CN110946802A - Camellia flower sleeping mask capable of relieving and moisturizing and preparation method of camellia flower sleeping mask - Google Patents
Camellia flower sleeping mask capable of relieving and moisturizing and preparation method of camellia flower sleeping mask Download PDFInfo
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/74—Biological properties of particular ingredients
- A61K2800/78—Enzyme modulators, e.g. Enzyme agonists
- A61K2800/782—Enzyme inhibitors; Enzyme antagonists
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Abstract
The invention discloses a camellia sleep mask capable of relieving and moisturizing and a preparation method thereof. The facial mask provided by the invention has no stimulation to skin, stable property, safe use and no toxic or side effect, the formula of the facial mask provided by the invention is scientifically prepared, the permeability to skin is good, water in the facial mask permeates into the horny layer of the epidermis of the skin, the skin becomes soft, the elasticity is increased, and the high-efficiency repair to sensitive skin can be realized.
Description
Technical Field
The invention relates to the technical field of cosmetics, and particularly relates to a camellia sleep mask capable of soothing and moisturizing and a preparation method thereof.
Background
The skin injury refers to skin injury caused by allergens, bacteria and other various external stimuli, and symptoms such as redness, swelling, itching, pain and inflammation, and skin allergy and inflammation caused by skin injury. Research shows that the damage of the facial skin can be nursed and repaired by using traditional Chinese medicine or chemical medicine components, and from the current research situation, the research on single plant extracts or chemical additive components is more, the mechanism of the single plant extracts or chemical additive components is deeply known, and the research on the formula is less. In theory or clinic, it is not difficult to find a single plant extract or chemical additive component with a soothing and repairing effect as an active component for soothing the skin, and the difficulty and key point of research are only to find a formula for promoting the treatment effect of each active component.
Disclosure of Invention
The invention aims to provide a camellia sleep mask capable of soothing and moisturizing and a preparation method thereof, and aims to solve the technical problems.
In order to achieve the purpose, the technical scheme of the invention is as follows:
according to the first aspect, the camellia sleep mask for soothing and moisturizing provided by the invention comprises the following raw materials in percentage by weight: 0.3-0.8% of thickening agent, 1.0-15.0% of camellia extract, 0.1-1.0% of sarcosine, 10.0-20.0% of humectant, 0.05-0.5% of exopolysaccharide, 0.01-0.2% of chelating agent, 0.05-0.5% of allantoin, 0.1-2.0% of hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer, 1.0-5.0% of emollient, 0.5-5.0% of camellia oil, 0.1-1.0% of vitamin, 0.1-1.0% of arginine, 0.05-0.5% of sodium hyaluronate, 0.05-0.5% of sodium polyglutamate, 80.5-3.0% of palmitoyl tripeptide, 0.5-3.0% of acetyl hexapeptide, 30.05-0.5% of ceramide, 0.1-5.0% of potato pulp extract, 0.1-5.0% of cordyceps militaris extract, 0.5-5.0% of angelica sinensis extract, 0.1-1.5% of magnolia liliflora extract and the balance of water.
Preferably, the camellia soothing and moisturizing sleeping mask comprises the following raw materials in percentage by weight: 0.5-0.7% of thickening agent, 5.0-10.0% of camellia extract, 0.2-0.5% of sarcosine, 11.2-17.5% of humectant, 0.1-0.3% of exopolysaccharide, 0.05-0.1% of chelating agent, 0.1-0.3% of allantoin, 0.5-1.5% of hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer, 2.0-5.0% of emollient, 1.0-2.0% of camellia oil, 0.2-0.5% of vitamin, 0.2-0.5% of arginine, 0.1-0.2% of sodium hyaluronate, 0.1-0.3% of sodium polyglutamate, 80.5-2.0% of palmitoyl tripeptide, 81.0-2.0% of acetyl hexapeptide, 30.1-0.2% of ceramide, 1.0-2.0% of potato pulp extract, 0-1.0% of cordyceps militaris extract, 1.0-2.0% of angelica sinensis extract, 0.0-2.0.0% of lilac extract, 0.5-0.5% of magnolia officinalis extract and the balance of water preservative.
Preferably, the thickening agent is selected from one or more of carbomer 940, xanthan gum, cellulose, guar gum, sclerotium gum and alginate.
Further preferably, the thickening agent is composed of carbomer 940 and xanthan gum in a weight ratio of 2-5: 1-3.
Preferably, the humectant is selected from one or more of panthenol, glycerin, butylene glycol.
More preferably, the humectant consists of panthenol, glycerin and butanediol in a weight ratio of 0.2-0.5: 3-5: 8-12.
Preferably, the chelating agent is disodium edetate.
Preferably, the emollient is a silicone oil emollient selected from one or more of silicone oil DC100, silicone oil DC200, silicone oil DC345 and silicone oil DC 350.
Further preferably, the silicone oil emollient is composed of silicone oil DC200 and silicone oil DC345 in a weight ratio of 1-2: 1-3.
Preferably, the vitamin is vitamin E.
Preferably, the preservative is selected from one or more of pentanediol, phenoxyethanol, hexanediol, octanediol and caprylyl hydroximic acid.
More preferably, the preservative comprises 1-3: 0.1-0.5: 0.2-1 parts by weight of pentanediol, phenoxyethanol and hexanediol.
In a second aspect, the invention provides a preparation method of the camellia facial mask for soothing and moisturizing sleep, which comprises the following steps:
(1) uniformly mixing water, a thickening agent, a camellia extract, sarcosine, a humectant, exopolysaccharide, a chelating agent and allantoin, and stirring at 70-80 ℃ for 10-60 min to obtain a component A;
(2) uniformly mixing hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer, silicone oil DC200, silicone oil DC350, camellia seed oil and vitamin E to obtain a component B, uniformly stirring arginine to obtain a component C, adding the component B and the component C into the component A, and uniformly stirring at 70-80 ℃ to obtain a mixture;
(3) mixing sodium hyaluronate and sodium polyglutamate, stirring well to obtain component D, mixing palmitoyl tripeptide-8, acetyl hexapeptide-8, ceramide-3, potato pulp extract, Cordyceps militaris extract, Angelica maritima extract, centella asiatica extract and Magnolia liliflora extract, stirring well to obtain component E, and stirring well preservative to obtain component F; and cooling the mixture to a temperature not higher than 45 ℃, adding the component D, the component E and the component F into the mixture A, keeping the temperature, stirring uniformly, and filtering to obtain the camellia soothing and moisturizing sleeping mask.
Compared with the prior art, the invention has the beneficial effects that:
the facial mask provided by the invention has no stimulation to skin, stable property, safe use and no toxic or side effect, the formula of the facial mask provided by the invention is scientifically prepared, the permeability to skin is good, water in the facial mask permeates into the horny layer of the epidermis of the skin, the skin becomes soft, the elasticity is increased, and the high-efficiency repair to sensitive skin can be realized, the invention discovers that the compound of extracellular polysaccharide, vitamin, palmitoyl tripeptide-8 and a plurality of plant extracts (such as camellia extract, centella extract, magnolia extract and the like) as active ingredients according to a certain proportion can play a role in synergy, the anti-allergic activity of the skin can be effectively improved, the activity of hyaluronidase can be inhibited, the multiple protection to sensitive skin can be realized, the anti-allergic and anti-stimulation effects to the skin after being dried in the sun can be realized, the continuous calming and refreshing effects can be realized, effectively relieve the symptoms of skin stabbing pain, burning sensation and the like.
Detailed Description
The following further describes the embodiments of the present invention. It should be noted that the description of the embodiments is provided to help understanding of the present invention, but the present invention is not limited thereto. In addition, the technical features involved in the embodiments of the present invention described below may be combined with each other as long as they do not conflict with each other.
Examples 1 to 5
The preparation method of the camellia soothing and moisturizing sleeping mask provided by the embodiment comprises the following steps:
(1) weighing the raw materials according to the formula shown in the table 1;
(2) mixing water, carbomer 940, xanthan gum, flos Camelliae Japonicae extract, sarcosine, panthenol, glycerol, butanediol, exopolysaccharide, disodium ethylene diamine tetraacetate, and allantoin uniformly, and stirring at 75 deg.C for 30min to obtain component A;
(3) uniformly mixing hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer (EMT-10 for short), emollient, camellia oil and vitamins to obtain a component B, uniformly stirring arginine to obtain a component C, adding the component B and the component C into the component A, and uniformly stirring at 75 ℃ to obtain a mixture;
(4) mixing sodium hyaluronate and sodium polyglutamate, stirring well to obtain component D, mixing palmitoyl tripeptide-8, acetyl hexapeptide-8, ceramide-3, potato pulp extract, Cordyceps militaris extract, Angelica maritima extract, centella asiatica extract and Magnolia liliflora extract, stirring well to obtain component E, and stirring uniformly pentanediol, phenoxyethanol and hexanediol to obtain component F; and cooling the mixture to 40 ℃, adding the component D, the component E and the component F into the mixture A, keeping the temperature, stirring uniformly, and filtering to obtain the camellia soothing and moisturizing sleeping mask.
TABLE 1 statistics of the amounts of the raw materials in examples 1 to 5
Example 6
The preparation method of the camellia soothing and moisturizing sleeping mask provided by the embodiment comprises the following steps:
(1) weighing the raw materials according to the formula shown in the table 2;
(2) mixing water, carbomer 940, xanthan gum, flos Camelliae Japonicae extract, sarcosine, panthenol, glycerol, butanediol, exopolysaccharide, disodium ethylene diamine tetraacetate, and allantoin uniformly, and stirring at 70 deg.C for 60min to obtain component A;
(3) uniformly mixing hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer (EMT-10 for short), emollient, camellia oil and vitamins to obtain a component B, uniformly stirring arginine to obtain a component C, adding the component B and the component C into the component A, and uniformly stirring at 70 ℃ to obtain a mixture;
(4) mixing sodium hyaluronate and sodium polyglutamate, stirring well to obtain component D, mixing palmitoyl tripeptide-8, acetyl hexapeptide-8, ceramide-3, potato pulp extract, Cordyceps militaris extract, Angelica maritima extract, centella asiatica extract and Magnolia liliflora extract, stirring well to obtain component E, and stirring uniformly pentanediol, phenoxyethanol and hexanediol to obtain component F; and cooling the mixture to 40 ℃, adding the component D, the component E and the component F into the mixture A, keeping the temperature, stirring uniformly, and filtering to obtain the camellia soothing and moisturizing sleeping mask.
Example 7
The preparation method of the camellia soothing and moisturizing sleeping mask provided by the embodiment comprises the following steps:
(1) weighing the raw materials according to the formula shown in the table 2;
(2) mixing water, carbomer 940, xanthan gum, flos Camelliae Japonicae extract, sarcosine, panthenol, glycerol, butanediol, exopolysaccharide, disodium ethylene diamine tetraacetate, and allantoin uniformly, stirring at 80 deg.C for 10min to obtain component A;
(3) uniformly mixing hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer (EMT-10 for short), emollient, camellia oil and vitamins to obtain a component B, uniformly stirring arginine to obtain a component C, adding the component B and the component C into the component A, and uniformly stirring at 70 ℃ to obtain a mixture;
(4) mixing sodium hyaluronate and sodium polyglutamate, stirring well to obtain component D, mixing palmitoyl tripeptide-8, acetyl hexapeptide-8, ceramide-3, potato pulp extract, Cordyceps militaris extract, Angelica maritima extract, centella asiatica extract and Magnolia liliflora extract, stirring well to obtain component E, and stirring uniformly pentanediol, phenoxyethanol and hexanediol to obtain component F; and cooling the mixture to 45 ℃, adding the component D, the component E and the component F into the mixture A, keeping the temperature, stirring uniformly, and filtering to obtain the camellia soothing and moisturizing sleeping mask.
Examples 8 to 9
The raw materials are weighed according to the table 2, and then the camellia soothing and moisturizing sleeping mask is prepared according to the preparation method of the example 1.
TABLE 2 statistics of the amounts of the raw materials in examples 6 to 9
Comparative example 1
To further illustrate the beneficial effects of the present invention, this comparative example prepared a sleeping mask similar to that of example 4, and differed from example 4 only in the following amounts of raw materials: the amount of butylene glycol used in this comparative example was 18% and no camellia extract was added.
Comparative example 2
To further illustrate the beneficial effects of the present invention, this comparative example prepared a sleeping mask similar to that of example 4, and differed from example 4 only in the following amounts of raw materials: the amount of butylene glycol used in this comparative example was 10% and palmitoyl tripeptide-8 was not added.
Comparative example 3
To further illustrate the beneficial effects of the present invention, this comparative example prepared a sleeping mask similar to that of example 4, and differed from example 4 only in the following amounts of raw materials: the amount of butylene glycol used in this comparative example was 11% and no centella asiatica extract was added.
Comparative example 4
To further illustrate the beneficial effects of the present invention, this comparative example prepared a sleeping mask similar to that of example 4, and differed from example 4 only in the following amounts of raw materials: the amount of butylene glycol used in this comparative example was 9% and no magnolia extract was added.
Comparative example 5
To further illustrate the beneficial effects of the present invention, this comparative example prepared a sleeping mask similar to that of example 4, and differed from example 4 only in the following amounts of raw materials: the amount of butylene glycol used in this comparative example was 8.5% and no vitamin E was added.
Comparative example 6
To further illustrate the beneficial effects of the present invention, this comparative example prepared a sleeping mask similar to that of example 4, and differed from example 4 only in the following amounts of raw materials: the amount of butylene glycol used in this comparative example was 8.2% and no exopolysaccharide was added.
To further illustrate the advantageous effects of the present invention, the mask obtained in the above examples and comparative examples was also tested as follows:
(1) stability test
The facial masks obtained in examples 1 to 9 and comparative examples 1 to 6 were stored at 40 ℃ for 25 days, and the facial masks were observed visually before and after the test without changes in the properties and colors, and without delamination and oil floating.
(2) The hyaluronidase is a participant of type I anaphylactic reaction, the hyaluronidase has strong correlation with inflammation and allergy, the inhibition of the activity of the hyaluronidase is used as an index for researching the antiallergic effect, the inhibition rate of the facial masks obtained in examples 1-9 and comparative examples 1-6 on the hyaluronidase is measured by a hyaluronidase in vitro inhibition test, and the test result is shown in table 3.
TABLE 3 test results of hyaluronidase in vitro inhibition assay
The test results in table 3 show that camellia sinensis flower extract, palmitoyl tripeptide-8, centella asiatica extract, magnolia liliflora extract, exopolysaccharides and vitamin E in the formula disclosed by the invention are effective components capable of effectively inhibiting hyaluronidase, and the components are deficient and have a synergistic effect; in addition, the inhibition rate of the facial masks obtained in examples 1-5 on hyaluronidase is greater than 73%, and the inhibition effect is obviously better than that of other facial masks.
(3) Post-basking repair efficacy test
And selecting the products obtained in the examples 1-5 to carry out the after-sun repair effect test according to the test result of the hyaluronidase in-vitro inhibition test. Selecting 50 female testers with approximate sunburn, wherein the female testers are 22-45 years old and randomly divided into 5 groups, and 5 people in each group are cleaned at night, respectively coating the facial masks obtained in the embodiments 1-5 on the face, continuously using for 4 days, taking facial pictures before and after use, obtaining the area of the sunburn skin of the face according to the pictures, and calculating the fading rate of the sunburn of the skin, wherein the calculation formula is as follows: the skin sunburn regression rate (%) (area of sunburned skin before use-area of sunburned skin after use)/area of sunburned skin before use x 100%, and the test results are shown in table 4.
Table 4 post-basking repair test results
| Serial number | Testing the origin of the mask | Regression rate of sunburn (%) |
| 1 | Example 1 | 93.1 |
| 2 | Example 2 | 90.5 |
| 3 | Example 3 | 89.3 |
| 4 | Example 4 | 94.5 |
| 5 | Example 5 | 84.2 |
The embodiments of the present invention have been described in detail, but the present invention is not limited to the described embodiments. It will be apparent to those skilled in the art that various changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, and the scope of protection is still within the scope of the invention.
Claims (10)
1. The camellia flower sleeping mask capable of relieving and moisturizing is characterized by comprising the following raw materials in percentage by weight: 0.1-1.0% of thickening agent, 1.0-15.0% of camellia extract, 0.1-1.0% of sarcosine, 10.0-20.0% of humectant, 0.05-0.5% of exopolysaccharide, 0.01-0.2% of chelating agent, 0.05-0.5% of allantoin, 0.1-2.0% of hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer, 0.5-5.0% of emollient, 0.5-5.0% of camellia seed oil, 0.1-1.0% of vitamin, 0.1-1.0% of arginine, 0.05-0.5% of sodium hyaluronate, 0.05-0.5% of sodium polyglutamate, 80.1-2.0% of palmitoyl tripeptide, 0.5-5.0% of acetyl hexapeptide, 30.05-0.5% of ceramide, 0.1-5.0% of potato pulp extract, 0.1-5.0% of cordyceps militaris extract, 0.5-5.0.0% of angelica sinensis extract, 0.5-0.0.5% of magnolia lilyturf extract and the balance of water.
2. The camellia facial mask for soothing and moisturizing according to claim 1, which comprises the following raw materials in percentage by weight: 0.3-0.8% of thickening agent, 5.0-10.0% of camellia extract, 0.2-0.5% of sarcosine, 11.2-17.5% of humectant, 0.1-0.3% of exopolysaccharide, 0.05-0.1% of chelating agent, 0.1-0.3% of allantoin, 0.5-1.5% of hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer, 2.0-5.0% of emollient, 1.0-2.0% of camellia oil, 0.2-0.5% of vitamin, 0.2-0.5% of arginine, 0.1-0.2% of sodium hyaluronate, 0.1-0.3% of sodium polyglutamate, 80.5-2.0% of palmitoyl tripeptide, 81.0-2.0% of acetyl hexapeptide, 30.1-0.2% of ceramide, 1.0-2.0% of potato pulp extract, 0-1.0% of cordyceps militaris extract, 1.0-2.0% of angelica sinensis extract, 0.0-2.0.0% of lilac extract, 0.5-0.5% of magnolia officinalis extract and the balance of water preservative.
3. The camellia soothing and moisturizing sleeping mask as claimed in claim 1, wherein the thickening agent is selected from one or more of carbomer 940, xanthan gum, cellulose, guar gum, sclerotium gum and alginate.
4. The camellia soothing and moisturizing sleeping mask as claimed in claim 1, wherein the moisturizer is one or more selected from panthenol, glycerin and butylene glycol.
5. The camellia flower sleep mask for soothing and moisturizing as claimed in claim 4, wherein the moisturizing agent is composed of panthenol, glycerin and butylene glycol in a weight ratio of 0.2-0.5: 3-5: 8-12.
6. The camellia soothing and moisturizing sleeping mask as claimed in claim 1, wherein the chelating agent is disodium ethylenediamine tetraacetic acid.
7. The camellia soothing and moisturizing sleeping mask as claimed in claim 1, wherein the emollient is a silicone oil emollient selected from one or more of silicone oil DC100, silicone oil DC200, silicone oil DC345 and silicone oil DC 350.
8. The camellia soothing and moisturizing sleeping mask as claimed in claim 1, wherein the vitamin is vitamin E.
9. The camellia soothing and moisturizing sleeping mask as claimed in claim 1, wherein the preservative is one or more selected from pentanediol, phenoxyethanol, hexanediol, octanediol, and caprylhydroxamic acid.
10. A method for preparing a camellia soothing and moisturizing sleeping mask as claimed in any one of claims 1 to 9, wherein the method comprises the following steps:
(1) uniformly mixing water, a thickening agent, a camellia extract, sarcosine, a humectant, exopolysaccharide, a chelating agent and allantoin, and stirring at 70-80 ℃ for 10-60 min to obtain a component A;
(2) uniformly mixing hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer, an emollient, camellia seed oil and vitamins to obtain a component B, uniformly stirring arginine to obtain a component C, adding the component B and the component C into the component A, and uniformly stirring at 70-80 ℃ to obtain a mixture;
(3) mixing sodium hyaluronate and sodium polyglutamate, stirring well to obtain component D, mixing palmitoyl tripeptide-8, acetyl hexapeptide-8, ceramide-3, potato pulp extract, Cordyceps militaris extract, Angelica maritima extract, centella asiatica extract and Magnolia liliflora extract, stirring well to obtain component E, and stirring well preservative to obtain component F; and cooling the mixture to a temperature not higher than 45 ℃, adding the component D, the component E and the component F into the mixture A, keeping the temperature, stirring uniformly, and filtering to obtain the camellia soothing and moisturizing sleeping mask.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112057411A (en) * | 2020-10-19 | 2020-12-11 | 湖南金昌生物技术有限公司 | Deep-repairing camellia hydrolat mask and preparation method thereof |
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| CN113925812A (en) * | 2021-11-12 | 2022-01-14 | 广州睿森生物科技有限公司 | Composition with effects of promoting sleep and repairing skin and application of composition in cosmetics |
| CN113925812B (en) * | 2021-11-12 | 2023-08-11 | 广州睿森生物科技有限公司 | Functional composition for promoting sleep and skin repair and application of functional composition in cosmetics |
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