CN111482266B - 一种原生脉铂矿尾矿分步分类综合回收有价元素的选矿方法 - Google Patents
一种原生脉铂矿尾矿分步分类综合回收有价元素的选矿方法 Download PDFInfo
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- CN111482266B CN111482266B CN202010320413.3A CN202010320413A CN111482266B CN 111482266 B CN111482266 B CN 111482266B CN 202010320413 A CN202010320413 A CN 202010320413A CN 111482266 B CN111482266 B CN 111482266B
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- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 title claims abstract description 130
- 229910052697 platinum Inorganic materials 0.000 title claims abstract description 57
- 238000000034 method Methods 0.000 title claims abstract description 43
- 210000003462 vein Anatomy 0.000 title claims abstract description 22
- 239000012141 concentrate Substances 0.000 claims abstract description 98
- KDLHZDBZIXYQEI-UHFFFAOYSA-N palladium Substances [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 claims abstract description 93
- 229910052763 palladium Inorganic materials 0.000 claims abstract description 65
- 238000005188 flotation Methods 0.000 claims abstract description 38
- 229910052500 inorganic mineral Inorganic materials 0.000 claims abstract description 36
- 239000011707 mineral Substances 0.000 claims abstract description 36
- 238000007885 magnetic separation Methods 0.000 claims abstract description 24
- 238000000227 grinding Methods 0.000 claims abstract description 12
- 238000000926 separation method Methods 0.000 claims abstract description 7
- 239000011651 chromium Substances 0.000 claims description 30
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 28
- 230000002000 scavenging effect Effects 0.000 claims description 21
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims description 20
- 229910052804 chromium Inorganic materials 0.000 claims description 20
- 239000003795 chemical substances by application Substances 0.000 claims description 18
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- QTANTQQOYSUMLC-UHFFFAOYSA-O Ethidium cation Chemical compound C12=CC(N)=CC=C2C2=CC=C(N)C=C2[N+](CC)=C1C1=CC=CC=C1 QTANTQQOYSUMLC-UHFFFAOYSA-O 0.000 claims description 5
- 229920002907 Guar gum Polymers 0.000 claims description 5
- 229920002472 Starch Polymers 0.000 claims description 5
- TUZCOAQWCRRVIP-UHFFFAOYSA-N butoxymethanedithioic acid Chemical compound CCCCOC(S)=S TUZCOAQWCRRVIP-UHFFFAOYSA-N 0.000 claims description 5
- 239000003518 caustics Substances 0.000 claims description 5
- 229910000365 copper sulfate Inorganic materials 0.000 claims description 5
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 claims description 5
- 235000010417 guar gum Nutrition 0.000 claims description 5
- 239000000665 guar gum Substances 0.000 claims description 5
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
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- HBROZNQEVUILML-UHFFFAOYSA-N salicylhydroxamic acid Chemical compound ONC(=O)C1=CC=CC=C1O HBROZNQEVUILML-UHFFFAOYSA-N 0.000 claims description 4
- WVYWICLMDOOCFB-UHFFFAOYSA-N 4-methyl-2-pentanol Chemical compound CC(C)CC(C)O WVYWICLMDOOCFB-UHFFFAOYSA-N 0.000 claims description 3
- 229910002651 NO3 Inorganic materials 0.000 claims description 2
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 claims description 2
- 239000012190 activator Substances 0.000 claims description 2
- WUOACPNHFRMFPN-UHFFFAOYSA-N alpha-terpineol Chemical compound CC1=CCC(C(C)(C)O)CC1 WUOACPNHFRMFPN-UHFFFAOYSA-N 0.000 claims description 2
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 2
- SQIFACVGCPWBQZ-UHFFFAOYSA-N delta-terpineol Natural products CC(C)(O)C1CCC(=C)CC1 SQIFACVGCPWBQZ-UHFFFAOYSA-N 0.000 claims description 2
- 239000003350 kerosene Substances 0.000 claims description 2
- RLJMLMKIBZAXJO-UHFFFAOYSA-N lead nitrate Chemical compound [O-][N+](=O)O[Pb]O[N+]([O-])=O RLJMLMKIBZAXJO-UHFFFAOYSA-N 0.000 claims description 2
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- 229940116411 terpineol Drugs 0.000 claims description 2
- PGKQTZHDCHKDQK-UHFFFAOYSA-N 2-phenylethenylphosphonic acid Chemical compound OP(O)(=O)C=CC1=CC=CC=C1 PGKQTZHDCHKDQK-UHFFFAOYSA-N 0.000 claims 1
- 230000003750 conditioning effect Effects 0.000 claims 1
- 238000011084 recovery Methods 0.000 abstract description 31
- QDOXWKRWXJOMAK-UHFFFAOYSA-N chromium(III) oxide Inorganic materials O=[Cr]O[Cr]=O QDOXWKRWXJOMAK-UHFFFAOYSA-N 0.000 abstract description 14
- 239000012535 impurity Substances 0.000 abstract description 11
- 230000008901 benefit Effects 0.000 abstract description 6
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- 229910052751 metal Inorganic materials 0.000 description 16
- PAWQVTBBRAZDMG-UHFFFAOYSA-N 2-(3-bromo-2-fluorophenyl)acetic acid Chemical compound OC(=O)CC1=CC=CC(Br)=C1F PAWQVTBBRAZDMG-UHFFFAOYSA-N 0.000 description 7
- -1 platinum group metals Chemical class 0.000 description 7
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 6
- 239000000843 powder Substances 0.000 description 6
- 229910044991 metal oxide Inorganic materials 0.000 description 5
- 150000004706 metal oxides Chemical class 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- NWXHSRDXUJENGJ-UHFFFAOYSA-N calcium;magnesium;dioxido(oxo)silane Chemical compound [Mg+2].[Ca+2].[O-][Si]([O-])=O.[O-][Si]([O-])=O NWXHSRDXUJENGJ-UHFFFAOYSA-N 0.000 description 4
- 229910052637 diopside Inorganic materials 0.000 description 4
- SZVJSHCCFOBDDC-UHFFFAOYSA-N iron(II,III) oxide Inorganic materials O=[Fe]O[Fe]O[Fe]=O SZVJSHCCFOBDDC-UHFFFAOYSA-N 0.000 description 4
- SRIJLARXVRHZKD-UHFFFAOYSA-N OP(O)=O.C=CC1=CC=CC=C1 Chemical compound OP(O)=O.C=CC1=CC=CC=C1 SRIJLARXVRHZKD-UHFFFAOYSA-N 0.000 description 3
- 238000003723 Smelting Methods 0.000 description 3
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- 229910052599 brucite Inorganic materials 0.000 description 3
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- 239000002184 metal Substances 0.000 description 3
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- VSIIXMUUUJUKCM-UHFFFAOYSA-D pentacalcium;fluoride;triphosphate Chemical compound [F-].[Ca+2].[Ca+2].[Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O VSIIXMUUUJUKCM-UHFFFAOYSA-D 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 238000005070 sampling Methods 0.000 description 2
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- HKNFUVXCJNYKQH-UHFFFAOYSA-N [As].[Pt] Chemical compound [As].[Pt] HKNFUVXCJNYKQH-UHFFFAOYSA-N 0.000 description 1
- NEIHULKJZQTQKJ-UHFFFAOYSA-N [Cu].[Ag] Chemical compound [Cu].[Ag] NEIHULKJZQTQKJ-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
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- DVRDHUBQLOKMHZ-UHFFFAOYSA-N chalcopyrite Chemical compound [S-2].[S-2].[Fe+2].[Cu+2] DVRDHUBQLOKMHZ-UHFFFAOYSA-N 0.000 description 1
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- 229910001608 iron mineral Inorganic materials 0.000 description 1
- BBCCCLINBSELLX-UHFFFAOYSA-N magnesium;dihydroxy(oxo)silane Chemical compound [Mg+2].O[Si](O)=O BBCCCLINBSELLX-UHFFFAOYSA-N 0.000 description 1
- 230000005389 magnetism Effects 0.000 description 1
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- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
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- 239000010970 precious metal Substances 0.000 description 1
- 229910052683 pyrite Inorganic materials 0.000 description 1
- 239000011028 pyrite Substances 0.000 description 1
- NIFIFKQPDTWWGU-UHFFFAOYSA-N pyrite Chemical compound [Fe+2].[S-][S-] NIFIFKQPDTWWGU-UHFFFAOYSA-N 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- JOKPITBUODAHEN-UHFFFAOYSA-N sulfanylideneplatinum Chemical compound [Pt]=S JOKPITBUODAHEN-UHFFFAOYSA-N 0.000 description 1
- 229910052569 sulfide mineral Inorganic materials 0.000 description 1
Images
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03B—SEPARATING SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS
- B03B9/00—General arrangement of separating plant, e.g. flow sheets
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03B—SEPARATING SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS
- B03B1/00—Conditioning for facilitating separation by altering physical properties of the matter to be treated
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CN202010320413.3A CN111482266B (zh) | 2020-04-22 | 2020-04-22 | 一种原生脉铂矿尾矿分步分类综合回收有价元素的选矿方法 |
PCT/CN2020/092230 WO2021212595A1 (zh) | 2020-04-22 | 2020-05-26 | 一种原生脉铂矿尾矿分步分类综合回收有价元素的选矿方法 |
ZA2021/01503A ZA202101503B (en) | 2020-04-22 | 2021-03-04 | Mirror |
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CN202010320413.3A CN111482266B (zh) | 2020-04-22 | 2020-04-22 | 一种原生脉铂矿尾矿分步分类综合回收有价元素的选矿方法 |
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CN112538567B (zh) * | 2020-10-30 | 2022-08-09 | 河南佰利联新材料有限公司 | 一种从含铬钛中矿综合回收铬铁矿的方法 |
CN112844857A (zh) * | 2021-01-05 | 2021-05-28 | 广东省科学院资源综合利用研究所 | 一种贵金属定向富集的选矿方法 |
CN112837762B (zh) * | 2021-01-05 | 2023-12-22 | 广东省科学院资源综合利用研究所 | 一种铂钯共生矿的浮选精矿中铂钯品位的预测方法 |
CN114029157B (zh) * | 2021-11-10 | 2024-03-15 | 长春黄金研究院有限公司 | 一种浮选工艺的优化方法 |
CN114453139B (zh) * | 2022-02-28 | 2023-08-04 | 矿冶科技集团有限公司 | 一种脉石矿物的选铁尾矿中回收极低品位磷矿物的选矿方法及其应用 |
CN114534906B (zh) * | 2022-03-08 | 2023-11-17 | 昆明冶金研究院有限公司 | 一种含钼高锌复杂镁硅酸盐蚀变矽卡岩型铜矿的选矿方法 |
CN114602644B (zh) * | 2022-03-14 | 2023-08-18 | 中国地质科学院郑州矿产综合利用研究所 | 一种萤石矿高品位中矿再磨分选方法 |
CN114653472B (zh) * | 2022-03-17 | 2023-09-15 | 中钢集团马鞍山矿山研究总院股份有限公司 | 一种极微细粒赤铁矿石的磁-浮联合选矿新工艺 |
CN114870984B (zh) * | 2022-03-17 | 2023-12-01 | 中钢集团马鞍山矿山研究总院股份有限公司 | 一种极微细粒赤铁矿石的选矿方法 |
CN115055278B (zh) * | 2022-05-25 | 2023-11-14 | 西北矿冶研究院 | 一种从混合型炉渣中综合回收铜及伴生金属的选矿方法 |
CN115010302A (zh) * | 2022-06-14 | 2022-09-06 | 云南农业大学 | 铅锌浮选废水中重金属和黄药类浮选药剂去除装置及方法 |
CN115025885B (zh) * | 2022-06-15 | 2024-04-12 | 金平长安矿业有限公司 | 一种用于提升金矿堆浸尾渣浮选精矿品位的新药剂及其使用方法 |
CN115007327B (zh) * | 2022-07-25 | 2023-08-04 | 矿冶科技集团有限公司 | 高碳难选硫铁矿的选矿方法 |
CN115672564A (zh) * | 2022-10-10 | 2023-02-03 | 西部矿业股份有限公司 | 一种从铜-铅阳极泥侧吹炉高硅炉砖中回收金银的方法 |
CN117019379B (zh) * | 2023-08-10 | 2024-05-24 | 昆明理工大学 | 一种泥质锂云母矿的控泡浮选方法 |
CN117258996B (zh) * | 2023-11-13 | 2024-03-08 | 矿冶科技集团有限公司 | 铬铁矿尾矿综合回收铬和铂钯的选矿方法 |
Family Cites Families (7)
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US4685963A (en) * | 1978-05-22 | 1987-08-11 | Texasgulf Minerals And Metals, Inc. | Process for the extraction of platinum group metals |
JP3276616B2 (ja) * | 1998-10-19 | 2002-04-22 | 日本磁力選鉱株式会社 | 使用済みアルミ加工品からアルミニウムを回収する方法 |
GB0905324D0 (en) * | 2009-03-27 | 2009-05-13 | Univ Birmingham | Metal recovery |
CN102886311B (zh) * | 2012-07-25 | 2014-01-01 | 广州有色金属研究院 | 一种含铂矿物紫硫镍矿的浮选方法 |
CN103212483B (zh) * | 2013-04-17 | 2014-12-31 | 广州有色金属研究院 | 一种含磷铂矿的选矿方法 |
CN105032621B (zh) * | 2015-07-09 | 2017-05-24 | 广东省工业技术研究院(广州有色金属研究院) | 一种原生铂矿选矿方法 |
US11203044B2 (en) * | 2017-06-23 | 2021-12-21 | Anglo American Services (UK) Ltd. | Beneficiation of values from ores with a heap leach process |
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- 2020-04-22 CN CN202010320413.3A patent/CN111482266B/zh active Active
- 2020-05-26 WO PCT/CN2020/092230 patent/WO2021212595A1/zh active Application Filing
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Address after: 510651 No. 363, Changxin Road, Guangzhou, Guangdong, Tianhe District Patentee after: Institute of resource utilization and rare earth development, Guangdong Academy of Sciences Address before: 510651 No. 363, Changxin Road, Guangzhou, Guangdong, Tianhe District Patentee before: Institute of resources comprehensive utilization, Guangdong Academy of Sciences |
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Address after: 510651 No. 363, Changxin Road, Guangzhou, Guangdong, Tianhe District Patentee after: Institute of resources comprehensive utilization, Guangdong Academy of Sciences Address before: No. 363, Changxing Road, Tianhe District, Guangzhou, Guangdong 510650 Patentee before: GUANGDONG INSTITUTE OF RESOURCES COMPREHENSIVE UTILIZATION |
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Application publication date: 20200804 Assignee: Dongguan Linxi Intelligent Technology Co.,Ltd. Assignor: Institute of resource utilization and rare earth development, Guangdong Academy of Sciences Contract record no.: X2023980042097 Denomination of invention: A beneficiation method for step-by-step classification and comprehensive recovery of valuable elements from primary vein platinum ore tailings Granted publication date: 20210827 License type: Common License Record date: 20230919 Application publication date: 20200804 Assignee: Huizhou qingleyuan Intelligent Technology Co.,Ltd. Assignor: Institute of resource utilization and rare earth development, Guangdong Academy of Sciences Contract record no.: X2023980042094 Denomination of invention: A beneficiation method for step-by-step classification and comprehensive recovery of valuable elements from primary vein platinum ore tailings Granted publication date: 20210827 License type: Common License Record date: 20230919 Application publication date: 20200804 Assignee: Foshan chopsticks Technology Co.,Ltd. Assignor: Institute of resource utilization and rare earth development, Guangdong Academy of Sciences Contract record no.: X2023980042086 Denomination of invention: A beneficiation method for step-by-step classification and comprehensive recovery of valuable elements from primary vein platinum ore tailings Granted publication date: 20210827 License type: Common License Record date: 20230919 Application publication date: 20200804 Assignee: Foshan WanChen Technology Co.,Ltd. Assignor: Institute of resource utilization and rare earth development, Guangdong Academy of Sciences Contract record no.: X2023980042075 Denomination of invention: A beneficiation method for step-by-step classification and comprehensive recovery of valuable elements from primary vein platinum ore tailings Granted publication date: 20210827 License type: Common License Record date: 20230919 |
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Application publication date: 20200804 Assignee: Bainuo Zhongcheng (Chongqing) Electronic Technology Co.,Ltd. Assignor: Institute of resource utilization and rare earth development, Guangdong Academy of Sciences Contract record no.: X2023980042504 Denomination of invention: A beneficiation method for step-by-step classification and comprehensive recovery of valuable elements from primary vein platinum ore tailings Granted publication date: 20210827 License type: Common License Record date: 20230925 |
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Application publication date: 20200804 Assignee: MEIZHOU HUALIFENG INDUSTRIAL CO.,LTD. Assignor: Institute of resource utilization and rare earth development, Guangdong Academy of Sciences Contract record no.: X2023980049301 Denomination of invention: A beneficiation method for stepwise classification and comprehensive recovery of valuable elements from primary vein platinum ore tailings Granted publication date: 20210827 License type: Common License Record date: 20231204 |