CN1122726A - 在蒽醌法制造过氧化氢的氢化流程中分离不含催化剂的操作液的方法 - Google Patents
在蒽醌法制造过氧化氢的氢化流程中分离不含催化剂的操作液的方法 Download PDFInfo
- Publication number
- CN1122726A CN1122726A CN95106619A CN95106619A CN1122726A CN 1122726 A CN1122726 A CN 1122726A CN 95106619 A CN95106619 A CN 95106619A CN 95106619 A CN95106619 A CN 95106619A CN 1122726 A CN1122726 A CN 1122726A
- Authority
- CN
- China
- Prior art keywords
- filter
- filter cylinder
- catalyzer
- catalyst
- pore size
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims abstract description 55
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 title claims abstract description 26
- 238000005984 hydrogenation reaction Methods 0.000 title claims abstract description 26
- 238000000926 separation method Methods 0.000 title claims abstract description 13
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 12
- PYKYMHQGRFAEBM-UHFFFAOYSA-N anthraquinone Natural products CCC(=O)c1c(O)c2C(=O)C3C(C=CC=C3O)C(=O)c2cc1CC(=O)OC PYKYMHQGRFAEBM-UHFFFAOYSA-N 0.000 title claims abstract description 10
- 150000004056 anthraquinones Chemical class 0.000 title claims abstract description 10
- 239000012224 working solution Substances 0.000 title abstract 4
- 238000001914 filtration Methods 0.000 claims abstract description 38
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 claims abstract description 31
- 239000012528 membrane Substances 0.000 claims abstract description 30
- 239000011148 porous material Substances 0.000 claims abstract description 22
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 21
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 21
- 239000007788 liquid Substances 0.000 claims description 55
- 229910052751 metal Inorganic materials 0.000 claims description 9
- 239000002184 metal Substances 0.000 claims description 9
- 239000010970 precious metal Substances 0.000 claims description 9
- 239000002904 solvent Substances 0.000 claims description 6
- 229910004298 SiO 2 Inorganic materials 0.000 claims description 5
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 claims description 4
- 229910010271 silicon carbide Inorganic materials 0.000 claims description 4
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 claims description 3
- 239000003054 catalyst Substances 0.000 abstract description 8
- 229910000510 noble metal Inorganic materials 0.000 abstract description 2
- 229910010293 ceramic material Inorganic materials 0.000 abstract 2
- 239000010410 layer Substances 0.000 abstract 1
- 239000002356 single layer Substances 0.000 abstract 1
- 239000000706 filtrate Substances 0.000 description 14
- 239000000919 ceramic Substances 0.000 description 13
- 238000012360 testing method Methods 0.000 description 11
- 239000000463 material Substances 0.000 description 8
- 238000006243 chemical reaction Methods 0.000 description 7
- 230000000052 comparative effect Effects 0.000 description 6
- 230000008901 benefit Effects 0.000 description 5
- 239000000969 carrier Substances 0.000 description 5
- 230000007423 decrease Effects 0.000 description 5
- 239000000203 mixture Substances 0.000 description 5
- 239000002245 particle Substances 0.000 description 5
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 3
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 3
- 230000003647 oxidation Effects 0.000 description 3
- 238000007254 oxidation reaction Methods 0.000 description 3
- 230000000717 retained effect Effects 0.000 description 3
- 238000005245 sintering Methods 0.000 description 3
- 239000011877 solvent mixture Substances 0.000 description 3
- JORLUGVBYJSSAW-UHFFFAOYSA-N 2-ethyl-1,2,3,4-tetrahydroanthracene-9,10-dione Chemical compound O=C1C2=CC=CC=C2C(=O)C2=C1CC(CC)CC2 JORLUGVBYJSSAW-UHFFFAOYSA-N 0.000 description 2
- -1 5 and 50mm between Chemical compound 0.000 description 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
- 230000001464 adherent effect Effects 0.000 description 2
- 238000013461 design Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 238000012423 maintenance Methods 0.000 description 2
- 238000001471 micro-filtration Methods 0.000 description 2
- 229910052763 palladium Inorganic materials 0.000 description 2
- 238000009738 saturating Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 240000004859 Gamochaeta purpurea Species 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- WUOFAZKBVWWYER-UHFFFAOYSA-N anthracene-9,10-dione;hydrogen peroxide Chemical compound OO.C1=CC=C2C(=O)C3=CC=CC=C3C(=O)C2=C1 WUOFAZKBVWWYER-UHFFFAOYSA-N 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 235000013877 carbamide Nutrition 0.000 description 1
- 239000003575 carbonaceous material Substances 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000009295 crossflow filtration Methods 0.000 description 1
- 238000005202 decontamination Methods 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000011010 flushing procedure Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 230000008676 import Effects 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 239000007769 metal material Substances 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 230000000737 periodic effect Effects 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000002441 reversible effect Effects 0.000 description 1
- 230000001360 synchronised effect Effects 0.000 description 1
- 150000003672 ureas Chemical class 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
- B01D61/14—Ultrafiltration; Microfiltration
- B01D61/147—Microfiltration
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/24—Stationary reactors without moving elements inside
- B01J19/2415—Tubular reactors
- B01J19/243—Tubular reactors spirally, concentrically or zigzag wound
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/90—Regeneration or reactivation
- B01J23/96—Regeneration or reactivation of catalysts comprising metals, oxides or hydroxides of the noble metals
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/009—Preparation by separation, e.g. by filtration, decantation, screening
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
- C01B15/01—Hydrogen peroxide
- C01B15/022—Preparation from organic compounds
- C01B15/023—Preparation from organic compounds by the alkyl-anthraquinone process
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/584—Recycling of catalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- Water Supply & Treatment (AREA)
- Inorganic Chemistry (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
- Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEP4418931.1 | 1994-05-31 | ||
| DE4418931A DE4418931C2 (de) | 1994-05-31 | 1994-05-31 | Verfahren zur Abtrennung katalysatorfreier Arbeitslösung aus dem Hydrierkreislauf des Anthrachinonverfahrens zur Herstellung von Wasserstoffperoxid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1122726A true CN1122726A (zh) | 1996-05-22 |
Family
ID=6519389
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN95106619A Pending CN1122726A (zh) | 1994-05-31 | 1995-05-30 | 在蒽醌法制造过氧化氢的氢化流程中分离不含催化剂的操作液的方法 |
Country Status (14)
| Country | Link |
|---|---|
| US (1) | US5534149A (cg-RX-API-DMAC7.html) |
| EP (1) | EP0687649B1 (cg-RX-API-DMAC7.html) |
| JP (1) | JPH07330311A (cg-RX-API-DMAC7.html) |
| CN (1) | CN1122726A (cg-RX-API-DMAC7.html) |
| AT (1) | ATE162158T1 (cg-RX-API-DMAC7.html) |
| BR (1) | BR9502610A (cg-RX-API-DMAC7.html) |
| CA (1) | CA2150492C (cg-RX-API-DMAC7.html) |
| DE (2) | DE4418931C2 (cg-RX-API-DMAC7.html) |
| ES (1) | ES2113692T3 (cg-RX-API-DMAC7.html) |
| FI (1) | FI114090B (cg-RX-API-DMAC7.html) |
| IL (1) | IL113915A0 (cg-RX-API-DMAC7.html) |
| NZ (1) | NZ272235A (cg-RX-API-DMAC7.html) |
| TW (1) | TW287145B (cg-RX-API-DMAC7.html) |
| ZA (1) | ZA954428B (cg-RX-API-DMAC7.html) |
Families Citing this family (26)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10052323A1 (de) * | 2000-10-21 | 2002-05-02 | Degussa | Kontinierliches Verfahren zur Hydrierung |
| FR2832937B1 (fr) * | 2001-12-04 | 2004-01-16 | Technip France | Procede et dispositif de reaction chimique entre un gaz et au moins un compose en solution, mis en oeuvre en presence d'un catalyseur solide |
| US7282148B2 (en) * | 2003-10-30 | 2007-10-16 | International Business Machines Corporation | Porous silicon composite structure as large filtration array |
| EP1810001A4 (en) * | 2004-10-08 | 2008-08-27 | Sdc Materials Llc | APPARATUS AND METHOD FOR SAMPLING AND COLLECTING POWDERS FLOWING IN A GAS STREAM |
| JP5275342B2 (ja) | 2007-05-11 | 2013-08-28 | エスディーシー マテリアルズ インコーポレイテッド | 粒子生産システム及び粒子生産方法 |
| US8507401B1 (en) | 2007-10-15 | 2013-08-13 | SDCmaterials, Inc. | Method and system for forming plug and play metal catalysts |
| US7901036B2 (en) | 2007-11-12 | 2011-03-08 | Hon Hai Precision Industry Co., Ltd. | Print head unit and method for manufacturing patterned layer on substrate with the same |
| USD627900S1 (en) | 2008-05-07 | 2010-11-23 | SDCmaterials, Inc. | Glove box |
| US9126191B2 (en) | 2009-12-15 | 2015-09-08 | SDCmaterials, Inc. | Advanced catalysts for automotive applications |
| US8803025B2 (en) | 2009-12-15 | 2014-08-12 | SDCmaterials, Inc. | Non-plugging D.C. plasma gun |
| US8557727B2 (en) | 2009-12-15 | 2013-10-15 | SDCmaterials, Inc. | Method of forming a catalyst with inhibited mobility of nano-active material |
| US8470112B1 (en) | 2009-12-15 | 2013-06-25 | SDCmaterials, Inc. | Workflow for novel composite materials |
| US8652992B2 (en) | 2009-12-15 | 2014-02-18 | SDCmaterials, Inc. | Pinning and affixing nano-active material |
| US9119309B1 (en) | 2009-12-15 | 2015-08-25 | SDCmaterials, Inc. | In situ oxide removal, dispersal and drying |
| US9149797B2 (en) | 2009-12-15 | 2015-10-06 | SDCmaterials, Inc. | Catalyst production method and system |
| US8545652B1 (en) | 2009-12-15 | 2013-10-01 | SDCmaterials, Inc. | Impact resistant material |
| US8669202B2 (en) | 2011-02-23 | 2014-03-11 | SDCmaterials, Inc. | Wet chemical and plasma methods of forming stable PtPd catalysts |
| HK1199222A1 (en) | 2011-08-19 | 2015-06-26 | SDCmaterials, Inc. | Coated substrates for use in catalysis and catalytic converters and methods of coating substrates with washcoat compositions |
| US9156025B2 (en) | 2012-11-21 | 2015-10-13 | SDCmaterials, Inc. | Three-way catalytic converter using nanoparticles |
| US9511352B2 (en) | 2012-11-21 | 2016-12-06 | SDCmaterials, Inc. | Three-way catalytic converter using nanoparticles |
| JP2015020940A (ja) * | 2013-07-22 | 2015-02-02 | 国立大学法人静岡大学 | 過酸化水素合成方法 |
| CN105592921A (zh) | 2013-07-25 | 2016-05-18 | Sdc材料公司 | 用于催化转化器的洗涂层和经涂覆基底及其制造和使用方法 |
| CA2926135A1 (en) | 2013-10-22 | 2015-04-30 | SDCmaterials, Inc. | Compositions of lean nox trap |
| CN106061600A (zh) | 2013-10-22 | 2016-10-26 | Sdc材料公司 | 用于重型柴油机的催化剂设计 |
| US9687811B2 (en) | 2014-03-21 | 2017-06-27 | SDCmaterials, Inc. | Compositions for passive NOx adsorption (PNA) systems and methods of making and using same |
| CN104402142B (zh) * | 2014-11-26 | 2016-06-01 | 柳州化工股份有限公司 | 一种蒽醌法生产双氧水工业中污水预处理的方法 |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1272292B (de) * | 1965-12-04 | 1968-07-11 | Degussa | Abtrennung von suspendierten traegerlosen Hydrierungs-Katalysatoren der Platinmetallgruppe aus fluessigen organischen Hydrierungsgemischen |
| NL141400B (nl) * | 1965-12-04 | 1974-03-15 | Degussa | Werkwijze voor het afscheiden van gesuspendeerde, dragerloze edelmetaalkatalysatoren uit organische vloeistoffen door middel van filters. |
| US4428923A (en) * | 1982-11-09 | 1984-01-31 | Degussa Aktiengesellschaft | Continuous process for the production of hydrogen peroxide according to the anthraquinone process |
| SE8207376L (sv) * | 1982-12-23 | 1984-06-24 | Eka Ab | Forfarande vid avskiljning av i vetska suspenderade katalysatorpartiklar |
| FI86380C (fi) * | 1990-09-10 | 1992-08-25 | Kemira Oy | Foerfarande foer rening av filter. |
| DE4217245A1 (de) * | 1992-05-25 | 1993-12-02 | Degussa | Verfahren zur Abtrennung katalysatorfreier Arbeitslösung aus dem Hydrierkreislauf des Anthrachionverfahrens zur Herstellung von Wasserstoffperoxid |
-
1994
- 1994-05-31 DE DE4418931A patent/DE4418931C2/de not_active Expired - Fee Related
-
1995
- 1995-03-20 US US08/406,519 patent/US5534149A/en not_active Expired - Lifetime
- 1995-05-10 AT AT95107071T patent/ATE162158T1/de not_active IP Right Cessation
- 1995-05-10 EP EP95107071A patent/EP0687649B1/de not_active Expired - Lifetime
- 1995-05-10 ES ES95107071T patent/ES2113692T3/es not_active Expired - Lifetime
- 1995-05-10 DE DE59501253T patent/DE59501253D1/de not_active Expired - Fee Related
- 1995-05-23 JP JP7123866A patent/JPH07330311A/ja active Pending
- 1995-05-29 NZ NZ272235A patent/NZ272235A/en unknown
- 1995-05-29 TW TW084105412A patent/TW287145B/zh active
- 1995-05-30 CA CA002150492A patent/CA2150492C/en not_active Expired - Fee Related
- 1995-05-30 ZA ZA954428A patent/ZA954428B/xx unknown
- 1995-05-30 CN CN95106619A patent/CN1122726A/zh active Pending
- 1995-05-30 IL IL11391595A patent/IL113915A0/xx unknown
- 1995-05-30 FI FI952631A patent/FI114090B/fi not_active IP Right Cessation
- 1995-05-31 BR BR9502610A patent/BR9502610A/pt not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| FI952631L (fi) | 1995-12-01 |
| DE59501253D1 (de) | 1998-02-19 |
| CA2150492C (en) | 2001-01-16 |
| BR9502610A (pt) | 1996-01-02 |
| JPH07330311A (ja) | 1995-12-19 |
| EP0687649A1 (de) | 1995-12-20 |
| ES2113692T3 (es) | 1998-05-01 |
| IL113915A0 (en) | 1995-08-31 |
| ATE162158T1 (de) | 1998-01-15 |
| NZ272235A (en) | 1996-05-28 |
| TW287145B (cg-RX-API-DMAC7.html) | 1996-10-01 |
| ZA954428B (en) | 1996-01-24 |
| CA2150492A1 (en) | 1995-12-01 |
| FI114090B (fi) | 2004-08-13 |
| DE4418931A1 (de) | 1995-12-07 |
| EP0687649B1 (de) | 1998-01-14 |
| US5534149A (en) | 1996-07-09 |
| DE4418931C2 (de) | 1997-06-19 |
| FI952631A0 (fi) | 1995-05-30 |
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