CN108210421A - A kind of whitening mask liquid of the extract containing Magnolia binodii and preparation method thereof - Google Patents
A kind of whitening mask liquid of the extract containing Magnolia binodii and preparation method thereof Download PDFInfo
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- CN108210421A CN108210421A CN201810249996.8A CN201810249996A CN108210421A CN 108210421 A CN108210421 A CN 108210421A CN 201810249996 A CN201810249996 A CN 201810249996A CN 108210421 A CN108210421 A CN 108210421A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
- A61K8/675—Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/74—Biological properties of particular ingredients
- A61K2800/78—Enzyme modulators, e.g. Enzyme agonists
- A61K2800/782—Enzyme inhibitors; Enzyme antagonists
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
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Abstract
The present invention discloses a kind of whitening mask liquid of extract containing Magnolia binodii, including component A, B component, component C, D components, component E and F components；The preparation method of the facial mask liquid includes the component A for 1) weighing formula ratio, and input is emulsified in pot, is heated with stirring to 80 85 DEG C, makes its dissolving complete, starts to cool down after keeping the temperature 10 20min；2) after being cooled to 50 DEG C, the B component of formula ratio is sequentially added, is stirred evenly, continue to cool down；3) when temperature drops to 45 DEG C, the C, D being pre-mixed, component E is added in, is stirred evenly；4) F phases are eventually adding, adjust pH；5) continue to cool down, when temperature is dropped to below 40 DEG C, filtering and discharging.Effective active composition in Magnolia binodii bud/spend as whitening agent, by ultrasonic extraction is extracted using the extract of the traditional Chinese medicine flower bud of lily magnolia, avoids destroying its activity whitening composition under high temperature, whitening effect is more notable by the facial mask liquid of the present invention at a lower temperature.
Description
Technical field
Whitening mask liquid the present invention relates to a kind of extract containing Magnolia binodii and preparation method thereof belongs to cosmetic art neck
Domain.
Background technology
Facial mask is an important class in cosmetics and skincare product, and very big market ratio is occupied in skin care field, wherein,
Mask product (abbreviation mask) loosens body compared to other functional cosmetics due to that can be brought when in use to consumer
The heart, pleasant comfortable experience are enjoyed, and therefore, the usage amount bigger of mask is most important product type in facial mask category.Face
The principle of film exactly using the of short duration time for being covered in face, is temporarily isolating extraneous air and pollution, improves skin temperature,
So that skin pore expansion, promotes sweat gland secretion and metabolism, the oxygen content of skin is made to increase, be conducive to skin and exclude epidermis
The product of cell metabolism and the oil substances of accumulation, the moisture in facial mask penetrate into the cuticula of epidermis, and skin becomes
Softness, skin are naturally bright flexible.
Flos micheliae Albae also known as Magnolia binodii, the dry flower also known as the flower bud of lily magnolia of the plant Magnolia binodii of Magnoliaceae, main product is in Henan, peace
The provinces such as emblem, Hubei, Sichuan, Shaanxi.Magnolia binodii bud contains volatile oil, and Magnolin, α-bornene, Cineole etc. are contained in oil, and
Containing alkaloid, lignanoid；Yulan bud contains volatile oil, in oil containing citral, Eugenol, Cineole alkaloid etc. naturally into
Point, skin condition can be improved, Zhang Huajian is sent out when studying 10 taste Chinese medicines involved in " the seven white cream " in different documents
It is existing, the flower bud of lily magnolia be in these medicinal materials to melanocyte proliferation inhibiting effect the most it will be evident that the generation of melanin can be reduced simultaneously,
Also have effects that oxidation resistant.
At present, there is Chinese patent " a kind of facial mask liquid " (application No. is 201611209696.4), component and raw material weight
Percentage is：Carbomer 0.1~1%, 1,3-BDO 0.1~5%, methyl hydroxybenzoate 0.01~2%, hyaluronic acid 0.01~
3%th, pyridine-3-carboxamide 0.5~15%, trimethylglycine 0.01~5%, triethanolamine 0.01~3%, dipotassium glycyrrhizinate
0.01~6%, Phenoxyethanol 0.01~8%, balance deionized water are solvent.
Separately have, Chinese patent " a kind of whitening mask liquid " (application No. is 201610112756.4), the weight proportion of ingredient
Including：6-8 parts of vitamin C, white 1-3 parts of U.S.'s drawing, 1-3 parts of Arbutin, 1-2 parts of licorice, 1-2 parts of mulberries extract, rose
Rare essential oil 1-2 parts, 1-2 parts of orange essential oil, 0.1-1 parts of Astragalus Root P.E, 50 parts of mineral water.
In addition, Chinese patent " whitening moisturizing face masque liquid and preparation method thereof " (application No. is 201610678542.3), institute
Facial mask liquid is stated to be process by following raw materials according：30-40 parts of sea cucumber intestine extract, 8-12 parts of asparagus juice, 1-3 parts of egg white, reduced form
1-5 parts of glutathione, 0.8-1.2 parts of hydrolyzed pearl, 2-8 parts of hyaluronic acid, 20-30 parts of honey, 50-80 parts of deionized water, sea
The preparation of ginseng intestines extract includes the following steps：(1) sea cucumber intestine pre-processes；(2) homogeneous of sea cucumber intestine；(3) primary enzymolysis；(4)
Secondary enzymolysis；(5) ultrafiltration；(6) nanofiltration；(7) it is concentrated and dried.
It is poor to the whitening effect of skin in existing facial mask liquid, while cannot effectively meet people to natural, healthy shield
The demand of skin product.
Invention content
In view of the above existing problems in the prior art, the present invention provides a kind of extract containing Magnolia binodii whitening mask liquid and
Preparation method can meet the needs of people are to skin whitening, natural, healthy skin care item.
To achieve these goals, the whitening mask liquid of a kind of extract containing Magnolia binodii that the present invention uses, by weight
Meter, the facial mask liquid specifically include following components,
Component A：0.1-1 parts of thickener, 1-15 parts of polyalcohol, 0.01-0.5 parts of allantoin, 0.01-2 parts of ethoxy urea are gone
60-80 parts of ionized water；
B component：0.1-1 parts of Magnolia binodii extract, 0.05-1 parts of carbohydrate isomer, 0.1-5 parts of water-soluble grease, tooth
0.01-1 parts of leaf olibanum resin extract, 0.01-1 parts of Gotu Kola P.E, trimethylpentanediol/adipic acid/glycerine crosslinking are poly-
0.1-2 parts of object of conjunction, 0.1-1 parts of preservative, 0.1-1 parts of panthenol, 0.01-1 parts of high mountain plant extraction, 0.01-1 parts of peony extract,
0.01-1 parts of bermuda lily flower extract, 0.01-1 parts of white pond lily flower extract, 0.01-1 parts of dried tremella extract；
Component C：0.05-5 parts of niacinamide, 0.1-2 parts of ursin, 5 parts of deionized water；
D components：0.01-0.5 parts of macromolecule moisturizer, 2 parts of propylene glycol, 5 parts of deionized water；
Component E：0.001 part of essence, 0.01 part of essence solubilizer；
F components：0.01-0.2 parts of triethanolamine.
Thickener is using carbomer, hydroxyethyl cellulose, xanthans, one kind in Scleroglucan or more in the component A
Kind mixing.Polyalcohol uses the mixing of glycerine, propylene glycol, butanediol in the component A, and glycerine, propylene glycol, butanediol is mixed
Composition and division in a proportion example is 1:1:1.
Magnolia binodii extract in the B component is Magnolia binodii bud/flower extract, by ultrasonic wave extraction, is specifically carried
Take step as follows：First Magnolia binodii bud/flower is ground, according to 1:20 solid-liquid ratio is added in presses body by deionized water and ethyl alcohol
Product is than (2-3):The mixed solution of 1 composition, then puts it into the container that inner wall is ceramic material, carries out ultrasound bath and adds
Thermal extraction, 50 DEG C of bath temperature, ultrasonic time 1 hour is to get Magnolia binodii bud/flower extract.
Carbohydrate isomer ingredient in the B component is psicose, glucose, mannose, fructose, galactolipin
Mixture.
Water-soluble grease in the B component is using PEG-12 Dimethicone Crosspolymers, double-PEG-15 first
One or more mixing in base ether dimethyl silicone polymer, PEG-7 glyceryl cocoates.
Preservative is using Phenoxyethanol, Sensiva SC50, parahydroxyacet-ophenone, methyl hydroxybenzoate, oxybenzene in the B component
One or more mixing in propyl ester, Bis(hydroxymethyl)imidazolidinyl urea.
High mountain is planted extraction and is carried using gold fork Herba Dendrobii extract, angelica extract, Herba Verbenae, Radix Notoginseng in the B component
Object, wild rose extract, radix paeoniae rubrathe medicament extract are taken according to 1:2:3:1:1:2 mixing.
In the D components macromolecule moisturizer using beta glucan, glycerine polyacrylate, Sodium Hyaluronate one kind or
A variety of mixing.
Essence uses daily essence in the component E；The essence solubilizer is using coceth -7, PPG-1-PEG-
The mixing of September osmanthus glycol ethers, Cremophor RH40, and mixed proportion is 3:1:1.
In addition, a kind of preparation method of the whitening mask liquid the present invention also provides extract containing Magnolia binodii, specifically
Include the following steps：
1) component A of formula ratio is weighed, input is emulsified in pot, is heated with stirring to 80-85 DEG C, makes its dissolving complete, heat preservation
Start to cool down after 10-20min；
2) after being cooled to 50 DEG C, the B component of formula ratio is sequentially added, is stirred evenly, continue to cool down；
3) when temperature drops to 45 DEG C, the C, D being pre-mixed, component E is added in, is stirred evenly；
4) F phases are eventually adding, adjust pH；
5) continue to cool down, when temperature is dropped to below 40 DEG C, filtering and discharging.
Compared with prior art, the beneficial effects of the invention are as follows：
1) facial mask liquid of the invention will be hoped the spring using the extract of the traditional Chinese medicine flower bud of lily magnolia as whitening agent by ultrasonic extraction
Effective active composition in flower bud/spend extracts at a lower temperature, avoids destroying its active whitening composition under high temperature, beautiful
White effect is more notable.
2) other than containing Magnolia binodii bud/flower extract, reasonably combined tree peony branch/flower/leaf carries facial mask liquid of the invention
The functional components such as object, bermuda lily flower extract, white pond lily flower extract, allantoin, glucan, niacinamide, panthenol are taken, in U.S.
Energy effective activation nourishes skin, delaying skin aging while white.
3) facial mask liquid of the invention is using Magnolia binodii extract, and Magnolia binodii is rich in flavones, volatile oil and lignanoid,
In, total flavonoids substance has antioxidant activity, has good Scavenging activity to hydroxyl radical free radical and DPPH free radicals, with general Shandong
Scholar's indigo plant photometry also indicates that it with stronger reducing power, Magnolia binodii extract can by inhibiting the activity of tyrosinase, from
And with apparent whitening function, the effect of the good raising colour of skin can be played, improve skin glossiness, while can significantly it subtract
Few free radical s, effectively inhibits tyrosinase activity, and prevent melanin transfer.
Specific embodiment
Understand to make the object, technical solutions and advantages of the present invention clearer, below by embodiment, to the present invention into
Row is further described.However, it should be understood that the specific embodiments described herein are merely illustrative of the present invention, and do not have to
In limiting the scope of the invention.
Unless otherwise defined, all technical terms and scientific terms used herein are led with belonging to the technology of the present invention
The normally understood meaning of technical staff in domain is identical, and used term is intended merely to retouch in the description of the invention herein
State the purpose of specific embodiment, it is not intended that in the limitation present invention.
A kind of whitening mask liquid of extract containing Magnolia binodii, by weight, the facial mask liquid specifically includes following components,
Component A：0.1-1 parts of thickener, 1-15 parts of polyalcohol, 0.01-0.5 parts of allantoin, 0.01-2 parts of ethoxy urea are gone
60-80 parts of ionized water；
B component：0.1-1 parts of Magnolia binodii extract, 0.05-1 parts of carbohydrate isomer, 0.1-5 parts of water-soluble grease, tooth
0.01-1 parts of leaf olibanum resin extract, 0.01-1 parts of Gotu Kola P.E, trimethylpentanediol/adipic acid/glycerine crosslinking are poly-
0.1-2 parts of object of conjunction, 0.1-1 parts of preservative, 0.1-1 parts of panthenol, 0.01-1 parts of high mountain plant extraction, 0.01-1 parts of peony extract,
0.01-1 parts of bermuda lily flower extract, 0.01-1 parts of white pond lily flower extract, 0.01-1 parts of dried tremella extract；
Component C：0.05-5 parts of niacinamide, 0.1-2 parts of ursin, 5 parts of deionized water；
D components：0.01-0.5 parts of macromolecule moisturizer, 2 parts of propylene glycol, 5 parts of deionized water；
Component E：0.001 part of essence, 0.01 part of essence solubilizer；
F components：0.01-0.2 parts of triethanolamine.
Wherein, the allantoin can effectively cure damage and stasis of blood trace, accelerate cytothesis, have anti-inflammatory, antiallergic, moisturizing,
The effect of soft skin.The niacinamide is a kind of highly stable vitamin B3, it can be by promoting dividing for keratinocyte
Change and maintain cuticula entire run to increase the flexibility of cell, reduce skin sensitivity.Meanwhile niacinamide PC can promote
Into synthesis collagen, elasticity of skin is helped to maintain, strengthens skin barrier, improves microgroove and wrinkle.
The panthenol is provitamin B5, cuticula can be effectively permeated, there is potent moistening effect, effectively soothe the skin
Uncomfortable, itch stimulates epidermal growth, repair tissue wound.The ursin also known as Arbutin, white acicular crystal or
Powder.It extracts from the leaf of black bearberry, the generation of melanin can be prevented, by inhibiting the activity of internal tyrosinase so as to subtract
Few Skin pigmentation, dispelling stain and freckle, while also have the effect of sterilization, anti-inflammatory.
Thickener is using carbomer, hydroxyethyl cellulose, xanthans, one kind in Scleroglucan or more in the component A
Kind mixing.Polyalcohol uses the mixing of glycerine, propylene glycol, butanediol in the component A, and glycerine, propylene glycol, butanediol is mixed
Composition and division in a proportion example is 1:1:1.
Magnolia binodii extract in the B component is Magnolia binodii bud/flower extract, by ultrasonic wave extraction, is specifically carried
Take step as follows：First Magnolia binodii bud/flower is ground, according to 1:20 solid-liquid ratio is added in presses body by deionized water and ethyl alcohol
Product is than (2-3):The mixed solution of 1 composition, then puts it into the container that inner wall is ceramic material, carries out ultrasound bath and adds
Thermal extraction, 50 DEG C of bath temperature, ultrasonic time 1 hour is to get Magnolia binodii bud/flower extract.
Carbohydrate isomer ingredient in the B component is psicose, glucose, mannose, fructose, galactolipin.
The carbohydrate isomer is a kind of natural moisture preserving agent extracted from sugarcane carbohydrate synthesis, and moisture content combination angle is assisted in moisturizing
Keratin in matter layer, to reach moistening effect.
Water-soluble grease in the B component is using PEG-12 Dimethicone Crosspolymers, double-PEG-15 first
One or more mixing in base ether dimethyl silicone polymer, PEG-7 glyceryl cocoates.
Preservative is using Phenoxyethanol, Sensiva SC50, parahydroxyacet-ophenone, methyl hydroxybenzoate, oxybenzene in the B component
One or more mixing in propyl ester, Bis(hydroxymethyl)imidazolidinyl urea.
High mountain is planted extraction and is carried using gold fork Herba Dendrobii extract, angelica extract, Herba Verbenae, Radix Notoginseng in the B component
Object, wild rose extract, radix paeoniae rubrathe medicament extract are taken according to 1:2:3:1:1:2 mixing.Using the herbaceous plant of Yunnan high mountain as original
Material according to the prescription thought of Traditional Chinese Medicine " monarch, minister, help, make ", is allocated meticulously.Wherein, monarch pitches the stem of noble dendrobium with gold, and nourishing Yin and promoting production of body fluid is grown
Water moisturizing；Minister is with Radix Angelicae Sinensis, nourshing blood and promoting blood circulation；Assistant is with Verbena officinalis, promoting blood circulation to remove blood stasis；Make with Radix Notoginseng, nourshing blood and promoting blood circulation, wild rose heat clearing and blood circulation promoting
The stasis of blood is dissipated, RADIX PAEONIAE RUBRA promoting blood circulation to remove blood stasis promotes metabolism.High mountain, which plants extraction skin-protecting factor, to be had good antioxidant activity and inhibits tyrosine
Enzymatic activity, and the effect of skin microcirculation is can effectively improve, the work(of good " improving the colour of skin, improve skin glossiness " can be played
Effect.
In the D components macromolecule moisturizer using beta glucan, glycerine polyacrylate, Sodium Hyaluronate one kind or
A variety of mixing.Wherein, beta glucan can help to update and repair nervous skin, effectively reduce wrinkle of skin and red blood silk, increase
Strong cutaneous immunisation power, promotes the healing and regeneration of scar, improves the moisture retention of skin and the smoothness that compacts.
Essence uses daily essence in the component E；The essence solubilizer is using coceth -7, PPG-1-PEG-
The mixing of September osmanthus glycol ethers, Cremophor RH40, and mixed proportion is 3:1:1.
In addition, a kind of preparation method of the whitening mask liquid the present invention also provides extract containing Magnolia binodii, specifically
Include the following steps：
1) component A of formula ratio is weighed, input is emulsified in pot, is heated with stirring to 80-85 DEG C, makes its dissolving complete, heat preservation
Start to cool down after 10-20min；
2) after being cooled to 50 DEG C, the B component of formula ratio is sequentially added, is stirred evenly, continue to cool down；
3) when temperature drops to 45 DEG C, the C, D being pre-mixed, component E is added in, is stirred evenly；
4) F phases are eventually adding, adjust pH；
5) continue to cool down, when temperature is dropped to below 40 DEG C, filtering and discharging.
Embodiment 1
A kind of whitening mask liquid of extract containing Magnolia binodii, by weight, the facial mask liquid specifically includes following components,
Component A：0.1 part of thickener, 1 part of polyalcohol, 0.01 part of allantoin, 0.01 part of ethoxy urea, 60 parts of deionized water；
B component：0.1 part of Magnolia binodii extract, 0.05 part of carbohydrate isomer, 0.1 part of water-soluble grease, boswellia serrata
0.01 part of resin extract, 0.01 part of Gotu Kola P.E, trimethylpentanediol/0.1 part of adipic acid/glycerin crosspolymers,
0.1 part of preservative, 0.1 part of panthenol, high mountain plant 0.01 part of extraction, 0.01 part of peony extract, bermuda lily flower extract 0.01
Part, 0.01 part of white pond lily flower extract, 0.01 part of dried tremella extract；
Component C：0.05 part of niacinamide, 0.1 part of ursin, 5 parts of deionized water；
D components：0.01 part of macromolecule moisturizer, 2 parts of propylene glycol, 5 parts of deionized water；
Component E：0.001 part of essence, 0.01 part of essence solubilizer；
F components：0.01 part of triethanolamine.
Thickener uses carbomer in the component A.Polyalcohol is using glycerine, propylene glycol, butanediol in the component A
Mixing, and the mixed proportion of glycerine, propylene glycol, butanediol is 1:1:1.
Magnolia binodii extract in the B component is Magnolia binodii bud/flower extract, by ultrasonic wave extraction, is specifically carried
Take step as follows：First Magnolia binodii bud/flower is ground, according to 1:20 solid-liquid ratio is added in presses body by deionized water and ethyl alcohol
Product ratio 2:The mixed solution of 1 composition, then puts it into the container that inner wall is ceramic material, carries out ultrasound bath heating and carries
It takes, 50 DEG C of bath temperature, ultrasonic time 1 hour is to get Magnolia binodii bud/flower extract.
Carbohydrate isomer ingredient in the B component is psicose, glucose, mannose, fructose, galactolipin are pressed
According to 1:1:1:2:1 mixing.
Water-soluble grease in the B component uses PEG-12 Dimethicone Crosspolymers.
Preservative uses Phenoxyethanol in the B component.
High mountain is planted extraction and is carried using gold fork Herba Dendrobii extract, angelica extract, Herba Verbenae, Radix Notoginseng in the B component
Object, wild rose extract, radix paeoniae rubrathe medicament extract are taken according to 1:2:3:1:1:2 mixing.
Macromolecule moisturizer uses beta glucan in the D components.
Essence uses daily essence in the component E；The essence solubilizer is using coceth -7, PPG-1-PEG-
The mixing of September osmanthus glycol ethers, Cremophor RH40, and mixed proportion is 3:1:1.
In addition, a kind of preparation method of the whitening mask liquid the present invention also provides extract containing Magnolia binodii, specifically
Include the following steps：
1) component A of formula ratio is weighed, input is emulsified in pot, is heated with stirring to 80 DEG C, makes its dissolving complete, heat preservation
Start to cool down after 10min；
2) after being cooled to 50 DEG C, the B component of formula ratio is sequentially added, is stirred evenly, continue to cool down；
3) when temperature drops to 45 DEG C, the C, D being pre-mixed, component E is added in, is stirred evenly；
4) F phases are eventually adding, adjust pH；
5) continue to cool down, when temperature is dropped to below 40 DEG C, filtering and discharging.
Embodiment 2
A kind of whitening mask liquid of extract containing Magnolia binodii, by weight, the facial mask liquid specifically includes following components,
Component A：0.5 part of thickener, 10 parts of polyalcohol, 0.2 part of allantoin, 1 part of ethoxy urea, 70 parts of deionized water；
B component：0.5 part of Magnolia binodii extract, 0.5 part of carbohydrate isomer, 3 parts of water-soluble grease, boswellia serrata tree
0.5 part of fat extract, 0.5 part of Gotu Kola P.E, trimethylpentanediol/1 part of adipic acid/glycerin crosspolymers, preservative
0.5 part, 0.5 part of panthenol, high mountain plants 0.6 part of extraction, 0.5 part of peony extract, 0.4 part of bermuda lily flower extract, white pond lily
0.5 part of flower extract, 0.4 part of dried tremella extract；
Component C：3 parts of niacinamide, 1 part of ursin, 5 parts of deionized water；
D components：0.3 part of macromolecule moisturizer, 2 parts of propylene glycol, 5 parts of deionized water；
Component E：0.001 part of essence, 0.01 part of essence solubilizer；
F components：0.1 part of triethanolamine.
Thickener uses carbomer, hydroxyethyl cellulose, xanthans according to 1 in the component A:2:1 mixing.The A groups
Polyalcohol uses the mixing of glycerine, propylene glycol, butanediol in point, and the mixed proportion of glycerine, propylene glycol, butanediol is 1:1:1.
Magnolia binodii extract in the B component is Magnolia binodii bud/flower extract, by ultrasonic wave extraction, is specifically carried
Take step as follows：First Magnolia binodii bud/flower is ground, according to 1:20 solid-liquid ratio is added in presses body by deionized water and ethyl alcohol
Product ratio 2.5:The mixed solution of 1 composition, then puts it into the container that inner wall is ceramic material, carries out ultrasound bath heating
Extraction, 50 DEG C of bath temperature, ultrasonic time 1 hour is to get Magnolia binodii bud/flower extract.
Carbohydrate isomer ingredient in the B component is psicose, glucose, mannose, fructose, galactolipin are pressed
According to 1:2:1:1:2 mixing.
Water-soluble grease in the B component is using PEG-12 Dimethicone Crosspolymers, double-PEG-15 first
Base ether dimethyl silicone polymer is according to 2:1 mixing.
Preservative uses 2 using Phenoxyethanol, Sensiva SC50 in the B component:1 mixing.
High mountain is planted extraction and is carried using gold fork Herba Dendrobii extract, angelica extract, Herba Verbenae, Radix Notoginseng in the B component
Object, wild rose extract, radix paeoniae rubrathe medicament extract are taken according to 1:2:3:1:1:2 mixing.
Macromolecule moisturizer uses Sodium Hyaluronate in the D components.
Essence uses daily essence in the component E；The essence solubilizer is using coceth -7, PPG-1-PEG-
The mixing of September osmanthus glycol ethers, Cremophor RH40, and mixed proportion is 3:1:1.
In addition, a kind of preparation method of the whitening mask liquid the present invention also provides extract containing Magnolia binodii, specifically
Include the following steps：
1) component A of formula ratio is weighed, input is emulsified in pot, is heated with stirring to 82 DEG C, makes its dissolving complete, heat preservation
Start to cool down after 15min；
2) after being cooled to 50 DEG C, the B component of formula ratio is sequentially added, is stirred evenly, continue to cool down；
3) when temperature drops to 45 DEG C, the C, D being pre-mixed, component E is added in, is stirred evenly；
4) F phases are eventually adding, adjust pH；
5) continue to cool down, when temperature is dropped to below 40 DEG C, filtering and discharging.
Embodiment 3
A kind of whitening mask liquid of extract containing Magnolia binodii, by weight, the facial mask liquid specifically includes following components,
Component A：1 part of thickener, 15 parts of polyalcohol, 0.5 part of allantoin, 2 parts of ethoxy urea, 80 parts of deionized water；
B component：1 part of Magnolia binodii extract, 1 part of carbohydrate isomer, 5 parts of water-soluble grease, boswellia serrata resin carries
Take 1 part of object, 1 part of Gotu Kola P.E, trimethylpentanediol/2 parts of adipic acid/glycerin crosspolymers, 1 part of preservative, panthenol 1
Part, high mountain plants 1 part of extraction, 1 part of peony extract, 1 part of bermuda lily flower extract, 1 part of white pond lily flower extract, white fungus extraction
1 part of object；
Component C：5 parts of niacinamide, 2 parts of ursin, 5 parts of deionized water；
D components：0.5 part of macromolecule moisturizer, 2 parts of propylene glycol, 5 parts of deionized water；
Component E：0.001 part of essence, 0.01 part of essence solubilizer；
F components：0.2 part of triethanolamine.
Thickener uses hydroxyethyl cellulose, xanthans according to 2 in the component A:3 mixing.Polyalcohol in the component A
It is 1 using glycerine, the mixing of propylene glycol, butanediol, and the mixed proportion of glycerine, propylene glycol, butanediol:1:1.
Magnolia binodii extract in the B component is Magnolia binodii bud/flower extract, by ultrasonic wave extraction, is specifically carried
Take step as follows：First Magnolia binodii bud/flower is ground, according to 1:20 solid-liquid ratio is added in presses body by deionized water and ethyl alcohol
Product ratio 3:The mixed solution of 1 composition, then puts it into the container that inner wall is ceramic material, carries out ultrasound bath heating and carries
It takes, 50 DEG C of bath temperature, ultrasonic time 1 hour is to get Magnolia binodii bud/flower extract.
Carbohydrate isomer ingredient in the B component is psicose, glucose, mannose, fructose, galactolipin
Mixture.Water-soluble grease in the B component is using double-PEG-15 methyl ether dimethicones.
Preservative uses parahydroxyacet-ophenone in the B component.
High mountain is planted extraction and is carried using gold fork Herba Dendrobii extract, angelica extract, Herba Verbenae, Radix Notoginseng in the B component
Object, wild rose extract, radix paeoniae rubrathe medicament extract are taken according to 1:2:3:1:1:2 mixing.
Macromolecule moisturizer uses beta glucan, glycerine polyacrylate according to 1 in the D components:1 mixing.
Essence uses daily essence in the component E；The essence solubilizer is using coceth -7, PPG-1-PEG-
The mixing of September osmanthus glycol ethers, Cremophor RH40, and mixed proportion is 3:1:1.
In addition, a kind of preparation method of the whitening mask liquid the present invention also provides extract containing Magnolia binodii, specifically
Include the following steps：
1) component A of formula ratio is weighed, input is emulsified in pot, is heated with stirring to 85 DEG C, makes its dissolving complete, heat preservation
Start to cool down after 20min；
2) after being cooled to 50 DEG C, the B component of formula ratio is sequentially added, is stirred evenly, continue to cool down；
3) when temperature drops to 45 DEG C, the C, D being pre-mixed, component E is added in, is stirred evenly；
4) F phases are eventually adding, adjust pH；
5) continue to cool down, when temperature is dropped to below 40 DEG C, filtering and discharging.
Embodiment 4
A kind of whitening mask liquid of extract containing Magnolia binodii, by weight, the facial mask liquid specifically includes following components,
Component A：0.3 part of thickener, 3 parts of glycerine, 3 parts of propylene glycol, 1 part of butanediol, 0.2 part of allantoin, ethoxy urea 0.3
Part, 70 parts of deionized water；
B component：Magnolia binodii bud/0.2 part of flower extract, 0.05 part of carbohydrate isomer, 0.3 part of water-soluble grease,
0.01 part of boswellia serrata resin extract, 0.01 part of Gotu Kola P.E, trimethylpentanediol/adipic acid/glycerine cross-linked polymeric
0.2 part of object, 0.5 part of Phenoxyethanol, 0.1 part of methyl hydroxybenzoate, 0.1-1 parts of panthenol, high mountain plant 1 part of extraction, the extraction of tree peony branch/flower/leaf
1 part of object, 1 part of bermuda lily flower extract, 1 part of white pond lily flower extract, 1 part of dried tremella extract；
Component C：1 part of niacinamide, 0.6 part of ursin, 5 parts of deionized water；
D components：0.05 part of Sodium Hyaluronate, 2 parts of propylene glycol, 5 parts of deionized water；
Component E：0.001 part of essence, 0.006 part of coceth -7, PPG-1-PEG-9 bays glycol ethers 0.002,
0.002 part of Cremophor RH40；
F components：0.3 part of triethanolamine.
Thickener uses carbomer in the component A.
Magnolia binodii extract in the B component is Magnolia binodii bud/flower extract, by ultrasonic wave extraction, is specifically carried
Take step as follows：First Magnolia binodii bud/flower is ground, according to 1:20 solid-liquid ratio is added in presses body by deionized water and ethyl alcohol
Product ratio 2:The mixed solution of 1 composition, then puts it into the container that inner wall is ceramic material, carries out ultrasound bath heating and carries
It takes, 50 DEG C of bath temperature, ultrasonic time 1 hour is to get Magnolia binodii bud/flower extract.
Carbohydrate isomer ingredient in the B component is psicose, glucose, mannose, fructose, galactolipin are pressed
According to 1:3:2:1:1 mixing.
Water-soluble grease is PEG-12 Dimethicone Crosspolymers in the B component.
High mountain is planted extraction and is carried using gold fork Herba Dendrobii extract, angelica extract, Herba Verbenae, Radix Notoginseng in the B component
Object, wild rose extract, radix paeoniae rubrathe medicament extract are taken according to 1:2:3:1:1:2 mixing.
Essence uses daily essence in the component E.
In addition, a kind of preparation method of the whitening mask liquid the present invention also provides extract containing Magnolia binodii, specifically
Include the following steps：
1) component A of formula ratio is weighed, input is emulsified in pot, is heated with stirring to 80 DEG C, makes its dissolving complete, heat preservation
Start to cool down after 14min；
2) after being cooled to 50 DEG C, the B component of formula ratio is sequentially added, is stirred evenly, continue to cool down；
3) when temperature drops to 45 DEG C, the C, D being pre-mixed, component E is added in, is stirred evenly；
4) F phases are eventually adding, adjust pH；
5) continue to cool down, when temperature is dropped to below 40 DEG C, filtering and discharging.
Whitening mask liquid made from above-described embodiment is detected, specific testing result is as shown in table 1 below.
The detection performance of 1 facial mask liquid of table
It is found that the pH value of whitening mask liquid of the present invention is 6.5-6.9 (standard 4.0-8.5), viscosity performance is analytical table 1
1539-2101 (standard 1000-3000cp), relative density is 0.985-1.015 (standard 0.98-1.02), in addition, outside it
Sight, odor type, cold-resistant and heat resistance are also qualified.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all essences in the present invention
Any modification, equivalent replacement or improvement made within refreshing and principle etc., should all be included in the protection scope of the present invention.
Claims (11)
1. the whitening mask liquid of a kind of extract containing Magnolia binodii, which is characterized in that by weight, the facial mask liquid specifically includes
Following components,
Component A：0.1-1 parts of thickener, 1-15 parts of polyalcohol, 0.01-0.5 parts of allantoin, 0.01-2 parts of ethoxy urea, deionization
60-80 parts of water；
B component：0.1-1 parts of Magnolia binodii extract, 0.05-1 parts of carbohydrate isomer, 0.1-5 parts of water-soluble grease, tingia breast
0.01-1 parts of botany bar gum extract, 0.01-1 parts of Gotu Kola P.E, trimethylpentanediol/adipic acid/glycerin crosspolymers
0.1-2 parts, 0.1-1 parts of preservative, 0.1-1 parts of panthenol, 0.01-1 parts of high mountain plant extraction, 0.01-1 parts of peony extract, white flower
0.01-1 parts of Flos Lilii viriduli extract, 0.01-1 parts of white pond lily flower extract, 0.01-1 parts of dried tremella extract；
Component C：0.05-5 parts of niacinamide, 0.1-2 parts of ursin, 5 parts of deionized water；
D components：0.01-0.5 parts of macromolecule moisturizer, 2 parts of propylene glycol, 5 parts of deionized water；
Component E：0.001 part of essence, 0.01 part of essence solubilizer；
F components：0.01-0.2 parts of triethanolamine.
A kind of 2. whitening mask liquid of extract containing Magnolia binodii according to claim 1, which is characterized in that the component A
Middle thickener is using one or more mixing in carbomer, hydroxyethyl cellulose, xanthans, Scleroglucan.
A kind of 3. whitening mask liquid of extract containing Magnolia binodii according to claim 1, which is characterized in that the component A
Middle polyalcohol uses the mixing of glycerine, propylene glycol, butanediol, and the mixed proportion of glycerine, propylene glycol, butanediol is 1:1:1.
A kind of 4. whitening mask liquid of extract containing Magnolia binodii according to claim 1, which is characterized in that the B component
In Magnolia binodii extract for Magnolia binodii bud/flower extract, by ultrasonic wave extraction, specific extraction step is as follows：
First Magnolia binodii bud/flower is ground, according to 1:20 solid-liquid ratio is added in by deionized water and ethyl alcohol (2- by volume
3):The mixed solution of 1 composition, then puts it into the container that inner wall is ceramic material, carries out ultrasound bath heating extraction,
50 DEG C of bath temperature, ultrasonic time 1 hour is to get Magnolia binodii bud/flower extract.
A kind of 5. whitening mask liquid of extract containing Magnolia binodii according to claim 1, which is characterized in that the B component
In carbohydrate isomer ingredient for psicose, glucose, mannose, fructose, galactolipin mixture.
A kind of 6. whitening mask liquid of extract containing Magnolia binodii according to claim 1, which is characterized in that the B component
In water-soluble grease using PEG-12 Dimethicone Crosspolymers, double-PEG-15 methyl ethers polydimethylsiloxanes
One or more mixing in alkane, PEG-7 glyceryl cocoates.
A kind of 7. whitening mask liquid of extract containing Magnolia binodii according to claim 1, which is characterized in that the B component
Middle preservative is using Phenoxyethanol, Sensiva SC50, parahydroxyacet-ophenone, methyl hydroxybenzoate, Nipasol, bis- (methylol) miaows
One or more mixing in oxazolidinyl urea.
A kind of 8. whitening mask liquid of extract containing Magnolia binodii according to claim 1, which is characterized in that the B component
Middle high mountain plant extraction using gold fork Herba Dendrobii extract, angelica extract, Herba Verbenae, Notogineng Extract, wild rose extract,
Radix paeoniae rubrathe medicament extract is according to 1:2:3:1:1:2 mixing.
A kind of 9. whitening mask liquid of extract containing Magnolia binodii according to claim 1, which is characterized in that the D components
Middle macromolecule moisturizer uses one or more mixing of beta glucan, glycerine polyacrylate, Sodium Hyaluronate.
A kind of 10. whitening mask liquid of extract containing Magnolia binodii according to claim 1, which is characterized in that the component E
Middle essence uses daily essence；The essence solubilizer is using coceth -7, PPG-1-PEG-9 bays glycol ethers, PEG-
The mixing of 40 rilanit specials, and mixed proportion is 3:1:1.
11. a kind of preparation method of the whitening mask liquid of the extract containing Magnolia binodii described in any one of claim 1-10, feature
It is, specifically includes following steps：
1) component A of formula ratio is weighed, input is emulsified in pot, is heated with stirring to 80-85 DEG C, is made its dissolving complete, is kept the temperature 10-
Start to cool down after 20min；
2) after being cooled to 50 DEG C, the B component of formula ratio is sequentially added, is stirred evenly, continue to cool down；
3) when temperature drops to 45 DEG C, the C, D being pre-mixed, component E is added in, is stirred evenly；
4) F phases are eventually adding, adjust pH；
5) continue to cool down, when temperature is dropped to below 40 DEG C, filtering and discharging.
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| CN113876640B (en) * | 2021-11-16 | 2023-10-31 | 北京青颜博识健康管理有限公司 | Anti-saccharification seaweed source composition, preparation method thereof and application thereof in cosmetic product |
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| CN114557933B (en) * | 2022-03-09 | 2024-06-04 | 上海珈凯生物股份有限公司 | Extract of flos verrucae and preparation method and application thereof |
| CN115337226A (en) * | 2022-08-22 | 2022-11-15 | 广州雅纯化妆品制造有限公司 | Whitening composition, cosmetic and preparation method thereof |
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Application publication date: 20180629 |