CN111617014A - Centipeda minima mask with whitening and relieving effects and preparation method thereof - Google Patents

Centipeda minima mask with whitening and relieving effects and preparation method thereof Download PDF

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Publication number
CN111617014A
CN111617014A CN202010487234.9A CN202010487234A CN111617014A CN 111617014 A CN111617014 A CN 111617014A CN 202010487234 A CN202010487234 A CN 202010487234A CN 111617014 A CN111617014 A CN 111617014A
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extract
percent
mask
facial mask
whitening
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黄超伯
李芳华
周阿影
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Nanjing Forestry University
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783—Angiosperms [Magnoliophyta]
    • A61K8/9794—Liliopsida [monocotyledons]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0212—Face masks
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
    • A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67—Vitamins
    • A61K8/673—Vitamin B group
    • A61K8/675—Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/08—Anti-ageing preparations
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/74—Biological properties of particular ingredients
    • A61K2800/78—Enzyme modulators, e.g. Enzyme agonists
    • A61K2800/782—Enzyme inhibitors; Enzyme antagonists

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Abstract

The invention relates to the field of cosmetics, and particularly relates to a mask with whitening and relieving effects and a preparation method thereof. The facial mask comprises facial mask liquid and facial mask cloth, wherein the facial mask liquid comprises centipeda minima extract, rhizoma bolbostemmae extract, purslane extract, glycerol, propylene glycol, sodium hyaluronate, trehalose, nicotinamide, allantoin, glabridin, 1, 3-butanediol, PEG-40 hydrogenated castor oil, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, triethanolamine, xanthan gum, essence, methyl hydroxybenzoate, propyl hydroxybenzoate, EDTA-2Na and purified water. The whitening cream is particularly suitable for sensitive skin, can play an effective whitening role, and is also suitable for other various skins.

Description

Centipeda minima mask with whitening and relieving effects and preparation method thereof
Technical Field
The invention relates to the field of cosmetics, and particularly relates to a centipeda minima mask with whitening and relieving effects and a preparation method thereof.
Background
The facial mask is an instant skin care product, and the condition of the skin can be improved by naked eyes when the facial mask is used, so the facial mask is a necessary skin care product for many women loving beauty.
In a common saying, "one white hides ugly", whitening is the skin care effect that many modern women pursue. Whether the skin is fair depends on the content and distribution of melanin, and the formation of melanin is complicated and is associated with various enzymes. Tyrosine present in melanocytes undergoes a series of oxidation reactions under the action of various enzymes to finally form melanin.
The plants are rich in flavonoid, organic acid, polyphenol and other substances, and the substances are proved to have certain whitening effect. The plant extract with the whitening effect is added into the facial mask, and other safe and effective whitening and relieving components are added, so that the advantages of the plant extract and the facial mask can be fully exerted, and better skin care experience is brought to people.
Modern people have great living pressure and irregular life, and the skin is sensitive easily because more and more skin care products in different shapes and colors are used. By adding the soothing component and the whitening component into the mask, the basic moisturizing effect of the mask can be ensured, and more secure whitening can be provided for sensitive skin.
Disclosure of Invention
The invention aims to provide a mask with whitening and relieving effects and a preparation method thereof.
The mask with the whitening and relieving effects comprises mask liquid and mask cloth, wherein the mask liquid comprises the following components in parts by weight:
1 to 5 percent of centipeda minima extract, 1 to 5 percent of rhizoma bolbostemmae extract, 1 to 6 percent of purslane extract, 1 to 10 percent of glycerin, 1 to 5 percent of propylene glycol, 0.01 to 0.1 percent of sodium hyaluronate, 0.5 to 5 percent of trehalose, 0.5 to 3 percent of nicotinamide, 0.1 to 1 percent of allantoin, 0.1 to 1 percent of glabridin, 1 to 5 percent of 1, 3-butanediol, 0.1 to 1 percent of PEG-40 hydrogenated castor oil, 0.1 to 1 percent of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.1 to 1 percent of triethanolamine, 0.1 to 1 percent of xanthan gum, 0.01 to 0.5 percent of essence, 0.05 to 1 percent of methyl hydroxybenzoate, 0.05 to 1 percent of propyl hydroxybenzoate, 0.01 to 0.1 percent of EDTA-2Na and purified water which are added to 100 percent.
Preferably, the facial mask liquid comprises, by weight, 1% -3% of centipeda minima extract, 1% -2% of rhizoma bolbostemmae extract, 1% -3% of purslane extract, 2% -6% of glycerol, 2% -4% of propylene glycol, 0.01% -0.05% of sodium hyaluronate, 1% -3% of trehalose, 1% -3% of nicotinamide, 0.15% -0.3% of allantoin, 0.2% -0.7% of glabridin, 2% -4% of 1, 3-butanediol, 0.1% -0.3% of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.1% -0.3% of triethanolamine, 0.1% -0.3% of xanthan gum, 0.1% -0.5% of PEG-40 hydrogenated castor oil, 0.01% -0.1% of essence, 0.05% -0.5% of methylparaben, 0.05% -0.5% of hydroxyphenyl ether, 0.05% -0.5% of sodium alginate, 0.01% -2% of EDTA-2.05% -2% of Na, purified water is made up to 100%.
The mask cloth is biological fiber or tencel mask cloth.
The invention relates to a mask with whitening and relieving effects, which is characterized in that: the preparation method of the facial mask comprises the following steps:
the method comprises the following steps: uniformly spreading acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer on a purified water surface, fully soaking, and stirring for 15 minutes until uniform;
step two: mixing glycerol, trehalose, xanthan gum, 1, 3-butanediol, propylene glycol, sodium hyaluronate, nicotinamide, allantoin, glabridin, centipeda minima extract, rhizoma bolbostemmae extract, purslane extract, methyl hydroxybenzoate, propyl hydroxybenzoate and a proper amount of purified water, adding the mixture obtained in the step one, and stirring at 85 ℃ to obtain a uniform mixture;
step three: cooling the mixture obtained in the second step to 40 ℃, adding triethanolamine and EDTA-2Na, and uniformly stirring;
step four: cooling the mixture obtained in the step three to room temperature, adding essence and PEG-40 hydrogenated castor oil, and stirring uniformly to obtain a finished product;
step five: and (4) inspecting the physical and chemical indexes of the product, discharging after the product is qualified, inspecting, and filling into a mask bag filled with mask cloth after each index is qualified.
The centipeda minima is widely distributed in China and has a long use history, and the existing research shows that the centipeda minima is rich in volatile oil, terpenoids, polyphenols, organic acid and other components, and the components and the content of the centipeda minima in different growth environments are different. Rich bioactive components, and has antiinflammatory, antibacterial, antiallergic, antiasthmatic, and neuroprotective effects.
The rhizoma bolbostemmae is a widely applied traditional Chinese medicine, belongs to the cucurbitaceae family, and roots and stems of the rhizoma bolbostemmae can be used as a medicine, and the existing research shows that the rhizoma bolbostemmae contains rich bioactive substances and has the effects of resisting inflammation, resisting tumors and the like. The experimental results prove that the rhizoma bolbostemmae extract also has a certain antioxidant effect.
Niacinamide, a member of B vitamins, is also called niacinamide, is an amide compound of niacin, is a common whitening functional ingredient, and can slow down the formation of melanin in various ways.
The ingredients such as the centipeda minima extract and the nicotinamide with the whitening effect and the ingredients such as the allantoin and the purslane extract with the soothing effect are added together through a proper process, so that the mask has the whitening and soothing effects at the same time, and the skin whitening effect is realized under the condition that the skin is not stimulated as far as possible.
Drawings
FIG. 1 is a graph showing the inhibitory effect of centipeda minima extract on tyrosinase.
FIG. 2 shows the effect of Bolbostemma paniculatum extract on scavenging DPPH free radicals.
Detailed Description
The present invention is further illustrated by the following examples, which are not intended to limit the invention in any way.
Example 1:
the invention provides a composition of a facial mask with whitening and relieving effects, which comprises facial mask cloth and facial mask liquid, wherein the facial mask cloth is biological fiber facial mask cloth, and the facial mask liquid comprises:
centipeda minima extract: 3 percent of
The rhizoma bolbostemmae extract: 1 percent of
And (3) purslane extract: 2 percent of
Glycerol: 4 percent of
Propylene glycol: 2 percent of
Sodium hyaluronate: 0.04 percent
Trehalose: 1 percent of
Nicotinamide: 1 percent of
Allantoin: 0.5 percent
Glabridin: 0.5 percent
1, 3-butanediol: 3 percent of
acrylic/C10-30 alkanol acrylate crosspolymer: 0.17 percent
Triethanolamine: 0.17 percent
Xanthan gum: 0.13 percent
PEG-40 hydrogenated castor oil: 0.25 percent
0.05 percent of essence
Methyl hydroxybenzoate: 0.2 percent of
Propyl hydroxybenzoate: 0.3 percent of
EDTA-2Na：0.02％
A preparation method of a mask with whitening and relieving effects is characterized by comprising the following steps:
the method comprises the following steps: uniformly spreading acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer on a purified water surface, fully soaking, and stirring for 15 minutes until uniform;
step two: mixing glycerol, trehalose, xanthan gum, 1, 3-butanediol, propylene glycol, sodium hyaluronate, nicotinamide, allantoin, glabridin, centipeda minima extract, rhizoma bolbostemmae extract, purslane extract, methyl hydroxybenzoate, propyl hydroxybenzoate and a proper amount of purified water, adding the mixture obtained in the step one, and stirring at 85 ℃ to obtain a uniform mixture;
step three: cooling the mixture obtained in the second step to 40 ℃, adding triethanolamine and EDTA-2Na, and uniformly stirring;
step four: cooling the mixture obtained in the step three to room temperature, adding essence and PEG-40 hydrogenated castor oil, and stirring uniformly to obtain a finished product;
step five: and (4) inspecting the physical and chemical indexes of the product, discharging after the product is qualified, inspecting, and filling into a mask bag filled with mask cloth after each index is qualified.
Example 2:
the invention provides a composition of a facial mask with whitening and relieving effects, which comprises facial mask cloth and facial mask liquid, wherein the facial mask cloth is biological fiber facial mask cloth, and the facial mask liquid comprises:
centipeda minima extract: 2 percent of
The rhizoma bolbostemmae extract: 1 percent of
And (3) purslane extract: 3 percent of
Glycerol: 3 percent of
Propylene glycol: 2 percent of
Sodium hyaluronate: 0.04 percent
Trehalose: 1 percent of
Nicotinamide: 2 percent of
Allantoin: 0.5 percent
Glabridin: 0.5 percent
1, 3-butanediol: 3 percent of
acrylic/C10-30 alkanol acrylate crosspolymer: 0.17 percent
Triethanolamine: 0.17 percent
Xanthan gum: 0.13 percent
PEG-40 hydrogenated castor oil: 0.25 percent
0.05 percent of essence
Methyl hydroxybenzoate: 0.2 percent of
Propyl hydroxybenzoate: 0.3 percent of
EDTA-2Na：0.02％
A preparation method of a mask with whitening and relieving effects is characterized by comprising the following steps:
the method comprises the following steps: uniformly spreading acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer on a purified water surface, fully soaking, and stirring for 15 minutes until uniform;
step two: mixing glycerol, trehalose, xanthan gum, 1, 3-butanediol, propylene glycol, sodium hyaluronate, nicotinamide, allantoin, glabridin, centipeda minima extract, rhizoma bolbostemmae extract, purslane extract, methyl hydroxybenzoate, propyl hydroxybenzoate and a proper amount of purified water, adding the mixture obtained in the step one, and stirring at 85 ℃ to obtain a uniform mixture;
step three: cooling the mixture obtained in the second step to 40 ℃, adding triethanolamine and EDTA-2Na, and uniformly stirring;
step four: cooling the mixture obtained in the step three to room temperature, adding essence and PEG-40 hydrogenated castor oil, and stirring uniformly to obtain a finished product;
step five: and (4) inspecting the physical and chemical indexes of the product, discharging after the product is qualified, inspecting, and filling into a mask bag filled with mask cloth after each index is qualified.
Example 3:
the invention provides a composition of a facial mask with whitening and relieving effects, which comprises facial mask cloth and facial mask liquid, wherein the facial mask cloth is biological fiber facial mask cloth, and the facial mask liquid comprises:
centipeda minima extract: 4 percent of
The rhizoma bolbostemmae extract: 2 percent of
And (3) purslane extract: 3 percent of
Glycerol: 3 percent of
Propylene glycol: 1 percent of
Sodium hyaluronate: 0.04 percent
Trehalose: 1 percent of
Nicotinamide: 2 percent of
Allantoin: 0.3 percent of
Glabridin: 0.5 percent
1, 3-butanediol: 2 percent of
acrylic/C10-30 alkanol acrylate crosspolymer: 0.15 percent
Triethanolamine: 0.15 percent
Xanthan gum: 0.15 percent
PEG-40 hydrogenated castor oil: 0.25 percent
0.05 percent of essence
Methyl hydroxybenzoate: 0.2 percent of
Propyl hydroxybenzoate: 0.3 percent of
EDTA-2Na：0.02％
A preparation method of a mask with whitening and relieving effects is characterized by comprising the following steps:
the method comprises the following steps: uniformly spreading acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer on a purified water surface, fully soaking, and stirring for 15 minutes until uniform;
step two: mixing glycerol, trehalose, xanthan gum, 1, 3-butanediol, propylene glycol, sodium hyaluronate, nicotinamide, allantoin, glabridin, centipeda minima extract, rhizoma bolbostemmae extract, purslane extract, methyl hydroxybenzoate, propyl hydroxybenzoate and a proper amount of purified water, adding the mixture obtained in the step one, and stirring at 85 ℃ to obtain a uniform mixture;
step three: cooling the mixture obtained in the second step to 40 ℃, adding triethanolamine and EDTA-2Na, and uniformly stirring;
step four: cooling the mixture obtained in the step three to room temperature, adding essence and PEG-40 hydrogenated castor oil, and stirring uniformly to obtain a finished product;
step five: and (4) inspecting the physical and chemical indexes of the product, discharging after the product is qualified, inspecting, and filling into a mask bag filled with mask cloth after each index is qualified.
Example 4: test of whitening Effect
1) Tyrosinase is an enzyme involved in melanin formation, and inhibition of tyrosinase activity can inhibit melanin formation to some extent.
And (3) determining the in-vitro tyrosinase activity of the centipeda minima extract by adopting a tyrosinase dopa rate oxidation method. Sequentially adding PBS, herba Centipedae extract solution and tyrosinase into a centrifuge tube, heating at 37 deg.C for 10min, adding L-dopa solution (0.98g/L), measuring absorbance at 475nm after 3min, respectively adding required reagents as shown in Table 1, wherein the absorbance is A1，A2，A3And A4。
Tyrosinase activity inhibition rate [ [ (A)1-A2)-(A3-A4)]/(A1-A2)×100％
TABLE 1
Figure BSA0000210247880000071
Figure BSA0000210247880000081
The experimental result is shown in fig. 1, and it can be seen that centipeda minima has a certain inhibition effect on tyrosinase activity, and the higher the concentration is, the stronger the activity inhibition effect is, so that the whitening effect can be exerted by adding the centipeda minima into the facial mask.
2) The DPPH free radical scavenging effect can reflect the quality of the antioxidant capacity of the sample, and the antioxidant effect also influences the skin condition to a certain extent.
Measuring DPPH free radical scavenging rate of rhizoma Bolbostematis extract, mixing the sample solution and DPPH free radical solution uniformly, measuring absorbance A of the solution at 517nm1And deionized water is adopted to replace the sample solution as a blank control A2Mixing the sample solution with absolute ethyl alcohol, and recording the absorbance as A3。
DPPH radical scavenging ratio (A)2+A3-A1)/A2×100％
The experimental results are shown in figure 2, and the results show that the rhizoma bolbostemmae has good antioxidant effect and can play a certain antioxidant effect when being added into cosmetics.
The above description is only a preferred embodiment of the present invention, and the present invention is not limited to the above embodiments, and other modifications and variations directly derived by those skilled in the art without departing from the spirit and concept of the present invention should be considered as not departing from the protection scope of the present invention.

Claims (4)

1. A facial mask with skin whitening and relieving effects comprises facial mask solution and facial mask cloth.
2. The mask liquid as claimed in claim 1, wherein the mask liquid comprises, by weight, 1% to 5% of centipeda minima extract, 1% to 5% of rhizoma bolbostemmae extract, 1% to 6% of purslane extract, 1% to 10% of glycerol, 1% to 5% of propylene glycol, 0.01% to 0.1% of sodium hyaluronate, 0.5% to 5% of trehalose, 0.5% to 3% of niacinamide, 0.1% to 1% of allantoin, 0.1% to 1% of glabridin, 1% to 5% of 1, 3-butanediol, 0.1% to 1% of PEG-40 hydrogenated castor oil, 0.1% to 1% of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.1% to 1% of triethanolamine, 0.1% to 1% of xanthan gum, 0.01% to 0.5% of essence, 0.05% to 1% of methylparaben, 0.05% to 1% of propylparaben, 0.01 to 0.1 percent of EDTA-2Na and purified water to 100 percent.
3. The mask pack according to claim 2, wherein the mask solution comprises, by weight, 1% to 3% of centipeda minima extract, 1% to 2% of rhizoma bolbostemmae extract, 1% to 3% of purslane extract, 2% to 6% of glycerol, 2% to 4% of propylene glycol, 0.01% to 0.05% of sodium hyaluronate, 1% to 3% of trehalose, 1% to 3% of niacinamide, 0.15% to 0.3% of allantoin, 0.2% to 0.7% of glabridin, 2% to 4% of 1, 3-butylene glycol, 0.1% to 0.3% of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.1% to 0.3% of triethanolamine, 0.1% to 0.3% of xanthan gum, 0.1% to 0.5% of PEG-40 hydrogenated castor oil, 0.01% to 0.1% of essence, 0.05% to 0.5% of methylparaben, 0.05% of propylparaben, 0.01 to 0.05 percent of EDTA-2Na and purified water to 100 percent.
4. The mask according to claim 2, wherein the preparation method comprises the steps of:
the method comprises the following steps: uniformly spreading acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer on a purified water surface, fully soaking, and stirring for 15 minutes until uniform;
step two: mixing glycerol, trehalose, xanthan gum, 1, 3-butanediol, propylene glycol, sodium hyaluronate, nicotinamide, allantoin, glabridin, centipeda minima extract, rhizoma bolbostemmae extract, purslane extract, methyl hydroxybenzoate, propyl hydroxybenzoate and a proper amount of purified water, adding the mixture obtained in the step one, and stirring at 85 ℃ to obtain a uniform mixture;
step three: cooling the mixture obtained in the step two to about 40 ℃, adding triethanolamine and EDTA-2Na, and uniformly stirring;
step four: cooling the mixture obtained in the step three to room temperature, adding essence and PEG-40 hydrogenated castor oil, and stirring uniformly to obtain a finished product;
step five: and (4) inspecting the physical and chemical indexes of the product, discharging after the product is qualified, inspecting, and filling into a mask bag filled with mask cloth after each index is qualified.
CN202010487234.9A 2020-06-01 2020-06-01 Centipeda minima mask with whitening and relieving effects and preparation method thereof Pending CN111617014A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112057382A (en) * 2020-09-24 2020-12-11 福建拓烯新材料科技有限公司 Folium mori spot-fading essence and preparation method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112057382A (en) * 2020-09-24 2020-12-11 福建拓烯新材料科技有限公司 Folium mori spot-fading essence and preparation method thereof

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