CN110962415A - Preparation method of salicylic acid p-tert-butyl ester uvioresistant blended fabric - Google Patents

Preparation method of salicylic acid p-tert-butyl ester uvioresistant blended fabric Download PDF

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Publication number
CN110962415A
CN110962415A CN201811148003.4A CN201811148003A CN110962415A CN 110962415 A CN110962415 A CN 110962415A CN 201811148003 A CN201811148003 A CN 201811148003A CN 110962415 A CN110962415 A CN 110962415A
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China
Prior art keywords
fabric
layer
blended
tert
cotton fibers
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Withdrawn
Application number
CN201811148003.4A
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Chinese (zh)
Inventor
周建
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Jiangsu Yunfu Fashion Co Ltd
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Jiangsu Yunfu Fashion Co Ltd
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Priority to CN201811148003.4A priority Critical patent/CN110962415A/en
Publication of CN110962415A publication Critical patent/CN110962415A/en
Withdrawn legal-status Critical Current

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B5/00—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts
    • B32B5/02—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by structural features of a fibrous or filamentary layer
    • B32B5/024—Woven fabric
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B27/00—Layered products comprising a layer of synthetic resin
    • B32B27/12—Layered products comprising a layer of synthetic resin next to a fibrous or filamentary layer
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B33/00—Layered products characterised by particular properties or particular surface features, e.g. particular surface coatings; Layered products designed for particular purposes not covered by another single class
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B37/00—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding
    • B32B37/06—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding characterised by the heating method
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B37/00—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding
    • B32B37/10—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding characterised by the pressing technique, e.g. using action of vacuum or fluid pressure
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B5/00—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts
    • B32B5/02—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by structural features of a fibrous or filamentary layer
    • B32B5/06—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by structural features of a fibrous or filamentary layer characterised by a fibrous or filamentary layer mechanically connected, e.g. by needling to another layer, e.g. of fibres, of paper
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B5/00—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts
    • B32B5/02—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by structural features of a fibrous or filamentary layer
    • B32B5/08—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by structural features of a fibrous or filamentary layer the fibres or filaments of a layer being of different substances, e.g. conjugate fibres, mixture of different fibres
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B5/00—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts
    • B32B5/22—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by the presence of two or more layers which are next to each other and are fibrous, filamentary, formed of particles or foamed
    • B32B5/24—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by the presence of two or more layers which are next to each other and are fibrous, filamentary, formed of particles or foamed one layer being a fibrous or filamentary layer
    • B32B5/26—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by the presence of two or more layers which are next to each other and are fibrous, filamentary, formed of particles or foamed one layer being a fibrous or filamentary layer another layer next to it also being fibrous or filamentary
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B7/00—Layered products characterised by the relation between layers; Layered products characterised by the relative orientation of features between layers, or by the relative values of a measurable parameter between layers, i.e. products comprising layers having different physical, chemical or physicochemical properties; Layered products characterised by the interconnection of layers
    • B32B7/04—Interconnection of layers
    • B32B7/12—Interconnection of layers using interposed adhesives or interposed materials with bonding properties
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B9/00—Layered products comprising a layer of a particular substance not covered by groups B32B11/00 - B32B29/00
    • B32B9/04—Layered products comprising a layer of a particular substance not covered by groups B32B11/00 - B32B29/00 comprising such particular substance as the main or only constituent of a layer, which is next to another layer of the same or of a different material
    • B32B9/047—Layered products comprising a layer of a particular substance not covered by groups B32B11/00 - B32B29/00 comprising such particular substance as the main or only constituent of a layer, which is next to another layer of the same or of a different material made of fibres or filaments
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2250/00—Layers arrangement
    • B32B2250/20—All layers being fibrous or filamentary
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2262/00—Composition or structural features of fibres which form a fibrous or filamentary layer or are present as additives
    • B32B2262/02—Synthetic macromolecular fibres
    • B32B2262/0276—Polyester fibres
    • B32B2262/0284—Polyethylene terephthalate [PET] or polybutylene terephthalate [PBT]
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2262/00—Composition or structural features of fibres which form a fibrous or filamentary layer or are present as additives
    • B32B2262/02—Synthetic macromolecular fibres
    • B32B2262/0292—Polyurethane fibres
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2262/00—Composition or structural features of fibres which form a fibrous or filamentary layer or are present as additives
    • B32B2262/06—Vegetal fibres
    • B32B2262/062—Cellulose fibres, e.g. cotton
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2307/00—Properties of the layers or laminate
    • B32B2307/70—Other properties
    • B32B2307/71—Resistive to light or to UV
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2437/00—Clothing

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  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Textile Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Fluid Mechanics (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Abstract

The invention particularly relates to a preparation method of salicylic acid p-tert-butyl methyl ester uvioresistant blended fabric, which comprises the following steps: manufacturing a surface layer: the surface layer is made of an ultraviolet-resistant fabric, the ultraviolet-resistant fabric is formed by interweaving warps and wefts, the warps are blended yarns of spandex fibers and cotton fibers, and the wefts are blended yarns of polyester cotton fibers and cotton fibers; manufacturing the intermediate layer: the polyester-cotton fibers and the cotton fibers in the first fabric layer and the third fabric layer are firstly blended, then are blended with the spandex fibers, and are woven into cloth, the second fabric layer is manufactured by cotton fiber spinning, and the first fabric layer, the second fabric layer and the third fabric layer are sequentially attached together in a dispensing or needle and thread sewing mode; manufacturing an inner layer; and (6) attaching the components into a whole. According to the preparation method of the salicylic acid p-tert-butyl methyl ester uvioresistant blended fabric, the prepared fabric has a good uvioresistant function, and the preparation process is simple and easy to operate.

Description

Preparation method of salicylic acid p-tert-butyl ester uvioresistant blended fabric
Technical Field
The invention belongs to the technical field of fabrics, and particularly relates to a preparation method of a salicylic acid p-tert-butyl ester uvioresistant blended fabric.
Background
With the increasing awareness of environmental protection and health care, more and more people are paying attention to natural fibers, and cotton fibers are widely applied to the production of various textiles as the most common natural fibers. At present, yarns on the market come out endlessly, are different in material structure, and are widely applied to the living fields of weaving, rope making, thread making and the like. Xinjiang cotton fiber is well known in the textile industry due to its flexibility and is known as a cotton top grade product by people, and has the advantages of less frequent combing, uniform and smooth evenness and high dyeability. However, the elasticity and the heat retention of the cotton fiber blended yarn on the market at present are not good, so that the woven fabric has the defects of poor heat retention effect and poor elasticity.
Preventing ultraviolet rays from damaging human bodies is being paid more and more attention by consumers. Ultraviolet rays in the solar spectrum not only cause the color fading and embrittlement of textiles, but also cause the sunburn and aging of human skin, generate melanin and color spots, and further induce canceration to harm human health. The ultraviolet-resistant fabric is a protective material for preventing excessive ultraviolet radiation of human bodies.
In view of the above, a preparation method of an anti-ultraviolet blended fabric of p-tert-butyl benzoate is urgently needed to be developed.
Disclosure of Invention
The invention aims to provide a preparation method of salicylic acid p-tert-butyl methyl ester uvioresistant blended fabric, which is characterized by comprising the following steps of:
a. manufacturing a surface layer: the surface layer is made of an ultraviolet-resistant fabric, the ultraviolet-resistant fabric is formed by interweaving warps and wefts, the warps are blended yarns of spandex fibers and cotton fibers, and the wefts are blended yarns of polyester cotton fibers and cotton fibers;
b. manufacturing the intermediate layer: the polyester-cotton fibers and the cotton fibers in the first fabric layer and the third fabric layer are firstly blended, then are blended with the spandex fibers, and are woven into cloth, the second fabric layer is manufactured by cotton fiber spinning, and the first fabric layer, the second fabric layer and the third fabric layer are sequentially attached together in a dispensing or needle and thread sewing mode;
c. manufacturing an inner layer: firstly, uniformly mixing spandex fibers, polyester cotton fibers and cotton fibers, then carrying out cotton cleaning, cotton carding, drawing, roving, fine sand, automatic spooling, yarn steaming, high-speed doubling and double twisting treatment to obtain fine imitation yarns, and then weaving to obtain lining fabric;
d. laminating integrally: and sequentially laminating the surface layer, the middle layer and the inner layer, and then curing, shaping and calendaring to obtain the product.
Preferably, in the step a, the uvioresistant fabric is added with the p-tert-butyl benzoate anti-ultraviolet finishing agent for soaking for 15-45 minutes and then is baked for 25-35 minutes at 35-60 ℃.
Preferably, after the step c, adding 3% of detergent and 16% of softening agent into the lining fabric for water washing treatment, controlling the water temperature at 25-45 ℃ and washing for 65-85 minutes.
Preferably, in the step d, the time for the ripening processing is 25-65h, the temperature is 35-85 ℃, and the humidity is 35-69%.
Preferably, in the step d, the calendering temperature is 55-95 ℃, the pressure is 51-101Kg/cm2, and the speed is 11-41 m/min.
Due to the adoption of the technical scheme, the invention has the following advantages and beneficial effects:
according to the preparation method of the salicylic acid p-tert-butyl methyl ester uvioresistant blended fabric, the prepared fabric has a good uvioresistant function, and the preparation process is simple and easy to operate.
Detailed Description
In order to more clearly illustrate the invention, the invention is further described below in connection with preferred embodiments. It is to be understood by persons skilled in the art that the following detailed description is illustrative and not restrictive, and is not to be taken as limiting the scope of the invention.
Example 1
The invention aims to provide a preparation method of salicylic acid p-tert-butyl methyl ester uvioresistant blended fabric, which is characterized by comprising the following steps of:
a. manufacturing a surface layer: the surface layer is made of an ultraviolet-resistant fabric, the ultraviolet-resistant fabric is formed by interweaving warps and wefts, the warps are blended yarns of spandex fibers and cotton fibers, and the wefts are blended yarns of polyester cotton fibers and cotton fibers;
b. manufacturing the intermediate layer: the polyester-cotton fibers and the cotton fibers in the first fabric layer and the third fabric layer are firstly blended, then are blended with the spandex fibers, and are woven into cloth, the second fabric layer is manufactured by cotton fiber spinning, and the first fabric layer, the second fabric layer and the third fabric layer are sequentially attached together in a dispensing or needle and thread sewing mode;
c. manufacturing an inner layer: firstly, uniformly mixing spandex fibers, polyester cotton fibers and cotton fibers, then carrying out cotton cleaning, cotton carding, drawing, roving, fine sand, automatic spooling, yarn steaming, high-speed doubling and double twisting treatment to obtain fine imitation yarns, and then weaving to obtain lining fabric;
d. laminating integrally: and sequentially laminating the surface layer, the middle layer and the inner layer, and then curing, shaping and calendaring to obtain the product.
In the step a, the uvioresistant fabric is added with the p-tert-butyl benzoate anti-ultraviolet finishing agent for soaking for 15 minutes and then is baked for 25 minutes at 35 ℃.
And c, after the step c, adding 3% of detergent and 16% of softening agent into the inner fabric for washing treatment, controlling the water temperature at 25 ℃ and washing for 65 minutes.
In the step d, the curing processing time is 25 hours, the temperature is 35 ℃, and the humidity is 35%.
In the step d, the calendering temperature is 55 ℃, the pressure is 51Kg/cm2, and the speed is 11 m/min.
Example 2
The invention aims to provide a preparation method of salicylic acid p-tert-butyl methyl ester uvioresistant blended fabric, which is characterized by comprising the following steps of:
a. manufacturing a surface layer: the surface layer is made of an ultraviolet-resistant fabric, the ultraviolet-resistant fabric is formed by interweaving warps and wefts, the warps are blended yarns of spandex fibers and cotton fibers, and the wefts are blended yarns of polyester cotton fibers and cotton fibers;
b. manufacturing the intermediate layer: the polyester-cotton fibers and the cotton fibers in the first fabric layer and the third fabric layer are firstly blended, then are blended with the spandex fibers, and are woven into cloth, the second fabric layer is manufactured by cotton fiber spinning, and the first fabric layer, the second fabric layer and the third fabric layer are sequentially attached together in a dispensing or needle and thread sewing mode;
c. manufacturing an inner layer: firstly, uniformly mixing spandex fibers, polyester cotton fibers and cotton fibers, then carrying out cotton cleaning, cotton carding, drawing, roving, fine sand, automatic spooling, yarn steaming, high-speed doubling and double twisting treatment to obtain fine imitation yarns, and then weaving to obtain lining fabric;
d. laminating integrally: and sequentially laminating the surface layer, the middle layer and the inner layer, and then curing, shaping and calendaring to obtain the product.
In the step a, the uvioresistant fabric is added with the p-tert-butyl benzoate anti-ultraviolet finishing agent for soaking for 45 minutes and then is baked for 35 minutes at the temperature of 60 ℃.
And c, after the step c, adding 3% of detergent and 16% of softening agent into the fabric on the inner layer for washing, controlling the water temperature at 45 ℃ and washing for 85 minutes.
In the step d, the curing processing time is 65 hours, the temperature is 85 ℃, and the humidity is 69%.
In the step d, the calendering temperature is 95 ℃, the pressure is 101Kg/cm2, and the speed is 41 m/min.
Through detection, all indexes of the ultraviolet-resistant fabric prepared in the two embodiments are as follows
Breaking Strength N (warp direction) Breaking Strength N (weft) Ultraviolet transmittance/%)
Example 1 241N 211N 4.24
Example 2 241N 213N 4.41
The foregoing shows and describes the general principles, essential features, and advantages of the invention. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, which are given by way of illustration of the principles of the present invention, and that various changes and modifications may be made without departing from the spirit and scope of the invention as defined by the appended claims. The scope of the invention is defined by the appended claims and equivalents thereof.

Claims (5)

1. A preparation method of salicylic acid p-tert-butyl methyl ester uvioresistant blended fabric is characterized by comprising the following steps:
a. manufacturing a surface layer: the surface layer is made of an ultraviolet-resistant fabric, the ultraviolet-resistant fabric is formed by interweaving warps and wefts, the warps are blended yarns of spandex fibers and cotton fibers, and the wefts are blended yarns of polyester cotton fibers and cotton fibers;
b. manufacturing the intermediate layer: the polyester-cotton fibers and the cotton fibers in the first fabric layer and the third fabric layer are firstly blended, then are blended with the spandex fibers, and are woven into cloth, the second fabric layer is manufactured by cotton fiber spinning, and the first fabric layer, the second fabric layer and the third fabric layer are sequentially attached together in a dispensing or needle and thread sewing mode;
c. manufacturing an inner layer: firstly, uniformly mixing spandex fibers, polyester cotton fibers and cotton fibers, then carrying out cotton cleaning, cotton carding, drawing, roving, fine sand, automatic spooling, yarn steaming, high-speed doubling and double twisting treatment to obtain fine imitation yarns, and then weaving to obtain lining fabric;
d. laminating integrally: and sequentially laminating the surface layer, the middle layer and the inner layer, and then curing, shaping and calendaring to obtain the product.
2. The preparation method of the salicylic acid p-tert-butyl methyl ester ultraviolet-resistant blended fabric according to claim 1, characterized in that: in the step a, the uvioresistant fabric is added with the p-tert-butyl benzoate uvioresistant finishing agent for soaking for 15-45 minutes and then is baked for 25-35 minutes at 35-60 ℃.
3. The preparation method of the salicylic acid p-tert-butyl methyl ester ultraviolet-resistant blended fabric according to claim 1, characterized in that: and c, after the step c, adding 3% of detergent and 16% of softening agent into the fabric in the inner layer for washing, controlling the water temperature at 25-45 ℃ and washing for 65-85 minutes.
4. The preparation method of the salicylic acid p-tert-butyl methyl ester ultraviolet-resistant blended fabric according to claim 1, characterized in that: in the step d, the curing processing time is 25-65h, the temperature is 35-85 ℃, and the humidity is 35-69%.
5. The preparation method of the salicylic acid p-tert-butyl methyl ester ultraviolet-resistant blended fabric as claimed in claim 1, which is characterized in that: in the step d, the calendering temperature is 55-95 ℃, the pressure is 51-101Kg/cm2, and the speed is 11-41 m/min.
CN201811148003.4A 2018-09-29 2018-09-29 Preparation method of salicylic acid p-tert-butyl ester uvioresistant blended fabric Withdrawn CN110962415A (en)

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CN201811148003.4A CN110962415A (en) 2018-09-29 2018-09-29 Preparation method of salicylic acid p-tert-butyl ester uvioresistant blended fabric

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