CN110897994A - Garlic element moistening and revitalizing essence cream and preparation method thereof - Google Patents

Abstract

The invention discloses a selective allicin revitalizing essence cream which is prepared from the following raw materials in parts by weight: 50-55 parts of phase A, 10-15 parts of phase B1, 4-5 parts of phase B2, 2.7-3.2 parts of phase C, 12-15 parts of phase D1, 8-10 parts of phase D2, 4-5 parts of phase D3, 2.5-3 parts of phase D4, 1-2 parts of phase E1 and 0.05-0.1 part of phase E2; phase A: a humectant complex; b1 phase: an emulsifier complex; b2 phase: conditioning emollient formulations; and C phase: a film-forming agent complex; d1 phase: plant extracts and fermentation product combinations; d2 phase: an aqueous tranexamic acid solution; d3 phase: an aqueous solution of tetrahydro-methyl-pyrimidine-carboxylic acid; d4 phase: an aqueous solution of allicin; e1 phase: a preservative composition; e2 phase: an essence; the allicin moistening revitalizing essence cream disclosed by the invention has good moisturizing and nourishing effects and strong anti-aging capability, and can provide continuous power for resisting skin aging.

Description

Garlic element moistening and revitalizing essence cream and preparation method thereof

Technical Field

The invention relates to the technical field of cosmetics, in particular to a garlic moistening and revitalizing essence cream.

Background

Skin aging is a progressive physiological process and also a result of the combined action of various factors such as heredity, environment, psychology and the like. With the improvement of living standard of people, the functional requirements on skin care products are higher and higher, and skin care products with anti-aging effect are also in the endlessly. The essence cream is a skin care product added with concentrated high-nutrition components, and has the effects of resisting aging, resisting wrinkles, tightening, moisturizing, whitening and the like according to the pertinence of the formula; the essence is one of skin care products for face, contains more precious functional components such as plant extract, ceramide, squalane, etc., and has the effects of preventing aging, removing wrinkle, keeping moisture, whitening skin, removing speckles, etc. The essence is divided into different subdivided products such as essence liquid, essence lotion, essence cream, essence injection and the like, and the essence liquid and the essence cream are two products with the widest application range;

the essence is suitable for oily skin, and the essence cream has good effect on neutral skin. And the concentration of the essence cream is higher. When the weather is dry, the skin is rough, and the essence cream can achieve good conditioning and improving effects.

Allicin is a trithioallyl ether compound, and naturally exists in the bulb of garlic of Liliaceae. Allicin has strong antibacterial and anti-inflammatory effects, and also has effects in removing dandruff, relieving itching, preventing neuralgia, treating mercury poisoning, resisting radiation, resisting oxidation and aging, protecting biological membrane, resisting aging, preventing and treating mosquito bite, and resisting common cold. Experiments show that the product can prevent and treat hepatic fibrosis and is an antioxidant and anti-aging agent. Allicin is not used in the cosmetic field as long as it is used for dietary therapy at present.

Allicin is a tasteless transparent liquid, and can promote skin blood circulation, remove aged cutin of skin, soften skin and enhance its elasticity, and also can be used for preventing sunburn, preventing melanin deposition, removing mottle and whitening skin. Allicin is also rich in selenium, has strong anticancer effect, and selenium plays a role in oxidation resistance in the form of glutathione oxidase, thereby playing a role in protecting the membrane. Allicin contains 17 amino acids. It contains rich minerals, with phosphorus being the highest, and magnesium, calcium, iron, silicon, aluminum, zinc, etc. being the second.

Allicin is currently used only in the fields of medicines and foods, and has not yet been used in the field of cosmetics, and is considered to be applied to the field of cosmetics because it has an effect of promoting blood circulation to human skin.

Therefore, the allicin is applied to the essence cream product in the field of cosmetics, so that the allicin can be well applied.

Disclosure of Invention

The invention aims to provide an allicin revitalizing essence cream to solve the problems in the background art.

In order to achieve the purpose, the invention provides the following technical scheme:

a garlic moistening and revitalizing essence cream is prepared from the following raw materials in parts by weight:

50-55 parts of phase A, 10-15 parts of phase B1, 4-5 parts of phase B2, 2.7-3.2 parts of phase C, 12-15 parts of phase D1, 8-10 parts of phase D2, 4-5 parts of phase D3, 2.5-3 parts of phase D4, 1-2 parts of phase E1 and 0.05-0.1 part of phase E2;

phase A: a humectant complex;

b1 phase: an emulsifier complex;

b2 phase: conditioning emollient formulations;

and C phase: a film-forming agent complex;

d1 phase: plant extracts and fermentation product combinations;

d2 phase: an aqueous tranexamic acid solution;

d3 phase: an aqueous solution of tetrahydro-methyl-pyrimidine-carboxylic acid;

d4 phase: an aqueous solution of allicin;

e1 phase: a preservative composition;

e2 phase: and (4) essence.

As a further scheme of the invention: the phase A comprises the following components in parts by weight: 48-50 parts of water, 0.05-0.1 part of EDTA disodium, 2-3 parts of trehalose, 2-3 parts of betaine and 1-3 parts of 1, 3-butanediol.

As a further scheme of the invention: the B1 phase comprises the following components in parts by weight: 1-2 parts of cetearyl olive oil, 1-2 parts of sorbitan olive oleate, 1-2 parts of glyceryl stearate, 1-2 parts of PEG-100 stearate, 2-3 parts of cetyl ethyl hexanoate, 0.5-1 part of cetearyl alcohol, 2-4 parts of glyceryl tri (ethyl hexanoate), 0.1-0.2 part of methyl hydroxybenzoate and 2-3 parts of polydimethylsiloxane.

As a further scheme of the invention: the B2 phase comprises the following components in parts by weight: 2-4 parts of phytosterol and 2-4 parts of lanolin.

As a further scheme of the invention: the phase C comprises the following components in parts by weight: 1-3 parts of cyclopenta dimethyl siloxane, 0.5-1 part of hydroxyethyl acrylate and 0.5-1 part of acryloyl dimethyl sodium taurate copolymer;

as a further scheme of the invention: the D1 phase comprises the following components in parts by weight: 0.5-0.8 part of butanediol, 0.1-0.3 part of centella asiatica extract, 0.1-0.3 part of polygonum cuspidatum root extract, 0.1-0.3 part of scutellaria baicalensis root extract, 0.1-0.3 part of tea extract, 0.1-0.3 part of chamomile flower extract, 0.1-0.3 part of rosemary leaf extract, 0.1-0.3 part of red clover flower extract, 2-4 parts of carbohydrate isomer, 0.8-1 part of isoprene glycol, 1-2 parts of lactobacillus/rice fermentation product, 0.1-0.5 part of schizosaccharomyces cerevisiae fermentation product lysate, 1.2-1.5 parts of xanthan gum, 0.8-1 part of methylparaben and 0.8-1 part of phenoxyethanol.

As a further scheme of the invention: the D2 phase comprises the following components in parts by weight: 5 parts of water and 3 parts of tranexamic acid;

the D3 phase comprises the following components in parts by weight: 3 parts of water and 1 part of tetrahydro-methylpyrimidine carboxylic acid;

the D4 phase comprises the following components in parts by weight: 2 parts of water and 0.5-0.8 part of garlic extract;

the E1 phase comprises the following components in parts by weight: 0.1 part of caprylyl hydroximic acid, 0.2 part of ethylhexyl glycerol, 0.5 part of 1, 2-hexanediol and 0.3 part of propylene glycol.

As a further scheme of the invention: the allicin refining rejuvenating essence cream is added with phase F: an animal collagen composition;

the animal collagen composition is a composition of fish collagen and ossein, and the mixture ratio of the fish collagen is that the fish collagen: bone collagen 1-3: 3-5.

The preparation method of the allicin refined rejuvenation essence cream without adding the F phase comprises the following steps:

adding the phase A into a clean and sterile emulsifying pot, heating to 90 ℃, preserving heat, sterilizing for 30 minutes, and preserving heat for later use;

secondly, adding B1 into a clean sterile oil phase pot, heating to 90 ℃, stirring to completely melt all the components, adding B2 phase, stirring to completely melt all the components to obtain B phase, and keeping the temperature at 78 ℃ for later use;

thirdly, premixing the phase C uniformly for later use;

fourthly, uniformly premixing the D2 phase, the D3 phase, the D4 phase, the E1 phase and the E2 phase for later use;

filtering and sucking the phase B prepared in the step two into an emulsifying pot, adjusting the vacuum degree to be-0.05 MPa, adjusting the stirring speed to be 58-30rpm, starting homogenizing, adjusting the homogenizing speed to be 30-40rpm, carrying out vacuum homogenizing stirring for 5 minutes, then adding the premixed and uniform phase C, adjusting the homogenizing speed to be 30-40rpm, carrying out vacuum homogenizing stirring for 5 minutes, starting cooling water after carrying out heat preservation and defoaming for 20 minutes, carrying out vacuum stirring for cooling, and properly adjusting the stirring speed during cooling so as to avoid exciting foams and influencing the appearance of the paste body;

sixthly, adding the D1 phase and the uniformly premixed D2 phase, D3 phase, E1 phase and E2 phase at the temperature of below 45 ℃, fully and uniformly stirring, adding the uniformly premixed D4 phase, uniformly stirring and mixing, discharging after detection at 38 ℃, and aseptically packaging to obtain the finished product.

Compared with the prior art, the invention has the beneficial effects that:

the allicin is innovatively added, so that the skin care cream has the functions of strong antioxidation, anti-aging, moisturizing, repairing, sterilizing and calming the skin.

The conditioning emollient compound consisting of phytosterol and oil-soluble lanolin has the functions of conditioning and moisturizing skin and optimizing essence cream skin feeling;

the cyclopentadimethylsiloxane, hydroxyethyl acrylate and acryloyl dimethyl sodium taurate copolymer form a film agent compound, so that the water loss can be locked, and the moisturizing effect of the essence cream is improved;

the plant extract and fermentation product compound comprises plant extraction essence and fermentation products such as a centella extract, a polygonum cuspidatum root extract, a scutellaria baicalensis root extract, a tea extract, a chamomile extract, a rosemary leaf extract, an red clover flower extract, a carbohydrate isomer, isoprene glycol, a lactobacillus/rice fermentation product, a schizosaccharomyces cerevisiae fermentation product lysate and the like, and is used as another main anti-aging component of the essence cream.

The fermentation product can enhance skin immunity and repair activity, promote the repair of damaged skin cells, and keep skin in a young state of full vitality.

Therefore, the allicin refined rejuvenation essence cream has good moisturizing and nourishing effects and strong anti-aging capability, and can provide continuous power for skin anti-aging.

Detailed Description

The present application is described in further detail below, and it should be noted that the following detailed description is provided for illustrative purposes only, and is not intended to limit the scope of the present application, which is defined by the appended claims.

Example one

A garlic moistening and revitalizing essence cream is prepared from the following raw materials in parts by weight:

50 parts of phase A, 10 parts of phase B1, 4 parts of phase B2, 2.7 parts of phase C, 12 parts of phase D1, 8 parts of phase D2, 4 parts of phase D3, 2.5 parts of phase D4, 1 part of phase E1 and 0.05 part of phase E2;

phase A: a humectant complex;

b1 phase: an emulsifier complex;

b2 phase: conditioning emollient formulations;

and C phase: a film-forming agent complex;

d1 phase: plant extracts and fermentation product combinations;

d2 phase: an aqueous tranexamic acid solution;

d3 phase: an aqueous solution of tetrahydro-methyl-pyrimidine-carboxylic acid;

d4 phase: an aqueous solution of allicin;

e1 phase: a preservative composition;

e2 phase: and (4) essence.

The phase A comprises the following components in parts by weight: 48-50 parts of water, 0.05-0.1 part of EDTA disodium, 2-3 parts of trehalose, 2-3 parts of betaine and 1-3 parts of 1, 3-butanediol.

The B1 phase comprises the following components in parts by weight: 1-2 parts of cetearyl olive oleate, 1-2 parts of sorbitan olive oleate, 1-2 parts of glyceryl stearate, 1-2 parts of PEG-100 stearate, 2-3 parts of cetyl ethyl hexanoate, 0.5-1 part of whale wax stearyl alcohol, 2-4 parts of glycerol tri (ethyl hexanoate), 0.1-0.2 part of methyl hydroxybenzoate and 2-3 parts of polydimethylsiloxane.

The B2 phase comprises the following components in parts by weight: 2-4 parts of phytosterol and 2-4 parts of lanolin.

The phase C comprises the following components in parts by weight: 1-3 parts of cyclopentadimethylsiloxane, 0.5-1 part of hydroxyethyl acrylate and 0.5-1 part of acryloyl dimethyl sodium taurate copolymer;

the D1 phase comprises the following components in parts by weight: 0.5-0.8 part of butanediol, 0.1-0.3 part of centella asiatica extract, 0.1-0.3 part of polygonum cuspidatum root extract, 0.1-0.3 part of scutellaria baicalensis root extract, 0.1-0.3 part of tea extract, 0.1-0.3 part of chamomile flower extract, 0.1-0.3 part of rosemary leaf extract, 0.1-0.3 part of red clover flower extract, 2-4 parts of carbohydrate isomer, 0.8-1 part of isoprene glycol, 1-2 parts of lactobacillus/rice fermentation product, 0.1-0.5 part of schizosaccharomyces cerevisiae fermentation product lysate, 1.2-1.5 parts of xanthan gum, 0.8-1 part of methylparaben and 0.8-1 part of phenoxyethanol.

The D2 phase comprises the following components in parts by weight: 5 parts of water and 3 parts of tranexamic acid.

The D3 phase comprises the following components in parts by weight: 3 parts of water and 1 part of tetrahydro-methyl pyrimidine carboxylic acid.

The D4 phase comprises the following components in parts by weight: 2 parts of water and 0.5-0.8 part of garlic extract.

The E1 phase comprises the following components in parts by weight: 0.1 part of caprylyl hydroximic acid, 0.2 part of ethylhexyl glycerol, 0.5 part of 1, 2-hexanediol and 0.3 part of propylene glycol.

A preparation method of allicin refined rejuvenation essence cream comprises the following steps:

adding the phase A into a clean and sterile emulsifying pot, heating to 90 ℃, preserving heat, sterilizing for 30 minutes, and preserving heat for later use;

secondly, adding B1 into a clean sterile oil phase pot, heating to 90 ℃, stirring to completely melt all the components, adding B2 phase, stirring to completely melt all the components to obtain B phase, and keeping the temperature at 78 ℃ for later use;

thirdly, premixing the phase C uniformly for later use;

fourthly, uniformly premixing the D2 phase, the D3 phase, the D4 phase, the E1 phase and the E2 phase for later use;

filtering and sucking the phase B prepared in the step two into an emulsifying pot, adjusting the vacuum degree to be-0.05 MPa, adjusting the stirring speed to be 58-30rpm, starting homogenizing, adjusting the homogenizing speed to be 30-40rpm, carrying out vacuum homogenizing stirring for 5 minutes, then adding the premixed and uniform phase C, adjusting the homogenizing speed to be 30-40rpm, carrying out vacuum homogenizing stirring for 5 minutes, starting cooling water after carrying out heat preservation and defoaming for 20 minutes, carrying out vacuum stirring for cooling, and properly adjusting the stirring speed during cooling so as to avoid exciting foams and influencing the appearance of the paste body;

sixthly, adding the D1 phase and the uniformly premixed D2 phase, D3 phase, E1 phase and E2 phase at the temperature of below 45 ℃, fully and uniformly stirring, adding the uniformly premixed D4 phase, uniformly stirring and mixing, discharging after detection at 38 ℃, and aseptically packaging to obtain the finished product.

Example two

A garlic moistening and revitalizing essence cream is prepared from the following raw materials in parts by weight:

52 parts of phase A, 12 parts of phase B1, 4.3 parts of phase B2, 2.9 parts of phase C, 13 parts of phase D1, 8.5 parts of phase D2, 4.3 parts of phase D3, 2.7 parts of phase D4, 1.2 parts of phase E1 and 0.07 part of phase E2;

phase A: a humectant complex;

b1 phase: an emulsifier complex;

b2 phase: conditioning emollient formulations;

and C phase: a film-forming agent complex;

d1 phase: plant extracts and fermentation product combinations;

d2 phase: an aqueous tranexamic acid solution;

d3 phase: an aqueous solution of tetrahydro-methyl-pyrimidine-carboxylic acid;

d4 phase: an aqueous solution of allicin;

e1 phase: a preservative composition;

e2 phase: and (4) essence.

The phase A comprises the following components in parts by weight: 48-50 parts of water, 0.05-0.1 part of EDTA disodium, 2-3 parts of trehalose, 2-3 parts of betaine and 1-3 parts of 1, 3-butanediol.

The B1 phase comprises the following components in parts by weight: 1-2 parts of cetearyl olive oleate, 1-2 parts of sorbitan olive oleate, 1-2 parts of glyceryl stearate, 1-2 parts of PEG-100 stearate, 2-3 parts of cetyl ethyl hexanoate, 0.5-1 part of whale wax stearyl alcohol, 2-4 parts of glycerol tri (ethyl hexanoate), 0.1-0.2 part of methyl hydroxybenzoate and 2-3 parts of polydimethylsiloxane.

The B2 phase comprises the following components in parts by weight: 2-4 parts of phytosterol and 2-4 parts of lanolin.

The phase C comprises the following components in parts by weight: 1-3 parts of cyclopentadimethylsiloxane, 0.5-1 part of hydroxyethyl acrylate and 0.5-1 part of acryloyl dimethyl sodium taurate copolymer;

the D1 phase comprises the following components in parts by weight: 0.5-0.8 part of butanediol, 0.1-0.3 part of centella asiatica extract, 0.1-0.3 part of polygonum cuspidatum root extract, 0.1-0.3 part of scutellaria baicalensis root extract, 0.1-0.3 part of tea extract, 0.1-0.3 part of chamomile flower extract, 0.1-0.3 part of rosemary leaf extract, 0.1-0.3 part of red clover flower extract, 2-4 parts of carbohydrate isomer, 0.8-1 part of isoprene glycol, 1-2 parts of lactobacillus/rice fermentation product, 0.1-0.5 part of schizosaccharomyces cerevisiae fermentation product lysate, 1.2-1.5 parts of xanthan gum, 0.8-1 part of methylparaben and 0.8-1 part of phenoxyethanol.

The D2 phase comprises the following components in parts by weight: 5 parts of water and 3 parts of tranexamic acid.

The D3 phase comprises the following components in parts by weight: 3 parts of water and 1 part of tetrahydro-methyl pyrimidine carboxylic acid.

The D4 phase comprises the following components in parts by weight: 2 parts of water and 0.5-0.8 part of garlic extract.

The E1 phase comprises the following components in parts by weight: 0.1 part of caprylyl hydroximic acid, 0.2 part of ethylhexyl glycerol, 0.5 part of 1, 2-hexanediol and 0.3 part of propylene glycol.

A preparation method of allicin refined rejuvenation essence cream comprises the following steps:

adding the phase A into a clean and sterile emulsifying pot, heating to 90 ℃, preserving heat, sterilizing for 30 minutes, and preserving heat for later use;

secondly, adding B1 into a clean sterile oil phase pot, heating to 90 ℃, stirring to completely melt all the components, adding B2 phase, stirring to completely melt all the components to obtain B phase, and keeping the temperature at 78 ℃ for later use;

thirdly, premixing the phase C uniformly for later use;

fourthly, uniformly premixing the D2 phase, the D3 phase, the D4 phase, the E1 phase and the E2 phase for later use;

filtering and sucking the phase B prepared in the step two into an emulsifying pot, adjusting the vacuum degree to be-0.05 MPa, adjusting the stirring speed to be 58-30rpm, starting homogenizing, adjusting the homogenizing speed to be 30-40rpm, carrying out vacuum homogenizing stirring for 5 minutes, then adding the premixed and uniform phase C, adjusting the homogenizing speed to be 30-40rpm, carrying out vacuum homogenizing stirring for 5 minutes, starting cooling water after carrying out heat preservation and defoaming for 20 minutes, carrying out vacuum stirring for cooling, and properly adjusting the stirring speed during cooling so as to avoid exciting foams and influencing the appearance of the paste body;

sixthly, adding the D1 phase and the uniformly premixed D2 phase, D3 phase, E1 phase and E2 phase at the temperature of below 45 ℃, fully and uniformly stirring, adding the uniformly premixed D4 phase, uniformly stirring and mixing, discharging after detection at 38 ℃, and aseptically packaging to obtain the finished product.

EXAMPLE III

A garlic moistening and revitalizing essence cream is prepared from the following raw materials in parts by weight:

54 parts of A phase, 13 parts of B1 phase, 4.7 parts of B2 phase, 3.1 parts of C phase, 14 parts of D1 phase, 9 parts of D2 phase, 4.8 parts of D3 phase, 2.8 parts of D4 phase, 1.9 parts of E1 phase and 0.08 part of E2 phase;

phase A: a humectant complex;

b1 phase: an emulsifier complex;

b2 phase: conditioning emollient formulations;

and C phase: a film-forming agent complex;

d1 phase: plant extracts and fermentation product combinations;

d2 phase: an aqueous tranexamic acid solution;

d3 phase: an aqueous solution of tetrahydro-methyl-pyrimidine-carboxylic acid;

d4 phase: an aqueous solution of allicin;

e1 phase: a preservative composition;

e2 phase: and (4) essence.

The phase A comprises the following components in parts by weight: 48-50 parts of water, 0.05-0.1 part of EDTA disodium, 2-3 parts of trehalose, 2-3 parts of betaine and 1-3 parts of 1, 3-butanediol.

The B1 phase comprises the following components in parts by weight: 1-2 parts of cetearyl olive oleate, 1-2 parts of sorbitan olive oleate, 1-2 parts of glyceryl stearate, 1-2 parts of PEG-100 stearate, 2-3 parts of cetyl ethyl hexanoate, 0.5-1 part of whale wax stearyl alcohol, 2-4 parts of glycerol tri (ethyl hexanoate), 0.1-0.2 part of methyl hydroxybenzoate and 2-3 parts of polydimethylsiloxane.

The B2 phase comprises the following components in parts by weight: 2-4 parts of phytosterol and 2-4 parts of lanolin.

The phase C comprises the following components in parts by weight: 1-3 parts of cyclopentadimethylsiloxane, 0.5-1 part of hydroxyethyl acrylate and 0.5-1 part of acryloyl dimethyl sodium taurate copolymer;

the D1 phase comprises the following components in parts by weight: 0.5-0.8 part of butanediol, 0.1-0.3 part of centella asiatica extract, 0.1-0.3 part of polygonum cuspidatum root extract, 0.1-0.3 part of scutellaria baicalensis root extract, 0.1-0.3 part of tea extract, 0.1-0.3 part of chamomile flower extract, 0.1-0.3 part of rosemary leaf extract, 0.1-0.3 part of red clover flower extract, 2-4 parts of carbohydrate isomer, 0.8-1 part of isoprene glycol, 1-2 parts of lactobacillus/rice fermentation product, 0.1-0.5 part of schizosaccharomyces cerevisiae fermentation product lysate, 1.2-1.5 parts of xanthan gum, 0.8-1 part of methylparaben and 0.8-1 part of phenoxyethanol.

The D2 phase comprises the following components in parts by weight: 5 parts of water and 3 parts of tranexamic acid.

The D3 phase comprises the following components in parts by weight: 3 parts of water and 1 part of tetrahydro-methyl pyrimidine carboxylic acid.

The D4 phase comprises the following components in parts by weight: 2 parts of water and 0.5-0.8 part of garlic extract.

The E1 phase comprises the following components in parts by weight: 0.1 part of caprylyl hydroximic acid, 0.2 part of ethylhexyl glycerol, 0.5 part of 1, 2-hexanediol and 0.3 part of propylene glycol.

A preparation method of allicin refined rejuvenation essence cream comprises the following steps:

adding the phase A into a clean and sterile emulsifying pot, heating to 90 ℃, preserving heat, sterilizing for 30 minutes, and preserving heat for later use;

secondly, adding B1 into a clean sterile oil phase pot, heating to 90 ℃, stirring to completely melt all the components, adding B2 phase, stirring to completely melt all the components to obtain B phase, and keeping the temperature at 78 ℃ for later use;

thirdly, premixing the phase C uniformly for later use;

fourthly, uniformly premixing the D2 phase, the D3 phase, the D4 phase, the E1 phase and the E2 phase for later use;

filtering and sucking the phase B prepared in the step two into an emulsifying pot, adjusting the vacuum degree to be-0.05 MPa, adjusting the stirring speed to be 58-30rpm, starting homogenizing, adjusting the homogenizing speed to be 30-40rpm, carrying out vacuum homogenizing stirring for 5 minutes, then adding the premixed and uniform phase C, adjusting the homogenizing speed to be 30-40rpm, carrying out vacuum homogenizing stirring for 5 minutes, starting cooling water after carrying out heat preservation and defoaming for 20 minutes, carrying out vacuum stirring for cooling, and properly adjusting the stirring speed during cooling so as to avoid exciting foams and influencing the appearance of the paste body;

sixthly, adding the D1 phase and the uniformly premixed D2 phase, D3 phase, E1 phase and E2 phase at the temperature of below 45 ℃, fully and uniformly stirring, adding the uniformly premixed D4 phase, uniformly stirring and mixing, discharging after detection at 38 ℃, and aseptically packaging to obtain the finished product.

Example four

A garlic moistening and revitalizing essence cream is prepared from the following raw materials in parts by weight:

55 parts of phase A, 15 parts of phase B1, 5 parts of phase B2, 3.2 parts of phase C, 15 parts of phase D1, 10 parts of phase D2, 5 parts of phase D3, 3 parts of phase D4, 2 parts of phase E1 and 0.1 part of phase E2;

phase A: a humectant complex;

b1 phase: an emulsifier complex;

b2 phase: conditioning emollient formulations;

and C phase: a film-forming agent complex;

d1 phase: plant extracts and fermentation product combinations;

d2 phase: an aqueous tranexamic acid solution;

d3 phase: an aqueous solution of tetrahydro-methyl-pyrimidine-carboxylic acid;

d4 phase: an aqueous solution of allicin;

e1 phase: a preservative composition;

e2 phase: and (4) essence.

The phase A comprises the following components in parts by weight: 48-50 parts of water, 0.05-0.1 part of EDTA disodium, 2-3 parts of trehalose, 2-3 parts of betaine and 1-3 parts of 1, 3-butanediol.

The B1 phase comprises the following components in parts by weight: 1-2 parts of cetearyl olive oleate, 1-2 parts of sorbitan olive oleate, 1-2 parts of glyceryl stearate, 1-2 parts of PEG-100 stearate, 2-3 parts of cetyl ethyl hexanoate, 0.5-1 part of whale wax stearyl alcohol, 2-4 parts of glycerol tri (ethyl hexanoate), 0.1-0.2 part of methyl hydroxybenzoate and 2-3 parts of polydimethylsiloxane.

The B2 phase comprises the following components in parts by weight: 2-4 parts of phytosterol and 2-4 parts of lanolin.

The phase C comprises the following components in parts by weight: 1-3 parts of cyclopentadimethylsiloxane, 0.5-1 part of hydroxyethyl acrylate and 0.5-1 part of acryloyl dimethyl sodium taurate copolymer;

the D1 phase comprises the following components in parts by weight: 0.5-0.8 part of butanediol, 0.1-0.3 part of centella asiatica extract, 0.1-0.3 part of polygonum cuspidatum root extract, 0.1-0.3 part of scutellaria baicalensis root extract, 0.1-0.3 part of tea extract, 0.1-0.3 part of chamomile flower extract, 0.1-0.3 part of rosemary leaf extract, 0.1-0.3 part of red clover flower extract, 2-4 parts of carbohydrate isomer, 0.8-1 part of isoprene glycol, 1-2 parts of lactobacillus/rice fermentation product, 0.1-0.5 part of schizosaccharomyces cerevisiae fermentation product lysate, 1.2-1.5 parts of xanthan gum, 0.8-1 part of methylparaben and 0.8-1 part of phenoxyethanol.

The D2 phase comprises the following components in parts by weight: 5 parts of water and 3 parts of tranexamic acid.

The D3 phase comprises the following components in parts by weight: 3 parts of water and 1 part of tetrahydro-methyl pyrimidine carboxylic acid.

The D4 phase comprises the following components in parts by weight: 2 parts of water and 0.5-0.8 part of garlic extract.

The E1 phase comprises the following components in parts by weight: 0.1 part of caprylyl hydroximic acid, 0.2 part of ethylhexyl glycerol, 0.5 part of 1, 2-hexanediol and 0.3 part of propylene glycol.

A preparation method of allicin refined rejuvenation essence cream comprises the following steps:

adding the phase A into a clean and sterile emulsifying pot, heating to 90 ℃, preserving heat, sterilizing for 30 minutes, and preserving heat for later use;

secondly, adding B1 into a clean sterile oil phase pot, heating to 90 ℃, stirring to completely melt all the components, adding B2 phase, stirring to completely melt all the components to obtain B phase, and keeping the temperature at 78 ℃ for later use;

thirdly, premixing the phase C uniformly for later use;

fourthly, uniformly premixing the D2 phase, the D3 phase, the D4 phase, the E1 phase and the E2 phase for later use;

filtering and sucking the phase B prepared in the step two into an emulsifying pot, adjusting the vacuum degree to be-0.05 MPa, adjusting the stirring speed to be 58-30rpm, starting homogenizing, adjusting the homogenizing speed to be 30-40rpm, carrying out vacuum homogenizing stirring for 5 minutes, then adding the premixed and uniform phase C, adjusting the homogenizing speed to be 30-40rpm, carrying out vacuum homogenizing stirring for 5 minutes, starting cooling water after carrying out heat preservation and defoaming for 20 minutes, carrying out vacuum stirring for cooling, and properly adjusting the stirring speed during cooling so as to avoid exciting foams and influencing the appearance of the paste body;

sixthly, adding the D1 phase and the uniformly premixed D2 phase, D3 phase, E1 phase and E2 phase at the temperature of below 45 ℃, fully and uniformly stirring, adding the uniformly premixed D4 phase, uniformly stirring and mixing, discharging after detection at 38 ℃, and aseptically packaging to obtain the finished product.

EXAMPLE five

A garlic moistening and revitalizing essence cream is prepared from the following raw materials in parts by weight:

50 parts of phase A, 10 parts of phase B1, 4 parts of phase B2, 2.7 parts of phase C, 12 parts of phase D1, 8 parts of phase D2, 4 parts of phase D3, 2.5 parts of phase D4, 1 part of phase E1, 0.05 part of phase E2 and 5 parts of phase F;

phase A: a humectant complex;

b1 phase: an emulsifier complex;

b2 phase: conditioning emollient formulations;

and C phase: a film-forming agent complex;

d1 phase: plant extracts and fermentation product combinations;

d2 phase: an aqueous tranexamic acid solution;

d3 phase: an aqueous solution of tetrahydro-methyl-pyrimidine-carboxylic acid;

d4 phase: an aqueous solution of allicin;

e1 phase: a preservative composition;

e2 phase: an essence;

and (3) phase F: an animal collagen composition.

The phase A comprises the following components in parts by weight: 48-50 parts of water, 0.05-0.1 part of EDTA disodium, 2-3 parts of trehalose, 2-3 parts of betaine and 1-3 parts of 1, 3-butanediol.

The B1 phase comprises the following components in parts by weight: 1-2 parts of cetearyl olive oleate, 1-2 parts of sorbitan olive oleate, 1-2 parts of glyceryl stearate, 1-2 parts of PEG-100 stearate, 2-3 parts of cetyl ethyl hexanoate, 0.5-1 part of whale wax stearyl alcohol, 2-4 parts of glycerol tri (ethyl hexanoate), 0.1-0.2 part of methyl hydroxybenzoate and 2-3 parts of polydimethylsiloxane.

The B2 phase comprises the following components in parts by weight: 2-4 parts of phytosterol and 2-4 parts of lanolin.

The phase C comprises the following components in parts by weight: 1-3 parts of cyclopentadimethylsiloxane, 0.5-1 part of hydroxyethyl acrylate and 0.5-1 part of acryloyl dimethyl sodium taurate copolymer;

the D1 phase comprises the following components in parts by weight: 0.5-0.8 part of butanediol, 0.1-0.3 part of centella asiatica extract, 0.1-0.3 part of polygonum cuspidatum root extract, 0.1-0.3 part of scutellaria baicalensis root extract, 0.1-0.3 part of tea extract, 0.1-0.3 part of chamomile flower extract, 0.1-0.3 part of rosemary leaf extract, 0.1-0.3 part of red clover flower extract, 2-4 parts of carbohydrate isomer, 0.8-1 part of isoprene glycol, 1-2 parts of lactobacillus/rice fermentation product, 0.1-0.5 part of schizosaccharomyces cerevisiae fermentation product lysate, 1.2-1.5 parts of xanthan gum, 0.8-1 part of methylparaben and 0.8-1 part of phenoxyethanol.

The D2 phase comprises the following components in parts by weight: 5 parts of water and 3 parts of tranexamic acid.

The D3 phase comprises the following components in parts by weight: 3 parts of water and 1 part of tetrahydro-methyl pyrimidine carboxylic acid.

The D4 phase comprises the following components in parts by weight: 2 parts of water and 0.5-0.8 part of garlic extract.

The E1 phase comprises the following components in parts by weight: 0.1 part of caprylyl hydroximic acid, 0.2 part of ethylhexyl glycerol, 0.5 part of 1, 2-hexanediol and 0.3 part of propylene glycol.

The phase F is a composition of fish collagen and ossein, and the mixture ratio of the fish collagen is that: 1-3: 3-5.

The collagen has strong ability of absorbing water around the environment; when the moisture-retaining agent is covered on the skin, the moisture can be prevented from evaporating from the surface, and the moisture-retaining effect is very obvious. The unique triple-helical structure of the ossein and the hydrophilic group in collagen molecules strengthen the primary hydrodynamic force of the skin, ensure the circulation of water on the surface and the deep layer of the skin, improve lymphatic circulation and enable the skin to be full of water and active. The composition of fish collagen and ossein protein is adopted, and the collagen protein is enabled to be effective through reasonable proportion, and the increase of the ossein protein to the viscosity of the essence can be reduced.

The fish collagen is mainly extracted from cod, salmon and fresh skin scales by a biological enzyme directional shearing technology.

A preparation method of allicin refined rejuvenation essence cream comprises the following steps:

adding the phase A into a clean and sterile emulsifying pot, heating to 90 ℃, preserving heat, sterilizing for 30 minutes, and preserving heat for later use;

secondly, adding B1 into a clean sterile oil phase pot, heating to 90 ℃, stirring to completely melt all the components, adding B2 phase, stirring to completely melt all the components to obtain B phase, and keeping the temperature at 78 ℃ for later use;

thirdly, premixing the phase C uniformly for later use;

fourthly, uniformly premixing the D2 phase, the D3 phase, the D4 phase, the E1 phase, the E2 phase and the F phase for later use;

filtering and sucking the phase B prepared in the step two into an emulsifying pot, adjusting the vacuum degree to be-0.05 MPa, adjusting the stirring speed to be 58-30rpm, starting homogenizing, adjusting the homogenizing speed to be 30-40rpm, carrying out vacuum homogenizing stirring for 5 minutes, then adding the premixed and uniform phase C, adjusting the homogenizing speed to be 30-40rpm, carrying out vacuum homogenizing stirring for 5 minutes, starting cooling water after carrying out heat preservation and defoaming for 20 minutes, carrying out vacuum stirring for cooling, and properly adjusting the stirring speed during cooling so as to avoid exciting foams and influencing the appearance of the paste body;

sixthly, adding the D1 phase and the uniformly premixed D2 phase, D3 phase, E1 phase and E2 phase at the temperature of below 45 ℃, fully and uniformly stirring, adding the uniformly premixed D4 phase and F phase, uniformly stirring and mixing, discharging after the detection at 38 ℃ is qualified, and aseptically packaging to obtain the finished product.

EXAMPLE six

A garlic moistening and revitalizing essence cream is prepared from the following raw materials in parts by weight:

52 parts of phase A, 12 parts of phase B1, 4.3 parts of phase B2, 2.9 parts of phase C, 13 parts of phase D1, 8.5 parts of phase D2, 4.3 parts of phase D3, 2.7 parts of phase D4, 1.2 parts of phase E1, 0.07 part of phase E2 and 6 parts of phase F;

phase A: a humectant complex;

b1 phase: an emulsifier complex;

b2 phase: conditioning emollient formulations;

and C phase: a film-forming agent complex;

d1 phase: plant extracts and fermentation product combinations;

d2 phase: an aqueous tranexamic acid solution;

d3 phase: an aqueous solution of tetrahydro-methyl-pyrimidine-carboxylic acid;

d4 phase: an aqueous solution of allicin;

e1 phase: a preservative composition;

e2 phase: an essence;

and (3) phase F: an animal collagen composition.

The phase A comprises the following components in parts by weight: 48-50 parts of water, 0.05-0.1 part of EDTA disodium, 2-3 parts of trehalose, 2-3 parts of betaine and 1-3 parts of 1, 3-butanediol.

The B1 phase comprises the following components in parts by weight: 1-2 parts of cetearyl olive oleate, 1-2 parts of sorbitan olive oleate, 1-2 parts of glyceryl stearate, 1-2 parts of PEG-100 stearate, 2-3 parts of cetyl ethyl hexanoate, 0.5-1 part of whale wax stearyl alcohol, 2-4 parts of glycerol tri (ethyl hexanoate), 0.1-0.2 part of methyl hydroxybenzoate and 2-3 parts of polydimethylsiloxane.

The B2 phase comprises the following components in parts by weight: 2-4 parts of phytosterol and 2-4 parts of lanolin.

The phase C comprises the following components in parts by weight: 1-3 parts of cyclopentadimethylsiloxane, 0.5-1 part of hydroxyethyl acrylate and 0.5-1 part of acryloyl dimethyl sodium taurate copolymer;

the D1 phase comprises the following components in parts by weight: 0.5-0.8 part of butanediol, 0.1-0.3 part of centella asiatica extract, 0.1-0.3 part of polygonum cuspidatum root extract, 0.1-0.3 part of scutellaria baicalensis root extract, 0.1-0.3 part of tea extract, 0.1-0.3 part of chamomile flower extract, 0.1-0.3 part of rosemary leaf extract, 0.1-0.3 part of red clover flower extract, 2-4 parts of carbohydrate isomer, 0.8-1 part of isoprene glycol, 1-2 parts of lactobacillus/rice fermentation product, 0.1-0.5 part of schizosaccharomyces cerevisiae fermentation product lysate, 1.2-1.5 parts of xanthan gum, 0.8-1 part of methylparaben and 0.8-1 part of phenoxyethanol.

The D2 phase comprises the following components in parts by weight: 5 parts of water and 3 parts of tranexamic acid.

The D3 phase comprises the following components in parts by weight: 3 parts of water and 1 part of tetrahydro-methyl pyrimidine carboxylic acid.

The D4 phase comprises the following components in parts by weight: 2 parts of water and 0.5-0.8 part of garlic extract.

The E1 phase comprises the following components in parts by weight: 0.1 part of caprylyl hydroximic acid, 0.2 part of ethylhexyl glycerol, 0.5 part of 1, 2-hexanediol and 0.3 part of propylene glycol.

The phase F is a composition of fish collagen and ossein, and the mixture ratio of the fish collagen is that: 1-3: 3-5.

The collagen has strong ability of absorbing water around the environment; when the moisture-retaining agent is covered on the skin, the moisture can be prevented from evaporating from the surface, and the moisture-retaining effect is very obvious. The unique triple-helical structure of the ossein and the hydrophilic group in collagen molecules strengthen the primary hydrodynamic force of the skin, ensure the circulation of water on the surface and the deep layer of the skin, improve lymphatic circulation and enable the skin to be full of water and active. The composition of fish collagen and ossein protein is adopted, and the collagen protein is enabled to be effective through reasonable proportion, and the increase of the ossein protein to the viscosity of the essence can be reduced.

The fish collagen is mainly extracted from cod, salmon and fresh skin scales by a biological enzyme directional shearing technology.

A preparation method of allicin refined rejuvenation essence cream comprises the following steps:

adding the phase A into a clean and sterile emulsifying pot, heating to 90 ℃, preserving heat, sterilizing for 30 minutes, and preserving heat for later use;

secondly, adding B1 into a clean sterile oil phase pot, heating to 90 ℃, stirring to completely melt all the components, adding B2 phase, stirring to completely melt all the components to obtain B phase, and keeping the temperature at 78 ℃ for later use;

thirdly, premixing the phase C uniformly for later use;

fourthly, uniformly premixing the D2 phase, the D3 phase, the D4 phase, the E1 phase, the E2 phase and the F phase for later use;

filtering and sucking the phase B prepared in the step two into an emulsifying pot, adjusting the vacuum degree to be-0.05 MPa, adjusting the stirring speed to be 58-30rpm, starting homogenizing, adjusting the homogenizing speed to be 30-40rpm, carrying out vacuum homogenizing stirring for 5 minutes, then adding the premixed and uniform phase C, adjusting the homogenizing speed to be 30-40rpm, carrying out vacuum homogenizing stirring for 5 minutes, starting cooling water after carrying out heat preservation and defoaming for 20 minutes, carrying out vacuum stirring for cooling, and properly adjusting the stirring speed during cooling so as to avoid exciting foams and influencing the appearance of the paste body;

sixthly, adding the D1 phase and the uniformly premixed D2 phase, D3 phase, E1 phase and E2 phase at the temperature of below 45 ℃, fully and uniformly stirring, adding the uniformly premixed D4 phase and F phase, uniformly stirring and mixing, discharging after the detection at 38 ℃ is qualified, and aseptically packaging to obtain the finished product.

EXAMPLE seven

A garlic moistening and revitalizing essence cream is prepared from the following raw materials in parts by weight:

54 parts of phase A, 13 parts of phase B1, 4.7 parts of phase B2, 3.1 parts of phase C, 14 parts of phase D1, 9 parts of phase D2, 4.8 parts of phase D3, 2.8 parts of phase D4, 1.9 parts of phase E1, 0.08 part of phase E2 and 6.5 parts of phase F;

phase A: a humectant complex;

b1 phase: an emulsifier complex;

b2 phase: conditioning emollient formulations;

and C phase: a film-forming agent complex;

d1 phase: plant extracts and fermentation product combinations;

d2 phase: an aqueous tranexamic acid solution;

d3 phase: an aqueous solution of tetrahydro-methyl-pyrimidine-carboxylic acid;

d4 phase: an aqueous solution of allicin;

e1 phase: a preservative composition;

e2 phase: an essence;

and (3) phase F: an animal collagen composition.

The phase A comprises the following components in parts by weight: 48-50 parts of water, 0.05-0.1 part of EDTA disodium, 2-3 parts of trehalose, 2-3 parts of betaine and 1-3 parts of 1, 3-butanediol.

The B1 phase comprises the following components in parts by weight: 1-2 parts of cetearyl olive oleate, 1-2 parts of sorbitan olive oleate, 1-2 parts of glyceryl stearate, 1-2 parts of PEG-100 stearate, 2-3 parts of cetyl ethyl hexanoate, 0.5-1 part of whale wax stearyl alcohol, 2-4 parts of glycerol tri (ethyl hexanoate), 0.1-0.2 part of methyl hydroxybenzoate and 2-3 parts of polydimethylsiloxane.

The B2 phase comprises the following components in parts by weight: 2-4 parts of phytosterol and 2-4 parts of lanolin.

The phase C comprises the following components in parts by weight: 1-3 parts of cyclopentadimethylsiloxane, 0.5-1 part of hydroxyethyl acrylate and 0.5-1 part of acryloyl dimethyl sodium taurate copolymer;

the D1 phase comprises the following components in parts by weight: 0.5-0.8 part of butanediol, 0.1-0.3 part of centella asiatica extract, 0.1-0.3 part of polygonum cuspidatum root extract, 0.1-0.3 part of scutellaria baicalensis root extract, 0.1-0.3 part of tea extract, 0.1-0.3 part of chamomile flower extract, 0.1-0.3 part of rosemary leaf extract, 0.1-0.3 part of red clover flower extract, 2-4 parts of carbohydrate isomer, 0.8-1 part of isoprene glycol, 1-2 parts of lactobacillus/rice fermentation product, 0.1-0.5 part of schizosaccharomyces cerevisiae fermentation product lysate, 1.2-1.5 parts of xanthan gum, 0.8-1 part of methylparaben and 0.8-1 part of phenoxyethanol.

The D2 phase comprises the following components in parts by weight: 5 parts of water and 3 parts of tranexamic acid.

The D3 phase comprises the following components in parts by weight: 3 parts of water and 1 part of tetrahydro-methyl pyrimidine carboxylic acid.

The D4 phase comprises the following components in parts by weight: 2 parts of water and 0.5-0.8 part of garlic extract.

The E1 phase comprises the following components in parts by weight: 0.1 part of caprylyl hydroximic acid, 0.2 part of ethylhexyl glycerol, 0.5 part of 1, 2-hexanediol and 0.3 part of propylene glycol.

The phase F is a composition of fish collagen and ossein, and the mixture ratio of the fish collagen is that: 1-3: 3-5.

The collagen has strong ability of absorbing water around the environment; when the moisture-retaining agent is covered on the skin, the moisture can be prevented from evaporating from the surface, and the moisture-retaining effect is very obvious. The unique triple-helical structure of the ossein and the hydrophilic group in collagen molecules strengthen the primary hydrodynamic force of the skin, ensure the circulation of water on the surface and the deep layer of the skin, improve lymphatic circulation and enable the skin to be full of water and active. The composition of fish collagen and ossein protein is adopted, and the collagen protein is enabled to be effective through reasonable proportion, and the increase of the ossein protein to the viscosity of the essence can be reduced.

The fish collagen is mainly extracted from cod, salmon and fresh skin scales by a biological enzyme directional shearing technology.

A preparation method of allicin refined rejuvenation essence cream comprises the following steps:

adding the phase A into a clean and sterile emulsifying pot, heating to 90 ℃, preserving heat, sterilizing for 30 minutes, and preserving heat for later use;

secondly, adding B1 into a clean sterile oil phase pot, heating to 90 ℃, stirring to completely melt all the components, adding B2 phase, stirring to completely melt all the components to obtain B phase, and keeping the temperature at 78 ℃ for later use;

thirdly, premixing the phase C uniformly for later use;

fourthly, uniformly premixing the D2 phase, the D3 phase, the D4 phase, the E1 phase, the E2 phase and the F phase for later use;

filtering and sucking the phase B prepared in the step two into an emulsifying pot, adjusting the vacuum degree to be-0.05 MPa, adjusting the stirring speed to be 58-30rpm, starting homogenizing, adjusting the homogenizing speed to be 30-40rpm, carrying out vacuum homogenizing stirring for 5 minutes, then adding the premixed and uniform phase C, adjusting the homogenizing speed to be 30-40rpm, carrying out vacuum homogenizing stirring for 5 minutes, starting cooling water after carrying out heat preservation and defoaming for 20 minutes, carrying out vacuum stirring for cooling, and properly adjusting the stirring speed during cooling so as to avoid exciting foams and influencing the appearance of the paste body;

sixthly, adding the D1 phase and the uniformly premixed D2 phase, D3 phase, E1 phase and E2 phase at the temperature of below 45 ℃, fully and uniformly stirring, adding the uniformly premixed D4 phase and F phase, uniformly stirring and mixing, discharging after the detection at 38 ℃ is qualified, and aseptically packaging to obtain the finished product.

Example eight

A garlic moistening and revitalizing essence cream is prepared from the following raw materials in parts by weight:

55 parts of phase A, 15 parts of phase B1, 5 parts of phase B2, 3.2 parts of phase C, 15 parts of phase D1, 10 parts of phase D2, 5 parts of phase D3, 3 parts of phase D4, 2 parts of phase E1, 0.1 part of phase E2 and 7 parts of phase F;

phase A: a humectant complex;

b1 phase: an emulsifier complex;

b2 phase: conditioning emollient formulations;

and C phase: a film-forming agent complex;

d1 phase: plant extracts and fermentation product combinations;

d2 phase: an aqueous tranexamic acid solution;

d3 phase: an aqueous solution of tetrahydro-methyl-pyrimidine-carboxylic acid;

d4 phase: an aqueous solution of allicin;

e1 phase: a preservative composition;

e2 phase: an essence;

and (3) phase F: an animal collagen composition.

The phase A comprises the following components in parts by weight: 48-50 parts of water, 0.05-0.1 part of EDTA disodium, 2-3 parts of trehalose, 2-3 parts of betaine and 1-3 parts of 1, 3-butanediol.

The B1 phase comprises the following components in parts by weight: 1-2 parts of cetearyl olive oleate, 1-2 parts of sorbitan olive oleate, 1-2 parts of glyceryl stearate, 1-2 parts of PEG-100 stearate, 2-3 parts of cetyl ethyl hexanoate, 0.5-1 part of whale wax stearyl alcohol, 2-4 parts of glycerol tri (ethyl hexanoate), 0.1-0.2 part of methyl hydroxybenzoate and 2-3 parts of polydimethylsiloxane.

The B2 phase comprises the following components in parts by weight: 2-4 parts of phytosterol and 2-4 parts of lanolin.

The phase C comprises the following components in parts by weight: 1-3 parts of cyclopentadimethylsiloxane, 0.5-1 part of hydroxyethyl acrylate and 0.5-1 part of acryloyl dimethyl sodium taurate copolymer;

the D1 phase comprises the following components in parts by weight: 0.5-0.8 part of butanediol, 0.1-0.3 part of centella asiatica extract, 0.1-0.3 part of polygonum cuspidatum root extract, 0.1-0.3 part of scutellaria baicalensis root extract, 0.1-0.3 part of tea extract, 0.1-0.3 part of chamomile flower extract, 0.1-0.3 part of rosemary leaf extract, 0.1-0.3 part of red clover flower extract, 2-4 parts of carbohydrate isomer, 0.8-1 part of isoprene glycol, 1-2 parts of lactobacillus/rice fermentation product, 0.1-0.5 part of schizosaccharomyces cerevisiae fermentation product lysate, 1.2-1.5 parts of xanthan gum, 0.8-1 part of methylparaben and 0.8-1 part of phenoxyethanol.

The D2 phase comprises the following components in parts by weight: 5 parts of water and 3 parts of tranexamic acid.

The D3 phase comprises the following components in parts by weight: 3 parts of water and 1 part of tetrahydro-methyl pyrimidine carboxylic acid.

The D4 phase comprises the following components in parts by weight: 2 parts of water and 0.5-0.8 part of garlic extract.

The E1 phase comprises the following components in parts by weight: 0.1 part of caprylyl hydroximic acid, 0.2 part of ethylhexyl glycerol, 0.5 part of 1, 2-hexanediol and 0.3 part of propylene glycol.

The phase F is a composition of fish collagen and ossein, and the mixture ratio of the fish collagen is that: 1-3: 3-5.

The collagen has strong ability of absorbing water around the environment; when the moisture-retaining agent is covered on the skin, the moisture can be prevented from evaporating from the surface, and the moisture-retaining effect is very obvious. The unique triple-helical structure of the ossein and the hydrophilic group in collagen molecules strengthen the primary hydrodynamic force of the skin, ensure the circulation of water on the surface and the deep layer of the skin, improve lymphatic circulation and enable the skin to be full of water and active. The composition of fish collagen and ossein protein is adopted, and the collagen protein is enabled to be effective through reasonable proportion, and the increase of the ossein protein to the viscosity of the essence can be reduced.

The fish collagen is mainly extracted from cod, salmon and fresh skin scales by a biological enzyme directional shearing technology.

A preparation method of allicin refined rejuvenation essence cream comprises the following steps:

adding the phase A into a clean and sterile emulsifying pot, heating to 90 ℃, preserving heat, sterilizing for 30 minutes, and preserving heat for later use;

secondly, adding B1 into a clean sterile oil phase pot, heating to 90 ℃, stirring to completely melt all the components, adding B2 phase, stirring to completely melt all the components to obtain B phase, and keeping the temperature at 78 ℃ for later use;

thirdly, premixing the phase C uniformly for later use;

fourthly, uniformly premixing the D2 phase, the D3 phase, the D4 phase, the E1 phase, the E2 phase and the F phase for later use;

filtering and sucking the phase B prepared in the step two into an emulsifying pot, adjusting the vacuum degree to be-0.05 MPa, adjusting the stirring speed to be 58-30rpm, starting homogenizing, adjusting the homogenizing speed to be 30-40rpm, carrying out vacuum homogenizing stirring for 5 minutes, then adding the premixed and uniform phase C, adjusting the homogenizing speed to be 30-40rpm, carrying out vacuum homogenizing stirring for 5 minutes, starting cooling water after carrying out heat preservation and defoaming for 20 minutes, carrying out vacuum stirring for cooling, and properly adjusting the stirring speed during cooling so as to avoid exciting foams and influencing the appearance of the paste body;

sixthly, adding the D1 phase and the uniformly premixed D2 phase, D3 phase, E1 phase and E2 phase at the temperature of below 45 ℃, fully and uniformly stirring, adding the uniformly premixed D4 phase and F phase, uniformly stirring and mixing, discharging after the detection at 38 ℃ is qualified, and aseptically packaging to obtain the finished product.

Results of the experiment

In the first to eighth embodiments, all the sanitation indexes and the sensory indexes of the product meet the standards of QB/T1857-2013 cream, massage cream and vanishing cream.

The products in the first to eighth examples are taken as samples to carry out experiments, and the control variables of the components in the first to eighth examples are as follows:

the phase A comprises the following components in parts by weight: 48 parts of water, 0.05 part of EDTA disodium, 2 parts of trehalose, 2 parts of betaine and 1 part of 1, 3-butanediol.

The B1 phase comprises the following components in parts by weight: 1 part of cetearyl olive oleate, 1 part of sorbitan olive oleate, 1 part of glycerol stearate, 1 part of PEG-100 stearate, 2 parts of cetearyl ethyl hexanoate, 0.5 part of cetearyl alcohol, 2 parts of glycerol tri (ethyl hexanoate), 0.1 part of methylparaben and 2 parts of polydimethylsiloxane.

The B2 phase comprises the following components in parts by weight: 2 parts of phytosterol and 2 parts of lanolin.

The phase C comprises the following components in parts by weight: 1 part of cyclopenta dimethyl siloxane, 0.5 part of hydroxyethyl acrylate and 0.5 part of acryloyl dimethyl sodium taurate copolymer;

the D1 phase comprises the following components in parts by weight: 0.5 part of butanediol, 0.1 part of centella extract, 0.1 part of polygonum cuspidatum root extract, 0.1 part of radix scutellariae extract, 0.1 part of tea extract, 0.1 part of chamomile extract, 0.1 part of rosemary leaf extract, 0.1 part of red clover flower extract, 2 parts of saccharide isomer, 0.8 part of isoprene glycol, 1 part of lactobacillus/rice fermentation product, 0.1 part of schizosaccharomyces cerevisiae fermentation product lysate, 1.2 parts of xanthan gum, 0.8 part of methylparaben and 0.8 part of phenoxyethanol.

The D2 phase comprises the following components in parts by weight: 5 parts of water and 3 parts of tranexamic acid.

The D3 phase comprises the following components in parts by weight: 3 parts of water and 1 part of tetrahydro-methyl pyrimidine carboxylic acid.

The D4 phase comprises the following components in parts by weight: 2 parts of water and 0.5 part of garlic extract.

The E1 phase comprises the following components in parts by weight: 0.1 part of caprylyl hydroximic acid, 0.2 part of ethylhexyl glycerol, 0.5 part of 1, 2-hexanediol and 0.3 part of propylene glycol.

The value of each phase component is adopted in the experiment. It is of course also possible to use products whose phase composition is at its maximum.

The phase F is a composition of fish collagen and ossein, and the mixture ratio of the fish collagen is that: bone collagen ═ 1: 3.

the following table was obtained:

in the moisture loss test, the average value of the moisture loss (%) in the control area was 41%.

DPPH method determination of antioxidant Activity of essence cream the control test, in which only DPPH ethanol solution was added, showed a radical scavenging rate of 10.2%.

The above experimental results were obtained by the following experimental methods:

experimental method for determining antioxidant activity of essence cream by DPPH (denaturing high pH) method

Antioxidant is any substance that is present at low concentrations to effectively inhibit the oxidation reaction of free radicals, either by acting directly on the free radicals or by indirectly consuming substances that readily form free radicals, preventing further reactions from occurring.

The current research methods for free radical scavengers mainly belong to 2 types, one type is an in vitro model, and the other type is an in vivo model, wherein the DPPH method is the most common method in the in vitro model.

DPPH is also called 1, 1-diphenyl-2-trinitrophenylhydrazine, is a very stable free radical with a nitrogen center, and the stability of DPPH mainly comes from the steric hindrance of 3 benzene rings with resonance stabilization effect, so that unpaired electrons on the nitrogen atom in the middle cannot play the role of electron pairing. Its absolute ethyl alcohol solution is purple, and has maximum absorption at wavelength of 517nm, and its absorbance and concentration are in linear relation. When a radical scavenger is added thereto, DPPH may be combined with or substituted for the radical scavenger, whereby the radical scavenging ability can be evaluated by decreasing the number of radicals, decreasing the absorbance, and decreasing the color of the solution. Namely, the antioxidant capacity was calculated by measuring the DPPH-removing effect of the sample at a wavelength of 517 nm.

Experimental materials: DPPH (1, 1-diphenyl-2-trinitrophenylhydrazine); absolute ethyl alcohol;

an experimental instrument: spectrophotometer

Preparation of DPPH stock solution

Accurately weighing 3.5mg of DPPH reagent, dissolving with absolute ethyl alcohol, quantitatively transferring into a 10mL volumetric flask, fixing the volume to a scale with the absolute ethyl alcohol, taking 2mL to 100mL volumetric flask, shaking up to obtain DPPH stock solution with the concentration of 0.0178mmol/L, and placing in a refrigerator for storage.

Preparation of essence cream solution

Weighing 3.5mg of essence cream (products in the first to eighth embodiments), and adding 100ml of water to obtain essence cream solution.

Measurement of two, DPPH and clearance

Adding 4.0mL of the LDPPH solution and the essence cream solution into a 10mL colorimetric tube in sequence, adding absolute ethyl alcohol to the scale, immediately mixing, measuring a light absorption value (A) at a wavelength of 517nm by using a 1cm cuvette, marking the light absorption value as Ai, then measuring the light absorption value after storing in a greenhouse in a dark place for 30min, marking the light absorption value as Aj, and marking the light absorption value as Ac in a contrast test by using an ethanol solution only added with DPPH. The radical clearance (K) is calculated as follows:

K(％)＝[1-(Ai-Aj)/Ac]*100％

the test was repeated three times, and the average value was taken as the final result.

Medicine preparation: DPPH (1, 1-diphenyl-2-trinitrophenylhydrazine);

the manufacturer: shanghai such as Ji Biotech development Inc. or Beijing Nuo Bo Laide technology Inc.;

and (4) quotation: 380 yuan/bottle; 500 yuan/bottle;

specification: 1 g/bottle;

the content is as follows: 99 percent;

the producing area: imported from Japan.

Method for testing moisture loss rate

An experimental instrument: the model is as follows:

percutaneous water loss (TEWL) determinator for AS-VT100RS

1) Subjects were uniformly cleaned of the inside of the forearm by laboratory test personnel. The subject sits still in a laboratory at a temperature of 21 + -1 deg.C, 50 + -5% RH for at least 20 minutes, during which time water and drink cannot be consumed, the forearm is exposed and remains relaxed;

2) selecting and marking two face areas, namely a product area and a comparison area, wherein the area of each area is 2cm multiplied by 2 cm;

3) testing stratum corneum water content basic value of the face area of the subject;

4) using the test sample in the product area according to the product use requirement;

5) the stratum corneum moisture content measurements of the test subject product and control zones were taken 3h later (fan on side to accelerate moisture loss).

Water loss rate (%) (measured value of water content in horny layer-water content basis value of horny layer)/water content basis value of horny layer.

The above-mentioned embodiments only express several embodiments of the present invention, and the description thereof is more specific and detailed, but not construed as limiting the scope of the present invention. It should be noted that, for a person skilled in the art, several variations and modifications can be made without departing from the spirit of the invention, which falls within the scope of the invention.

Claims (9)

1. The allicin moistening and revitalizing essence cream is characterized by being prepared from the following raw materials in parts by weight:

50-55 parts of phase A, 10-15 parts of phase B1, 4-5 parts of phase B2, 2.7-3.2 parts of phase C, 12-15 parts of phase D1, 8-10 parts of phase D2, 4-5 parts of phase D3, 2.5-3 parts of phase D4, 1-2 parts of phase E1 and 0.05-0.1 part of phase E2;

phase A: a humectant complex;

b1 phase: an emulsifier complex;

b2 phase: conditioning emollient formulations;

and C phase: a film-forming agent complex;

d1 phase: plant extracts and fermentation product combinations;

d2 phase: an aqueous tranexamic acid solution;

d3 phase: an aqueous solution of tetrahydro-methyl-pyrimidine-carboxylic acid;

d4 phase: an aqueous solution of allicin;

e1 phase: a preservative composition;

e2 phase: and (4) essence.

2. The allicin refining rejuvenation essence cream according to claim 1, wherein the phase a comprises the following components in parts by weight: 48-50 parts of water, 0.05-0.1 part of EDTA disodium, 2-3 parts of trehalose, 2-3 parts of betaine and 1-3 parts of 1, 3-butanediol.

3. The allicin refining rejuvenation essence cream according to claim 1, wherein the phase B1 comprises the following components in parts by weight: 1-2 parts of cetearyl olive oleate, 1-2 parts of sorbitan olive oleate, 1-2 parts of glyceryl stearate, 1-2 parts of PEG-100 stearate, 2-3 parts of cetyl ethyl hexanoate, 0.5-1 part of cetearyl alcohol, 2-4 parts of glycerol tri (ethyl hexanoate), 0.1-0.2 part of methyl hydroxybenzoate and 2-3 parts of polydimethylsiloxane.

4. The allicin refining rejuvenation essence cream according to claim 1, wherein the phase B2 comprises the following components in parts by weight: 2-4 parts of phytosterol and 2-4 parts of lanolin.

5. The allicin refining rejuvenation essence cream according to claim 1, wherein the phase C comprises the following components in parts by weight: 1-3 parts of cyclopentadimethylsiloxane, 0.5-1 part of hydroxyethyl acrylate and 0.5-1 part of acryloyl dimethyl sodium taurate copolymer.

6. The allicin refining rejuvenation essence cream according to claim 1, wherein the phase D1 comprises the following components in parts by weight: 0.5-0.8 part of butanediol, 0.1-0.3 part of centella asiatica extract, 0.1-0.3 part of polygonum cuspidatum root extract, 0.1-0.3 part of scutellaria baicalensis root extract, 0.1-0.3 part of tea extract, 0.1-0.3 part of chamomile flower extract, 0.1-0.3 part of rosemary leaf extract, 0.1-0.3 part of red clover flower extract, 2-4 parts of carbohydrate isomer, 0.8-1 part of isoprene glycol, 1-2 parts of lactobacillus/rice fermentation product, 0.1-0.5 part of schizosaccharomyces cerevisiae fermentation product lysate, 1.2-1.5 parts of xanthan gum, 0.8-1 part of methylparaben and 0.8-1 part of phenoxyethanol.

7. The allicin refining rejuvenation essence cream according to claim 1, wherein the phase D2 comprises the following components in parts by weight: 5 parts of water and 3 parts of tranexamic acid;

the D3 phase comprises the following components in parts by weight: 3 parts of water and 1 part of tetrahydro-methylpyrimidine carboxylic acid;

the D4 phase comprises the following components in parts by weight: 2 parts of water and 0.5-0.8 part of garlic extract;

the E1 phase comprises the following components in parts by weight: 0.1 part of caprylyl hydroximic acid, 0.2 part of ethylhexyl glycerol, 0.5 part of 1, 2-hexanediol and 0.3 part of propylene glycol.

8. The allicin refining rejuvenating essence cream according to claim 1, which is prepared from the following raw materials in parts by weight:

50-55 parts of phase A, 10-15 parts of phase B1, 4-5 parts of phase B2, 2.7-3.2 parts of phase C, 12-15 parts of phase D1, 8-10 parts of phase D2, 4-5 parts of phase D3, 2.5-3 parts of phase D4, 1-2 parts of phase E1, 0.05-0.1 part of phase E2 and 5-7 parts of phase F;

phase A: a humectant complex;

b1 phase: an emulsifier complex;

b2 phase: conditioning emollient formulations;

and C phase: a film-forming agent complex;

d1 phase: plant extracts and fermentation product combinations;

d2 phase: an aqueous tranexamic acid solution;

d3 phase: an aqueous solution of tetrahydro-methyl-pyrimidine-carboxylic acid;

d4 phase: an aqueous solution of allicin;

e1 phase: a preservative composition;

e2 phase: an essence;

and (3) phase F: an animal collagen composition;

the animal collagen composition is a composition of fish collagen and ossein, and the mixture ratio of the fish collagen is that the fish collagen: 1-3: 3-5.

9. A method of preparing a garlic fine rejuvenating essence according to any one of claims 1 to 7, comprising the steps of:

adding the phase A into a clean and sterile emulsifying pot, heating to 90 ℃, preserving heat, sterilizing for 30 minutes, and preserving heat for later use;

secondly, adding B1 into a clean sterile oil phase pot, heating to 90 ℃, stirring to completely melt all the components, adding B2 phase, stirring to completely melt all the components to obtain B phase, and keeping the temperature at 78 ℃ for later use;

thirdly, premixing the phase C uniformly for later use;

fourthly, uniformly premixing the D2 phase, the D3 phase, the D4 phase, the E1 phase and the E2 phase for later use;

filtering and sucking the phase B prepared in the step two into an emulsifying pot, adjusting the vacuum degree to be-0.05 MPa, adjusting the stirring speed to be 58-30rpm, starting homogenizing, adjusting the homogenizing speed to be 30-40rpm, carrying out vacuum homogenizing stirring for 5 minutes, then adding the premixed and uniform phase C, adjusting the homogenizing speed to be 30-40rpm, carrying out vacuum homogenizing stirring for 5 minutes, starting cooling water after carrying out heat preservation and defoaming for 20 minutes, carrying out vacuum stirring for cooling, and properly adjusting the stirring speed during cooling so as to avoid exciting foams and influencing the appearance of the paste body;

sixthly, adding the D1 phase and the uniformly premixed D2 phase, D3 phase, E1 phase and E2 phase at the temperature of below 45 ℃, fully and uniformly stirring, adding the uniformly premixed D4 phase, uniformly stirring and mixing, discharging after detection at 38 ℃, and aseptically packaging to obtain the finished product.