CN111588673A - Freeze-dried solid mask and preparation method thereof - Google Patents

Freeze-dried solid mask and preparation method thereof Download PDF

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Publication number
CN111588673A
CN111588673A CN202010625190.1A CN202010625190A CN111588673A CN 111588673 A CN111588673 A CN 111588673A CN 202010625190 A CN202010625190 A CN 202010625190A CN 111588673 A CN111588673 A CN 111588673A
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Prior art keywords
freeze
essence
mask
weight
parts
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CN202010625190.1A
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Chinese (zh)
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于慧敏
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Priority to CN202010625190.1A priority Critical patent/CN111588673A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9728Fungi, e.g. yeasts
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0212Face masks
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/84Products or compounds obtained by lyophilisation, freeze-drying
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/85Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Epidemiology (AREA)
  • Birds (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Dermatology (AREA)
  • Gerontology & Geriatric Medicine (AREA)
  • Cosmetics (AREA)

Abstract

The invention relates to the technical field of cosmetics, in particular to a freeze-dried solid mask and a preparation method thereof, wherein the preparation method comprises the following preparation steps: s1, preparing essence; s2, coating and drying; s3, punching and forming; s4, bagging; s5, injecting liquid; s6, freeze-drying; s7, sealing; and S8, dormancy processing. According to the freeze-dried solid mask, the active ingredients in the essence can be effectively ensured through freeze-drying treatment, the essence base solution is coated on the base material cloth and is dried in the preparation process, then the essence active solution is injected, the interference of the complex component environment in the essence base solution on the essence active solution is reduced, meanwhile, due to the fact that the water content in the mask bag is low, the subsequent freeze-drying treatment time can be greatly reduced, and the effect that freeze-drying can be fully performed in a short time is achieved.

Description

Freeze-dried solid mask and preparation method thereof
Technical Field
The invention relates to the technical field of cosmetics, in particular to a freeze-dried solid mask and a preparation method thereof.
Background
The mask is a widely applied skin care product, the existing membrane mask is usually prepared by directly injecting essence into a mask bag with a mask carrier and then packaging, and the preparation method causes that some active ingredients which are easy to degrade and oxidize are difficult to store, thereby influencing the using effect.
Disclosure of Invention
The invention aims to provide a freeze-dried solid facial mask and a preparation method thereof aiming at the existing technical current situation.
In order to achieve the purpose, the invention adopts the following technical scheme:
the invention provides a preparation method of a freeze-dried solid mask, which is characterized by comprising the following preparation steps:
s1, preparing essence: respectively preparing essence base liquid and essence active liquid, wherein the essence base liquid comprises water and a thickening agent;
the essence is divided into an essence base solution and an essence active solution, wherein the essence active solution comprises at least one active ingredient which is easy to degrade and oxidize or unstable in a liquid state, such as a polypeptide active ingredient and a vitamin ingredient, and the essence base solution is other components except the active ingredient which is easy to degrade and oxidize or unstable in the liquid state, such as water, a thickening agent, a humectant and the like, in an essence formula.
S2, coating and drying: coating the essence base solution on a base material cloth, and then drying at the temperature of 80-120 ℃;
among the prior art, generally be to cut into the facial mask shape with the base material cloth punching, just inject the essence after packing into the facial mask bag, in this application, coat the essence base fluid on the base material cloth, dry afterwards, just carry out die-cut shaping afterwards, be favorable to the essence base fluid evenly to adhere to the facial mask carrier, follow-up result of use is better.
According to the invention, the essence base solution is coated on the base material cloth and is dried, and then the essence active solution is injected, so that the interference of a complex component environment in the essence base solution on the essence active solution is reduced, and meanwhile, because the water content in the mask bag is low, the subsequent freeze-drying treatment time can be greatly reduced, and the effect of fully freeze-drying after short-time freeze-drying is achieved.
S3, punching and forming: rolling up the dried base material cloth, and punching by a punch press to form a mask carrier in a mask shape;
s4, bagging: folding the mask carrier and putting into a mask bag;
s5, liquid injection: injecting the essence active liquid into the mask bag in the last step;
s6, freeze-drying: freeze-drying the facial mask bag after liquid injection for 1-15 minutes at-40 ℃ in freeze-drying equipment;
according to the invention, through freeze-drying treatment, the active ingredients in the essence, especially the biological activity of the essence active liquid, can be effectively ensured, the water content of the freeze-dried product is low, the storage time can be prolonged, the weight of the product is reduced, and the transportation is convenient.
S7, sealing: sealing the mask bag to form a semi-finished product;
s8, dormancy processing: the sealed facial mask bag is put into a dormancy treatment cabin, wherein the dormancy treatment cabin can be a box body with good sealing performance, and then low-temperature nitrogen is injected into the dormancy treatment cabin, so that the activity of active ingredients is reduced.
Preferably, the essence base solution in step S1 further includes a humectant, such as sodium hyaluronate.
Preferably, the drying time of the step S2 is 3 to 5 seconds.
Preferably, in the step S4, after bagging, the method further comprises the step of carrying out ozone disinfection by ozone disinfection equipment for 1-2 hours.
Preferably, the base material cloth is one of non-woven fabrics, all cotton, blended fabrics and biological fiber composite materials, and the non-woven fabrics are preferred.
The invention also provides a freeze-dried solid facial mask prepared by the preparation method of the freeze-dried solid facial mask, which is characterized by comprising essence base solution and essence active solution,
the essence base solution comprises the following components in parts by weight:
70-80 parts by weight of water;
0.1-0.3 parts of thickening agent;
the essence active liquid comprises the following components in parts by weight:
hexapeptide-113-6 parts by weight;
5-10 parts by weight of a secondary split yeast fermentation product filtrate;
12-5 parts by weight of oligopeptide;
5-8 parts of carnosine.
Hexapeptide-11 is a naturally occurring polypeptide, acts on dermal fibroblasts at the same time, promotes the synthesis of collagen, elastin and extracellular matrix components, can effectively enhance skin firmness, improve water retention capacity, reduce wrinkles, resist aging and enable skin to return to a tender and compact state.
Oligopeptide-1 is polypeptide composed of glycine, histidine and lysine, as small molecular protein, oligopeptide-1 can be easily absorbed by skin, and is used as raw material to participate in the extension of peptide chain, and improve the synthesis of protein, especially dermal collagen and elastin, thereby helping skin to improve metabolism and increase the repair capacity of skin.
Carnosine is a dipeptide amino acid consisting of two amino acids (beta alanine and L-histidine), is a natural antioxidant, has anti-inflammatory, antioxidant and free radical scavenging properties, and has strong immune enhancing and anti-aging properties.
According to the invention, hexapeptide-11, oligopeptide-1 and carnosine are compounded with various peptide active components, and the components supplement each other, so that the metabolism and the repair capacity of human skin are effectively improved, and the anti-aging effect is good.
The secondary fission yeast fermentation product filtrate is a filtrate of a mixture generated after the fermentation of bifidobacteria and the cracking of thalli, and the metabolic product contains amino acid, micromolecular polypeptide, vitamin B group, mineral substance and other micromolecules which are beneficial to skin care, contains trace organic acid, can strengthen the metabolism of cuticle, can capture free radicals, inhibits the peroxidation of lipid, and has the effects of resisting aging and repairing damaged skin.
According to the invention, the secondary fission yeast fermentation product filtrate is matched with various peptide active components, so that the skin repair capacity and the anti-aging effect are further improved.
Preferably, the thickener is xanthan gum.
Preferably, the essence base solution further comprises the following components in parts by weight:
0.8-1.5 parts by weight of centella asiatica extract;
0.1-0.4 part by weight of sodium hyaluronate.
Preferably, the essence base solution further comprises 0.3-0.6 weight part of collagen.
Preferably, the essence base solution further comprises 0.01-0.04 parts by weight of disodium EDTA.
The asiaticoside in the centella asiatica extract has obvious anti-inflammatory effect, reduces the generation of pro-inflammatory mediators, and improves and repairs the barrier function of the skin.
Asiaticoside has proliferation effect on epidermal keratinocyte and vascular endothelial cell, and has inhibitory effect on fibroblast, so as to promote granulation tissue formation in early stage of wound healing, and inhibit scar formation in late stage of wound healing. Meanwhile, the asiaticoside can promote the synthesis of KGF-2mRNA, thereby playing the roles of KGF-2mRNA in promoting the proliferation, differentiation and chemotaxis of keratinocytes, promoting the healing of wound surfaces and indirectly promoting the generation of granulation tissues and forming the virtuous cycle of wound healing.
The centella asiatica extract can promote the synthesis of collagen I and III, promote the secretion of mucopolysaccharide (such as the synthesis of sodium hyaluronate), increase the water retention of skin, activate and renew skin cells, relieve skin, and improve and make skin have luster.
Asiaticoside, asiatic acid and madecassic acid in the centella asiatica extract have obvious antioxidant activity.
According to the invention, the centella asiatica extract, the secondary fission yeast fermentation product filtrate and various peptide active components are combined, so that the synergistic effect is exerted, the skin repairing capability is further improved, and the anti-aging effect is effectively improved.
The invention has the beneficial effects that:
1) according to the invention, through freeze-drying treatment, the active ingredients in the essence, especially the biological activity of the essence active liquid, can be effectively ensured, the water content of the freeze-dried product is low, the storage time can be prolonged, the weight of the product is reduced, and the transportation is convenient.
2) According to the invention, the essence base solution is coated on the base material cloth and is dried, and then the essence active solution is injected, so that the interference of a complex component environment in the essence base solution on the essence active solution is reduced, and meanwhile, because the water content in the mask bag is low, the subsequent freeze-drying treatment time can be greatly reduced, and the effect of fully freeze-drying after short-time freeze-drying is achieved.
3) The freeze-dried solid mask disclosed by the invention has the beneficial effects that the centella asiatica extract, the secondary fission yeast fermentation product filtrate and various peptide active components are combined, so that the synergistic effect is exerted, the skin repairing capability is further improved, and the anti-aging effect is effectively improved.
Detailed Description
The invention is further illustrated by the following examples:
example 1
A preparation method of a freeze-dried solid mask comprises the following preparation steps:
s1, preparing essence: respectively preparing essence base liquid and essence active liquid, wherein the essence base liquid comprises water and a thickening agent;
s2, coating and drying: coating the essence base solution on a base material cloth (non-woven fabric), and then drying at the temperature of 80-120 ℃ for 3-5 seconds;
s3, punching and forming: rolling up the dried base material cloth, and punching by a punch press to form a mask carrier in a mask shape;
s4, bagging: folding the mask carrier, putting the mask carrier into a mask bag, and then carrying out ozone disinfection by ozone disinfection equipment for 1-2 hours;
s5, liquid injection: injecting the essence active liquid into the mask bag in the last step;
s6, freeze-drying: freeze-drying the facial mask bag after liquid injection for 1-15 minutes at-40 ℃ in freeze-drying equipment;
s7, sealing: sealing the mask bag to form a semi-finished product;
s8, dormancy processing: and (3) putting the sealed facial mask bag into a dormancy treatment cabin, then injecting low-temperature nitrogen into the dormancy treatment cabin to enable the active ingredients to enter a dormant state, and reviving the active ingredients again by using water when the product is used.
Example 2
The freeze-dried solid facial mask prepared according to the preparation method of the freeze-dried solid facial mask in embodiment 1, wherein the freeze-dried solid facial mask comprises an essence base solution and an essence active solution,
the essence base solution comprises the following components in parts by weight:
70-80 parts by weight of water;
0.1-0.3 parts by weight of xanthan gum;
the essence active liquid comprises the following components in parts by weight:
hexapeptide-113-6 parts by weight;
5-10 parts by weight of a secondary split yeast fermentation product filtrate;
12-5 parts by weight of oligopeptide;
5-8 parts of carnosine.
Example 3
The freeze-dried solid facial mask prepared according to the preparation method of the freeze-dried solid facial mask in embodiment 1, wherein the freeze-dried solid facial mask comprises an essence base solution and an essence active solution,
the essence base solution comprises the following components in parts by weight:
80 parts of water;
0.2 part by weight of xanthan gum;
0.03 part by weight of EDTA disodium;
the essence active liquid comprises the following components in parts by weight:
hexapeptide-115 parts by weight;
8 parts of secondary fission yeast fermentation product filtrate;
oligopeptide-14 parts by weight;
7 parts of carnosine.
Example 4
The freeze-dried solid facial mask prepared according to the preparation method of the freeze-dried solid facial mask in embodiment 1, wherein the freeze-dried solid facial mask comprises an essence base solution and an essence active solution,
the essence base solution comprises the following components in parts by weight:
70-80 parts by weight of water;
0.1-0.3 parts by weight of xanthan gum;
0.8-1.5 parts by weight of centella asiatica extract;
0.1-0.4 part by weight of sodium hyaluronate;
0.3-0.6 parts by weight of collagen;
the essence active liquid comprises the following components in parts by weight:
hexapeptide-113-6 parts by weight;
5-10 parts by weight of a secondary split yeast fermentation product filtrate;
12-5 parts by weight of oligopeptide;
5-8 parts of carnosine.
The technical principles of the present invention have been described above in connection with specific embodiments. The description is made for the purpose of illustrating the principles of the invention and should not be construed in any way as limiting the scope of the invention. Based on the explanations herein, those skilled in the art will be able to conceive of other embodiments of the present invention without any inventive step, which shall fall within the scope of the present invention.

Claims (10)

1. The preparation method of the freeze-dried solid mask is characterized by comprising the following preparation steps:
s1, preparing essence: respectively preparing essence base liquid and essence active liquid, wherein the essence base liquid comprises water and a thickening agent;
s2, coating and drying: coating the essence base solution on a base material cloth, and then drying at the temperature of 80-120 ℃;
s3, punching and forming: rolling up the dried base material cloth, and punching by a punch press to form a mask carrier in a mask shape;
s4, bagging: folding the mask carrier and putting into a mask bag;
s5, liquid injection: injecting the essence active liquid into the mask bag in the last step;
s6, freeze-drying: freeze-drying the facial mask bag after liquid injection for 1-15 minutes at-40 ℃ in freeze-drying equipment;
s7, sealing: sealing the mask bag to form a semi-finished product;
s8, dormancy processing: and (3) putting the sealed mask bag into a dormant treatment chamber, and then injecting low-temperature nitrogen into the dormant treatment chamber.
2. The method of preparing a lyophilized solid mask pack according to claim 1, wherein the essence base solution of step S1 further comprises a moisturizer.
3. The method for preparing a freeze-dried solid mask according to claim 1, wherein the drying time of the step S2 is 3-5 seconds.
4. The method for preparing a freeze-dried solid mask according to claim 1, wherein the step S4 further comprises the step of performing ozone sterilization by an ozone sterilization device after bagging, wherein the sterilization time is 1-2 hours.
5. The method for preparing a freeze-dried solid mask according to any one of claims 1 to 4, wherein the base material cloth is one of non-woven fabric, all cotton, blended fabric and bio-fiber composite material.
6. The freeze-dried solid mask prepared by the preparation method of the freeze-dried solid mask according to any one of claims 1 to 4, wherein the freeze-dried solid mask comprises an essence base solution and an essence active solution,
the essence base solution comprises the following components in parts by weight:
70-80 parts by weight of water;
0.1-0.3 parts of thickening agent;
the essence active liquid comprises the following components in parts by weight:
hexapeptide-113-6 parts by weight;
5-10 parts by weight of a secondary split yeast fermentation product filtrate;
12-5 parts by weight of oligopeptide;
5-8 parts of carnosine.
7. The freeze-dried solid mask as claimed in claim 6, wherein the thickener is xanthan gum.
8. The freeze-dried solid mask as claimed in claim 6, wherein the essence base solution further comprises the following components in parts by weight:
0.8-1.5 parts by weight of centella asiatica extract;
0.1-0.4 part by weight of sodium hyaluronate.
9. The freeze-dried solid mask as claimed in claim 6, wherein the essence base solution further comprises 0.3 to 0.6 weight part of collagen.
10. The freeze-dried solid mask as claimed in claim 6, wherein the essence base solution further comprises 0.01 to 0.04 parts by weight of disodium EDTA.
CN202010625190.1A 2020-07-01 2020-07-01 Freeze-dried solid mask and preparation method thereof Pending CN111588673A (en)

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CN112691840A (en) * 2020-11-30 2021-04-23 苏州缘佑科技材料有限公司 Production device of solid mask, solid mask and preparation method of solid mask
CN113277177A (en) * 2021-05-19 2021-08-20 薇树未来(广州)生物科技有限公司 Freeze-drying method of freeze-drying mask capable of efficiently keeping activity of mask
CN115177532A (en) * 2022-07-13 2022-10-14 中英阿诺康(宁夏)生物科技有限公司 Collagen polypeptide young face fresh and alive freeze-dried mask and preparation method thereof

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112691840A (en) * 2020-11-30 2021-04-23 苏州缘佑科技材料有限公司 Production device of solid mask, solid mask and preparation method of solid mask
CN113277177A (en) * 2021-05-19 2021-08-20 薇树未来(广州)生物科技有限公司 Freeze-drying method of freeze-drying mask capable of efficiently keeping activity of mask
CN115177532A (en) * 2022-07-13 2022-10-14 中英阿诺康(宁夏)生物科技有限公司 Collagen polypeptide young face fresh and alive freeze-dried mask and preparation method thereof

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Application publication date: 20200828