CN111407858A - Chinese eaglewood mixture for sterilizing, disinfecting, diminishing inflammation and dispelling wind-damp and preparation method thereof - Google Patents
Chinese eaglewood mixture for sterilizing, disinfecting, diminishing inflammation and dispelling wind-damp and preparation method thereof Download PDFInfo
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
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Abstract
The invention relates to a sterilizing, disinfecting, inflammation diminishing and rheumatism expelling agilawood mixture and a preparation method thereof, wherein the sterilizing, disinfecting, inflammation diminishing and rheumatism expelling agilawood mixture adopts agilawood, lignum dalbergiae odoriferae, mulberry branches, mint, herba eriosemae praeparata, desmodium, Chinese alpinia, herba plantaginis, houttuynia cordata, hyssop and purslane as main raw materials and is prepared by proper weight proportion, and finally the agilawood mixture with the effects of sterilizing, diminishing inflammation, disinfecting, expelling rheumatism and the like is prepared. The preparation method of the agilawood mixture is simple to operate, the effective components of the raw material components can be reserved to the maximum extent, and the prepared agilawood mixture for sterilizing, diminishing inflammation and dispelling wind and dampness has good sterilizing, disinfecting, diminishing inflammation and dispelling wind and dampness effects; convenient carrying and use, no toxic or side effect, high-efficiency sterilization and disinfection, and can be directly sprayed on the body or the surrounding environment, thereby achieving the purpose of protecting the user in all directions.
Description
Technical Field
The invention belongs to the technical field of traditional Chinese medicines, and particularly relates to a sterilizing, disinfecting, inflammation diminishing and rheumatism removing agilawood mixture and a preparation method thereof.
Background
In modern living environments, a large number of pathogenic microorganisms exist, and pathogenic bacteria and viruses among them cause various diseases. People can adopt various methods to sterilize and disinfect the surrounding environment, such as spraying chemical preparations to achieve the purpose of killing bacteria, viruses and other microorganisms; or the traditional Chinese medicine burning smoking prevention method is adopted, although the method has obvious effect, the smoke generated by burning is easy to derive a plurality of new diseases, such as a plurality of allergic diseases, and the method can pollute the natural environment and does not meet the requirements of scientific development. In a word, the existing sterilization and disinfection method is single and incomplete, so that an environment-friendly and efficient sterilization and disinfection preparation is urgently needed.
Rheumatism is a group of diseases mainly attacking joints, bones, muscles, blood vessels and related soft tissues or connective tissues, and most of them are autoimmune diseases. The disease is more hidden and slow, the disease course is longer, most diseases have genetic tendency, and diagnosis and treatment are difficult to achieve. Western medicines for treating rheumatism have large side effects, few types of effective traditional Chinese medicines and poor effect, and the condition brings great trouble to patients.
Disclosure of Invention
In order to solve the problems in the prior art, the invention provides a Chinese eaglewood mixture for sterilizing and disinfecting, diminishing inflammation and dispelling wind-damp and a preparation method thereof. The agilawood mixture for sterilizing, diminishing inflammation and dispelling wind-damp has good effects of sterilizing, disinfecting, diminishing inflammation and dispelling wind-damp; the product is convenient to carry and use, has no toxic or side effect, and can be directly sprayed on the body and the surrounding environment to achieve the aim of protecting the user in all directions; can also permeate into the sprayed part of the human body to quickly diminish inflammation and relieve rheumatism symptoms.
The technical scheme adopted by the invention is as follows:
an agilawood mixture for sterilizing, disinfecting, diminishing inflammation and dispelling wind-damp comprises the following raw material components:
10-30 parts of agilawood, 5-15 parts of lignum dalbergiae odoriferae, 400 parts of mint, 50-150 parts of mulberry branch, 40-60 parts of herba eriocauli, 40-60 parts of desmodium, 40-60 parts of Chinese alpine rush, 40-60 parts of plantain herb, 40-60 parts of houttuynia cordata, 40-60 parts of hyssop and 40-60 parts of purslane herb.
Further preferably, the agilawood mixture for sterilizing, diminishing inflammation and dispelling wind-damp comprises the following raw material components:
15 parts of agilawood, 8 parts of lignum dalbergiae odoriferae, 550 parts of mint, 80 parts of mulberry branch, 48 parts of herba felis, 48 parts of longhairy antenoron herb, 55 parts of Chinese alpine rush, 54 parts of plantain herb, 48 parts of heartleaf houttuynia herb, 55 parts of hyssop and 55 parts of purslane herb.
A method for preparing the agilawood mixture for sterilizing, disinfecting, diminishing inflammation and dispelling wind and dampness comprises the following steps:
(1) taking mulberry twigs according to the weight parts, sequentially removing impurities, cleaning, drying, crushing, adding water, mixing, grinding, adding malic acid for acidification, adding saccharomycetes for fermentation to obtain fermentation liquor, sterilizing the fermentation liquor, and filtering to obtain an extraction stock solution A;
(2) mixing the agilawood and the lignum dalbergiae odoriferae in parts by weight, sequentially removing impurities, cleaning, drying, crushing, decocting with water, adding the mint in parts by weight, boiling, and filtering to obtain an extraction stock solution B;
(3) taking the rest raw materials according to the parts by weight, sequentially removing impurities, cleaning, drying, crushing, mixing, adding water, decocting, and filtering to obtain filtrate; concentrating the filtrate to obtain concentrated filtrate; adding ethanol into the concentrated filtrate while stirring, refrigerating under sealed condition, filtering, distilling the filtrate, and recovering ethanol to obtain extract stock solution C;
(4) and mixing the extraction stock solution A, the extraction stock solution B and the extraction stock solution C, and filtering to obtain the agilawood mixture for sterilizing and disinfecting, diminishing inflammation and dispelling wind-damp.
Further, in the step (1), the mass of the added water is 4-6 times of that of the mulberry branches, the mass ratio of the malic acid to the mulberry branches is 1 (5-8), and the acidification time is 6-7 h.
Further, the mass ratio of the yeast to the mulberry branches is 1 (50-80), the fermentation temperature is 36-38 ℃, and the fermentation time is 20-30 days.
Further, the sterilization operation is heating at 150-200 ℃ for 3-5 h.
Further, in the step (2), the mass of the added water is 5-9 times of the total mass of the agilawood and the lignum dalbergiae odoriferae, the decocting temperature is 90-100 ℃, and the decocting time is 2-3 hours; adding herba Menthae, and boiling for 30-60 min.
Further, in the step (3), the mass of the added water is 3-5 times of the total mass of the rest raw materials, the decocting temperature is 90-100 ℃, and the decocting time is 1-2 hours; the concentration is to concentrate the filtrate to 1/2-1/3 of the original filtrate; the adding amount of the ethanol is 75-85% of the mass of the concentrated filtrate, the stirring speed is 100-200rad/min, and the stirring time is 20-40 min; the temperature of the closed refrigeration is 2-10 ℃, and the time of the closed refrigeration is 24-48 h.
Further, in the step (4), the filtration is performed by using a bacterial filter with the pore size of less than 0.22 μm.
The invention discloses a brief introduction of the efficacy of each traditional Chinese medicine:
chenxiang is pungent and bitter in flavor and warm in nature, enters spleen, stomach and kidney meridians, has descending weight, and can lower qi, check adverse flow of qi, warm middle energizer, dispel cold, warm spleen and stomach, and treat abdominal distending pain due to stomach cold and qi stagnation. It can be used for treating constipation caused by lung qi deficiency, and has strong penetrating power.
Reducing true fragrance, pungent taste, warm nature and no toxicity. It enters liver, spleen, lung and heart meridians. Dispel wind, activate blood, regulate qi-flowing and alleviate pain. Can be used for treating rheumatic lumbago, skelalgia, traumatic injury, bronchitis, gastralgia, and hernia pain. Has antibacterial and fungal hypha growth inhibiting effects, and can be used as perfume fixative and disinfectant. It also has effects in scavenging free radicals, resisting oxidation, resisting tumor, resisting lipid peroxidation, scavenging free radicals, resisting virus and allergy, stopping bleeding, relieving diarrhea, and treating burn.
The mulberry branch contains various natural medicinal components, has super-strong anti-inflammatory and antiviral abilities, can prevent the serious breeding in a human body, can enhance the phagocytic ability of macrophages in the human body, can also accelerate the transformation of lymphocytes in the human body, and can obviously enhance the antiviral ability of the human body; has anti-inflammatory, antibacterial, analgesic, and antipruritic effects; clearing heat, promoting diuresis, dispelling pathogenic wind, removing dampness, and dredging channels and collaterals.
Mint, pungent taste, cool in nature; entering lung and liver meridians; fragrant ascending and dispersing; has effects of dispelling pathogenic wind, clearing away heat, refreshing head, benefiting throat, promoting eruption, and relieving depression; can be used for treating wind-heat exterior syndrome, headache, giddiness, conjunctival congestion, swelling and pain, pharyngalgia, hoarseness, nasosinusitis, toothache, measles without adequate eruption, pruritus, liver depression, hypochondriac pain, abdominal distention, scrofula, and tuberculosis.
Mao Cao is sweet, bland and cool. Clear heat, relieve summer-heat and induce diuresis. Can be used for treating common cold, hyperpyrexia, heatstroke, urinary tract infection, nephritic edema, icteric hepatitis, diabetes, and infantile persistent fever. Clearing away heat and toxic materials; cooling blood to stop bleeding; to remove dampness. Polydipsia due to major heat; hematemesis; bleeding; hemoptysis; hematuria; metrorrhagia; jaundice; edema; stranguria with turbid discharge, diarrhea and dysentery; infantile malnutrition fever; furuncle, carbuncle and swelling.
Jin Qian Cao is sweet, salty and slightly cold. It enters liver, gallbladder, kidney and bladder meridians. Clear damp-heat, treat stranguria and relieve swelling. Can be used for treating heat stranguria, stranguria caused by sand, dysuria, jaundice, dark urine, carbuncle, furuncle, and snake bite; calculus of liver and gallbladder, and lithangiuria.
Buxue Cao, bland and cold. Clearing away heat and toxic material, promoting urination and relieving pain. It is indicated for stranguria with difficulty in micturition and impetigo.
Plantain herb, sweet and cold. It enters liver, kidney, lung and small intestine meridians. Clear heat and induce diuresis, dispel phlegm, cool blood and remove toxicity. Can be used for treating edema, oliguria, pyretic stranguria, pain, summer-heat, damp diarrhea, dysentery, phlegm heat, cough, hematemesis, epistaxis, carbuncle, swelling, and sore.
Yu xing Cao, pungent and slightly cold. It enters lung meridian. Clearing away heat and toxic material, curing abscess and discharging pus, inducing diuresis and treating stranguria. Can be used for treating lung abscess with purulent vomiting, phlegm heat, cough and asthma, dysentery, pyretic stranguria, carbuncle, swelling, and sore.
Hyssop has the effects of promoting blood circulation and stimulating the menstrual flow, is used for amenorrhea, dysmenorrheal, irregular menstruation, postpartum abdominal pain and traumatic injury caused by blood stasis, strengthening bones and muscles, is also used for treating lumbago due to kidney deficiency, soreness and weakness of waist and knees caused by chronic arthralgia, and the like, is used for treating fire-heat flaring up such as liver and kidney deficiency, headache, dizziness, hematemesis, epistaxis and the like, and treating the syndrome of fire-heat hyperactivity due to yin deficiency and fire hyperactivity, such as headache, dizziness and conjunctival congestion caused by liver-yang hyperactivity.
Purslane, sour, cold. Clear heat and promote diuresis, cool blood and remove toxicity. Can be used for treating bacillary dysentery, acute gastroenteritis, acute appendicitis, mastitis, hemorrhoid hemorrhage, and leucorrhea; it is used externally to treat furuncle, eczema and herpes zoster.
The invention has the beneficial effects that:
the agilawood mixture with the effects of sterilization, disinfection, inflammation diminishing and rheumatism dispelling is prepared by adopting agilawood, lignum dalbergiae odoriferae, mulberry branches, mint, herba eriosemae petatae, desmodium, Chinese alpine rush, plantain herb, houttuynia cordata, hyssop and portulaca oleracea as main raw materials in a proper weight ratio. The preparation method of the sterilizing, disinfecting, inflammation diminishing and rheumatism dispelling agilawood mixture is simple to operate, the effective components of the raw material components can be reserved to the maximum extent, and the prepared sterilizing, disinfecting, inflammation diminishing and rheumatism dispelling agilawood mixture has good sterilizing, disinfecting, inflammation diminishing and rheumatism dispelling effects; convenient carrying and use, environmental protection, no toxic or side effect, and can be directly sprayed on the body or in the surrounding environment, and the high-efficiency sterilization and disinfection can achieve the aim of protecting the user in all directions. The components in the formula interact with each other, and can permeate into the spraying part of the human body to diminish inflammation and sterilize, so that the rheumatism symptom is relieved: the rheumatic disease is a group of very common symptoms mainly including arthritis and wind chill, such as bone, joint, muscle and surrounding soft tissues, bursa, fascia and blood vessels, and the effective components of the rheumatic disease have the function of relieving the symptoms of rheumatism, arthritis and the like; human body tests show that when the product is used for a plurality of times at arthritis, inflammation and swelling can be gradually dissipated and become small, swelling and fading can occur after the product is used by patients with large rheumatic swelling, and the effective rate is 100%; meanwhile, the product of the invention also has the effects of sterilization and inflammation diminishing on rubella, skin itch, miliaria and the like, the discomfort of an affected part can be effectively relieved after the product is used, the red spots are lightened, and the itch disappears; the product of the invention also has good anti-inflammation and treatment effects on scalds.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the technical solutions of the present invention will be described in detail below. It is to be understood that the described embodiments are merely exemplary of the invention, and not restrictive of the full scope of the invention. All other embodiments, which can be derived by a person skilled in the art from the examples given herein without any inventive step, are within the scope of the present invention.
In the following examples 1g is represented by 1 part by weight.
Example 1
The embodiment provides a sterilizing, disinfecting, inflammation diminishing and rheumatism removing agilawood mixture, which comprises the following raw material components:
10 parts of agilawood, 5 parts of lignum dalbergiae odoriferae, 400 parts of mint, 50 parts of mulberry twig, 40 parts of herba felis, 40 parts of desmodium, 40 parts of Chinese alpine rush, 40 parts of plantain herb, 40 parts of houttuynia cordata, 40 parts of hyssop and 40 parts of purslane herb.
Further, the embodiment provides a preparation method of the agilawood mixture for sterilizing, disinfecting, diminishing inflammation and dispelling wind-damp, which comprises the following steps:
(1) taking mulberry branches according to the weight parts, sequentially removing impurities, cleaning, drying and crushing, adding water with the mass 4 times that of the mulberry branches, mixing and grinding, adding malic acid with the mass of 1/8 of the mulberry branches, acidifying for 7 hours, adding yeast with the mass of 1/80 of the mulberry branches, fermenting for 30 days at 36 ℃ to obtain fermentation liquor, heating the fermentation liquor at high temperature of 150 ℃ for 5 hours, and filtering to obtain an extraction stock solution A;
(2) mixing the agilawood and the lignum dalbergiae odoriferae in parts by weight, sequentially removing impurities, cleaning, drying and crushing, adding water which is 5 times of the total mass of the agilawood and the lignum dalbergiae odoriferae, decocting at 90 ℃ for 3 hours, adding the mint in parts by weight, boiling for 60min, and filtering to obtain an extraction stock solution B;
(3) taking the rest raw materials according to the parts by weight, sequentially removing impurities, cleaning, drying and crushing, mixing, adding water which is 3 times of the total mass of the rest raw materials, decocting at 90 ℃ for 2 hours, and filtering to obtain filtrate; concentrating the filtrate to 1/3 of the original filtrate mass to obtain concentrated filtrate; adding ethanol with the mass being 75% of that of the concentrated filtrate into the concentrated filtrate, stirring at the speed of 100rad/min for 40min, hermetically refrigerating at the temperature of 2 ℃ for 24h, filtering, distilling the obtained filtrate, and recovering the ethanol to obtain an extraction stock solution C;
(4) and mixing the extraction stock solution A, the extraction stock solution B and the extraction stock solution C, and filtering by using a bacterial filter with the pore diameter of less than 0.22 mu m to obtain the agilawood mixture for sterilizing, disinfecting, diminishing inflammation and dispelling wind and dampness.
Example 2
The embodiment provides a sterilizing, disinfecting, inflammation diminishing and rheumatism removing agilawood mixture, which comprises the following raw material components:
30 parts of agilawood, 15 parts of lignum dalbergiae odoriferae, 600 parts of mint, 150 parts of mulberry branch, 60 parts of herba eriocauli, 60 parts of desmodium, 60 parts of Chinese alpine rush, 60 parts of plantain herb, 60 parts of houttuynia cordata, 60 parts of hyssop and 60 parts of purslane herb.
Further, the embodiment provides a preparation method of the agilawood mixture for sterilizing, disinfecting, diminishing inflammation and dispelling wind-damp, which comprises the following steps:
(1) taking mulberry branches according to the weight parts, sequentially removing impurities, cleaning, drying and crushing, adding water with the mass 6 times that of the mulberry branches, mixing and grinding, adding malic acid with the mass of 1/5 of the mulberry branches, acidifying for 6 hours, adding yeast with the mass of 1/50 of the mulberry branches, fermenting for 20 days at 38 ℃ to obtain fermentation liquor, heating the fermentation liquor at a high temperature of 200 ℃ for 3 hours, and filtering to obtain an extraction stock solution A;
(2) mixing the agilawood and the lignum dalbergiae odoriferae in parts by weight, sequentially removing impurities, cleaning, drying and crushing, adding water which is 9 times of the total mass of the agilawood and the lignum dalbergiae odoriferae, decocting at 100 ℃ for 2 hours, adding the mint in parts by weight, boiling for 30min, and filtering to obtain an extraction stock solution B;
(3) taking the rest raw materials according to the parts by weight, sequentially removing impurities, cleaning, drying and crushing, mixing, adding water which is 5 times of the total mass of the rest raw materials, decocting at 100 ℃ for 1 hour, and filtering to obtain filtrate; concentrating the filtrate to 1/2 of the original filtrate mass to obtain concentrated filtrate; adding ethanol accounting for 85% of the mass of the concentrated filtrate into the concentrated filtrate, stirring at a speed of 200rad/min for 20min, hermetically refrigerating at 10 ℃ for 48h, filtering, distilling the obtained filtrate, and recovering ethanol to obtain an extraction stock solution C;
(4) and mixing the extraction stock solution A, the extraction stock solution B and the extraction stock solution C, and filtering by using a bacterial filter with the pore diameter of less than 0.22 mu m to obtain the agilawood mixture for sterilizing, disinfecting, diminishing inflammation and dispelling wind and dampness.
Example 3
The embodiment provides a sterilizing, disinfecting, inflammation diminishing and rheumatism removing agilawood mixture, which comprises the following raw material components:
15 parts of agilawood, 8 parts of lignum dalbergiae odoriferae, 550 parts of mint, 80 parts of mulberry branch, 48 parts of herba felis, 48 parts of longhairy antenoron herb, 55 parts of Chinese alpine rush, 54 parts of plantain herb, 48 parts of heartleaf houttuynia herb, 55 parts of hyssop and 55 parts of purslane herb.
Further, the embodiment provides a preparation method of the agilawood mixture for sterilizing, disinfecting, diminishing inflammation and dispelling wind-damp, which comprises the following steps:
(1) taking mulberry twigs according to the weight parts, sequentially removing impurities, cleaning, drying and crushing, adding water with the mass 5 times that of the mulberry twigs, mixing and grinding, adding malic acid with the mass of 1/6 of the mulberry twigs, acidifying for 6.5 hours, adding yeast with the mass of 1/60 of the mulberry twigs, fermenting for 25 days at 37 ℃ to obtain fermentation liquor, heating the fermentation liquor at high temperature of 160 ℃ for 4 hours, and filtering to obtain an extraction stock solution A;
(2) mixing the agilawood and the lignum dalbergiae odoriferae in parts by weight, sequentially removing impurities, cleaning, drying and crushing, adding water which is 7 times of the total mass of the agilawood and the lignum dalbergiae odoriferae, decocting at 95 ℃ for 2.5 hours, adding the mint in parts by weight, boiling for 45min, and filtering to obtain an extraction stock solution B;
(3) taking the rest raw materials according to the parts by weight, sequentially removing impurities, cleaning, drying and crushing, mixing, adding water which is 4 times of the total mass of the rest raw materials, decocting at 95 ℃ for 1.5h, and filtering to obtain filtrate; concentrating the filtrate to 5/12 of the original filtrate mass to obtain concentrated filtrate; adding ethanol with the mass percent of 80% of the concentrated filtrate into the concentrated filtrate, stirring at the same time for 30min at the speed of 150rad/min, carrying out sealed refrigeration at the temperature of 6 ℃ for 36h, then filtering, distilling the obtained filtrate, and recovering the ethanol to obtain an extraction stock solution C;
(4) and mixing the extraction stock solution A, the extraction stock solution B and the extraction stock solution C, and filtering by using a bacterial filter with the pore diameter of less than 0.22 mu m to obtain the agilawood mixture for sterilizing, disinfecting, diminishing inflammation and dispelling wind and dampness.
Example 4
The embodiment provides a sterilizing, disinfecting, inflammation diminishing and rheumatism removing agilawood mixture, which comprises the following raw material components:
20 parts of agilawood, 10 parts of lignum dalbergiae odoriferae, 500 parts of mint, 100 parts of mulberry twig, 50 parts of herba felis, 50 parts of desmodium, 50 parts of Chinese alpine rush, 50 parts of plantain herb, 50 parts of houttuynia cordata, 50 parts of hyssop and 50 parts of purslane.
Further, the embodiment provides a preparation method of the agilawood mixture for sterilizing, disinfecting, diminishing inflammation and dispelling wind-damp, which comprises the following steps:
(1) taking mulberry twigs according to the weight parts, sequentially removing impurities, cleaning, drying and crushing, adding water with the mass 5 times that of the mulberry twigs, mixing and grinding, adding malic acid with the mass of 1/7 of the mulberry twigs, acidifying for 6.5 hours, adding yeast with the mass of 1/70 of the mulberry twigs, fermenting for 25 days at 37 ℃ to obtain fermentation liquor, heating the fermentation liquor at high temperature of 180 ℃ for 4 hours, and filtering to obtain an extraction stock solution A;
(2) mixing the agilawood and the lignum dalbergiae odoriferae in parts by weight, sequentially removing impurities, cleaning, drying and crushing, adding water which is 8 times of the total mass of the agilawood and the lignum dalbergiae odoriferae, decocting at 95 ℃ for 2.5 hours, adding the mint in parts by weight, boiling for 45min, and filtering to obtain an extraction stock solution B;
(3) taking the rest raw materials according to the parts by weight, sequentially removing impurities, cleaning, drying and crushing, mixing, adding water which is 4 times of the total mass of the rest raw materials, decocting at 95 ℃ for 1.5h, and filtering to obtain filtrate; concentrating the filtrate to 5/12 of the original filtrate mass to obtain concentrated filtrate; adding ethanol with the mass percent of 80% of the concentrated filtrate into the concentrated filtrate, stirring at the same time for 30min at the speed of 150rad/min, carrying out sealed refrigeration at the temperature of 6 ℃ for 36h, then filtering, distilling the obtained filtrate, and recovering the ethanol to obtain an extraction stock solution C;
(4) and mixing the extraction stock solution A, the extraction stock solution B and the extraction stock solution C, and filtering by using a bacterial filter with the pore diameter of less than 0.22 mu m to obtain the agilawood mixture for sterilizing, disinfecting, diminishing inflammation and dispelling wind and dampness.
Examples of the experiments
Firstly, the anti-inflammation and rheumatism-expelling efficacy of the agilawood mixture obtained in the embodiment 4 of the invention is tested.
1. 386 patients with arthritis, scapulohumeral periarthritis, cervical spondylosis, rheumatism, swelling, muscle pain, articular cartilage pain, etc. of 20-70 years old with unlimited nature are selected; the treatment was carried out using the eaglewood mixture obtained in example 4 of the present invention.
2. Criteria for efficacy assessment
And (3) curing: the symptoms and physical signs are completely eliminated, and the self-care ability is completely recovered;
the effect is shown: the symptoms and physical signs are mostly eliminated, and the self-care ability is basically recovered;
the method has the following advantages: the symptoms and physical signs are obviously changed, and the self-care ability is recovered;
and (4) invalidation: the symptoms and physical signs are not obviously improved, and the self-care ability is not recovered;
3. the results of the efficacy evaluation are shown in Table 1
Table 1-results of efficacy testing of the eaglewood composition obtained in example 4.
Number of examples | Recovery method | Show effect | Is effective | Invalidation | Total effective rate (%) |
386 | 287 | 73 | 26 | 0 | 100 |
As can be seen from table 1, the agilawood mixture obtained in example 4 of the invention has an obvious curative effect on patients with inflammation such as muscle or articular cartilage tissue pain, such as arthritis, scapulohumeral periarthritis, cervical spondylosis, rheumatic swelling, and the like, and the total effective rate is 100%, which indicates that the agilawood mixture obtained in example 4 of the invention has good anti-inflammatory and rheumatism-expelling effects.
Secondly, the efficacy and the characteristics of the agarwood mixture obtained in the embodiment 4 of the invention are comprehensively evaluated and explained, and the specific contents are shown in table 2.
TABLE 2-evaluation of the efficacy and Properties of the compositions of example 4
The above description is only for the specific embodiments of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art can easily conceive of the changes or substitutions within the technical scope of the present invention, and all the changes or substitutions should be covered within the scope of the present invention. Therefore, the protection scope of the present invention shall be subject to the protection scope of the appended claims.
Claims (10)
1. The agilawood mixture for sterilizing and disinfecting, diminishing inflammation and dispelling wind-damp is characterized by comprising the following raw material components:
10-30 parts of agilawood, 5-15 parts of lignum dalbergiae odoriferae, 400 parts of mint, 50-150 parts of mulberry branch, 40-60 parts of herba eriocauli, 40-60 parts of desmodium, 40-60 parts of Chinese alpine rush, 40-60 parts of plantain herb, 40-60 parts of houttuynia cordata, 40-60 parts of hyssop and 40-60 parts of purslane herb.
2. The agilawood mixture for sterilizing and disinfecting, diminishing inflammation and dispelling wind-damp as claimed in claim 1, wherein the raw material components comprise:
15 parts of agilawood, 8 parts of lignum dalbergiae odoriferae, 550 parts of mint, 80 parts of mulberry branch, 48 parts of herba felis, 48 parts of longhairy antenoron herb, 55 parts of Chinese alpine rush, 54 parts of plantain herb, 48 parts of heartleaf houttuynia herb, 55 parts of hyssop and 55 parts of purslane herb.
3. The agilawood mixture for sterilizing and disinfecting, diminishing inflammation and dispelling wind-damp as claimed in claim 1, wherein the raw material components comprise:
20 parts of agilawood, 10 parts of lignum dalbergiae odoriferae, 500 parts of mint, 100 parts of mulberry twig, 50 parts of herba felis, 50 parts of desmodium, 50 parts of Chinese alpine rush, 50 parts of plantain herb, 50 parts of houttuynia cordata, 50 parts of hyssop and 50 parts of purslane.
4. A method for preparing the sterilizing, disinfecting, anti-inflammatory and rheumatism-expelling aquilaria resinifera mixture as defined in any one of claims 1 to 3, which comprises the following steps:
(1) taking mulberry twigs according to the weight parts, sequentially removing impurities, cleaning, drying, crushing, adding water, mixing, grinding, adding malic acid for acidification, adding saccharomycetes for fermentation to obtain fermentation liquor, sterilizing the fermentation liquor, and filtering to obtain an extraction stock solution A;
(2) mixing the agilawood and the lignum dalbergiae odoriferae in parts by weight, sequentially removing impurities, cleaning, drying, crushing, decocting with water, adding the mint in parts by weight, boiling, and filtering to obtain an extraction stock solution B;
(3) taking the rest raw materials according to the parts by weight, sequentially removing impurities, cleaning, drying, crushing, mixing, adding water, decocting, and filtering to obtain filtrate; concentrating the filtrate to obtain concentrated filtrate; adding ethanol into the concentrated filtrate while stirring, refrigerating under sealed condition, filtering, distilling the filtrate, and recovering ethanol to obtain extract stock solution C;
(4) and mixing the extraction stock solution A, the extraction stock solution B and the extraction stock solution C, and filtering to obtain the agilawood mixture for sterilizing and disinfecting, diminishing inflammation and dispelling wind-damp.
5. The agilawood mixture for sterilizing and disinfecting, diminishing inflammation and dispelling wind-damp as claimed in claim 4, wherein in step (1), the mass of the added water is 4-6 times of that of the mulberry branches, the mass ratio of malic acid to the mulberry branches is 1 (5-8), and the acidification time is 6-7 h.
6. The agilawood mixture for sterilizing and disinfecting, diminishing inflammation and dispelling wind-damp as claimed in claim 4, wherein in the step (1), the mass ratio of the yeast to the mulberry tree branches is 1 (50-80), the fermentation temperature is 36-38 ℃, and the fermentation time is 20-30 days.
7. The mixture as claimed in claim 4, wherein the sterilization, disinfection, anti-inflammation and wind-damp-dispelling is performed by heating at 200 ℃ for 3-5h in step (1).
8. The agilawood mixture for sterilizing and disinfecting, diminishing inflammation and dispelling wind-damp according to claim 4, wherein in the step (2), the mass of the added water is 5-9 times of the total mass of the agilawood and the lignum dalbergiae odoriferae, the decocting temperature is 90-100 ℃, and the decocting time is 2-3 hours; adding herba Menthae, and boiling for 30-60 min.
9. The agilawood mixture for sterilizing and disinfecting, diminishing inflammation and dispelling wind-damp according to claim 4, wherein in the step (3), the mass of the added water is 3-5 times of the total mass of the rest raw materials, the decocting temperature is 90-100 ℃, and the decocting time is 1-2 h; the concentration is to concentrate the filtrate to 1/2-1/3 of the original filtrate; the adding amount of the ethanol is 75-85% of the mass of the concentrated filtrate, the stirring speed is 100-200rad/min, and the stirring time is 20-40 min; the temperature of the closed refrigeration is 2-10 ℃, and the time of the closed refrigeration is 24-48 h.
10. The mixture of claim 4, wherein in step (4), the filter is a bacterial filter with a pore size less than 0.22 μm.
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