CN112220714A

CN112220714A - Red ginseng vigor activating oxygen eye cream and preparation method thereof

Info

Publication number: CN112220714A
Application number: CN202010954426.6A
Authority: CN
Inventors: 陈娟; 阳综业
Original assignee: Guangzhou Duomei Biotechnology Co ltd
Current assignee: Guangzhou Duomei Biotechnology Co ltd
Priority date: 2020-09-11
Filing date: 2020-09-11
Publication date: 2021-01-15

Abstract

The invention discloses red ginseng vigor activating oxygen eye cream and a preparation method thereof, and the red ginseng vigor activating oxygen eye cream comprises water, methyl propylene glycol, glycerol, hyaluronic acid, EDTA disodium, methyl ester, glyceryl polyether-26, PEG/PPG-17/6 copolymer, red ginseng extract, carnosine, dipalmitoyl hydroxyproline, glyceryl glucoside, chicory tiramer, a compound anti-allergy agent, essence, phenoxyethanol/chlorphenesin and the like. The invention has excellent moisturizing performance, and can effectively fade fine lines and black eye circles.

Description

Red ginseng vigor activating oxygen eye cream and preparation method thereof

Technical Field

The invention relates to the field of eye cream production and preparation, and particularly relates to red ginseng vigor activating oxygen eye cream and a preparation method thereof.

Background

The eye cream is one of skin care cosmetics and has the function of moistening eye skin. The eye mask can reduce the problems of dark circles and under-eye bags, and also has the effect of improving wrinkles and fine lines. The eye cream is used for protecting the thin skin around the eyes, has certain effects on pouches, black eye circles, crow's feet and the like, but different eye creams have different effects and are divided into moisturizing eye cream, firming eye cream, anti-aging eye cream, anti-allergy eye cream and the like in terms of functions.

The existing eye cream has poor moisturizing performance, and has common effects of fading fine lines and fading black eye circles. It is still difficult to meet the requirements of people. In view of the above, the present invention is particularly proposed.

Disclosure of Invention

The invention aims to design red ginseng original qi oxygen activating eye cream and a preparation method thereof, so that the red ginseng original qi oxygen activating eye cream has excellent moisturizing performance, and can effectively lighten fine lines and black eyes.

In order to achieve the purpose, the invention provides the following technical scheme:

red ginseng original qi oxygen activating eye cream is prepared from the following raw materials in percentage by weight:

phase A: water 31.05-68.43%, preferably 64.01%; 4-5%, preferably 4%; 2-5% of glycerol, preferably 2%; hyaluronic acid 0.01-0.05%, preferably 0.02%; disodium EDTA 0.01-0.05%, preferably 0.02%; methyl ester 0.1-0.2%, preferably 0.2%; glyceryl polyether-262-5%, preferably 3%; PEG/PPG-17/6 copolymer 0.5-3%, preferably 1%;

phase B: 2-4% of emulsifier A, preferably 2.5%; 0.5-1% of emulsifier B, preferably 0.5%; beeswax 0.5-1%, preferably 0.8%; GMS 30SE 0.5-1.5%, preferably 1.2%; 0.3-1% of 16\18 alcohol, preferably 0.4%; propyl ester 0.1-0.15%, preferably 0.1%; 0.5-1% of shea butter, preferably 0.5%; 0.5-1% of silicone oil A, preferably 0.5%; 0.5-1%, preferably 0.5%; 3-5%, preferably 3%; 2-5% of macadamia nut oil, preferably 2%; 2-5%, preferably 3%; 2-5% of silicone oil B, preferably 3%;

and C phase: sodium acrylate/sodium acryloyldimethyl taurate copolymer/isohexadecane/polysorbate-801-2%, preferably 1%;

phase D: 0.5-2%, preferably 0.6%; carnosine 0.2-0.5%, preferably 0.2%; dipalmitoyl hydroxyproline 1-3%, preferably 1%; 3-6% of water, preferably 3%;

phase E: 0.5-2% of glycerol glucoside, preferably 0.5%; chicory tiramer 0.5-2%, preferably 0.5%; 0.5-1% of composite anti-allergic agent, preferably 0.5%; 0.05 to 0.1 percent of essence, preferably 0.1 percent; 0.3 to 0.4 percent of phenoxyethanol/chlorphenesin, preferably 0.35 percent.

Further, silicone oil A in phase B is polydimethylsiloxane, silicone oil B is cyclopentadimethylsiloxane/cyclohexasiloxane, beeswax is beeswax 8044, emulsifier A is M68 emulsifier, and emulsifier B is A165 emulsifier.

Further, the water in the A phase and the D phase is deionized water.

The preparation method of the red ginseng vigor activating oxygen eye cream comprises the following steps:

step 1: proportioning raw materials of the phase A, the phase B, the phase C, the phase D and the phase E;

step 2: mixing, dispersing and stirring the phase D raw material uniformly to obtain a solution A;

step 2: putting the phase A raw material into a vacuum homogenizing emulsifying pot, starting stirring at the rotating speed of 60rpm, heating to 85-90 ℃, continuously stirring and preserving heat for 5-8min to obtain a solution B;

and step 3: putting the phase B raw material into an oil phase pot, starting stirring at the rotating speed of 40rpm, heating to 80-85 ℃, continuously stirring and preserving heat for 5-8min to completely dissolve the raw material to obtain a solution C;

and 4, step 4: opening the vacuum homogenizing emulsifying pot in the step 2 to be vacuum, starting stirring, rotating at the speed of 60rpm, pumping the solution C obtained in the step 3 into the vacuum homogenizing emulsifying pot, mixing the solution C with the solution B, opening the vacuum homogenizing emulsifying pot to be homogenized at the speed of 2800rpm, homogenizing for 5min, stirring at the speed of 30rpm, preserving heat, stirring for 8-10min, and then cooling to obtain a solution D;

and 5: cooling the solution D obtained in the step 4 to 60 ℃, adding the phase C raw material into a vacuum homogenizing emulsifying pot, mixing the phase C raw material with the solution D, starting homogenizing at the rotating speed of 2500rpm for 2min, and continuously stirring and cooling to obtain a solution E;

step 6: cooling the solution E obtained in the step 5 to 45 ℃, then adding the solution A and the E-phase raw material obtained in the step 1, and continuously stirring for 20-30min to obtain a solution F:

and 7: and (4) sampling and detecting the solution F obtained in the step (6), and filtering and discharging after the solution F is qualified.

Further, the detection in step 7 includes appearance detection, viscosity detection, pH value detection, heat resistance detection, cold resistance detection and centrifugation detection.

Compared with the prior art, the invention has the beneficial effects that:

the red ginseng is a cooked product of ginseng and has the effects of greatly tonifying primordial qi, recovering pulse, relieving depletion, benefiting qi and controlling blood. In clinic, the red ginseng extract can be applied to improve the related functions of the human body, particularly to regulate blood pressure, resist fatigue, calm the nerves, supplement the brain and the like. From the above-mentioned functions, the health value of red ginseng is very high. Because the red reference ginseng has larger potency of medicine, the warm and dry property is larger, and the dosage is a little less than that of the common ginseng.

In the eye cream production process, based on long-term continuous experimental data, the red ginseng extract is added in a reasonable amount, and the addition amounts of other raw materials are correspondingly and reasonably adjusted. The eye cream has excellent moisturizing performance, and can effectively fade fine lines and black eye circles.

Detailed Description

Examples 1 to 3:

red ginseng original qi oxygen activating eye cream of examples 1-3 was prepared according to the following raw materials in the following table 1 by weight percent, respectively.

Table 1:

wherein, the red ginseng original qi oxygen activating eye cream prepared in the following modes of example 1-3 respectively:

example 1:

step 2: putting the phase A raw material into a vacuum homogenizing emulsifying pot, starting stirring, rotating at the speed of 60rpm, heating to 85 ℃, continuously stirring and preserving heat for 5min to obtain a solution B;

and step 3: putting the phase B raw material into an oil phase pot, starting stirring, rotating at 40rpm, heating to 80 ℃, continuously stirring and preserving heat for 5min to completely dissolve the raw material to obtain a solution C;

and 4, step 4: opening the vacuum homogenizing emulsifying pot in the step 2 to vacuum, starting stirring at a rotating speed of 60rpm, pumping the solution C obtained in the step 3 into the vacuum homogenizing emulsifying pot, mixing the solution C with the solution B, opening the vacuum homogenizing emulsifying pot to homogenize at a rotating speed of 2800rpm for 5min, stirring at a rotating speed of 30rpm, preserving heat, stirring for 8min, and then cooling to obtain a solution D;

step 6: cooling the solution E obtained in the step 5 to 45 ℃, then adding the solution A obtained in the step 1 and the phase E raw material, and continuously stirring for 20min to obtain a solution F:

Example 2:

step 2: putting the phase A raw material into a vacuum homogenizing emulsifying pot, starting stirring, rotating at 60rpm, heating to 88 ℃, continuously stirring, and keeping the temperature for 5-8min to obtain a solution B;

and step 3: putting the phase B raw material into an oil phase pot, starting stirring, rotating speed of 40rpm, heating to 83 ℃, continuously stirring and keeping the temperature for 6min to completely dissolve the raw material to obtain a solution C;

and 4, step 4: opening the vacuum homogenizing emulsifying pot in the step 2 to vacuum, starting stirring at a rotating speed of 60rpm, pumping the solution C obtained in the step 3 into the vacuum homogenizing emulsifying pot, mixing the solution C with the solution B, opening the vacuum homogenizing emulsifying pot to homogenize at a rotating speed of 2800rpm for 5min, stirring at a rotating speed of 30rpm, preserving heat, stirring for 9min, and then cooling to obtain a solution D;

step 6: cooling the solution E obtained in the step 5 to 45 ℃, then adding the solution A obtained in the step 1 and the phase E raw material, and continuously stirring for 25min to obtain a solution F:

Example 3:

step 2: putting the phase A raw material into a vacuum homogenizing emulsifying pot, starting stirring, rotating at the speed of 60rpm, heating to 90 ℃, continuously stirring and preserving heat for 8min to obtain a solution B;

and step 3: putting the phase B raw material into an oil phase pot, starting stirring at the rotating speed of 40rpm, heating to 85 ℃, continuously stirring and preserving heat for 8min to completely dissolve the raw material to obtain a solution C;

and 4, step 4: opening the vacuum homogenizing emulsifying pot in the step 2 to vacuum, starting stirring at a rotating speed of 60rpm, pumping the solution C obtained in the step 3 into the vacuum homogenizing emulsifying pot, mixing the solution C with the solution B, opening the vacuum homogenizing emulsifying pot to homogenize at a rotating speed of 2800rpm for 5min, stirring at a rotating speed of 30rpm, keeping the temperature and stirring for 8-10min, and then, starting cooling to obtain a solution D;

step 6: cooling the solution E obtained in the step 5 to 45 ℃, then adding the solution A and the E-phase raw material obtained in the step 1, and continuously stirring for 30min to obtain a solution F:

Experimental example 1:

the red ginseng original qi activating oxygen eye cream products prepared in examples 1-3 were tested and compared. The detection items comprise appearance detection, viscosity detection, pH value detection, heat resistance detection, cold resistance detection and centrifugation detection. The detection results are shown in table 2:

wherein, the appearance detection detects whether the product appearance is white paste or not; detecting whether the viscosity of the product meets 60000 +/-1000 by viscosity detection; detecting whether the pH value of the product meets 7.2 +/-0.5 by pH value detection; the heat resistance detection detects that the product is put into a constant temperature box at 40 +/-1 ℃ for 24H, then is taken out and recovered to room temperature, and is compared with a standard sample to observe whether the material body is not obviously different; cold resistance detection is carried out to detect whether the product is placed in a refrigerator for 24H at minus 8 +/-2 ℃, then the product is taken out and recovered to room temperature, and the room temperature is compared with a standard sample, and whether the material body is not obviously different is observed; centrifugal test the product was spun in a centrifuge at 2000rpm for 30min and observed for lack of stratification.

TABLE 2

Detecting items	Example 1	Example 2	Example 3
				Appearance detection	Qualified	Qualified	Qualified
Viscosity detection	Qualified	Qualified	Qualified
				pH value detection	Qualified	Qualified	Qualified
Heat resistance detection	Qualified	Qualified	Qualified
				Cold resistance detection	Qualified	Qualified	Qualified
Centrifugal assay	Qualified	Qualified	Qualified

As can be seen from Table 1, examples 1-3 all satisfied the test requirements, and it was confirmed that the formulation and the preparation method of the present invention both satisfied the product requirements.

Experimental example 2:

the red ginseng original oxygen-activating eye cream prepared in example 1 was subjected to a skin elasticity index test. The experimental conditions are as follows: 40 women, age 30-50 years old, volunteers. The experimental steps are as follows: the skin elasticity CotomerMPA 580 host manufactured by Courage + Khazaka, Germany, was used as a probe for a Reviscometer RV600 elasto-fibrous tissue test probe, and the average was taken five times. Test area: the skin around the eyes. Blank values (R2, R5, R7) of 20min after cleaning of the tested area are measured, and then the tested area is provided with skin elasticity indexes R2, R5 and R7 values (the negative pressure is constant at 450mbar in the test process) after the tested area is subjected to the test article by the subjects for keeping the test articles in use for 1 week, 2 weeks, 3 weeks and 4 weeks every day.

Specification of indexes: the closer the skin elasticity indexes R2, R5, R7 are to 1, the better the elasticity of the skin.

R2＝Ua/Uf；R5＝Ur/Ue；R7＝Ur/Uf

Uf — maximum skin stretch;

ue — the amount of stretching of the skin at 0.1 second after constant negative pressure is applied to the skin, the amount of stretching of the elastic portion is located;

ur-after negative pressure is eliminated, the skin can quickly recover to the original state, and the skin is also divided into an elastic part value Ur, namely, after the negative pressure is eliminated for 0.1 second, the recovery value and the viscoelastic part value, or called as a plastic part value, of the skin;

ua-the recovery value of the skin from the elimination of the negative pressure to the next successive test of the skin surface plus the negative pressure.

The results are shown in Table 3

Experimental period	R2	R5	R7
				0	0.4287	0.4063	0.4573
1	0.6345	0.5883	0.6032
				2	0.7231	0.6632	0.7678
3	0.8502	0.8096	0.8512
				4	0.9231	0.9053	0.9131

As can be seen from table 3, R2, R5, and R7 increased after the first week using the red ginseng original oxygen-activating eye cream prepared in example 1, wherein the values of R2, R5, and R7 approached 1 at week 4, and the skin elasticity index of the subject was greatly improved, and thus, the red ginseng original oxygen-activating eye cream has the effects of increasing skin elasticity and anti-aging.

Experimental example 3:

the eye cream products produced in the early stage of the department are taken as comparative examples, and the red ginseng vigor activating oxygen eye cream products prepared in the examples 1 to 3 and the comparative examples are compared in clinical experiments. The test conditions were: 50 women aged 35-50, 2 times per day, were applied evenly around the eyes, and the skin was recommended to be cleaned and then used for 30 days. The volunteers who felt improved in moisturizing, lightening fine lines and lightening dark circles after the end of the test were compared to, for example, table 4:

table 4:

test items	Example 1	Example 2	Example 3	Comparative example
					Moisture retention and water retention	80％	82％	88％	60％
Thin lines of desalination	84％	78％	90％	56％
					Fading black eye	82％	84％	88％	56％

As can be seen from table 4, compared with the existing products, the red ginseng primordial qi activating oxygen eye cream in the embodiments 1 to 3 of the present invention is successfully qualified in the test items, and the high quality eye cream is realized. Meanwhile, in test items, the effects of moisture retention, fine line fading and dark eye circle fading shown in the examples 1 to 3 of the invention are superior to those of the existing eye cream, and the combined action of the red ginseng and other raw materials is fully exerted. Among them, the best effect is obtained in example 3.

Claims

1. Red ginseng original qi oxygen activating eye cream is characterized in that: the material is prepared from the following raw materials in percentage by weight:

phase A: 31.05-68.43% of water, 4-5% of methyl propylene glycol, 2-5% of glycerol, 0.01-0.05% of hyaluronic acid, 0.01-0.05% of EDTA disodium and 0.1-0.2% of methyl ester; glyceryl polyether-262-5%, PEG/PPG-17/6 copolymer 0.5-3%;

phase B: 2-4% of emulsifier A, 0.5-1% of emulsifier B, 0.5-1% of beeswax, 0.5-1.5% of GMS 30SE, 0.3-1% of 16\18 alcohol, 0.1-0.15% of propyl ester, 0.5-1% of shea butter, 0.5-1% of silicone oil A, 0.5-1% of vitamin E, 3-5% of hydrogenated polydecene, 2-5% of macadamia nut oil, 2-5% of octyldodecanol and 2-5% of silicone oil B;

and C phase: sodium acrylate/sodium acryloyldimethyl taurate copolymer/isohexadecane/polysorbate-801-2%;

phase D: 0.5-2% of red ginseng extract, 0.2-0.5% of carnosine, 1-3% of dipalmitoyl hydroxyproline and 3-6% of water;

phase E: 0.5-2% of glyceryl glucoside, 0.5-2% of chicory tilianin, 0.5-1% of compound anti-allergy agent, 0.05-0.1% of essence and 0.3-0.4% of phenoxyethanol/chlorphenesin.

2. The red ginseng vigor activating oxygen eye cream according to claim 1, wherein: the material is prepared from the following raw materials in percentage by weight:

phase A: 64.01 percent of water, 4 percent of methyl propylene glycol, 2 percent of glycerol, 0.02 percent of hyaluronic acid, 0.02 percent of EDTA disodium and 0.2 percent of methyl ester; glyceryl polyether-263%, PEG/PPG-17/6 copolymer 1%;

phase B: 2.5% of emulsifier A, 0.5% of emulsifier B, 0.8% of beeswax, 1.2% of GMS 30SE, 0.4% of 16\18 alcohol, 0.1% of propyl ester, 0.5% of shea butter, 0.5% of silicone oil A, 0.5% of vitamin E, 3% of hydrogenated polydecene, 2% of macadamia nut oil, 3% of octyldodecanol and 3% of silicone oil B;

and C phase: sodium acrylate/sodium acryloyldimethyl taurate copolymer/isohexadecane/polysorbate-801%;

phase D: 0.6% of red ginseng extract, 0.2% of carnosine, 1% of dipalmitoyl hydroxyproline and 3% of water;

phase E: 0.5 percent of glycerin glucoside, 0.5 percent of chicory tiraparin, 0.5 percent of composite anti-allergy agent, 0.1 percent of essence and 0.35 percent of phenoxyethanol/chlorphenesin.

3. The red ginseng vigor activating oxygen eye cream according to claim 1, wherein: and the silicone oil A in the phase B is polydimethylsiloxane, and the silicone oil B is cyclopenta polydimethylsiloxane/cyclohexasiloxane.

4. The red ginseng vigor activating oxygen eye cream according to claim 1, wherein: beeswax in phase B was beeswax 8044.

5. The red ginseng vigor activating oxygen eye cream according to claim 1, wherein: emulsifier A in phase B is M68 emulsifier, and emulsifier B is A165 emulsifier.

6. The red ginseng vigor activating oxygen eye cream according to claim 1, wherein: the water in phase A and phase D is deionized water.

7. The method for preparing red ginseng vigor activating oxygen eye cream according to any one of claims 1 to 6, comprising the steps of:

8. The method for preparing the vigor-activating and oxygen-activating eye cream according to claim 7, wherein the detection in the step 7 comprises appearance detection, viscosity detection, pH value detection, heat resistance detection, cold resistance detection and centrifugation detection.