CN1113246A - 酸性氨基酸树脂 - Google Patents
酸性氨基酸树脂 Download PDFInfo
- Publication number
- CN1113246A CN1113246A CN95104857A CN95104857A CN1113246A CN 1113246 A CN1113246 A CN 1113246A CN 95104857 A CN95104857 A CN 95104857A CN 95104857 A CN95104857 A CN 95104857A CN 1113246 A CN1113246 A CN 1113246A
- Authority
- CN
- China
- Prior art keywords
- amino acid
- acidic amino
- resin
- poly
- dehydration
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 229920005989 resin Polymers 0.000 title claims abstract description 51
- 239000011347 resin Substances 0.000 title claims abstract description 51
- 150000001413 amino acids Chemical class 0.000 title claims abstract description 44
- 230000002378 acidificating effect Effects 0.000 title claims abstract description 41
- 235000001014 amino acid Nutrition 0.000 claims abstract description 43
- 229920000768 polyamine Polymers 0.000 claims abstract description 21
- 238000004132 cross linking Methods 0.000 claims abstract description 9
- CKLJMWTZIZZHCS-REOHCLBHSA-N L-aspartic acid Chemical compound OC(=O)[C@@H](N)CC(O)=O CKLJMWTZIZZHCS-REOHCLBHSA-N 0.000 claims abstract description 5
- 235000003704 aspartic acid Nutrition 0.000 claims abstract description 4
- OQFSQFPPLPISGP-UHFFFAOYSA-N beta-carboxyaspartic acid Natural products OC(=O)C(N)C(C(O)=O)C(O)=O OQFSQFPPLPISGP-UHFFFAOYSA-N 0.000 claims abstract description 4
- 230000018044 dehydration Effects 0.000 claims description 22
- 238000006297 dehydration reaction Methods 0.000 claims description 22
- 238000006243 chemical reaction Methods 0.000 claims description 19
- 238000006460 hydrolysis reaction Methods 0.000 claims description 11
- 238000000034 method Methods 0.000 claims description 11
- 230000007062 hydrolysis Effects 0.000 claims description 6
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 claims description 5
- 229910052751 metal Inorganic materials 0.000 claims description 2
- 239000002184 metal Substances 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 claims description 2
- 125000005462 imide group Chemical group 0.000 claims 2
- 239000002250 absorbent Substances 0.000 abstract description 5
- 150000001339 alkali metal compounds Chemical class 0.000 abstract description 3
- 230000003301 hydrolyzing effect Effects 0.000 abstract 1
- 230000000379 polymerizing effect Effects 0.000 abstract 1
- 239000002562 thickening agent Substances 0.000 abstract 1
- 229940024606 amino acid Drugs 0.000 description 33
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 15
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 15
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 11
- 239000007864 aqueous solution Substances 0.000 description 10
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 7
- 238000010438 heat treatment Methods 0.000 description 7
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 6
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- 230000004927 fusion Effects 0.000 description 6
- 239000000843 powder Substances 0.000 description 6
- 238000000354 decomposition reaction Methods 0.000 description 5
- -1 household supplies Substances 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- 239000011541 reaction mixture Substances 0.000 description 5
- 239000000243 solution Substances 0.000 description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- 125000001931 aliphatic group Chemical group 0.000 description 4
- 239000003795 chemical substances by application Substances 0.000 description 4
- 238000001035 drying Methods 0.000 description 4
- 150000003949 imides Chemical group 0.000 description 4
- 230000008961 swelling Effects 0.000 description 4
- RSJKGSCJYJTIGS-UHFFFAOYSA-N undecane Chemical compound CCCCCCCCCCC RSJKGSCJYJTIGS-UHFFFAOYSA-N 0.000 description 4
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
- 230000002745 absorbent Effects 0.000 description 3
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 3
- 229960005261 aspartic acid Drugs 0.000 description 3
- 230000006837 decompression Effects 0.000 description 3
- 230000008034 disappearance Effects 0.000 description 3
- 238000001914 filtration Methods 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 238000001556 precipitation Methods 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- VILCJCGEZXAXTO-UHFFFAOYSA-N 2,2,2-tetramine Chemical compound NCCNCCNCCN VILCJCGEZXAXTO-UHFFFAOYSA-N 0.000 description 2
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 description 2
- 206010013786 Dry skin Diseases 0.000 description 2
- WHUUTDBJXJRKMK-VKHMYHEASA-N L-glutamic acid Chemical compound OC(=O)[C@@H](N)CCC(O)=O WHUUTDBJXJRKMK-VKHMYHEASA-N 0.000 description 2
- 229920003171 Poly (ethylene oxide) Polymers 0.000 description 2
- 229920000805 Polyaspartic acid Polymers 0.000 description 2
- 235000002597 Solanum melongena Nutrition 0.000 description 2
- 244000061458 Solanum melongena Species 0.000 description 2
- 238000007259 addition reaction Methods 0.000 description 2
- 239000003637 basic solution Substances 0.000 description 2
- 238000009833 condensation Methods 0.000 description 2
- 230000005494 condensation Effects 0.000 description 2
- 150000004985 diamines Chemical class 0.000 description 2
- 239000000706 filtrate Substances 0.000 description 2
- NAQMVNRVTILPCV-UHFFFAOYSA-N hexane-1,6-diamine Chemical compound NCCCCCCN NAQMVNRVTILPCV-UHFFFAOYSA-N 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 108010064470 polyaspartate Proteins 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 230000008719 thickening Effects 0.000 description 2
- RNLHGQLZWXBQNY-UHFFFAOYSA-N 3-(aminomethyl)-3,5,5-trimethylcyclohexan-1-amine Chemical compound CC1(C)CC(N)CC(C)(CN)C1 RNLHGQLZWXBQNY-UHFFFAOYSA-N 0.000 description 1
- YBRVSVVVWCFQMG-UHFFFAOYSA-N 4,4'-diaminodiphenylmethane Chemical compound C1=CC(N)=CC=C1CC1=CC=C(N)C=C1 YBRVSVVVWCFQMG-UHFFFAOYSA-N 0.000 description 1
- KSMVBYPXNKCPAJ-UHFFFAOYSA-N 4-Methylcyclohexylamine Chemical compound CC1CCC(N)CC1 KSMVBYPXNKCPAJ-UHFFFAOYSA-N 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- 229920002785 Croscarmellose sodium Polymers 0.000 description 1
- CKLJMWTZIZZHCS-UHFFFAOYSA-N D-OH-Asp Natural products OC(=O)C(N)CC(O)=O CKLJMWTZIZZHCS-UHFFFAOYSA-N 0.000 description 1
- MQJKPEGWNLWLTK-UHFFFAOYSA-N Dapsone Chemical compound C1=CC(N)=CC=C1S(=O)(=O)C1=CC=C(N)C=C1 MQJKPEGWNLWLTK-UHFFFAOYSA-N 0.000 description 1
- RPNUMPOLZDHAAY-UHFFFAOYSA-N Diethylenetriamine Chemical compound NCCNCCN RPNUMPOLZDHAAY-UHFFFAOYSA-N 0.000 description 1
- 241001640034 Heteropterys Species 0.000 description 1
- CKLJMWTZIZZHCS-UWTATZPHSA-N L-Aspartic acid Natural products OC(=O)[C@H](N)CC(O)=O CKLJMWTZIZZHCS-UWTATZPHSA-N 0.000 description 1
- SECXISVLQFMRJM-UHFFFAOYSA-N N-Methylpyrrolidone Chemical compound CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 description 1
- XUYPXLNMDZIRQH-LURJTMIESA-N N-acetyl-L-methionine Chemical compound CSCC[C@@H](C(O)=O)NC(C)=O XUYPXLNMDZIRQH-LURJTMIESA-N 0.000 description 1
- 239000004372 Polyvinyl alcohol Substances 0.000 description 1
- NSOXQYCFHDMMGV-UHFFFAOYSA-N Tetrakis(2-hydroxypropyl)ethylenediamine Chemical compound CC(O)CN(CC(C)O)CCN(CC(C)O)CC(C)O NSOXQYCFHDMMGV-UHFFFAOYSA-N 0.000 description 1
- FDLQZKYLHJJBHD-UHFFFAOYSA-N [3-(aminomethyl)phenyl]methanamine Chemical group NCC1=CC=CC(CN)=C1 FDLQZKYLHJJBHD-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000008065 acid anhydrides Chemical class 0.000 description 1
- 229940048053 acrylate Drugs 0.000 description 1
- 125000002723 alicyclic group Chemical group 0.000 description 1
- 150000001408 amides Chemical class 0.000 description 1
- 150000001414 amino alcohols Chemical class 0.000 description 1
- 150000008064 anhydrides Chemical group 0.000 description 1
- 239000001506 calcium phosphate Substances 0.000 description 1
- 229910000389 calcium phosphate Inorganic materials 0.000 description 1
- 235000011010 calcium phosphates Nutrition 0.000 description 1
- 239000007810 chemical reaction solvent Substances 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 229920001577 copolymer Polymers 0.000 description 1
- 239000003431 cross linking reagent Substances 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 230000000881 depressing effect Effects 0.000 description 1
- 230000003292 diminished effect Effects 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 239000012065 filter cake Substances 0.000 description 1
- 229960002989 glutamic acid Drugs 0.000 description 1
- 229920000578 graft copolymer Polymers 0.000 description 1
- 238000002329 infrared spectrum Methods 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 239000004816 latex Substances 0.000 description 1
- 229920000126 latex Polymers 0.000 description 1
- 235000012204 lemonade/lime carbonate Nutrition 0.000 description 1
- 229930182817 methionine Natural products 0.000 description 1
- 239000012046 mixed solvent Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- YWAKXRMUMFPDSH-UHFFFAOYSA-N pentene Chemical compound CCCC=C YWAKXRMUMFPDSH-UHFFFAOYSA-N 0.000 description 1
- 229920001495 poly(sodium acrylate) polymer Polymers 0.000 description 1
- 229920000570 polyether Polymers 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 229920002451 polyvinyl alcohol Polymers 0.000 description 1
- 238000011085 pressure filtration Methods 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- APSBXTVYXVQYAB-UHFFFAOYSA-M sodium docusate Chemical compound [Na+].CCCCC(CC)COC(=O)CC(S([O-])(=O)=O)C(=O)OCC(CC)CCCC APSBXTVYXVQYAB-UHFFFAOYSA-M 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- FAGUFWYHJQFNRV-UHFFFAOYSA-N tetraethylenepentamine Chemical compound NCCNCCNCCNCCN FAGUFWYHJQFNRV-UHFFFAOYSA-N 0.000 description 1
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 description 1
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1
- 229920002554 vinyl polymer Polymers 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F8/00—Chemical modification by after-treatment
- C08F8/30—Introducing nitrogen atoms or nitrogen-containing groups
- C08F8/32—Introducing nitrogen atoms or nitrogen-containing groups by reaction with amines
Landscapes
- Chemical & Material Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)
- Biological Depolymerization Polymers (AREA)
- Polyamides (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP101203/94 | 1994-05-16 | ||
| JP6101203A JPH07309943A (ja) | 1994-05-16 | 1994-05-16 | 酸性アミノ酸系樹脂 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1113246A true CN1113246A (zh) | 1995-12-13 |
Family
ID=14294379
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN95104857A Pending CN1113246A (zh) | 1994-05-16 | 1995-05-16 | 酸性氨基酸树脂 |
Country Status (5)
| Country | Link |
|---|---|
| EP (1) | EP0683177A2 (enExample) |
| JP (1) | JPH07309943A (enExample) |
| KR (1) | KR950032376A (enExample) |
| CN (1) | CN1113246A (enExample) |
| CA (1) | CA2149382A1 (enExample) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105037726A (zh) * | 2015-07-23 | 2015-11-11 | 罗美柏 | 一种环境友好型聚天冬高吸水性树脂的合成方法 |
| CN110054720A (zh) * | 2019-04-26 | 2019-07-26 | 台湾塑胶工业股份有限公司 | 吸水性树脂组成物 |
| CN110330956A (zh) * | 2019-07-10 | 2019-10-15 | 黑龙江益瑞化工有限公司 | 一种环保型钻井液用聚氨基酸类降粘剂及其制备方法 |
| CN110444113A (zh) * | 2018-05-04 | 2019-11-12 | 三星显示有限公司 | 可折叠显示设备和制造可折叠显示设备的方法 |
| CN116284751A (zh) * | 2022-09-09 | 2023-06-23 | 长江大学 | 聚天冬氨酸衍生物及其制备方法与作为润滑剂的应用、水基钻井液及其应用 |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5986042A (en) * | 1997-01-30 | 1999-11-16 | Mitsui Chemicals, Inc. | Cross-linked polymer |
| US6072024A (en) * | 1997-03-21 | 2000-06-06 | Mitsui Chemicals, Inc. | Production process of cross-linked polyaspartic acid resin |
| DE69821548T2 (de) * | 1997-05-29 | 2004-12-30 | Rohm And Haas Co. | Vernetzte Polyaminsäure und deren Verfahren zur Herstellung |
| US6360129B1 (en) | 1999-12-13 | 2002-03-19 | Cardiac Pacemakers, Inc. | Mannitol/hydrogel cap for tissue-insertable connections |
| JP2002179791A (ja) * | 2000-12-07 | 2002-06-26 | Mitsui Chemicals Inc | 架橋ポリアスパラギン酸（塩）及びその製造方法 |
| JP4541598B2 (ja) * | 2001-07-03 | 2010-09-08 | 三井化学株式会社 | 架橋ポリコハク酸イミドの連続式製造方法 |
| JP4586022B2 (ja) | 2003-09-29 | 2010-11-24 | 日東電工株式会社 | インビボポリヌクレオチド送達用生分解性ポリアセタール |
| US7364879B2 (en) | 2003-12-19 | 2008-04-29 | Tung Hai Biotechnology Corporation | Stable biodegradable, high water absorbable polyglutamic acid hydrogel by 3-dimensional cross-linking and its preparation method |
| JP2006213697A (ja) * | 2005-01-07 | 2006-08-17 | Mitsui Chemicals Inc | 皮膚外用剤組成物 |
| US7674452B2 (en) | 2005-03-16 | 2010-03-09 | Nitto Denko Corporation | Polymer coating of cells |
| US7588754B2 (en) | 2005-05-10 | 2009-09-15 | Nitto Denko Corporation | Biodegradable polyacetals and methods |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AU637332B2 (en) * | 1988-09-29 | 1993-05-27 | Chevron Research And Technology Company | Novel polymeric dispersants having alternating polyalkylene and succinic groups |
| US5286810A (en) * | 1992-08-07 | 1994-02-15 | Srchem Incorporated | Salt of polymer from maleic acid, polyamind and ammonia |
-
1994
- 1994-05-16 JP JP6101203A patent/JPH07309943A/ja active Pending
-
1995
- 1995-05-09 EP EP95106976A patent/EP0683177A2/en not_active Withdrawn
- 1995-05-11 KR KR1019950011561A patent/KR950032376A/ko not_active Withdrawn
- 1995-05-15 CA CA002149382A patent/CA2149382A1/en not_active Abandoned
- 1995-05-16 CN CN95104857A patent/CN1113246A/zh active Pending
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105037726A (zh) * | 2015-07-23 | 2015-11-11 | 罗美柏 | 一种环境友好型聚天冬高吸水性树脂的合成方法 |
| CN110444113A (zh) * | 2018-05-04 | 2019-11-12 | 三星显示有限公司 | 可折叠显示设备和制造可折叠显示设备的方法 |
| US11615721B2 (en) | 2018-05-04 | 2023-03-28 | Samsung Display Co., Ltd. | Foldable display device |
| US11688308B2 (en) | 2018-05-04 | 2023-06-27 | Samsung Display Co., Ltd. | Foldable display device and method of manufacturing foldable display device |
| US12211404B2 (en) | 2018-05-04 | 2025-01-28 | Samsung Display Co., Ltd. | Foldable display device and method of manufacturing foldable display device |
| CN110054720A (zh) * | 2019-04-26 | 2019-07-26 | 台湾塑胶工业股份有限公司 | 吸水性树脂组成物 |
| CN110330956A (zh) * | 2019-07-10 | 2019-10-15 | 黑龙江益瑞化工有限公司 | 一种环保型钻井液用聚氨基酸类降粘剂及其制备方法 |
| CN110330956B (zh) * | 2019-07-10 | 2020-07-03 | 黑龙江益瑞化工有限公司 | 一种环保型钻井液用聚氨基酸类降粘剂及其制备方法 |
| CN116284751A (zh) * | 2022-09-09 | 2023-06-23 | 长江大学 | 聚天冬氨酸衍生物及其制备方法与作为润滑剂的应用、水基钻井液及其应用 |
| CN116284751B (zh) * | 2022-09-09 | 2024-05-31 | 长江大学 | 聚天冬氨酸衍生物及其制备方法与作为润滑剂的应用、水基钻井液及其应用 |
Also Published As
| Publication number | Publication date |
|---|---|
| EP0683177A2 (en) | 1995-11-22 |
| CA2149382A1 (en) | 1995-11-17 |
| EP0683177A3 (enExample) | 1995-12-27 |
| KR950032376A (ko) | 1995-12-20 |
| JPH07309943A (ja) | 1995-11-28 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C01 | Deemed withdrawal of patent application (patent law 1993) | ||
| WD01 | Invention patent application deemed withdrawn after publication |