CN112642221B - Preparation method of particles for ternary cavity filter stick - Google Patents

Preparation method of particles for ternary cavity filter stick Download PDF

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Publication number
CN112642221B
CN112642221B CN202011480416.XA CN202011480416A CN112642221B CN 112642221 B CN112642221 B CN 112642221B CN 202011480416 A CN202011480416 A CN 202011480416A CN 112642221 B CN112642221 B CN 112642221B
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China
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particles
percent
mixture
filter stick
cavity filter
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CN112642221A (en
Inventor
刘鑫
张强
徐世涛
刘强
吴恒
赵立恒
肖永银
杜超
蒋卓芳
陈婉
王厚娴
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Yunnan China Tobacco New Material Technology Co ltd
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Yunnan China Tobacco New Material Technology Co ltd
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D39/00—Filtering material for liquid or gaseous fluids
    • B01D39/02—Loose filtering material, e.g. loose fibres
    • B01D39/04—Organic material, e.g. cellulose, cotton
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/06—Use of materials for tobacco smoke filters
    • A24D3/14—Use of materials for tobacco smoke filters of organic materials as additive
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/22—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising organic material
    • B01J20/24—Naturally occurring macromolecular compounds, e.g. humic acids or their derivatives
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28016—Particle form
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/0007—Aliphatic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/0007—Aliphatic compounds
    • C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2239/00—Aspects relating to filtering material for liquid or gaseous fluids
    • B01D2239/04—Additives and treatments of the filtering material
    • B01D2239/0407—Additives and treatments of the filtering material comprising particulate additives, e.g. adsorbents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2239/00—Aspects relating to filtering material for liquid or gaseous fluids
    • B01D2239/10—Filtering material manufacturing
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2220/00—Aspects relating to sorbent materials
    • B01J2220/40—Aspects relating to the composition of sorbent or filter aid materials
    • B01J2220/48—Sorbents characterised by the starting material used for their preparation
    • B01J2220/4812—Sorbents characterised by the starting material used for their preparation the starting material being of organic character
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2220/00—Aspects relating to sorbent materials
    • B01J2220/40—Aspects relating to the composition of sorbent or filter aid materials
    • B01J2220/48—Sorbents characterised by the starting material used for their preparation
    • B01J2220/4812—Sorbents characterised by the starting material used for their preparation the starting material being of organic character
    • B01J2220/4825—Polysaccharides or cellulose materials, e.g. starch, chitin, sawdust, wood, straw, cotton

Abstract

The invention discloses a preparation method of particles for a ternary cavity filter stick, which comprises the following steps: uniformly mixing the modified cassava starch and the porous starch according to the mass ratio of (10-60):1, and then carrying out primary flavoring treatment to obtain a first mixture; uniformly mixing the first mixture and the dried orange peel powder according to the mass ratio (20-1):1 to obtain a second mixture; performing granulation treatment on the second mixture and performing shot blasting treatment to obtain pills; performing secondary perfuming treatment on the pills to obtain perfumed particles, wherein the mass percentage of the secondary perfuming perfume is 3% -8% of that of the perfumed particles; and (4) coating the flavoring particles to obtain the particles for the ternary cavity filter stick. According to the method, through secondary flavoring, the limonene type essence is embedded in the modified starch to form small aroma clusters, and dissipation of limonene type components is blocked through the coating after granulation, so that the problem of mouth bursting in the preparation process of the filter stick and the problem of reduced suction quality caused by dissipation of the limonene type components are solved.

Description

Preparation method of particles for ternary cavity filter stick
Technical Field
The invention relates to the field of composite filter sticks, in particular to a preparation method of particles for a ternary cavity filter stick.
Background
In recent years, research on cigarette materials and application of novel materials are continuously driving innovation and innovation of cigarette products. The particle composite filter stick is a special filter stick which is most applied to cigarettes at home and abroad at present, and compared with single-structure filter sticks such as acetate fiber filter sticks, various functional particles are added in the inner section of the particle composite filter stick, so that the composite filter stick not only has the function of selectively adsorbing harmful ingredients in smoke, but also can compensate fragrance loss caused by harm reduction and tar reduction.
The existing orange flavor applied to the filter stick mainly comprises limonene components. However, the dispersion of the limonene components can affect the effect of the adhesive of the filter stick, and the problem of opening burst of the finished filter stick is caused. Moreover, the limonene-type components can also diffuse to the tobacco shred end during dissipation, so that the essence is partially volatilized to the tobacco shred end and participates in combustion during cigarette smoking, and the cigarette smoking quality is influenced.
Therefore, how to provide the particles for the filter stick, which can effectively reduce the dissipation of the limonene-based components, becomes a technical problem which needs to be solved in the field.
Disclosure of Invention
The invention aims to provide a novel technical scheme of a preparation method of particles for a ternary cavity filter stick, which can effectively reduce the dissipation of limonene components.
According to the first aspect of the invention, a preparation method of particles for a ternary cavity filter stick is provided.
The preparation method of the particles for the ternary cavity filter stick comprises the following steps:
step (1): uniformly mixing the modified cassava starch and the porous starch according to the mass ratio (10-60) of 1, and then performing primary flavoring treatment to obtain a first mixture;
step (2): uniformly mixing the first mixture and the dried orange peel powder according to the mass ratio (20-1):1 to obtain a second mixture;
and (3): granulating the second mixture to obtain preformed particles;
and (4): performing shot blasting treatment on the preformed particles to obtain pills, wherein the moisture content of the pills is 6% -9%;
and (5): performing secondary flavoring treatment on the pill to obtain flavored particles, wherein the mass percentage of secondary flavoring essence in the secondary flavoring treatment is 3% -8% of that of the flavored particles;
and (6): and (3) coating the aromatized particles to obtain the particles for the ternary cavity filter stick, wherein the mass percentage of the coating material in the particles for the ternary cavity filter stick is 5-15%.
Optionally, the step (1) is specifically as follows:
step (1-1): uniformly mixing the modified cassava starch and the porous starch according to the mass ratio of (10-60) 1 to obtain a first premix;
step (1-2): and uniformly mixing the first premix and the primary flavoring perfume to obtain a first mixture, wherein the mass percentage of the primary flavoring perfume in the first mixture is 2-30%.
Optionally, the primary perfuming perfume in the step (1-2) comprises the following components in percentage by mass:
4.0-20.0% of dried orange peel extract, 0.1-0.5% of tree moss extract, 0.5-5.0% of apple juice, 0.5-5.0% of snow pear extract, 0.1-2.0% of citral, 1.0-15.0% of limonene and 52.5-93.8% of propylene glycol.
Optionally, the step (2) is specifically as follows:
and (3) placing the first mixture and the dried orange peel powder into a conical mixer according to the mass ratio (20-1) of 1 to mix for 1 to 3 hours to obtain a second mixture.
Optionally, the adhesive used in the granulation treatment in step (3) is at least one of cellulose and derivatives thereof.
Optionally, the adhesive used in the granulation treatment in step (3) is a sodium carboxymethylcellulose aqueous solution with a mass percentage of 0.5% -5.0%.
Optionally, the step (4) is specifically as follows:
step (4-1): performing shot blasting treatment on the preformed particles to obtain mixed pellets;
step (4-2): and (4) screening the mixed pellets to obtain particles with 14-40 meshes, thus obtaining the pellets.
Optionally, the manner of the secondary perfuming treatment in the step (5) is spray perfuming.
Optionally, the secondary perfuming perfume in the step (5) comprises the following components in percentage by mass:
2.0 to 10.0 percent of limonene, 0.2 to 20.0 percent of bergamot oil, 2.0 to 40.0 percent of fructus Broussonetiae essential oil, 0.1 to 1.0 percent of methyl heptenone, 0.1 to 1.0 percent of damascenone, 0.1 to 0.5 percent of beta-ionone, 0.1 to 0.5 percent of phenethyl alcohol, 0.1 to 0.5 percent of anisic aldehyde, 0.1 to 0.5 percent of tree moss immersion oil, 0.1 to 0.5 percent of vanillin, 0.1 to 0.5 percent of cinnamaldehyde and 25.0 to 94.9 percent of propylene glycol.
Optionally, the coating material in the step (6) comprises propylene glycol and polyethylene glycol in a mass ratio of (70-95) to (5-30), and the polymerization degree of the polyethylene glycol is 1000-6000.
The preparation method of the particles for the ternary cavity filter stick has the following advantages:
1. modified cassava starch and porous starch are adopted as raw materials, so that the cost is low, and the material absorption performance is good;
2. through secondary flavoring, the limonene type essence is embedded in the modified starch to form small aroma clusters, and dissipation of limonene type components is blocked through a coating after granulation, so that the problem of opening burst in the preparation process of the filter stick and the problem of reduced suction quality caused by dissipation of the limonene type components are solved;
3. the particles treated by the shot blasting coating procedure have good fluidity and regular and beautiful appearance.
Detailed Description
Various exemplary embodiments of the present invention will now be described in detail. It should be noted that: the relative arrangement of the components and steps, the numerical expressions and numerical values set forth in these embodiments do not limit the scope of the present invention unless specifically stated otherwise.
The following description of at least one exemplary embodiment is merely illustrative in nature and is in no way intended to limit the invention, its application, or uses.
Techniques, methods, and apparatus known to those of ordinary skill in the relevant art may not be discussed in detail but are intended to be part of the specification where appropriate.
In all examples shown and discussed herein, any particular value should be construed as merely illustrative, and not limiting. Thus, other examples of the exemplary embodiments may have different values.
The preparation method of the particles for the ternary cavity filter stick comprises the following steps:
step (1): uniformly mixing the modified cassava starch and the porous starch according to the mass ratio of (10-60) 1, and then carrying out primary flavoring treatment to obtain a first mixture. The material absorption performance of the modified cassava starch can reach 40-50%, and the material absorption performance of the porous starch can reach 50-60%.
In order to more effectively reduce the burst of the finished filter stick and reduce the dissipation of limonene components, the step (1) is specifically as follows:
step (1-1): uniformly mixing the modified cassava starch and the porous starch according to the mass ratio of (10-60) 1 to obtain a first premix.
Step (1-2): and uniformly mixing the first premix and the primary flavoring perfume to obtain a first mixture, wherein the mass percentage of the primary flavoring perfume in the first mixture is 2-30%.
The primary perfuming perfume in the step (1-2) comprises the following components in percentage by mass:
4.0-20.0% of dried orange peel extract, 0.1-0.5% of tree moss extract, 0.5-5.0% of apple juice, 0.5-5.0% of snow pear extract, 0.1-2.0% of citral, 1.0-15.0% of limonene and 52.5-93.8% of propylene glycol.
Step (2): and uniformly mixing the first mixture and the dried orange peel powder according to the mass ratio (20-1):1 to obtain a second mixture.
In order to ensure that the fragrance of the particles for the ternary cavity filter stick is uniformly released, the step (2) can be specifically as follows:
and (3) placing the first mixture and the dried orange peel powder into a conical mixer according to the mass ratio (20-1) of 1 to mix for 1 to 3 hours to obtain a second mixture.
And (3): and granulating the second mixture to obtain preformed particles.
In order to granulate more efficiently, the binder used in the granulating treatment in step (3) is at least one of cellulose and derivatives thereof.
Further, the adhesive used in the granulation treatment in step (3) is a sodium carboxymethylcellulose aqueous solution with a mass percentage of 0.5% -5.0%.
And (4): performing shot blasting treatment on the preformed particles to obtain the pellets, wherein the moisture content of the pellets is 6% -9%. The water content of the pill grains is controlled, so that the problem of mildew of the grains is avoided, and the fragrance quality of the grains can be effectively improved.
In specific implementation, the temperature of air flow in the shot blasting treatment process does not exceed 40 ℃ so as to reduce fragrance loss.
In order to more effectively improve the flowability of the particles, the step (4) is specifically as follows:
step (4-1): and performing shot blasting treatment on the preformed particles to obtain the mixed pellets.
Step (4-2): and (4) screening the mixed pellets to obtain particles with 14-40 meshes, thus obtaining the pellets.
And (5): and (3) carrying out secondary perfuming treatment on the pellets to obtain the perfumed particles, wherein the mass percentage of the secondary perfuming perfume in the secondary perfuming treatment is 3% -8% of that of the perfumed particles.
For more efficient perfuming, the manner of the secondary perfuming treatment in step (5) is spray perfuming.
In specific implementation, the secondary perfuming perfume in the step (5) comprises the following components in percentage by mass:
2.0 to 10.0 percent of limonene, 0.2 to 20.0 percent of bergamot oil, 2.0 to 40.0 percent of fructus Broussonetiae essential oil, 0.1 to 1.0 percent of methyl heptenone, 0.1 to 1.0 percent of damascenone, 0.1 to 0.5 percent of beta-ionone, 0.1 to 0.5 percent of phenethyl alcohol, 0.1 to 0.5 percent of anisic aldehyde, 0.1 to 0.5 percent of tree moss immersion oil, 0.1 to 0.5 percent of vanillin, 0.1 to 0.5 percent of cinnamaldehyde and 25.0 to 94.9 percent of propylene glycol.
And (6): and (3) coating the aromatized particles to obtain the particles for the ternary cavity filter stick, wherein the mass percentage of the coating material in the particles for the ternary cavity filter stick is 5-15%.
In order to more effectively improve the fluidity of the particles and improve the appearance regularity of the particles, the coating material in the step (6) comprises propylene glycol and polyethylene glycol in a mass ratio of (70-95) to (5-30), and the polymerization degree of the polyethylene glycol is 1000-6000.
The particles for the ternary-cavity filter stick can solve the problems that the quality fluctuation of the traditional particles added in the ternary-cavity filter stick is large and the attractiveness is poor. In addition, the preparation method of the ternary cavity filter stick particle disclosed by the invention takes modified starch as a main raw material, the modified starch adsorbs spice to form small spice balls, and finally, the particles are granulated and formed, the formed particles are subjected to secondary perfuming, and after the perfuming, the coating treatment is performed by using a temperature-sensitive phase-change material, so that the ternary cavity filter stick particle which is harmonious with tobacco fragrance, fresh in taste, rich in tobacco fragrance and lasting in fragrance can be developed and produced.
The experimental procedures used in the examples below are conventional unless otherwise specified, the materials and reagents used therein are commercially available, and the equipment used in the experiments are well known to those skilled in the art without otherwise specified.
Example 1
Uniformly mixing modified cassava starch and porous starch according to the mass ratio of 40:1, and performing primary flavoring on the uniformly mixed raw materials (the primary flavoring comprises 12.0% of dried orange peel extract, 0.2% of tree moss extract, 1.0% of apple juice, 1.0% of snow pear extract, 1.0% of citral, 10.0% of limonene and 74.8% of propylene glycol), wherein the flavoring amount is 16%, so as to obtain a first mixture;
placing the first mixture and the dried orange peel powder in a conical mixer according to the mass ratio of 20:1 for mixing for 2 hours to obtain a second mixture;
adding an adhesive into the second mixture, wherein the adhesive is a 2% sodium carboxymethylcellulose aqueous solution, mixing, and adding into a granulator for granulation, wherein the granulator is a screw extrusion granulator;
performing shot blasting on the manufactured particles, and screening according to 14-20 meshes after shot blasting to obtain pills with the water content of 6%;
secondary perfuming of the pellets (secondary perfuming included 8.0% limonene, 10.0% bergamot oil, 1% Broussonetia papyrifera essential oil 12.0%, 1% methylheptenone 0.2%, 1% damascone 0.2%, 1% beta-ionone 0.2%, 1% phenethyl alcohol 0.2%, 0.1% anisaldehyde 0.2%, 0.1% tree moss essential oil 0.2%, 1% vanillin 0.1%, 0.1% cinnamaldehyde 0.1%, and propylene glycol 68.6%) with a perfuming amount of 6%;
coating by using a shot blasting and coating all-in-one machine, wherein the dosage of a coating material (the coating material comprises 92 mass percent of polyethylene glycol 1500 and 8 mass percent of propylene glycol) is 8 percent, and the particles S1 for the ternary cavity filter stick are obtained after coating.
Example 2
Uniformly mixing modified cassava starch and porous starch according to the mass ratio of 50:1, and performing primary flavoring on the uniformly mixed raw materials (the primary flavoring comprises 15.0% of dried orange peel extract, 0.1% of tree moss extract, 1.0% of apple juice, 1.0% of snow pear extract, 1% of citral 1.0%, 8.0% of limonene and 73.9% of propylene glycol) to obtain a first mixture, wherein the flavoring amount is 15%;
placing the first mixture and the dried orange peel powder in a conical mixer according to the mass ratio of 10:1 for mixing for 2 hours to obtain a second mixture;
adding an adhesive into the second mixture, wherein the adhesive is a 2% methyl cellulose aqueous solution, mixing, and then adding into a granulator for granulation, wherein the granulator is a screw extrusion granulator;
performing shot blasting on the manufactured particles, and screening according to 14-20 meshes after shot blasting to obtain pills with the water content of 7%;
secondary perfuming of the pellets (secondary perfuming included limonene 10.0%, 1% bergamot oil 12.0%, 1% broussonetia papyrifera essential oil 14.0%, 1% methylheptenone 0.2%, 1% damascone 0.2%, 1% beta-ionone 0.1%, 1% phenethyl alcohol 0.2%, 0.1% anisaldehyde 0.1%, 0.1% tree moss essential oil 0.1%, 1% vanillin 0.1%, 0.1% cinnamaldehyde 0.1%, and propylene glycol 62.9%) with a perfuming amount of 8%;
coating by using a shot blasting and coating integrated machine, wherein the dosage of a coating material (the coating material comprises 92 mass percent of polyethylene glycol 1500 and 8 mass percent of propylene glycol) is 8 percent, and the ternary cavity filter stick particles S2 are obtained after coating.
Example 3
Uniformly mixing modified cassava starch and porous starch according to a mass ratio of 49:1, and performing primary flavoring on the uniformly mixed raw materials (the primary flavoring comprises 18.0% of dried orange peel extract, 0.1% of tree moss extract, 1.0% of apple juice, 2.0% of snow pear extract, 0.5% of 1% of citral, 10.0% of limonene and 68.4% of propylene glycol) to obtain a first mixture, wherein the flavoring amount is 20%;
placing the first mixture and the dried orange peel powder in a conical mixer according to the mass ratio of 25:1 for mixing for 2 hours to obtain a second mixture;
adding an adhesive into the second mixture, wherein the adhesive is a 2% hydroxyethyl cellulose aqueous solution, mixing, and then adding into a granulator for granulation, wherein the granulator is a screw extrusion granulator;
performing shot blasting on the manufactured particles, and screening according to 14-20 meshes after shot blasting to obtain pills with the water content of 8%;
secondary perfuming of the pellets (secondary perfuming included limonene 6.0%, 1% bergamot oil 12.0%, 1% broussonetia papyrifera essential oil 20.0%, 1% methylheptenone 0.1%, 1% damascone 0.1%, 1% beta-ionone 0.1%, 1% phenethyl alcohol 0.2%, 0.1% anisaldehyde 0.1%, 0.1% tree moss essential oil 0.1%, 1% vanillin 0.1%, 0.1% cinnamaldehyde 0.2%, and propylene glycol 61.0%), a perfuming amount of 8%;
coating by using a shot blasting and coating all-in-one machine, wherein the dosage of a coating material (the coating material comprises 76% by mass of polyethylene glycol 4000 and 24% by mass of propylene glycol) is 8%, and the particles S3 for the ternary cavity filter stick are obtained after coating.
The smoking evaluation of the cigarettes manufactured by the ternary cavity filter stick added with the ternary cavity filter stick particles S1-S3 is found to have the characteristics of harmonious cigarette fragrance, fresh and cool taste, rich cigarette fragrance and lasting fragrance.
Although some specific embodiments of the present invention have been described in detail by way of examples, it should be understood by those skilled in the art that the above examples are for illustrative purposes only and are not intended to limit the scope of the present invention. It will be appreciated by those skilled in the art that modifications may be made to the above embodiments without departing from the scope and spirit of the invention. The scope of the invention is defined by the appended claims.

Claims (6)

1. A preparation method of particles for a ternary cavity filter stick is characterized by comprising the following steps:
step (1): uniformly mixing the modified cassava starch and the porous starch according to the mass ratio (10-60) of 1, and then performing primary flavoring treatment to obtain a first mixture;
the step (1) is specifically as follows:
step (1-1): uniformly mixing the modified cassava starch and the porous starch according to the mass ratio of (10-60) 1 to obtain a first premix;
step (1-2): uniformly mixing the first premix and the primary flavoring perfume to obtain a first mixture, wherein the mass percentage of the primary flavoring perfume in the first mixture is 2% -30%; the primary perfuming perfume in the step (1-2) comprises the following components in percentage by mass:
4.0-20.0% of dried orange peel extract, 0.1-0.5% of tree moss extract, 0.5-5.0% of apple juice, 0.5-5.0% of snow pear extract, 0.1-2.0% of citral, 1.0-15.0% of limonene and 52.5-93.8% of propylene glycol;
step (2): uniformly mixing the first mixture and the dried orange peel powder according to the mass ratio (20-1):1 to obtain a second mixture;
and (3): granulating the second mixture to obtain preformed particles;
and (4): performing shot blasting treatment on the preformed particles to obtain pills, wherein the moisture content of the pills is 6% -9%;
and (5): performing secondary flavoring treatment on the pill to obtain flavored particles, wherein the mass percentage of secondary flavoring essence in the secondary flavoring treatment is 3% -8% of that of the flavored particles;
the secondary perfuming treatment in the step (5) is spray perfuming, and the secondary perfuming perfume in the step (5) comprises the following components in percentage by mass:
2.0 to 10.0 percent of limonene, 0.2 to 20.0 percent of bergamot oil, 2.0 to 40.0 percent of fructus Broussonetiae essential oil, 0.1 to 1.0 percent of methyl heptenone, 0.1 to 1.0 percent of damascenone, 0.1 to 0.5 percent of beta-ionone, 0.1 to 0.5 percent of phenethyl alcohol, 0.1 to 0.5 percent of anisic aldehyde, 0.1 to 0.5 percent of tree moss immersion oil, 0.1 to 0.5 percent of vanillin, 0.1 to 0.5 percent of cinnamaldehyde and 25.0 to 94.9 percent of propylene glycol;
and (6): and (3) coating the aromatized particles to obtain the particles for the ternary cavity filter stick, wherein the mass percentage of the coating material in the particles for the ternary cavity filter stick is 5-15%.
2. The method for preparing the ternary cavity filter stick particle according to claim 1, wherein the step (2) is specifically as follows:
and (3) placing the first mixture and the dried orange peel powder into a conical mixer according to the mass ratio (20-1) of 1 to mix for 1 to 3 hours to obtain a second mixture.
3. The method for preparing particles for a ternary cavity filter stick according to claim 1, wherein the adhesive used in the granulation treatment in step (3) is at least one of cellulose and derivatives thereof.
4. The preparation method of the ternary cavity filter stick particle according to claim 3, wherein the adhesive used in the granulation treatment in the step (3) is a sodium carboxymethylcellulose aqueous solution with a mass percentage of 0.5% -5.0%.
5. The method for preparing the ternary cavity filter stick particle according to claim 1, wherein the step (4) is as follows:
step (4-1): performing shot blasting treatment on the preformed particles to obtain mixed pellets;
step (4-2): and (4) screening the mixed pellets to obtain particles with 14-40 meshes, thus obtaining the pellets.
6. The preparation method of the particles for the ternary cavity filter stick as claimed in claim 1, wherein the coating material in the step (6) comprises propylene glycol and polyethylene glycol in a mass ratio of (70-95) - (5-30), and the polymerization degree of the polyethylene glycol is 1000-.
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