.
embodiment 1rose Essentielle skin care oil
Selected Flos Rosae Rugosae, the base of a fruit will be spent to remove, and crushed after being dried is for subsequent use, the Oleum Camelliae 10kg being 0.2 colorless and odorless according to the homemade featured acid value of the method for the invention is joined in reactor, adds 0.008kg natural Vitamin E, pass into nitrogen, start stirring, chuck heats, and when temperature reaches 50 DEG C, adds 1.0kg Flos Rosae Rugosas pollen, continue to stir, temperature controls at 55 ± 5 DEG C, and maintain 4 hours, isolated by filtration waits until product.This product gives off a strong fragrance, the micro-Huang of color and luster, and be applied on skin and absorb soon, fragrance remaining time is long.Acid value is below 3.0, and peroxide value is below 10, and product stability is good, and the shelf-life reaches 30 months.
Flos Rosae Rugosae liposoluble constituent mainly has the volatile oil compositions of aromatic odor, and these components have regulating QI to relieve pain, and blood circulation promoting and blood stasis dispelling improves Peripheral Microcirculation effect, has Flavonoid substances in addition in addition, can scavenging free radicals, remove pigementation effect.In skin care oil of the present invention, under the osmosis of Oleum Camelliae, can well skin be improved, realize the effect of crease-resistant, moisturizing, skin whitening.In order to verify effect of product, have chosen 10 volunteers and smear product described in the present embodiment (as experimental group) at the left hand of every volunteer back of the body respectively every day, the skin care oil (as a control group) adopting base oil and Rose Essentielle quintessence oil to be mixed with is smeared in prior art at right hand the back of the hand, smear two weeks continuously, result display experimental group and the skin of matched group all make moderate progress before not smearing, and crease-resistant, the moisturizing of experimental group, whitening effect are significantly better than matched group.
embodiment 2
Selected Flos Rosae Rugosae, the base of a fruit will be spent to remove, and crushed after being dried is for subsequent use, be that the Oleum Camelliae 10kg of 0.5 colorless and odorless joins in reactor by featured acid value, add 0.005kg natural Vitamin E, pass into nitrogen, start stirring, chuck heats, and when temperature reaches 70 DEG C, adds 0.3kg Flos Rosae Rugosas pollen, continue to stir, temperature controls at 70 ± 5 DEG C, and maintain 2 hours, isolated by filtration waits until product.This product gives off a strong fragrance, the micro-Huang of color and luster, and be applied on skin and absorb soon, fragrance remaining time is long.Described in properties of product and embodiment 1, product is suitable.
embodiment 3the fragrant skin care oil of lavandula angustifolia
Selected lavandula angustifolia, remove dust and foreign material, crushed after being dried is for subsequent use, be that the Oleum Camelliae 10kg of 0.2 colorless and odorless joins in reactor by featured acid value, add 0.01kg natural Vitamin E, pass into nitrogen, start stirring, chuck heats, and when temperature reaches 45 DEG C, adds 0.5kg lavender powder, continue to stir, temperature controls at 45 ± 5 DEG C, and maintain 6 hours, isolated by filtration waits until product.It is fragrant that this product has stronger lavandula angustifolia, the micro-Huang of color and luster, and be applied on skin and absorb soon, fragrance remaining time is long.And product stability is good, the shelf-life reaches 30 months.
Lavandula angustifolia has fragrant medicinal herbs " good reputation; containing a large amount of Lignum cinnamomi camphorae esters and Lignum cinnamomi camphorae alcohols fragrance volatile oil component in its alabastrum; these compositions have promotion cell regeneration; the effects such as antibacterial, analgesia; in addition also containing can the component such as liposoluble luteolin, this compound be also the effect with anti-inflammation.The contrast experiment similar with embodiment confirms, the lavender flavor type skin care oil described in the present embodiment has certain promotion cell regeneration and antibacterial effect, and combination property is better than adopting base oil and the oily skin care oil be mixed with of lavandula angustifolia essence in prior art.
embodiment 4the fragrant skin care oil of Calendula officinalis
Selected Calendula officinalis, remove the flower base of a fruit and dust, crushed after being dried is for subsequent use, be that the Oleum Camelliae 10kg of 0.2 colorless and odorless joins in reactor by featured acid value, add 0.012kg natural Vitamin E, pass into nitrogen, start stirring, chuck heats, and when temperature reaches 60 DEG C, adds 0.8kg Calendula officinalis powder, continue to stir, temperature controls at 60 ± 5 DEG C, and maintain 10 hours, isolated by filtration waits until product.This product fragrance is simple and elegant, and color and luster is slightly yellow, and be applied on skin and absorb soon, fragrance remaining time is long.And product stability is good, the shelf-life reaches 30 months.
Its armaticity volatile matter limonene class of Calendula officinalis has anticancer, and triterpenoid compound has the effect of antiinflammatory and accelerating wound healing.The contrast experiment similar with embodiment confirms, the Calendula officinalis odor type skin care oil described in the present embodiment has certain antiinflammatory and effect of accelerating wound healing, and combination property is better than the skin care oil that adopts base oil and Calendula officinalis essential oil to be mixed with in prior art.
embodiment 5jasmin skin care oil
Selected Flos Jasmini Sambac, remove dust and foreign material, crushed after being dried is for subsequent use, be that the Oleum Camelliae 10kg of 0.2 colorless and odorless joins in reactor by featured acid value, add 0.015kg natural Vitamin E, pass into nitrogen, start stirring, chuck heats, and when temperature reaches 50 DEG C, adds 0.7kg jasmine pollen, continue to stir, temperature controls at 50 ± 5 DEG C, and maintain 10 hours, isolated by filtration waits until product.This product gives off a strong fragrance, and color and luster is yellowish, and be applied on skin and absorb soon, fragrance remaining time is long.And product stability is good, the shelf-life reaches 30 months.
Its pleasant aroma of Flos Jasmini Sambac, key component is the component such as benzyl alcohol and esters, jasmone, linalool, benzoic acid Lignum cinnamomi camphorae alcohol ester, has stable emotion, eliminates nervous, effect recovered from fatigue of refreshing oneself.Flos Jasmini Sambac polysaccharide component has infection, separates the effects such as sore in addition.The contrast experiment similar with embodiment confirms, jasmine fragrance skin care oil described in the present embodiment has certain stable emotion, it is nervous to eliminate, refresh oneself recover from fatigue and infection, solution sore effect, and combination property is better than the skin care oil that adopts base oil and jasmin quintessence oil to be mixed with in prior art.
embodiment 6 hybrid modulation
According to product demand, the product chosen in embodiment 1-5 mixes, and obtains a series of skin care oil products with mixing odor type and several functions.The indexs such as the purposes of product and fragrance, acid value, peroxide value can be considered during mixing seasoning.
The foregoing is only the preferred embodiments of the present invention, is only illustrative for the purpose of the present invention, and nonrestrictive; Those of ordinary skill in the art understand, and can carry out many changes in the spirit and scope that the claims in the present invention limit to it, amendment, and even equivalence is changed, but all will fall into protection scope of the present invention.
Claims (10)
1. not containing a pure natural skin care oil for antiseptic and compound essence, it is characterized in that, containing Oleum Camelliae, there is fragrance and there is oil-soluble extract and the natural Vitamin E of the natural plants tissue of beauty functions.
2. according to claim 1ly to it is characterized in that not containing the pure natural skin care oil of antiseptic, described in there is fragrance and the natural plants with beauty functions is organized as at least one in Flos Rosae Rugosae, lavender flower, lavandula angustifolia, Calendula officinalis, Flos Jasmini Sambac.
3. according to claim 1 not containing the pure natural skin care oil of antiseptic, it is characterized in that, described component proportioning is by mass Oleum Camelliae: 1000 parts, oil-soluble extract 0.5-5 part of natural plants tissue, natural Vitamin E: 0.5 ~ 1.5 part.
4. according to claim 1 not containing the pure natural skin care oil of antiseptic, it is characterized in that, described Oleum Camelliae acid value is less than 0.5, colourless free from extraneous odour.
5. a preparation method for pure natural skin care oil as claimed in claim 1, is characterized in that, comprise the following steps:
(1) Oleum Camelliae is added in reactor, add natural Vitamin E, under inert protective atmosphere, be heated with stirring to 40 ~ 75 DEG C;
(2) add and have fragrance and the natural plants with beauty functions organizes powder, under inert protective atmosphere, holding temperature stirs 2 ~ 10 hours;
(3) treat savory spilling, leave standstill cooling, then carry out solid-liquid separation, namely gained liquid phase part obtains skin care oil product.
6. preparation method according to claim 5, is characterized in that, each raw material is Oleum Camelliae by the proportioning of mass parts: 1000 parts, natural plants organizes powder: 20 ~ 100 parts, natural Vitamin E: 0.5 ~ 1.5 part.
7. preparation method according to claim 5, is characterized in that, described natural plants organizes powder to prepare in accordance with the following methods: select to have fragrance and the plant with certain beauty functions, carry out dedusting, roguing, crushed after being dried.
8. preparation method according to claim 5, is characterized in that, described Oleum Camelliae is prepared in accordance with the following methods: selected pollution-free Semen Camelliae, shells, and hydraulic pressure squeezes, through the process of physical deacidification, decolouring, deodorization procedures.
9. preparation method according to claim 5, it is characterized in that, described solid-liquid separation operation is specially first filters, and then carries out centrifugalize to the solid constituent of filtering, again the liquid phase that the centrifugal liquid phase obtained and filtration obtain is merged, obtain skin care oil product.
10. preparation method according to claim 5, is characterized in that, skin care oil obtained in step (3) sealing is preserved, then according to product demand, is mixed by different batches product.
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| CN107802524A (en) * | 2017-12-08 | 2018-03-16 | 广州若羽臣科技股份有限公司 | A kind of skin care oil |
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| CN104306259B (en) | 2017-08-25 |
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