CN113057901B - Oil tea seed oil skin care composition containing hydrolyzed vegetable protein and preparation method and application thereof - Google Patents

Oil tea seed oil skin care composition containing hydrolyzed vegetable protein and preparation method and application thereof Download PDF

Info

Publication number
CN113057901B
CN113057901B CN202110194988.XA CN202110194988A CN113057901B CN 113057901 B CN113057901 B CN 113057901B CN 202110194988 A CN202110194988 A CN 202110194988A CN 113057901 B CN113057901 B CN 113057901B
Authority
CN
China
Prior art keywords
seed oil
skin care
camellia seed
care composition
skin
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN202110194988.XA
Other languages
Chinese (zh)
Other versions
CN113057901A (en
Inventor
李永泉
张晖
王溢
代文魁
涂攀峰
薛彬娥
廖柏勇
李彩琴
张宪智
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Zhongkai University of Agriculture and Engineering
Original Assignee
Zhongkai University of Agriculture and Engineering
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Zhongkai University of Agriculture and Engineering filed Critical Zhongkai University of Agriculture and Engineering
Priority to CN202110194988.XA priority Critical patent/CN113057901B/en
Publication of CN113057901A publication Critical patent/CN113057901A/en
Application granted granted Critical
Publication of CN113057901B publication Critical patent/CN113057901B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
    • A61K8/645—Proteins of vegetable origin; Derivatives or degradation products thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783—Angiosperms [Magnoliophyta]
    • A61K8/9789—Magnoliopsida [dicotyledons]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/001—Refining fats or fatty oils by a combination of two or more of the means hereafter
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/10—General cosmetic use
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/52—Stabilizers
    • A61K2800/522—Antioxidants; Radical scavengers

Abstract

The invention discloses a camellia seed oil skin care composition containing hydrolyzed vegetable protein, a preparation method and application thereof, and belongs to the technical field of skin care products. According to the camellia seed oil skin care composition, the refined camellia seed oil with proper content is used for replacing the camellia seed oil prepared in the prior art to serve as an effective component, so that the peculiar smell is greatly reduced, and the skin compatibility is good; the camellia seed oil is rich in sterols, tocopherols, squalene and other antioxidant nutrients, so that symptoms such as wrinkles, chapping and the like of human skin can be effectively repaired; the whitening phenomenon of natural plant products in the application process can be effectively relieved by adding the hydrolyzed pea protein with specific content into the components of the product and matching with other components, so that the obtained skin care composition has light, non-sticky and lubricating texture. The invention also discloses a preparation method of the product, which has simple operation steps and can realize industrialized mass production. The invention also discloses application of the product in preparing skin care products.

Description

Oil tea seed oil skin care composition containing hydrolyzed vegetable protein and preparation method and application thereof
Technical Field
The invention relates to the technical field of skin care products, in particular to a camellia seed oil skin care composition containing plant protein and a preparation method and application thereof.
Background
The skin is the largest organ in human body organs, and has the functions of protecting, excreting, regulating body temperature, sensing external stimulus and the like. Skin is often irritated by various factors such as oxidation, dryness, ultraviolet rays, etc., and is easily damaged, and when care is not taken, the skin state deteriorates sooner or later, and dryness, lack of water, spots, fine lines, etc. are the most common problems. For example, modern life is busy and is full of dynamic long-term tiredness and running, and the skin is required to keep vigorous energy at any time and any place, sweat and oily thick skin are covered on the skin surface layer, the burden of the surface skin is increased, pores are completely blocked, in order to discharge more grease, the pores are gradually enlarged and obvious, the skin is gradually rough, and the skin is smoother and uneven.
In order to protect the skin from damage and to glow, care must be taken to the skin on a daily basis. To really achieve skin care, the skin needs to be softened, so that the stratum corneum can absorb more water, the permeation and absorption capacities can strengthen the contact of nutrients and epidermal cells at zero distance, and deep absorption is realized, thereby activating the skin, and ensuring that the skin is bright, clean, healthy and full of vigor.
The existing skin care product is added with a plurality of artificially synthesized additives or auxiliaries, and the product has certain specific properties (convenient preservation, unique smell and fashionable appearance), but often neglects the skin care effect of the product, and even part of the product can generate certain negative effects on the skin after long-time use; for these reasons, some natural plant ingredients are beginning to be used instead of these chemically synthesized substances. However, it has been found that, unlike natural plants, the more the types and contents of the natural plant are, the more the natural ingredients are, the more the skin becomes white after use, and the natural ingredients are not added blindly as the synthetic substances.
The camellia seed oil is used as a common plant extract, the fatty acid composition and glyceride configuration contained in the camellia seed oil are beneficial to human health, and the camellia seed oil contains various soluble vitamins, so that if the active substances are applied to skin care products, the prepared product can be more attached to human skin, the characteristics of moisturizing and repairing the skin can be endowed to the product, and the texture of the product is improved. CN107550805a discloses a silk protein hydrolysate, wherein water-soluble tea seed oil is matched with natural extracts such as black tea fungus fermentation liquor, silk protein hydrolysate and the like in the mask liquid product, so that the anti-aging and antioxidant effects of the tea seed oil are fully reserved and exerted; CN105902436a discloses an acne-removing and repairing mask using camellia seed meal extract, and in the technical scheme, a nutrition mask with strong sterilization and anti-inflammation activity is prepared by matching camellia seed oil with camellia seed meal extract.
However, the existing products often ignore the defects of the camellia seed oil. The oil tea seed oil has inherent unpleasant smell, but the existing product is often only used as a common functional agent or an oily matrix, and the content collocation or special treatment of the oil tea seed oil is not considered; the oil tea seed oil prepared by the traditional method is unstable in property and easy to oxidize due to more impurities, so that some sour odor can be further generated after the oil tea seed oil is stored or prepared into a product. Therefore, even if the oil tea seed oil is used for preparing a pure natural skin care product with high skin care effect, the product is difficult to get favour of consumers due to the unpleasant smell; if the odor of the skin care product is removed by subsequent processing of the skin care product or adding a deodorizing auxiliary agent, the production cost of the product is increased, and the economic benefit is lowered.
Disclosure of Invention
Based on the defects of the prior art, the invention aims to provide the camellia seed oil skin care composition containing the plant protein, which is rich in natural plant components and has no special heavy smell of the traditional camellia seed oil product, and has excellent skin moisturizing, repairing and whitening effects, and the whitening phenomenon can not occur after the composition is used.
In order to achieve the above purpose, the invention adopts the following technical scheme:
a camellia seed oil skin care composition containing hydrolyzed vegetable protein comprises the following components: plant extract, humectant and water; the plant extract comprises 0.3-0.7% of hydrolyzed pea protein and 0.3-0.7% of refined oil tea (CAMELLIA OLEIFERA) seed oil by weight of the oil tea seed oil skin care composition.
In the components of the camellia seed oil skin care composition containing the vegetable proteins, the refined camellia seed oil with proper content is used for replacing the camellia seed oil prepared conventionally as an effective component, so that the odor is greatly reduced, and the skin compatibility is good; the camellia seed oil is rich in sterols, tocopherols, squalene and other antioxidant nutrients, so that symptoms such as wrinkles, chapping and the like of human skin can be effectively repaired; the whitening phenomenon of natural plant products in the application process can be effectively relieved by adding the hydrolyzed pea protein with specific content into the components of the product and matching with other components, so that the obtained skin care composition has light, non-sticky and lubricating texture.
Preferably, the refined oil tea seed oil is obtained through low-temperature refining, wherein the low-temperature refining comprises degumming, deacidification, decolorization, deodorization and dewaxing steps, and the temperature of the deodorization step is not higher than 150 ℃.
More preferably, the acid value of the refined camellia seed oil is less than 0.5mg.KOH/g, the peroxide value is less than 1.5mmol/kg, and the mass percentage of moisture and volatile matters in the refined camellia seed oil is less than 0.15%.
The inventor discovers through multiple tests that the traditional preparation method of the camellia oleosa seed oil is often refined by a high-temperature method, and the product obtained by the method has the advantages of more impurities and strong smell, can cause loss and even inactivation of nutrient components such as sterols, and is extremely unfavorable for the use of the camellia oleosa seed oil in subsequent skin care products. According to the refined camellia seed oil disclosed by the invention, the refined camellia seed oil is refined by a low-temperature multi-step method, and simultaneously, the physicochemical indexes of the prepared camellia seed oil and the content of odor and instability sources (free fatty acid and the like) are strictly limited, so that the heavy odor can be eliminated, and the oxidation resistance and skin moisturizing capability of the prepared camellia seed oil skin care composition can be further improved.
More preferably, the refined tea-oil camellia seed oil can be organic tea-oil camellia seed oil produced by Guangdong Baohua agricultural technologies and technologies.
The product has high purity, small smell and high stability, and can be effectively used in the camellia oleosa seed oil skin care composition.
Preferably, the plant extract comprises 0.4-0.6% of hydrolyzed pea protein and 0.4-0.6% of refined camellia seed oil by weight of the camellia seed oil skin care composition;
more preferably, the plant extract comprises 0.5% of hydrolyzed pea protein and 0.5% of refined camellia seed oil by mass of the camellia seed oil skin care composition.
The skin care composition in the proportion has more coordinated smell, and simultaneously has better moisturizing and skin care effects and better skin compatibility.
Preferably, the plant extracts further comprise chamomile (CHAMOMILLA RECUTITA) flower extract and kava (PIPER METHYSTICUM) leaf/root/stem extract.
Among the plant extracts, the chamomile flower extract has rich volatile oil, flavonoid compounds, amino acids, chlorogenic acid, trace elements and the like, has remarkable biological activities of antibiosis, antioxidation, relaxation and allergy resistance when being used in cosmetic skin care products, and is suitable for various skin-property people; the kava leaf/root/stem extract is generally used as a skin conditioner because the kava leaf/root/stem extract contains important active ingredients such as kavain, dihydrokavain, methoxy kavain, demethoxy kavain and the like, and has better pharmacological antibacterial, anti-inflammatory and skin conditioning effects compared with other plant extracts. The skin care composition obtained by matching the two components with the hydrolyzed pea protein and the refined camellia seed oil has better skin care effect and higher applicability.
More preferably, the plant extract further comprises a chamomile flower extract accounting for 2-4% of the weight of the camellia seed oil skin care composition and a kava leaf/root/stem extract accounting for 0.4-0.6% of the weight of the camellia seed oil skin care composition.
The oil tea seed oil skin care composition prepared by the additive amount has more remarkable effects of relieving skin and repairing and moisturizing.
Preferably, the humectant comprises arginine, butylene glycol, panthenol, polyethylene glycol-32, polyethylene glycol-8, and 1, 2-hexanediol.
More preferably, the humectant comprises 0.1-0.3% of arginine, 2-4% of butanediol, 1-3% of panthenol, 1-3% of polyethylene glycol-32, 0.5-1.5% of polyethylene glycol-8 and 0.4-0.6% of 1, 2-hexanediol by weight of the camellia seed oil skin care composition.
In the humectant, arginine belongs to basic amino acid, is often used for conditioning dry skin, can have synergistic effect with plant components such as fruit acid, trehalose and the like, and can keep skin moisture and reduce dandruff; the panthenol is mainly used as a humectant and a skin conditioner, can increase the content of hyaluronic acid in skin after being absorbed by skin, promote the metabolism of protein, fat and sugar of human body, protect skin and mucous membrane, and has strong moisturizing effect; polyethylene glycol-8 is not only a humectant, but also a stabilizer in cosmetics, which is helpful for guaranteeing the stability of the product; the skin care composition product obtained by the synergistic combination of the components can fully improve the water content of skin, can be quickly absorbed by the skin after being used, and has mild properties and no irritation to the skin.
Preferably, the components of the camellia seed oil skin care composition containing hydrolyzed vegetable protein further comprise an emulsifier antioxidant and a skin conditioner;
more preferably, the emulsifier comprises PEG-20 methyl glucose sesquistearate, the antioxidant comprises p-hydroxyacetophenone, and the skin conditioning agent comprises dipotassium glycyrrhizinate;
more preferably, the components of the camellia seed oil skin care composition containing the hydrolyzed vegetable protein further comprise 0.2-0.4% of PEG-20 methyl glucose sesquistearate, 0.4-0.6% of p-hydroxyacetophenone and 0.1-0.3% of dipotassium glycyrrhizinate by mass of the camellia seed oil skin care composition.
By adding the proper functional auxiliary agent into the camellia seed oil skin care composition, the physical property of the product is more stable, the functionality of the product is enriched, and certain anti-aging oxidation, repairing and conditioning effects are achieved on the skin of a user.
Preferably, the camellia seed oil skin care composition containing the hydrolyzed vegetable protein comprises the following components in percentage by mass: 0.5% refined camellia seed oil, 0.3% PEG-20 methyl glucose sesquistearate, 0.5% hydrolyzed pea protein, 0.2% arginine, 3% butylene glycol, 0.5% p-hydroxyacetophenone, 2% panthenol, 2% polyethylene glycol-32, 1% polyethylene glycol-8, 3% chamomile extract, 0.5% 1, 2-hexanediol, 0.5% kava leaf/root/stem extract, 0.2% dipotassium glycyrrhizinate, and the balance water.
The camellia seed oil skin care composition obtained by the proportion has excellent skin moisturizing and whitening repairing effects, and the product has no special abnormal odor and no obvious whitening phenomenon after use.
The invention also provides a preparation method of the camellia seed oil skin care composition containing the vegetable protein, which comprises the following steps:
(1) Soaking refined oil tea seed oil, PEG-20 methyl glucose sesquistearate and hydrolyzed pea protein in water completely, heating, maintaining the temperature, stirring uniformly, and cooling to obtain a mixture A;
(2) Adding arginine into the mixture A obtained in the step (1), mixing and stirring until the arginine is dissolved to obtain a mixture B;
(3) Heating and uniformly mixing butylene glycol and p-hydroxyacetophenone, adding the mixture into the mixture B obtained in the step (2), mixing and stirring until the mixture is dissolved, and cooling to obtain a mixture C;
(4) And (3) adding panthenol, polyethylene glycol-32, polyethylene glycol-8, chamomile extract, 1, 2-hexanediol, kava leaf/root/stem extract and dipotassium glycyrrhizinate into the mixture C obtained in the step (3) in sequence, mixing and stirring until the mixture is completely dissolved, and cooling to obtain the camellia seed oil skin care composition containing the plant protein.
The preparation method of the camellia seed oil skin care composition containing the vegetable protein has simple operation steps and can realize industrialized mass production.
Preferably, the heating temperature in the step (1) is 70-80 ℃, and the heat preservation time is 15-25 min;
preferably, the temperature after cooling in step (1) is 60 ℃ or lower, the temperature after cooling in step (3) is 45 ℃ or lower, and the temperature after cooling in step (4) is 35 ℃ or lower.
Under the conditions, the components are fully dissolved and uniformly mixed, and the prepared product has higher stability.
The invention further aims at providing application of the oil tea seed oil skin care composition containing the vegetable protein in preparation of skin care products.
The camellia seed oil skin care composition disclosed by the invention has the advantages of good moisturizing and whitening effects, coordinated odor and strong skin adaptability, can be used in various skin care products, and can not cause whitening phenomenon after various products are used.
Preferably, the skin care product comprises a facial mask.
The invention has the beneficial effects that: the invention provides a camellia seed oil skin care composition containing hydrolyzed vegetable protein, which uses refined camellia seed oil with proper content to replace the camellia seed oil prepared in the prior art as an effective component, so that the odor is greatly reduced, and the skin compatibility is good; the camellia seed oil is rich in sterols, tocopherols, squalene and other antioxidant nutrients, so that symptoms such as wrinkles, chapping and the like of human skin can be effectively repaired; the whitening phenomenon of natural plant products in the application process can be effectively relieved by adding the hydrolyzed pea protein with specific content into the components of the product and matching with other components, so that the obtained skin care composition has light, non-sticky and lubricating texture. The invention also provides a preparation method of the camellia seed oil skin care composition containing the hydrolyzed vegetable protein, which has simple operation steps and can realize industrialized mass production. The invention also provides application of the oil tea seed oil skin care composition containing the hydrolyzed vegetable protein in preparing skin care products.
Detailed Description
The objects, technical solutions and advantages of the present invention will be further described with reference to specific examples, which are intended to be illustrative of the contents of the present invention in detail, not limiting the present invention.
Examples 1 to 5
In the embodiment of the oil tea seed oil skin care composition containing the hydrolyzed plant proteins, the formula of the oil tea seed oil skin care composition containing the hydrolyzed plant proteins in each embodiment is shown in table 1, the refined oil tea seed oil is 25-degree organic oil tea seed oil produced by Guangdong Baohua agriculture technologies Co., ltd, the acid value is 0.13 mg.KOH/g, the peroxide value is 1.1mmol/kg, and the mass percentage of moisture and volatile matters in the refined oil tea seed oil is 0.11%; the refined oil tea seed oil is obtained through low-temperature refining, the low-temperature refining comprises the steps of degumming, deacidification, decolorization, deodorization and dewaxing, and the temperature of the deodorization step is 150 ℃.
The preparation method of the camellia seed oil skin care composition containing the hydrolyzed vegetable protein comprises the following steps:
(1) Soaking refined oleum Camelliae Japonicae, PEG-20 methyl glucose sesquistearate and hydrolyzed pea protein in water completely, heating to 75deg.C, maintaining the temperature for 20min, stirring, and cooling to below 60deg.C to obtain mixture A;
(2) Adding arginine into the mixture A obtained in the step (1), mixing and stirring for 5min until the arginine is dissolved to obtain a mixture B;
(3) Heating butanediol and p-hydroxyacetophenone to 60 ℃ and uniformly mixing, adding the mixture into the mixture B obtained in the step (2), mixing and stirring for 5min until the mixture is dissolved, and cooling the mixture to below 45 ℃ to obtain a mixture C;
(4) And (3) adding panthenol, polyethylene glycol-32, polyethylene glycol-8, chamomile extract, 1, 2-hexanediol, kava leaf/root/stem extract and dipotassium glycyrrhizinate into the mixture C obtained in the step (3) in sequence, mixing and stirring for 10min until the mixture is completely dissolved, cooling to below 35 ℃, checking, filling and packaging to obtain the yellowish transparent liquid camellia seed oil skin care composition containing the plant protein.
The products obtained in examples 1-5 were subjected to component and property analysis, the test results are shown in Table 2, and the test method is QB/T1857-2013 skin cream. The components and physical and chemical tests of the products meet the indexes, and the products are inspected to be qualified, so that the industrial production and sales can be realized.
TABLE 1
TABLE 2
Comparative examples 1 to 4
The oil tea seed oil skin care compositions of comparative examples 1 to 4 differ from example 1 only in terms of the formulation, and the formulation of the oil tea seed oil skin care composition in each comparative example is shown in table 3.
TABLE 3 Table 3
Comparative example 5
The difference between the comparative example and the example 1 is that the camellia seed oil used in the comparative example is the common camellia seed oil which is not subjected to low-temperature refining and is commercially available, the acid value of the camellia seed oil is 0.37mg.KOH/g, the peroxide value is 2.6mmol/kg, and the mass percentage of water and volatile matters in the refined camellia seed oil is 0.18%.
Effect example 1
In order to verify the use efficacy of the camellia seed oil skin care composition, the camellia seed oil skin care compositions obtained in examples 1-5 and comparative examples 1-5 are prepared into masks, and moisturizing effect tests are carried out on each mask product.
The testing method comprises the following steps:
100 volunteers 20-45 years old are selected, and the volunteers are patients without serious system diseases, immunodeficiency or autoimmune diseases, active allergic diseases, and patients without serious allergic history to cosmetics, and patients without hormone drugs and immunosuppressants in the past month, and do not participate in other clinical test subjects. Volunteers were divided into 10 groups of 10 persons each, each group was tested once before the test (i.e., without using the products obtained in the examples and comparative examples of the present invention), after cleansing the face every evening, using the tested mask, and measuring the moisture content of the horny layer and the skin glossiness of the test area at 28 days from the time of using the sample. The test products are skin care products of examples 1-5 and comparative examples 1-6, respectively. The stratum corneum moisture content and Skin gloss were tested using the Skin moisture test probe Cornometer CM825 and the Skin gloss test probe Skin-GlossymeterGL200, respectively.
Analysis of the result data:
a. calculation of moisture and gloss Change amount
And subtracting the blank control value of the tested part before use from the measured value of the tested part after the sample to obtain the average value of the variation of the moisture content of the stratum corneum and the skin glossiness of the tested part before and after the product is used, wherein the calculation formulas are shown in the following formulas (1) and (2).
（1）T=(M x -M o )/10；（2）G=(N x -N o ) 10; wherein: t is skin moisture variation; m is M x A measurement of skin moisture 28 days after use of the product; m is M o Skin moisture control measurements; g is the skin glossiness variation; n (N) x To measure skin gloss 28 days after use of the product; n (N) o Is a skin gloss blank measurement.
The test results are shown in Table 4.
TABLE 4 Table 4
From the test results of table 4, it can be seen that the products obtained in examples 1 to 5 have a significant improvement effect on the moisture content and glossiness of the skin of the user, wherein the improvement degree of the products obtained in examples 1 to 3 is higher than that of the products obtained in examples 4 and 5, and from the test results of the products obtained in comparative examples 1 to 5, it can be seen that the content of the plant extract has a great influence on the moisturizing and whitening effects of the products, especially when the content of the camellia seed oil and the hydrolyzed pea protein is insufficient, the moisture content and glossiness of the skin after the use of the products are significantly reduced, but when the content thereof is gradually increased beyond the preferred range, the moisturizing and whitening effects of the products are not greatly improved, but the production cost is increased.
Effect example 2
In order to detect the use experience of the facial mask prepared by the oil tea seed oil skin care composition containing the hydrolyzed vegetable protein, 10 products of examples 1-5 and comparative examples 1-5 are subjected to user experience test, namely, the volunteers in effect example 1 are subjected to interview investigation, and statistics are carried out on whether whitening phenomenon, smell evaluation and skin comfort evaluation occur after the use of the volunteers. Wherein the odor evaluation total score is 5 points, and the 5 scoring criteria are: the smell is coordinated and natural, and pleasant aroma is obtained; the 4 scoring criteria were: the smell is coordinated, and a certain fragrance exists; the 3 scoring criteria are: the smell is general, has a certain special smell, but is generally coordinated and not objectionable; 2 scoring criteria: has certain unpleasant smell, weaker coordination and general adaptation after habit; score 1 criteria: the dissonance and peculiar smell are obvious, objectionable and cannot be adapted. The total score was rated 5 points using skin comfort, with 5 scoring criteria: the adhesive has good fit when in use, and the skin can absorb quickly after use; the 4 scoring criteria were: the mask has good fit when in use, and the skin can absorb the mask quickly after the mask is used; the 3 scoring criteria are: the mask has general fit when in use, and the skin absorption speed after use is general (the mask is generally the same as the commercially available mask); the scoring criteria for 2 were: the adhesive is not good (not natural enough) when in use, or the absorption speed is slower after use; the scoring criteria for 1 were: the skin is uncomfortable to attach when in use, and the skin absorption speed is low after use. The scores were counted and averaged, and the results are shown in Table 5.
TABLE 5
As can be seen from the table, only if the proper content of hydrolyzed pea protein is added into the product, the obtained product can avoid the whitening phenomenon after the use of the traditional commodity, and the effect of the product is amplified and weakened along with the gradual increase of the content of the hydrolyzed pea protein, so that the production cost is increased; the special odor source of the product is mainly camellia seed oil, and compared with the product obtained in comparative example 5 using traditional commercial camellia seed oil raw materials, the mask products prepared in examples 1-5 are pleasant in overall odor and have scores of more than 4 minutes; in combination, the products of examples 1-3 have good use experience and excellent skin quality enhancement, with the product of example 1 being the best.
Finally, it should be noted that the above embodiments are only for illustrating the technical solution of the present invention and not for limiting the scope of the present invention, and although the present invention has been described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that the technical solution of the present invention may be modified or substituted equally without departing from the spirit and scope of the technical solution of the present invention.

Claims (4)

1. The camellia seed oil skin care composition containing the hydrolyzed vegetable protein for the mask is characterized by comprising the following components: plant extract, humectant, emulsifier, antioxidant, skin conditioner and the balance of water; the plant extract comprises 0.5% of hydrolyzed pea protein, 0.5% of refined oil tea seed oil, 2-4% of chamomile extract and 0.4-0.6% of kava leaf/root/stem extract by mass of the oil tea seed oil skin care composition; the humectant comprises 0.1-0.3% of arginine, 2-4% of butanediol, 1-3% of panthenol, 1-3% of polyethylene glycol-32, 0.5-1.5% of polyethylene glycol-8 and 0.4-0.6% of 1, 2-hexanediol by weight of the camellia seed oil skin care composition; the emulsifier comprises PEG-20 methyl glucose sesquistearate accounting for 0.2-0.4% of the weight of the camellia seed oil skin care composition, the antioxidant comprises p-hydroxyacetophenone accounting for 0.4-0.6% of the weight of the camellia seed oil skin care composition, and the skin conditioner comprises dipotassium glycyrrhizinate accounting for 0.1-0.3% of the weight of the camellia seed oil skin care composition;
the refined oil tea seed oil is obtained through low-temperature refining, wherein the low-temperature refining comprises the steps of degumming, deacidification, decolorization, deodorization and dewaxing, and the temperature of the deodorization step is 150 ℃; the acid value of the refined camellia seed oil is less than 0.5mg.KOH/g, the peroxide value is less than 1.5mmol/kg, and the mass percentage of moisture and volatile substances in the refined camellia seed oil is less than 0.15%.
2. The plant protein containing camellia seed oil skin care composition for a mask according to claim 1, wherein the plant protein containing camellia seed oil skin care composition comprises the following components in percentage by mass: 0.5% refined camellia seed oil, 0.3% PEG-20 methyl glucose sesquistearate, 0.5% hydrolyzed pea protein, 0.2% arginine, 3% butylene glycol, 0.5% p-hydroxyacetophenone, 2% panthenol, 2% polyethylene glycol-32, 1% polyethylene glycol-8, 3% chamomile extract, 0.5% 1, 2-hexanediol, 0.5% kava leaf/root/stem extract, 0.2% dipotassium glycyrrhizinate, and the balance water.
3. The method for preparing the plant protein containing camellia seed oil skin care composition for a mask according to any one of claims 1 to 2, which is characterized by comprising the following steps:
(1) Soaking refined oil tea seed oil, PEG-20 methyl glucose sesquistearate and hydrolyzed pea protein in water completely, heating, maintaining the temperature, stirring uniformly, and cooling to obtain a mixture A;
(2) Adding arginine into the mixture A obtained in the step (1), mixing and stirring until the arginine is dissolved to obtain a mixture B;
(3) Heating and uniformly mixing butylene glycol and p-hydroxyacetophenone, adding the mixture into the mixture B obtained in the step (2), mixing and stirring until the mixture is dissolved, and cooling to obtain a mixture C;
(4) And (3) adding panthenol, polyethylene glycol-32, polyethylene glycol-8, chamomile extract, 1, 2-hexanediol, kava leaf/root/stem extract and dipotassium glycyrrhizinate into the mixture C obtained in the step (3) in sequence, mixing and stirring until the mixture is completely dissolved, and cooling to obtain the camellia seed oil skin care composition containing the plant protein.
4. Use of the vegetable protein containing camellia seed oil skin care composition for a mask according to any one of claims 1-2 in the preparation of a mask.
CN202110194988.XA 2021-02-20 2021-02-20 Oil tea seed oil skin care composition containing hydrolyzed vegetable protein and preparation method and application thereof Active CN113057901B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202110194988.XA CN113057901B (en) 2021-02-20 2021-02-20 Oil tea seed oil skin care composition containing hydrolyzed vegetable protein and preparation method and application thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202110194988.XA CN113057901B (en) 2021-02-20 2021-02-20 Oil tea seed oil skin care composition containing hydrolyzed vegetable protein and preparation method and application thereof

Publications (2)

Publication Number Publication Date
CN113057901A CN113057901A (en) 2021-07-02
CN113057901B true CN113057901B (en) 2023-10-03

Family

ID=76558862

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202110194988.XA Active CN113057901B (en) 2021-02-20 2021-02-20 Oil tea seed oil skin care composition containing hydrolyzed vegetable protein and preparation method and application thereof

Country Status (1)

Country Link
CN (1) CN113057901B (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116023265A (en) * 2022-12-22 2023-04-28 仲恺农业工程学院 Oleate, preparation method thereof and skin care product

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100755427B1 (en) * 2006-03-20 2007-09-04 주식회사 생그린 Cosmetic composition comprising green tea seed oil for enhancing skin elasticity
CN102885749A (en) * 2012-10-15 2013-01-23 管天球 Oil tea cosmetic
WO2013091975A1 (en) * 2011-12-21 2013-06-27 Henkel Ag & Co. Kgaa Biomimetic compositions for skin cleansing and skin care
WO2013187574A1 (en) * 2012-06-12 2013-12-19 ㈜제이알 코스메틱 Skin-whitening cosmetic composition
CN105902436A (en) * 2016-06-02 2016-08-31 长沙昊瑞生物科技有限公司 Acne removal restoring mask applying camellia oleifera seed meal and preparation method thereof
CN106433970A (en) * 2016-07-21 2017-02-22 江西省高正生物科技集团有限公司 Production method for high-quality cosmetic oil
CN107693456A (en) * 2017-11-15 2018-02-16 广西南宁荣威德新能源科技有限公司 A kind of natural tea pasta frost and preparation method thereof
CN109602686A (en) * 2019-02-02 2019-04-12 西安力邦制药有限公司 A kind of aqueous gelled cosmetic compositions and preparation method thereof

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100755427B1 (en) * 2006-03-20 2007-09-04 주식회사 생그린 Cosmetic composition comprising green tea seed oil for enhancing skin elasticity
WO2013091975A1 (en) * 2011-12-21 2013-06-27 Henkel Ag & Co. Kgaa Biomimetic compositions for skin cleansing and skin care
WO2013187574A1 (en) * 2012-06-12 2013-12-19 ㈜제이알 코스메틱 Skin-whitening cosmetic composition
CN102885749A (en) * 2012-10-15 2013-01-23 管天球 Oil tea cosmetic
CN105902436A (en) * 2016-06-02 2016-08-31 长沙昊瑞生物科技有限公司 Acne removal restoring mask applying camellia oleifera seed meal and preparation method thereof
CN106433970A (en) * 2016-07-21 2017-02-22 江西省高正生物科技集团有限公司 Production method for high-quality cosmetic oil
CN107693456A (en) * 2017-11-15 2018-02-16 广西南宁荣威德新能源科技有限公司 A kind of natural tea pasta frost and preparation method thereof
CN109602686A (en) * 2019-02-02 2019-04-12 西安力邦制药有限公司 A kind of aqueous gelled cosmetic compositions and preparation method thereof

Also Published As

Publication number Publication date
CN113057901A (en) 2021-07-02

Similar Documents

Publication Publication Date Title
CN113057902B (en) Oil tea seed oil facial cream containing hydrolyzed vegetable protein and preparation method thereof
CN106511135B (en) A kind of whitening compound essential oil and preparation method thereof
CN106333885A (en) Plant extract and eye essence liquid
CN104922244B (en) A kind of rose spray for alleviating eye strain and preparation method thereof
CN105168054A (en) Mask capable of supplementing water, whitening and removing wrinkles and preparation method of mask
CN107468563A (en) A kind of anti-dandruff silk quality lubrication is without silicone oil shampoo
CN106420482A (en) Skin energy activating sparkling essence
CN113041174B (en) Oil tea seed oil essence containing hydrolyzed vegetable protein and preparation method and application thereof
CN109350591A (en) A kind of U.S. face dried noodle film and preparation method thereof
CN111228174A (en) Skin soothing composition and skin care product
CN114712275A (en) Anti-wrinkle repair composition and preparation method thereof, and cosmetic and preparation method thereof
KR20120129600A (en) The cosmetic composition for anti-wrinkle comprising the mixture of extract of Allium cepa, Symphytum officinale, Eclipta prostrate, and Theobroma cacao
KR102047214B1 (en) Composition for scalp care and manufacturing method thereof
CN113057901B (en) Oil tea seed oil skin care composition containing hydrolyzed vegetable protein and preparation method and application thereof
CN107625690A (en) Moisten moisturizing camellia oleifera fruit lip gloss and preparation method thereof
CN107854403A (en) A kind of clean moisture surge treatment formula
CN113143820A (en) Anti-aging composition and preparation method thereof
CN107137316B (en) Dendrobium lip balm and preparation method thereof
KR20190075405A (en) Cosmetic composition including beeswax with animal oil and vegetable oil
CN110368336B (en) Skin-care lotion containing platycarya strobilacea infructescence as well as preparation method and application of skin-care lotion
CN109646359B (en) Rose-agaric mud membrane paste with effects of cleaning, purifying, maintaining beauty and keeping young and preparation method thereof
KR102108116B1 (en) A cosmetic composition comprising a natural component and an oil component
CN107822998B (en) Whitening and moisturizing cream containing Brazilian cocoa extract
KR101831756B1 (en) Cosmetic composition for improving wrinkles and the patch for the skin around eyes using the same
CN112294687A (en) Black tea fungus fermentation mask liquid and preparation method thereof

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant