CN110876811A - Water-soluble plant extract deodorant and preparation method thereof - Google Patents
Water-soluble plant extract deodorant and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
- A61L9/013—Deodorant compositions containing animal or plant extracts, or vegetable material
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/14—Disinfection, sterilisation or deodorisation of air using sprayed or atomised substances including air-liquid contact processes
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- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
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- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
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- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
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Abstract
The invention discloses a water-soluble plant extract deodorant, which is characterized by comprising the following components in parts by weight: comprises the following components in percentage by mass: 10-25% of plant extract composition, 3-8% of plant essential oil composition, 60-75% of surfactant composition, 0.5-2% of cosurfactant and 5-20% of deionized water. The preparation method of the water-soluble plant extract deodorant comprises the following steps: step 1): preparing a plant extract composition; step 2): preparing a plant essential oil composition; step 3): preparing a surfactant composition; step 4): adding the plant extract composition, the plant essential oil composition, the surfactant composition, the cosurfactant and the deionized water into a reaction kettle according to a proportion, mixing, and stirring to form a clear and transparent mixed solution to obtain the water-soluble plant extract deodorant. The process can effectively decompose various common malodorous gases in the malodorous environment, such as hydrogen sulfide, ammonia gas, sulfur dioxide, methyl mercaptan, amine and the like, and is suitable for industrial production.
Description
Technical Field
The invention relates to a water-soluble plant extract deodorant and a preparation method thereof.
Background
Along with the development and progress of social economy, the requirements of people on environmental awareness and quality of life are continuously improved, and the problems of malodorous gas control and treatment are more and more emphasized. Especially, the odor of the garbage landfill, the sewage treatment plant, the farm, the public toilet and the like seriously affects the environment. The chemical substances emitting foul odor to the environment are mainly divided into five types according to chemical compositions: sulfur-containing compounds such as hydrogen sulfide, mercaptans, thioethers, etc.; nitrogen-containing compounds such as ammonia, amines, amides, indoles, and the like; halogen and its derivatives such as chlorine, halogenated hydrocarbons; hydrocarbons such as alkanes, alkenes, and aromatics, etc.; oxygen-containing compounds such as alcohols, phenols, aldehydes, ketones, organic acids, and the like. At present, the deodorization methods widely adopted at home and abroad include a physical method, a chemical method, a microbiological method, a perfume masking method, a natural plant extract deodorization method and the like. The above methods have advantages and disadvantages, and thus, in actual deodorization requirements, it is often the combination of one or more deodorization methods to achieve the most satisfactory deodorization effect. The plant extract is an environment-friendly and natural odor remover, is obtained by extracting effective components from natural plants, can be completely degraded by organisms, is non-toxic, non-irritant and non-secondary-pollution, can convert malodorous substances into non-toxic substances, and has an action mechanism based on chemical reaction and biophysical processes. However, the main "deodorizing" mechanism of most plant extract deodorants on the market is still the masking effect of the perfume. The sterilization and disinfection effect is not very obvious, and the odor cannot be removed from the source.
Disclosure of Invention
The invention aims to solve the technical problem of providing a water-soluble plant extract deodorant and a preparation method thereof, which can effectively decompose various common malodorous gases such as hydrogen sulfide, ammonia gas, sulfur dioxide, methyl mercaptan, amine and the like in a malodorous environment.
In order to achieve the purpose, the invention adopts the following technical scheme:
the invention provides a water-soluble plant extract deodorant, which comprises the following components: comprises the following components in percentage by mass: 10-25% of plant extract composition, 3-8% of plant essential oil composition, 60-75% of surfactant composition, 0.5-2% of cosurfactant and 5-20% of deionized water.
As a further improvement of the invention: the plant extract composition is a filtrate obtained by mixing and crushing wormwood, chrysanthemum indicum, bamboo leaves and agilawood leaves, extracting with ethanol and carrying out vacuum filtration;
the fresh plant materials of the wormwood, the chrysanthemum indicum, the bamboo leaf and the agilawood leaf comprise, by weight, 5-10 parts of the wormwood, 1-10 parts of the chrysanthemum indicum, 1-10 parts of the bamboo leaf and 5-10 parts of the agilawood leaf.
As a further improvement of the invention: the plant essential oil composition comprises the following raw materials in parts by weight: 0.2-0.5 part of cedar wood oil, 0.2-0.8 part of turpentine, 0.2-0.5 part of eucalyptus oil, 0.1-0.3 part of geranium oil and 0.1-0.3 part of clove oil.
As a further improvement of the invention: the surfactant is a compound nonionic surfactant and is prepared from the following components in parts by weight: 45-50 parts of nonylphenol polyoxyethylene ether and 50-55 parts of octylphenol polyoxyethylene ether.
As a further improvement of the invention: the nonylphenol polyoxyethylene ether is selected from TX-9, and the octylphenol polyoxyethylene ether is selected from OP-13.
As a further improvement of the invention: the cosurfactant is one selected from propylene glycol and glycerol.
As a further improvement of the invention: the cosurfactant is propylene glycol.
The invention also provides a preparation method of the water-soluble plant extract deodorant, which is suitable for industrial production and has high effect: the method comprises the following steps:
step 1): the preparation of the plant extract composition comprises the steps of weighing wormwood, chrysanthemum indicum, bamboo leaves and agilawood leaves according to the parts by weight, mixing and crushing the wormwood, the chrysanthemum indicum, the bamboo leaves and the agilawood leaves, and mixing the wormwood, the chrysanthemum indicum, the bamboo leaves and the agilawood leaves according to a material-liquid ratio of 1: 10-1: adding 20 parts of the mixture into 40-80% ethanol in proportion, soaking for 24-48 hours, then carrying out vacuum filtration to obtain a first filtrate, repeatedly soaking the filter residue for 12-24 hours, carrying out vacuum filtration to obtain a second filtrate, fully mixing the first filtrate and the second filtrate, rectifying by using a rotary evaporator to recover the ethanol in the first filtrate, and thus obtaining the plant extract composition;
step 2): preparing the plant essential oil composition, namely weighing cedar wood oil, turpentine oil, eucalyptus oil, geranium oil and clove oil according to the parts by weight, and mixing and stirring the cedar wood oil, the turpentine oil, the eucalyptus oil, the geranium oil and the clove oil for 15-20 minutes to uniformly mix the cedar wood oil, the turpentine oil, the eucalyptus oil, the geranium oil and the clove oil to obtain the;
step 3): preparing a surfactant composition, namely weighing nonylphenol polyoxyethylene ether and octylphenol polyoxyethylene ether respectively according to parts by weight, and mixing and stirring the nonylphenol polyoxyethylene ether and the octylphenol polyoxyethylene ether uniformly to obtain the surfactant composition;
step 4): adding the plant extract composition, the plant essential oil composition, the surfactant composition, the cosurfactant and the deionized water into a reaction kettle according to a proportion, mixing, and stirring to form a clear and transparent mixed solution to obtain the water-soluble plant extract deodorant.
As a further improvement of the invention: in the step 4), the temperature is 50-70 ℃, preferably 55 ℃, and the rotation speed is 1200-3000r/min, preferably 2000r/min in the stirring treatment.
As a further improvement of the invention: in the step 4), the temperature is 55 ℃ and the rotating speed is 2000r/min in the stirring treatment.
Compared with the prior art, the water-soluble plant extract deodorant and the preparation method thereof have the following advantages:
1) the deodorant for the water-soluble plant extracts provided by the invention is rich in various bioactive components such as volatile oil, alkaloid, polysaccharide, amino acid, flavone, glycoside, phenols and the like, can be subjected to neutralization and condensation reaction with the lactosulfydryl, amino, aldehyde group, amino group and the like in odor substances, can convert pollutants in odor into harmless carbohydrates, and cannot cause any secondary pollution.
2) The deodorant is safe and convenient to use, and can be directly diluted by 50-1000 times of water according to the odor concentration, namely required by a use field, and then sprayed into mist through a nozzle or an atomizer to be sprayed into a pollution source or air to perform deodorization operation.
3) The water-soluble plant extract deodorant provided by the invention can be directly diluted with water for use, and can effectively decompose various common malodorous gases such as hydrogen sulfide, ammonia gas, sulfur dioxide, methyl mercaptan, amine and the like in a malodorous environment.
4) The water-soluble plant extract deodorant provided by the invention can be widely applied to places such as refuse landfills, sewage treatment plants, refuse transfer stations, refuse composting stations, livestock farms, refuse incineration plants, excrement treatment centers, municipal sewage treatment, public toilets and the like.
5) The active ingredients of the plant extract deodorant provided by the invention are all extracted from natural plants, so that the plant extract deodorant has no toxic or side effect on human bodies, does not stimulate the skin, has extremely low inhalation toxicity, and does not cause any secondary pollution.
6) The plant extract deodorant provided by the invention adopts a water-soluble formula, and the plant extract deodorant has stable chemical and physical properties, is biodegradable and is environment-friendly.
7) The plant extract deodorant provided by the invention is simple in preparation process, low in requirement on production equipment and capable of saving production cost.
Detailed Description
The water-soluble plant extract deodorant and the preparation method thereof provided by the present invention are further described in more detail by the following specific examples:
the invention relates to a water-soluble plant extract deodorant and a preparation method thereof, wherein the material-liquid ratio refers to the mass ratio, namely the mass ratio of raw materials to a soaking agent.
Test No.)
The water-soluble plant extract deodorant of the present invention comprises: comprises the following components in percentage by mass: 10-25% of plant extract composition, 3-8% of plant essential oil composition, 60-75% of surfactant composition, 0.5-2% of cosurfactant and 5-20% of deionized water.
The plant extract composition is a filtrate obtained by mixing and crushing wormwood, chrysanthemum indicum, bamboo leaves and agilawood leaves, extracting with ethanol and carrying out vacuum filtration;
the fresh plant materials of the wormwood, the chrysanthemum indicum, the bamboo leaf and the agilawood leaf comprise, by weight, 5-10 parts of the wormwood, 1-10 parts of the chrysanthemum indicum, 1-10 parts of the bamboo leaf and 5-10 parts of the agilawood leaf.
The plant essential oil composition comprises the following raw materials in parts by weight: 0.2-0.5 part of cedar wood oil, 0.2-0.8 part of turpentine, 0.2-0.5 part of eucalyptus oil, 0.1-0.3 part of geranium oil and 0.1-0.3 part of clove oil.
The surfactant is a compound nonionic surfactant and is prepared from the following components in parts by weight: 45-50 parts of nonylphenol polyoxyethylene ether and 50-55 parts of octylphenol polyoxyethylene ether.
The nonylphenol polyoxyethylene ether is selected from TX-9, and the octylphenol polyoxyethylene ether is selected from OP-13.
The cosurfactant is one selected from propylene glycol and glycerol.
The cosurfactant is propylene glycol.
The preparation method of the water-soluble plant extract deodorant comprises the following steps:
step 1: the preparation of the plant extract composition comprises the steps of weighing wormwood, chrysanthemum indicum, bamboo leaves and agilawood leaves according to the parts by weight, mixing and crushing the wormwood, the chrysanthemum indicum, the bamboo leaves and the agilawood leaves, and mixing the wormwood, the chrysanthemum indicum, the bamboo leaves and the agilawood leaves according to a material-liquid ratio of 1: 10-1: adding 40-80% ethanol at a ratio of 20, soaking for 24 hr, vacuum filtering to obtain first filtrate, soaking the residue for 24 hr, vacuum filtering to obtain second filtrate, mixing the first filtrate and the second filtrate, and recovering ethanol via rotary evaporator to obtain plant extract composition;
step 2: preparing a plant essential oil composition, namely weighing cedar wood oil, turpentine oil, eucalyptus oil, geranium oil and clove oil according to parts by weight, and mixing and stirring the cedar wood oil, the turpentine oil, the eucalyptus oil, the geranium oil and the clove oil uniformly to obtain the plant essential oil composition;
and step 3: preparing a surfactant composition, namely weighing nonylphenol polyoxyethylene ether and octylphenol polyoxyethylene ether respectively according to parts by weight, and mixing and stirring the nonylphenol polyoxyethylene ether and the octylphenol polyoxyethylene ether uniformly to obtain the surfactant composition;
and 4, step 4: adding the plant extract composition, the plant essential oil composition, the surfactant composition, the cosurfactant and the deionized water into a reaction kettle according to the proportion, mixing, and fully and uniformly stirring at the rotating speed of 3000r/min at 50-60 ℃, preferably at the rotating speed of 55 ℃, 2000r/min until clear and transparent mixed liquid is formed, thereby obtaining the water-soluble plant extract deodorant.
Changing the conditions of the cosurfactant and the dilution times of the product by adding water in the steps respectively, and observing the appearance effect of the product as shown in the following table 1:
TABLE 1 product appearance effect under different conditions
The test results show that the cosurfactant can reduce the interfacial tension, increase the fluidity and the flexibility of an interfacial film, facilitate the formation of micro-emulsion and enhance the stability of the emulsion, and the data in the table show that propylene glycol and glycerol are good cosurfactants for the plant deodorant of the invention.
Test II,
The water-soluble plant extract deodorant of the invention is tested, and the test result is compared with the deodorization effect of the deodorant in the prior art by changing the component conditions, so that the observation result is obtained: first group A
The water-soluble plant extract deodorant comprises the following raw materials in percentage by mass: 25% of plant extract composition, 3% of plant essential oil composition, 60% of surfactant composition, 0.5% of cosurfactant and 11.5% of deionized water.
The plant extraction composition is an extracting solution which is prepared by mixing and crushing 5 parts of wormwood, 5 parts of chrysanthemum indicum, 5 parts of bamboo leaves and 5 parts of agilawood leaves in proportion as extraction raw materials.
The plant essential oil composition comprises, by weight, 0.3 part of cedar wood oil, 0.5 part of turpentine, 0.3 part of eucalyptus oil, 0.2 part of geranium oil and 0.2 part of clove oil which are mixed together.
The surfactant is prepared by uniformly mixing 48 parts of nonylphenol polyoxyethylene ether and 52 parts of octylphenol polyoxyethylene ether.
The preparation method of the water-soluble plant extract deodorant comprises the following steps:
step 1: the preparation of the plant extract composition comprises the steps of weighing wormwood, chrysanthemum indicum, bamboo leaves and agilawood leaves according to the parts by weight, mixing and crushing the wormwood, the chrysanthemum indicum, the bamboo leaves and the agilawood leaves, and mixing the wormwood, the chrysanthemum indicum, the bamboo leaves and the agilawood leaves according to a material-liquid ratio of 1: adding 70% ethanol at a ratio of 20, soaking for 24 hr, vacuum filtering to obtain first filtrate, soaking the residue for 24 hr, vacuum filtering to obtain second filtrate, mixing the first filtrate and the second filtrate, and recovering ethanol by rotary evaporator to obtain the plant extract composition.
Step 2: preparing a plant essential oil composition, namely weighing cedar wood oil, turpentine oil, eucalyptus oil, geranium oil and clove oil according to parts by weight, and mixing and stirring the cedar wood oil, the turpentine oil, the eucalyptus oil, the geranium oil and the clove oil uniformly to obtain the plant essential oil composition;
and step 3: preparing the surfactant composition, namely weighing nonylphenol polyoxyethylene ether-9 and octylphenol polyoxyethylene ether-13 in parts by weight respectively, and mixing and stirring the weighed materials uniformly to obtain the surfactant composition.
And 4, step 4: adding the plant extract composition, the plant essential oil composition, the surfactant composition, the cosurfactant and the deionized water into a reaction kettle according to the proportion, mixing, and fully and uniformly stirring at 55 ℃ and 2000r/min until a clear and transparent mixed solution is formed, thereby obtaining the water-soluble plant extract deodorant.
Second group B
The water-soluble plant extract deodorant comprises the following raw materials in percentage by mass: 20% of plant extract composition, 5% of plant essential oil composition, 65% of surfactant composition, 1.5% of cosurfactant and 8.5% of deionized water.
The plant extraction composition is an extracting solution which is prepared by mixing and crushing 8 parts of wormwood, 8 parts of chrysanthemum indicum, 5 parts of bamboo leaves and 8 parts of agilawood leaves in proportion as an extraction raw material.
The plant essential oil composition is prepared by mixing 0.5 part of cedar wood oil, 0.5 part of turpentine, 0.5 part of eucalyptus oil, 0.2 part of geranium oil and 0.2 part of clove oil according to the weight part.
The surfactant is prepared by mixing 50 parts of nonylphenol polyoxyethylene ether and 50 parts of octylphenol polyoxyethylene ether.
The preparation method of the water-soluble plant extract deodorant comprises the following steps:
step 1: the preparation of the plant extract composition comprises the steps of weighing wormwood, chrysanthemum indicum, bamboo leaves and agilawood leaves according to the parts by weight, mixing and crushing the wormwood, the chrysanthemum indicum, the bamboo leaves and the agilawood leaves, and mixing the wormwood, the chrysanthemum indicum, the bamboo leaves and the agilawood leaves according to a material-liquid ratio of 1: adding 60% ethanol at a ratio of 15, soaking for 24 hr, vacuum filtering to obtain first filtrate, soaking the residue for 24 hr, vacuum filtering to obtain second filtrate, mixing the first filtrate and the second filtrate, and recovering ethanol by rotary evaporator to obtain the plant extract composition.
Step 2: preparing a plant essential oil composition, namely weighing cedar wood oil, turpentine oil, eucalyptus oil, geranium oil and clove oil according to parts by weight, and mixing and stirring the cedar wood oil, the turpentine oil, the eucalyptus oil, the geranium oil and the clove oil uniformly to obtain the plant essential oil composition;
and step 3: preparing the surfactant composition, namely weighing nonylphenol polyoxyethylene ether-9 and octylphenol polyoxyethylene ether-13 in parts by weight respectively, and mixing and stirring the weighed materials uniformly to obtain the surfactant composition.
And 4, step 4: adding the plant extract composition, the plant essential oil composition, the surfactant composition, the cosurfactant and the deionized water into a reaction kettle according to the proportion, mixing, and fully and uniformly stirring at the rotating speed of 2000r/min at the temperature of 60 ℃ until clear and transparent mixed liquid is formed, thereby obtaining the water-soluble plant extract deodorant.
Third group C
The water-soluble plant extract deodorant comprises the following raw materials in percentage by mass: 15% of plant extract composition, 6% of plant essential oil composition, 70% of surfactant composition, 2% of cosurfactant and 7% of deionized water.
The plant extraction composition is an extracting solution which is prepared by mixing and crushing 5 parts of wormwood, 10 parts of chrysanthemum indicum, 5 parts of bamboo leaves and 5 parts of agilawood leaves in proportion as extraction raw materials.
The plant essential oil composition is prepared by mixing 0.4 part of cedar wood oil, 0.5 part of turpentine, 0.4 part of eucalyptus oil, 0.3 part of geranium oil and 0.3 part of clove oil according to a proportion.
The surfactant is prepared by mixing 45 parts of nonylphenol polyoxyethylene ether and 55 parts of octylphenol polyoxyethylene ether.
The preparation method of the water-soluble plant extract deodorant comprises the following steps:
step 1: the preparation of the plant extract composition comprises the steps of weighing wormwood, chrysanthemum indicum, bamboo leaves and agilawood leaves according to the parts by weight, mixing and crushing the wormwood, the chrysanthemum indicum, the bamboo leaves and the agilawood leaves, and mixing the wormwood, the chrysanthemum indicum, the bamboo leaves and the agilawood leaves according to a material-liquid ratio of 1: adding ethanol with the concentration of 65% into the mixture according to the proportion of 20, soaking for 24 hours, then carrying out vacuum filtration to obtain a first filtrate, repeatedly soaking the filter residue for 24 hours, carrying out vacuum filtration to obtain a second filtrate, fully mixing the first filtrate and the second filtrate, and rectifying and recovering the ethanol in the first filtrate and the second filtrate by using a rotary evaporator to obtain the plant extract composition.
Step 2: preparing a plant essential oil composition, namely weighing cedar wood oil, turpentine oil, eucalyptus oil, geranium oil and clove oil according to parts by weight, and mixing and stirring the cedar wood oil, the turpentine oil, the eucalyptus oil, the geranium oil and the clove oil uniformly to obtain the plant essential oil composition;
and step 3: preparing the surfactant composition, namely weighing nonylphenol polyoxyethylene ether-9 and octylphenol polyoxyethylene ether-13 in parts by weight respectively, and mixing and stirring the weighed materials uniformly to obtain the surfactant composition.
And 4, step 4: adding the plant extract composition, the plant essential oil composition, the surfactant composition, the cosurfactant and the deionized water into a reaction kettle according to the proportion, mixing, and fully and uniformly stirring at the rotating speed of 2000r/min at the temperature of 60 ℃ until clear and transparent mixed liquid is formed, thereby obtaining the water-soluble plant extract deodorant.
Fourth group D
The water-soluble plant extract deodorant comprises the following raw materials in percentage by mass: 10% of plant extract composition, 8% of plant essential oil composition, 75% of surfactant composition, 2% of cosurfactant and 5% of deionized water.
The plant extraction composition is an extracting solution which is prepared by mixing and crushing 10 parts of wormwood, 10 parts of chrysanthemum indicum, 10 parts of bamboo leaves and 10 parts of agilawood leaves in proportion as extraction raw materials.
The plant essential oil composition is prepared by mixing 0.5 part of cedar wood oil, 0.5 part of turpentine, 0.5 part of eucalyptus oil, 0.2 part of geranium oil and 0.2 part of clove oil according to a proportion.
The surfactant is prepared by mixing 46 parts of nonylphenol polyoxyethylene ether and 54 parts of octylphenol polyoxyethylene ether.
The preparation method of the water-soluble plant extract deodorant comprises the following steps:
step 1: the preparation of the plant extract composition comprises the steps of weighing wormwood, chrysanthemum indicum, bamboo leaves and agilawood leaves according to the parts by weight, mixing and crushing the wormwood, the chrysanthemum indicum, the bamboo leaves and the agilawood leaves, and mixing the wormwood, the chrysanthemum indicum, the bamboo leaves and the agilawood leaves according to a material-liquid ratio of 1: adding ethanol with the concentration of 65% into the mixture according to the proportion of 20, soaking for 24 hours, then carrying out vacuum filtration to obtain a first filtrate, repeatedly soaking the filter residue for 24 hours, carrying out vacuum filtration to obtain a second filtrate, fully mixing the first filtrate and the second filtrate, and rectifying and recovering the ethanol in the first filtrate and the second filtrate by using a rotary evaporator to obtain the plant extract composition.
Step 2: preparing a plant essential oil composition, namely weighing cedar wood oil, turpentine oil, eucalyptus oil, geranium oil and clove oil according to parts by weight, and mixing and stirring the cedar wood oil, the turpentine oil, the eucalyptus oil, the geranium oil and the clove oil uniformly to obtain the plant essential oil composition;
and step 3: preparing the surfactant composition, namely weighing nonylphenol polyoxyethylene ether-9 and octylphenol polyoxyethylene ether-13 in parts by weight respectively, and mixing and stirring the weighed materials uniformly to obtain the surfactant composition.
And 4, step 4: adding the plant extract composition, the plant essential oil composition, the surfactant composition, the cosurfactant and the deionized water into a reaction kettle according to the proportion, mixing, and fully and uniformly stirring at the rotating speed of 2000r/min at the temperature of 60 ℃ until clear and transparent mixed liquid is formed, thereby obtaining the water-soluble plant extract deodorant.
Comparative example 1:
the other conditions were the same as in scheme B except that no plant essential oil composition was added.
Comparative example 2:
the other conditions were the same as in scheme D except that no plant extract composition was added.
Comparative example 3:
the plant deodorant is a plant deodorant produced by a certain company on the market.
Diluting the plant extract deodorizer prepared from the first group A, the second group B, the third group C and the fourth group D by 500 times with water, spraying the plant extract deodorizer on the surface of garbage by using spraying equipment, carrying out laboratory test according to the detection method of CJ/T516-2017 technical requirement for household garbage deodorizer, testing the deodorization effect, and simultaneously carrying out a comparative experiment by using the existing plant deodorizer, wherein the test results are as follows:
TABLE 2 comparison of Effect tests
Through the experiments, the plant extract deodorant disclosed by the invention has the advantage that the deodorization effect is remarkably improved compared with that of the existing deodorant.
Example 1
The water-soluble plant extract deodorant of the present embodiment includes: comprises the following components in percentage by mass: 16.5% of plant extract composition, 3% of plant essential oil composition, 60% of surfactant composition, 0.5% of cosurfactant and 20% of deionized water.
The plant extract composition is a filtrate obtained by mixing and crushing wormwood, chrysanthemum indicum, bamboo leaves and agilawood leaves, extracting with ethanol and carrying out vacuum filtration; the fresh plant materials of the wormwood, the chrysanthemum indicum, the bamboo leaf and the agilawood leaf comprise, by weight, 5 parts of the wormwood, 1 part of the chrysanthemum indicum, 1 part of the bamboo leaf and 5 parts of the agilawood leaf.
The plant essential oil composition comprises the following raw materials in parts by weight: 0.2 part of cedar wood oil, 0.2 part of turpentine, 0.2 part of eucalyptus oil, 0.1 part of geranium oil and 0.1 part of clove oil.
The surfactant is a compound nonionic surfactant and is prepared from the following components in parts by weight: 45 parts of nonylphenol polyoxyethylene ether and 50 parts of octylphenol polyoxyethylene ether.
The nonylphenol polyoxyethylene ether is selected from TX-9, and the octylphenol polyoxyethylene ether is selected from OP-13.
The cosurfactant is propylene glycol.
The preparation method of the water-soluble plant extract deodorant comprises the following steps: the method comprises the following steps:
step 1): the preparation of the plant extract composition comprises the steps of weighing wormwood, chrysanthemum indicum, bamboo leaves and agilawood leaves according to the parts by weight, mixing and crushing the wormwood, the chrysanthemum indicum, the bamboo leaves and the agilawood leaves, and mixing the wormwood, the chrysanthemum indicum, the bamboo leaves and the agilawood leaves according to a material-liquid ratio of 1: adding 10 percent of the mixture into 40 percent of ethanol, soaking for 24 hours, then carrying out vacuum filtration to obtain a first filtrate, repeatedly soaking the filter residue for 12 hours, carrying out vacuum filtration to obtain a second filtrate, fully mixing the first filtrate and the second filtrate, and rectifying and recovering the ethanol in the first filtrate and the second filtrate by using a rotary evaporator to obtain the plant extract composition;
step 2): preparing a plant essential oil composition, namely weighing cedar wood oil, turpentine oil, eucalyptus oil, geranium oil and clove oil according to parts by weight, mixing and stirring the cedar wood oil, the turpentine oil, the eucalyptus oil, the geranium oil and the clove oil for 15 minutes to uniformly mix the cedar wood oil, the turpentine oil, the eucalyptus oil, the geranium oil and the clove oil to obtain the plant essential;
step 3): preparing a surfactant composition, namely weighing nonylphenol polyoxyethylene ether and octylphenol polyoxyethylene ether respectively according to parts by weight, and mixing and stirring the nonylphenol polyoxyethylene ether and the octylphenol polyoxyethylene ether uniformly to obtain the surfactant composition;
step 4): adding the plant extract composition, the plant essential oil composition, the surfactant composition, the cosurfactant and the deionized water into a reaction kettle according to a proportion, mixing, and stirring to form a clear and transparent mixed solution to obtain the water-soluble plant extract deodorant.
In the step 4), the temperature is 50 ℃ and the rotating speed is 1200r/min in the stirring treatment.
After the water-soluble plant extract deodorant of the embodiment is diluted by 500 times by adding water, a deodorization rate test is carried out by a laboratory test method according to a detection method of CJ/T516-2017 technical requirement for household garbage deodorant, and test results show that removal rate data of hydrogen sulfide, ammonia, methyl mercaptan and methyl sulfide respectively reach 85.6%, 92.3%, 66.1% and 46.1%, which indicates that the plant extract deodorant has a remarkable removal effect on hydrogen sulfide, ammonia, methyl mercaptan and methyl sulfide.
Example 2
The water-soluble plant extract deodorant of the present embodiment includes: comprises the following components in percentage by mass: 25% of plant extract composition, 8% of plant essential oil composition, 60% of surfactant composition, 2% of cosurfactant and 5% of deionized water.
The plant extract composition is a filtrate obtained by mixing and crushing wormwood, chrysanthemum indicum, bamboo leaves and agilawood leaves, extracting with ethanol and carrying out vacuum filtration;
the fresh plant materials of the wormwood, the chrysanthemum indicum, the bamboo leaf and the agilawood leaf comprise, by weight, 10 parts of the wormwood, 10 parts of the chrysanthemum indicum, 10 parts of the bamboo leaf and 10 parts of the agilawood leaf.
The plant essential oil composition comprises the following raw materials in parts by weight: 0.2 part of cedar wood oil, 0.2 part of turpentine, 0.2 part of eucalyptus oil, 0.1 part of geranium oil and 0.1 part of clove oil.
The surfactant is a compound nonionic surfactant and is prepared from the following components in parts by weight: 50 parts of nonylphenol polyoxyethylene ether and 55 parts of octylphenol polyoxyethylene ether.
The nonylphenol polyoxyethylene ether is selected from TX-9, and the octylphenol polyoxyethylene ether is selected from OP-13.
The cosurfactant is propylene glycol.
The preparation method of the water-soluble plant extract deodorant comprises the following steps:
step 1): the preparation of the plant extract composition comprises the steps of weighing wormwood, chrysanthemum indicum, bamboo leaves and agilawood leaves according to the parts by weight, mixing and crushing the wormwood, the chrysanthemum indicum, the bamboo leaves and the agilawood leaves, and mixing the wormwood, the chrysanthemum indicum, the bamboo leaves and the agilawood leaves according to a material-liquid ratio of 1: adding the mixture into 80% ethanol in a proportion of 15, soaking for 48 hours, then carrying out vacuum filtration to obtain a first filtrate, repeatedly soaking the filter residue for 24 hours, carrying out vacuum filtration to obtain a second filtrate, fully mixing the first filtrate and the second filtrate, and rectifying and recovering the ethanol in the first filtrate and the second filtrate by using a rotary evaporator to obtain the plant extract composition;
step 2): preparing a plant essential oil composition, namely weighing cedar wood oil, turpentine oil, eucalyptus oil, geranium oil and clove oil according to parts by weight, mixing and stirring the cedar wood oil, the turpentine oil, the eucalyptus oil, the geranium oil and the clove oil for 20 minutes to uniformly mix the cedar wood oil, the turpentine oil, the eucalyptus oil, the geranium oil and the clove oil to obtain the plant essential;
step 3): preparing a surfactant composition, namely weighing nonylphenol polyoxyethylene ether and octylphenol polyoxyethylene ether respectively according to parts by weight, and mixing and stirring the nonylphenol polyoxyethylene ether and the octylphenol polyoxyethylene ether uniformly to obtain the surfactant composition;
step 4): adding the plant extract composition, the plant essential oil composition, the surfactant composition, the cosurfactant and the deionized water into a reaction kettle according to a proportion, mixing, and stirring to form a clear and transparent mixed solution to obtain the water-soluble plant extract deodorant.
In the step 4), the temperature is 55 ℃ and the rotating speed is 2000r/min in the stirring treatment.
After the water-soluble plant extract deodorant of the embodiment is diluted by 200 times by adding water, a deodorization rate test is carried out by a laboratory test method according to a detection method of CJ/T516-2017 technical requirement for household garbage deodorant, and test results show that removal rate data of hydrogen sulfide, ammonia, methyl mercaptan and methyl sulfide respectively reach 91.6%, 93.3%, 70.2% and 62.1%, which indicates that the plant extract deodorant has a remarkable removal effect on hydrogen sulfide, ammonia, methyl mercaptan and methyl sulfide.
Example 3
The water-soluble plant extract deodorant of the present embodiment includes: comprises the following components in percentage by mass: 13% of plant extract composition, 5% of plant essential oil composition, 61% of surfactant composition, 1% of cosurfactant and 20% of deionized water.
The plant extract composition is a filtrate obtained by mixing and crushing wormwood, chrysanthemum indicum, bamboo leaves and agilawood leaves, extracting with ethanol and carrying out vacuum filtration;
the fresh plant materials of the wormwood, the chrysanthemum indicum, the bamboo leaf and the agilawood leaf comprise, by weight, 7 parts of the wormwood, 3 parts of the chrysanthemum indicum, 4 parts of the bamboo leaf and 7 parts of the agilawood leaf.
The plant essential oil composition comprises the following raw materials in parts by weight: 0.3 part of cedar wood oil, 0.8 part of turpentine, 0.35 part of eucalyptus oil, 0.2 part of geranium oil and 0.2 part of clove oil.
The surfactant is a compound nonionic surfactant and is prepared from the following components in parts by weight: 47 parts of nonylphenol polyoxyethylene ether and 52 parts of octylphenol polyoxyethylene ether.
The nonylphenol polyoxyethylene ether is selected from TX-9, and the octylphenol polyoxyethylene ether is selected from OP-13.
The cosurfactant is propylene glycol.
The preparation method of the water-soluble plant extract deodorant comprises the following steps:
step 1): the preparation of the plant extract composition comprises the steps of weighing wormwood, chrysanthemum indicum, bamboo leaves and agilawood leaves according to the parts by weight, mixing and crushing the wormwood, the chrysanthemum indicum, the bamboo leaves and the agilawood leaves, and mixing the wormwood, the chrysanthemum indicum, the bamboo leaves and the agilawood leaves according to a material-liquid ratio of 1: adding 17 parts of the mixture into 40-80% ethanol in proportion, soaking for 24 hours, then carrying out vacuum filtration to obtain a first filtrate, repeatedly soaking the filter residue for 12 hours, carrying out vacuum filtration to obtain a second filtrate, fully mixing the first filtrate and the second filtrate, and rectifying by using a rotary evaporator to recover the ethanol in the first filtrate to obtain the plant extract composition;
step 2): preparing a plant essential oil composition, namely weighing cedar wood oil, turpentine oil, eucalyptus oil, geranium oil and clove oil according to parts by weight, mixing and stirring the cedar wood oil, the turpentine oil, the eucalyptus oil, the geranium oil and the clove oil for 20 minutes to uniformly mix the cedar wood oil, the turpentine oil, the eucalyptus oil, the geranium oil and the clove oil to obtain the plant essential;
step 3): preparing a surfactant composition, namely weighing nonylphenol polyoxyethylene ether and octylphenol polyoxyethylene ether respectively according to parts by weight, and mixing and stirring the nonylphenol polyoxyethylene ether and the octylphenol polyoxyethylene ether uniformly to obtain the surfactant composition;
step 4): adding the plant extract composition, the plant essential oil composition, the surfactant composition, the cosurfactant and the deionized water into a reaction kettle according to a proportion, mixing, and stirring to form a clear and transparent mixed solution to obtain the water-soluble plant extract deodorant.
In the step 4), the temperature is 55 ℃ and the rotating speed is 2000r/min in the stirring treatment.
After the water-soluble plant extract deodorant of the embodiment is diluted by 500 times by adding water, a deodorization rate test is carried out by a laboratory test method according to a detection method of CJ/T516-2017 technical requirement for household garbage deodorant, and test results show that removal rate data of hydrogen sulfide, ammonia, methyl mercaptan and methyl sulfide respectively reach 90.6%, 91.7%, 61.2% and 45.1%, which indicates that the plant extract deodorant has a remarkable removal effect on hydrogen sulfide, ammonia, methyl mercaptan and methyl sulfide.
Example 4
The water-soluble plant extract deodorant of the present embodiment includes: comprises the following components in percentage by mass: 12% of plant extract composition, 3% of plant essential oil composition, 75% of surfactant composition, 2% of cosurfactant and 8% of deionized water.
The plant extract composition is a filtrate obtained by mixing and crushing wormwood, chrysanthemum indicum, bamboo leaves and agilawood leaves, extracting with ethanol and carrying out vacuum filtration;
the fresh plant materials of the wormwood, the chrysanthemum indicum, the bamboo leaf and the agilawood leaf comprise, by weight, 7 parts of the wormwood, 8 parts of the chrysanthemum indicum, 3 parts of the bamboo leaf and 6 parts of the agilawood leaf.
The plant essential oil composition comprises the following raw materials in parts by weight: 0.25 part of cedar wood oil, 0.6 part of turpentine, 0.3 part of eucalyptus oil, 0.23 part of geranium oil and 0.22 part of clove oil.
The surfactant is a compound nonionic surfactant and is prepared from the following components in parts by weight: 45-50 parts of nonylphenol polyoxyethylene ether and 50-55 parts of octylphenol polyoxyethylene ether.
The nonylphenol polyoxyethylene ether is selected from TX-9, and the octylphenol polyoxyethylene ether is selected from OP-13.
The cosurfactant is propylene glycol.
The preparation method of the water-soluble plant extract deodorant comprises the following steps: the method comprises the following steps:
step 1): the preparation of the plant extract composition comprises the steps of weighing wormwood, chrysanthemum indicum, bamboo leaves and agilawood leaves according to the parts by weight, mixing and crushing the wormwood, the chrysanthemum indicum, the bamboo leaves and the agilawood leaves, and mixing the wormwood, the chrysanthemum indicum, the bamboo leaves and the agilawood leaves according to a material-liquid ratio of 1: adding 20 parts of the mixture into 60% ethanol at a ratio, soaking for 30 hours, then carrying out vacuum filtration to obtain a first filtrate, repeatedly soaking the filter residue for 15 hours, carrying out vacuum filtration to obtain a second filtrate, fully mixing the first filtrate and the second filtrate, and rectifying and recovering ethanol in the first filtrate and the second filtrate by using a rotary evaporator to obtain a plant extract composition;
step 2): preparing a plant essential oil composition, namely weighing cedar wood oil, turpentine oil, eucalyptus oil, geranium oil and clove oil according to parts by weight, mixing and stirring the cedar wood oil, the turpentine oil, the eucalyptus oil, the geranium oil and the clove oil for 18 minutes to uniformly mix the cedar wood oil, the turpentine oil, the eucalyptus oil, the geranium oil and the clove oil to obtain the plant essential;
step 3): preparing a surfactant composition, namely weighing nonylphenol polyoxyethylene ether and octylphenol polyoxyethylene ether respectively according to parts by weight, and mixing and stirring the nonylphenol polyoxyethylene ether and the octylphenol polyoxyethylene ether uniformly to obtain the surfactant composition;
step 4): adding the plant extract composition, the plant essential oil composition, the surfactant composition, the cosurfactant and the deionized water into a reaction kettle according to a proportion, mixing, and stirring to form a clear and transparent mixed solution to obtain the water-soluble plant extract deodorant.
In the step 4), the temperature is 60 ℃ and the rotating speed is 25000r/min in the stirring treatment.
After the water-soluble plant extract deodorant of the embodiment is diluted by 500 times by adding water, a deodorization rate test is carried out by a laboratory test method according to a detection method of CJ/T516-2017 technical requirement for household garbage deodorant, and test results show that removal rate data of hydrogen sulfide, ammonia, methyl mercaptan and methyl sulfide respectively reach 90.6%, 89.3%, 65.2% and 46.3%, which indicates that the plant extract deodorant has a remarkable removal effect on hydrogen sulfide, ammonia, methyl mercaptan and methyl sulfide.
Example 5
The water-soluble plant extract deodorant of the present embodiment includes: comprises the following components in percentage by mass: 22% of plant extract composition, 6% of plant essential oil composition, 62% of surfactant composition, 1% of cosurfactant and 9% of deionized water.
The plant extract composition is a filtrate obtained by mixing and crushing wormwood, chrysanthemum indicum, bamboo leaves and agilawood leaves, extracting with ethanol and carrying out vacuum filtration;
the fresh plant materials of the wormwood, the chrysanthemum indicum, the bamboo leaf and the agilawood leaf comprise, by weight, 8 parts of the wormwood, 2 parts of the chrysanthemum indicum, 2 parts of the bamboo leaf and 7 parts of the agilawood leaf.
The plant essential oil composition comprises the following raw materials in parts by weight: 0.35 parts of cedar wood oil, 0.25 parts of turpentine, 0.4 parts of eucalyptus oil, 0.25 parts of geranium oil and 0.2 parts of clove oil.
The surfactant is a compound nonionic surfactant and is prepared from the following components in parts by weight: 48 parts of nonylphenol polyoxyethylene ether and 51 parts of octylphenol polyoxyethylene ether.
The nonylphenol polyoxyethylene ether is selected from TX-9, and the octylphenol polyoxyethylene ether is selected from OP-13.
The cosurfactant is glycerol.
The preparation method of the water-soluble plant extract deodorant comprises the following steps: the method comprises the following steps:
step 1): the preparation of the plant extract composition comprises the steps of weighing wormwood, chrysanthemum indicum, bamboo leaves and agilawood leaves according to the parts by weight, mixing and crushing the wormwood, the chrysanthemum indicum, the bamboo leaves and the agilawood leaves, and mixing the wormwood, the chrysanthemum indicum, the bamboo leaves and the agilawood leaves according to a material-liquid ratio of 1: adding 16 parts of the mixture into 60% ethanol at a ratio, soaking for 30 hours, then carrying out vacuum filtration to obtain a first filtrate, repeatedly soaking the filter residue for 20 hours, carrying out vacuum filtration to obtain a second filtrate, fully mixing the first filtrate and the second filtrate, and rectifying and recovering ethanol in the first filtrate and the second filtrate by using a rotary evaporator to obtain a plant extract composition;
step 2): preparing a plant essential oil composition, namely weighing cedar wood oil, turpentine oil, eucalyptus oil, geranium oil and clove oil according to parts by weight, mixing and stirring the cedar wood oil, the turpentine oil, the eucalyptus oil, the geranium oil and the clove oil for 18 minutes to uniformly mix the cedar wood oil, the turpentine oil, the eucalyptus oil, the geranium oil and the clove oil to obtain the plant essential;
step 3): preparing a surfactant composition, namely weighing nonylphenol polyoxyethylene ether and octylphenol polyoxyethylene ether respectively according to parts by weight, and mixing and stirring the nonylphenol polyoxyethylene ether and the octylphenol polyoxyethylene ether uniformly to obtain the surfactant composition;
step 4): adding the plant extract composition, the plant essential oil composition, the surfactant composition, the cosurfactant and the deionized water into a reaction kettle according to a proportion, mixing, and stirring to form a clear and transparent mixed solution to obtain the water-soluble plant extract deodorant.
In the step 4), the temperature is 60 ℃ and the rotating speed is 1500r/min in the stirring treatment.
After the water-soluble plant extract deodorant of the embodiment is diluted by 1000 times by adding water, a deodorization rate test is carried out by a laboratory test method according to a detection method of CJ/T516-2017 technical requirement for household garbage deodorant, and test results show that removal rate data of hydrogen sulfide, ammonia, methyl mercaptan and methyl sulfide respectively reach 90.6%, 89.3%, 65.2% and 45.5%, which indicates that the plant extract deodorant has a remarkable removal effect on hydrogen sulfide, ammonia, methyl mercaptan and methyl sulfide.
It should be understood that these examples are for illustrative purposes only and are not intended to limit the scope of the present invention. Further, it should also be understood that various alterations, modifications and/or variations can be made to the present invention by those skilled in the art after reading the technical content of the present invention, and all such equivalents fall within the protective scope defined by the claims of the present application.
It will be appreciated by those skilled in the art that the invention may be embodied in other specific forms without departing from the spirit or essential characteristics thereof. The embodiments disclosed above are therefore to be considered in all respects as illustrative and not restrictive. All changes which come within the scope of or equivalence to the invention are intended to be embraced therein.
Claims (10)
1. A water-soluble plant extract deodorant characterized by comprising: comprises the following components in percentage by mass: 10-25% of plant extract composition, 3-8% of plant essential oil composition, 60-75% of surfactant composition, 0.5-2% of cosurfactant and 5-20% of deionized water.
2. The water-soluble plant extract deodorant according to claim 1, wherein: the plant extract composition is a filtrate obtained by mixing and crushing wormwood, chrysanthemum indicum, bamboo leaves and agilawood leaves, extracting with ethanol and carrying out vacuum filtration;
the fresh plant materials of the wormwood, the chrysanthemum indicum, the bamboo leaf and the agilawood leaf comprise, by weight, 5-10 parts of the wormwood, 1-10 parts of the chrysanthemum indicum, 1-10 parts of the bamboo leaf and 5-10 parts of the agilawood leaf.
3. The water-soluble plant extract deodorant according to claim 1, wherein: the plant essential oil composition comprises the following raw materials in parts by weight: 0.2-0.5 part of cedar wood oil, 0.2-0.8 part of turpentine, 0.2-0.5 part of eucalyptus oil, 0.1-0.3 part of geranium oil and 0.1-0.3 part of clove oil.
4. The water-soluble plant extract deodorant according to claim 1, wherein: the surfactant is a compound nonionic surfactant and is prepared from the following components in parts by weight: 45-50 parts of nonylphenol polyoxyethylene ether and 50-55 parts of octylphenol polyoxyethylene ether.
5. The water-soluble plant extract deodorant according to claim 4, wherein: the nonylphenol polyoxyethylene ether is selected from TX-9, and the octylphenol polyoxyethylene ether is selected from OP-13.
6. The water-soluble plant extract deodorant according to claim 1, wherein: the cosurfactant is one selected from propylene glycol and glycerol.
7. The water-soluble plant extract deodorant according to claim 6, wherein: the cosurfactant is propylene glycol.
8. A method for producing a water-soluble plant extract deodorant as claimed in any one of claims 1 to 7, characterized in that: the method comprises the following steps:
step 1): the preparation of the plant extract composition comprises the steps of weighing wormwood, chrysanthemum indicum, bamboo leaves and agilawood leaves according to the parts by weight, mixing and crushing the wormwood, the chrysanthemum indicum, the bamboo leaves and the agilawood leaves, and mixing the wormwood, the chrysanthemum indicum, the bamboo leaves and the agilawood leaves according to a material-liquid ratio of 1: 10-1: adding 20 parts of the mixture into 40-80% ethanol in proportion, soaking for 24-48 hours, then carrying out vacuum filtration to obtain a first filtrate, repeatedly soaking the filter residue for 12-24 hours, carrying out vacuum filtration to obtain a second filtrate, fully mixing the first filtrate and the second filtrate, rectifying by using a rotary evaporator to recover the ethanol in the first filtrate, and thus obtaining the plant extract composition;
step 2): preparing the plant essential oil composition, namely weighing cedar wood oil, turpentine oil, eucalyptus oil, geranium oil and clove oil according to the parts by weight, and mixing and stirring the cedar wood oil, the turpentine oil, the eucalyptus oil, the geranium oil and the clove oil for 15-20 minutes to uniformly mix the cedar wood oil, the turpentine oil, the eucalyptus oil, the geranium oil and the clove oil to obtain the;
step 3): preparing a surfactant composition, namely weighing nonylphenol polyoxyethylene ether and octylphenol polyoxyethylene ether respectively according to parts by weight, and mixing and stirring the nonylphenol polyoxyethylene ether and the octylphenol polyoxyethylene ether uniformly to obtain the surfactant composition;
step 4): adding the plant extract composition, the plant essential oil composition, the surfactant composition, the cosurfactant and the deionized water into a reaction kettle according to a proportion, mixing, and stirring to form a clear and transparent mixed solution to obtain the water-soluble plant extract deodorant.
9. The method for producing a water-soluble plant extract deodorant according to claim 8, characterized in that: in the step 4), the temperature is 50-70 ℃, preferably 55 ℃, and the rotation speed is 1200-3000r/min, preferably 2000r/min in the stirring treatment.
10. The method for producing a water-soluble plant extract deodorant according to claim 9, characterized in that: in the step 4), the temperature is 55 ℃ and the rotating speed is 2000r/min in the stirring treatment.
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Citations (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101366962A (en) * | 2008-09-27 | 2009-02-18 | 上海维翰环保工程有限公司 | Composition for purifying air, preparation and uses thereof |
| CN101947327A (en) * | 2010-08-30 | 2011-01-19 | 江门市和馨香精技术有限公司 | Deodorant |
| CN104307019A (en) * | 2014-10-30 | 2015-01-28 | 上海今拓环保设备工程有限公司 | Plant extract deodorizer for removing harmful gases |
| CN104524950A (en) * | 2015-01-09 | 2015-04-22 | 中节能六合天融环保科技有限公司 | Plant type deodorant for refuse landfill |
| CN105561365A (en) * | 2016-02-24 | 2016-05-11 | 荆门市凡创环境工程有限公司 | Plant-type deodorant liquid for municipal refuse transfer station and preparation method thereof |
| CN106310906A (en) * | 2016-08-31 | 2017-01-11 | 北京市理化分析测试中心 | Indoor air deodorant having sterilizing function and preparation method thereof |
| CN108465121A (en) * | 2018-06-30 | 2018-08-31 | 上海澳克林新材料科技有限公司 | A kind of plant essence extracting solution eliminating smell agent and preparation method thereof |
| CN108938558A (en) * | 2018-06-25 | 2018-12-07 | 宁波立华制药有限公司 | A kind of nano-emulsion compound and preparation method and application |
| CN109673669A (en) * | 2019-01-25 | 2019-04-26 | 太原市诚诚科技有限公司 | A kind of preparation method and applications of nanometer of micro emulsion iodine |
| CN109865423A (en) * | 2019-04-23 | 2019-06-11 | 惠州市铭铠防霉抗菌科技有限公司 | One Plant Extracts and the compound deodorizer of biological enzyme and preparation method thereof |
| CN110215532A (en) * | 2018-03-01 | 2019-09-10 | 上海交通大学 | A kind of plants essential oil water solvent combinations object and preparation method thereof |
| CN110506764A (en) * | 2019-09-29 | 2019-11-29 | 青岛动保国家工程技术研究中心有限公司 | A kind of farm disinfecting, deodorizing nanoemulsion and preparation method and application |
-
2019
- 2019-12-03 CN CN201911218790.XA patent/CN110876811A/en active Pending
Patent Citations (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101366962A (en) * | 2008-09-27 | 2009-02-18 | 上海维翰环保工程有限公司 | Composition for purifying air, preparation and uses thereof |
| CN101947327A (en) * | 2010-08-30 | 2011-01-19 | 江门市和馨香精技术有限公司 | Deodorant |
| CN104307019A (en) * | 2014-10-30 | 2015-01-28 | 上海今拓环保设备工程有限公司 | Plant extract deodorizer for removing harmful gases |
| CN104524950A (en) * | 2015-01-09 | 2015-04-22 | 中节能六合天融环保科技有限公司 | Plant type deodorant for refuse landfill |
| CN105561365A (en) * | 2016-02-24 | 2016-05-11 | 荆门市凡创环境工程有限公司 | Plant-type deodorant liquid for municipal refuse transfer station and preparation method thereof |
| CN106310906A (en) * | 2016-08-31 | 2017-01-11 | 北京市理化分析测试中心 | Indoor air deodorant having sterilizing function and preparation method thereof |
| CN110215532A (en) * | 2018-03-01 | 2019-09-10 | 上海交通大学 | A kind of plants essential oil water solvent combinations object and preparation method thereof |
| CN108938558A (en) * | 2018-06-25 | 2018-12-07 | 宁波立华制药有限公司 | A kind of nano-emulsion compound and preparation method and application |
| CN108465121A (en) * | 2018-06-30 | 2018-08-31 | 上海澳克林新材料科技有限公司 | A kind of plant essence extracting solution eliminating smell agent and preparation method thereof |
| CN109673669A (en) * | 2019-01-25 | 2019-04-26 | 太原市诚诚科技有限公司 | A kind of preparation method and applications of nanometer of micro emulsion iodine |
| CN109865423A (en) * | 2019-04-23 | 2019-06-11 | 惠州市铭铠防霉抗菌科技有限公司 | One Plant Extracts and the compound deodorizer of biological enzyme and preparation method thereof |
| CN110506764A (en) * | 2019-09-29 | 2019-11-29 | 青岛动保国家工程技术研究中心有限公司 | A kind of farm disinfecting, deodorizing nanoemulsion and preparation method and application |
Non-Patent Citations (3)
| Title |
|---|
| 刘操: "《直排污水应急处理技术手册》", 30 April 2015 * |
| 车如心: "《界面与胶体化学》", 31 August 2012 * |
| 高桥素子: "《科学问答166》", 30 April 2008 * |
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| CN111888512A (en) * | 2020-06-18 | 2020-11-06 | 四川盟达谊家环保科技有限公司 | Efficient environment-friendly deodorant and preparation method thereof |
| CN112138528A (en) * | 2020-09-04 | 2020-12-29 | 杭州纳源环境科技有限公司 | Deodorant and preparation method thereof |
| CN112293430A (en) * | 2020-10-19 | 2021-02-02 | 郑州绿城生物技术有限公司 | Composition for removing ammonia and/or sulfur-containing compounds, method for producing same, and use thereof |
| CN113025439A (en) * | 2021-03-02 | 2021-06-25 | 袁锋 | Splash-proof deodorizing foam liquid for flush toilet |
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Application publication date: 20200313 |