CN114345110A

CN114345110A - Plant type efficient environment-friendly deodorant and preparation method thereof

Info

Publication number: CN114345110A
Application number: CN202210060200.0A
Authority: CN
Inventors: 吕林翰; 常兰; 熊进
Original assignee: Sichuan Kunjing Biotechnology Co ltd; Engineering and Technical College of Chengdu University of Technology
Current assignee: Sichuan Kunjing Biotechnology Co ltd; Engineering and Technical College of Chengdu University of Technology
Priority date: 2022-01-19
Filing date: 2022-01-19
Publication date: 2022-04-15

Abstract

The invention relates to the technical field of air purification, in particular to a plant type efficient environment-friendly deodorant and a preparation method thereof. The plant type efficient environment-friendly deodorant comprises a culture substrate and also comprises the following components in percentage by mass: 10% -15% of chamomile, 2% -6% of spanishneedles, 32% -43% of dandelion, 21% -25% of low-grain bamboo and 19% -21% of cocoa bark extract; the culture substrate is filled with purified water at 37-41.5 ℃. The invention solves the problems that the deodorant in the prior art is easy to generate secondary pollution gas after deodorization and has poor deodorization effect.

Description

Plant type efficient environment-friendly deodorant and preparation method thereof

Technical Field

The invention relates to the technical field of air purification, and relates to a plant type efficient environment-friendly deodorant and a preparation method thereof.

Background

The deodorant is a liquid drop type solution which is atomized by a deodorization device to form a mist shape and is diffused in a space, the surface of the solution can effectively absorb peculiar smell molecules in the air, the spatial configuration of the absorbed peculiar smell molecules can be changed, chemical bonds in the peculiar smell molecules are weakened, the instability of the peculiar smell molecules is increased, the peculiar smell molecules can easily perform chemical reaction with other molecules and an acid buffer solution in plant liquid, and finally, a tasteless and nontoxic substance is generated.

The natural plant extract deodorant in the prior art is a deodorant prepared by adopting a plant extraction technology and can be used for treating peculiar smells in various environments, but the prior art generally adopts a wide deodorization method for production, certain specific deodorization operation cannot be carried out necessarily, and meanwhile, after the deodorization operation is carried out on the deodorant, secondary pollution is easy to generate, so that although gas odor is removed, newly generated toxic gas can again influence the health of people in the nearby environment, meanwhile, the deodorization effect is poor, and a large amount of spray reagent is needed for elimination.

Disclosure of Invention

The invention aims to provide a plant type efficient environment-friendly deodorant and a preparation method thereof, and solves the problems that secondary pollution gas is easily generated after deodorization of the deodorant in the prior art and the deodorization effect is poor.

The purpose of the invention is realized by the following technical scheme, which comprises a culture substrate and also comprises the following components in percentage by mass: 10% -15% of chamomile, 2% -6% of spanishneedles, 32% -43% of dandelion, 21% -25% of low-grain bamboo and 19% -21% of cocoa bark extract; the culture substrate is filled with purified water at 37-41.5 ℃.

It should be noted that, in the above components of the present application, mikania micrantha, sticktight, dandelion and low-striped bamboo are all components obtained after the applicant has tried many different components, wherein, in the prior art, horsetail, pearl grass and bio-enzyme are generally adopted for carrying out, meanwhile, the prepared and extracted herbal plant extract is generally directly selected for use, and due to the limitation of pre-preparation in the process, when the extract reacts with bio-enzyme and the like, the deodorization effect caused by unstable mass fraction can occur, meanwhile, due to the addition of bio-enzyme, a relatively continuous reaction can be necessarily carried out, in the process, the plant extract can be dissolved with gas and the like generated by the reaction, and after the dissolution, harmful gas can be inevitably generated in later use, which affects human bodies in the environment and is harmful to health, and the components and culture medium adopted in the present application can maximally ensure the decomposition and dissolution of the harmful gas, meanwhile, the safety of the original components is improved, and the elimination of methyl mercaptan in odor is further improved.

Also comprises 3-5 parts of mushroom by mass, wherein the mushroom is blocky.

The applicant finds in practical experiments that the volume of the mushroom is easy to ignore, the whole addition is usually carried out in the prior art, although the overall effect of the mushroom can be ensured, the activity of the inner molecules of the mushroom is slowed down, and when the mushroom is mixed with a solution, the activation energy of the mushroom can be directly influenced, so that the effect of the deodorant ingredient is reduced.

In another aspect of the present application, a method for preparing a plant-type efficient and environmentally friendly deodorant, based on the deodorant of any one of claims 1-2, comprises the steps of:

step 1, sequentially adding chamomile, bidens, dandelion and low-striped bamboo into a culture substrate, standing for 12-15 min, fishing for water control for 2 min;

step 2, mixing the components obtained in the step 1 after water control, adding the mixture into a culture cavity, and simultaneously pouring 50% of ethanol by mass fraction for soaking;

step 3, heating the soaked components at the temperature of 30-35 ℃ for 6-6.5 min, and standing for 2-3 s;

step 4, standing, heating at 50-52 ℃ again, and standing for 2.5 s;

step 5, after standing, adding KOH solution according to the proportion of 1:2.5, and then immediately adding the mixture into a water bath at 37 ℃ for soaking for 10min-15 min;

step 6, adding mushrooms and 80-85% of acetone solution by mass after soaking, wherein the adding amount of the mushrooms and the acetone is 1:0.5, and further heating the mixed solution at the temperature of 6-8.5 ℃ for 3 hours;

step 7, carrying out fumigation treatment, carrying out condensation treatment after fumigation, and collecting after condensation treatment;

and 8, circulating the steps 1 to 7 until the circulation is finished.

It should be noted that, the above-mentioned steps are different from the prior art, step reaction has been carried out, there are more detailed ingredient that has carried out ration and definite ratio in step reaction and the settlement of experiment preparation parameter, simultaneously before the preparation is finished, add fumigation treatment, can carry out the purification of macromolecule in the deodorant, when guaranteeing the deodorant operation, can better carry out parcel dissolving process, than the simple macromolecule of prior art swallows the micromolecule, it is higher deodorization effect to carry out the settlement absorption after increasing the mass fraction.

The step 1 specifically comprises the following steps: the mikania micrantha, the spanishneedles herb, the dandelion and the low-grain bamboo are added according to the proportion of 2:3:2.5: 4.

The applicant of the above ratio has found the above ratio after a long time of experiments, and the addition of the components in the prior art does not have a certain standard, and the extract is generally used as it is, so the deodorization effect is not greatly deviated, and the main problem is the addition of the ratio, and the present application refines the addition of the ratio to obtain a high treatment effect.

The step 2 specifically comprises the following steps: the soaking duration is 35min-44min, wherein intermittent stirring is required in the soaking process, and the intermittent interval duration is 8min-9.5 min.

It should be noted that, in the prior art, no stirring treatment is performed during the soaking process, and the skilled person usually performs continuous soaking during the relevant treatment, but the applicant of the present application found in practical studies that intermittent stirring during the soaking process can help the reaction to proceed, so that the reaction is more uniform.

In the step 7, the duration of the fumigation treatment is 15-25 min, and the duration of the condensation is 1-1.5 h.

The application applies the fumigation treatment on the preparation of the deodorant, gives full play to and utilizes the principle that substances which can directly purify molecules to the maximum extent in the fumigation process, and ensures the purity of the components.

Compared with the prior art, the invention has the following advantages and beneficial effects:

1. the components and the culture medium adopted in the application can ensure the decomposition and dissolution of harmful gas to the maximum extent, and simultaneously improve the safety of the preparation of the original components, thereby improving the elimination of methyl mercaptan in odor;

2. the steps are different from the prior art, step-by-step reaction is carried out, the addition of components with quantitative and definite ratios and the setting of experimental preparation parameters are carried out in the step-by-step reaction, meanwhile, fumigation treatment is added before the preparation is finished, the purification of macromolecules in the deodorant can be carried out, the coating and dissolving treatment can be better carried out when the deodorant is ensured to operate, and compared with the simple processes of swallowing the macromolecules and micromolecules in the prior art, the deodorant has higher deodorization effect by settling and adsorbing after the mass fraction is increased;

3. the fumigation treatment is generally used for traditional Chinese medicines, the application enables the fumigation treatment to act on the prepared deodorant, gives full play to the basic principle that substances with direct molecules can be purified to the greatest extent in the fumigation process, and ensures the purity of components.

Drawings

FIG. 1 is a flow chart of the preparation of the present invention.

Detailed Description

Referring to the accompanying drawing 1, the embodiment provides a plant type efficient environment-friendly deodorant and a preparation method thereof, and the plant type efficient environment-friendly deodorant and the preparation method thereof are mainly used for solving the problems that after deodorization, a deodorant in the prior art is easy to generate secondary pollution gas and has poor deodorization effect, and the plant type efficient environment-friendly deodorant and the preparation method thereof are already in practical experimental use.

The implementation mode of the application is that the culture substrate comprises a culture substrate and also comprises the following components in percentage by mass: 10% -15% of chamomile, 2% -6% of spanishneedles, 32% -43% of dandelion, 21% -25% of low-grain bamboo and 19% -21% of cocoa bark extract; the culture substrate is filled with purified water at 37-41.5 ℃, and also comprises 3-5 parts of mushroom by mass, wherein the mushroom is in a block shape.

The deodorant provided by the application is prepared by adopting plant extracts, and the components in the plants realize the neutralization and fusion reaction with odor, chlorogenic acid and other acid components contained in mikania micrantha, coumaric acid, sitosterol and the like contained in sticktight, dandelion contains caffeic acid, chlorogenic acid and the like, oleanolic acid, isophytol, palmitic acid, benzoic acid, trans-para-hydroxycinnamic acid and the like contained in phyllostachys pubescens can realize the neutralization reaction with the components in the odor, and the absorption and removal of harmful substances such as methyl mercaptan and the like in the odor can be realized. Simultaneously, extract the composition that obtains from the plant, even after it carries out chemical reaction, can not produce secondary pollution and can also effectual recovery simultaneously and by the reutilization good, this application is effectively solving among the prior art that methyl mercaptan gets rid of the not good effect simultaneously, can also solve among the prior art the serious extravagant problem of product resource. On the other hand, the mushroom also contains components such as nicotinic acid, acetimidase, folic acid and the like, so that the active ingredients in the mushroom body are not weakened, the mushroom is extracted by using blocks, and meanwhile, the mushroom has more acid components, and the deodorization effect can be better realized.

Embodiments of another aspect of the present application are:

example 1

A preparation method of a plant type high-efficiency environment-friendly deodorant comprises the following steps: step 1, sequentially adding chamomile, bidens, dandelion and low-striped bamboo into a culture substrate, standing for 12min, fishing for water control for 2 min; step 2, mixing the components obtained in the step 1 after water control, adding the mixture into a culture cavity, and simultaneously pouring 50% of ethanol by mass fraction for soaking; step 3, heating the soaked components in an environment of 30 ℃ for 6min, and standing for 2 s; step 4, standing, heating at 50 ℃ again, and standing for 2.5 s; step 5, after standing, adding KOH solution according to the proportion of 1:2.5, and then immediately adding the mixture into a water bath at 37 ℃ for soaking for 10 min; step 6, adding mushrooms and an acetone solution with the mass fraction of 80% after soaking, wherein the adding amount of the mushrooms and the acetone is 1:0.5, and further heating the mixed solution at the heating temperature of 6 ℃ for 3 hours; step 7, carrying out fumigation treatment, carrying out condensation treatment after fumigation, and collecting after condensation treatment; and 8, circulating the steps 1 to 7 until the circulation is finished.

Wherein the step 1 specifically comprises the following steps: adding the mikania micrantha, the spanishneedles herb, the dandelion and the low-grain bamboo according to the proportion of 2:3:2.5:4, wherein the step 2 specifically comprises the following steps: the soaking duration is 35min, wherein intermittent stirring is required in the soaking process, the intermittent interval duration is 8min, the fumigating treatment duration in the step 7 is 15min-25min, and the condensation duration is 1 h.

The added fumigation process can further mix and blend the extract in a fumigation mode before the deodorant is prepared to be packaged for use, so that the effective ingredients of the plants can be effectively utilized, and the utilization rate of raw materials is improved.

Example 2

A preparation method of a plant type high-efficiency environment-friendly deodorant comprises the following steps: step 1, sequentially adding chamomile, bidens, dandelion and low-striped bamboo into a culture substrate, standing for 13min, fishing for water control for 2 min; step 2, mixing the components obtained in the step 1 after water control, adding the mixture into a culture cavity, and simultaneously pouring 50% of ethanol by mass fraction for soaking; step 3, heating the soaked components in an environment of 33 ℃ for 6.5min, and standing for 3 s; step 4, standing, heating at 51 ℃ again, and standing for 2.5 s; step 5, after standing, adding KOH solution according to the proportion of 1:2.5, and then immediately adding the mixture into a water bath at 37 ℃ for soaking for 14 min; step 6, adding mushrooms and 83% acetone solution in percentage by mass after soaking, wherein the adding amount of the mushrooms and the acetone is 1:0.5, and further heating the mixed solution at the heating temperature of 8 ℃ for 3 hours; step 7, carrying out fumigation treatment, carrying out condensation treatment after fumigation, and collecting after condensation treatment; and 8, circulating the steps 1 to 7 until the circulation is finished.

Wherein the step 1 specifically comprises the following steps: adding the mikania micrantha, the spanishneedles herb, the dandelion and the low-grain bamboo according to the proportion of 2:3:2.5:4, wherein the step 2 specifically comprises the following steps: the soaking duration is 40min, wherein intermittent stirring is required in the soaking process, the intermittent interval duration is 9min, the fumigating treatment duration in the step 7 is 20min, and the condensation duration is 1.3 h.

The deodorant raw material provided by the application has high contents of acid components and alcohol components, and the preparation method provided by the application can ensure that the extraction rate of the required components in the raw material is kept between 99.1% and 100%, so that the extraction rate of the effective substances in the prior art is obviously improved, and the problem that the raw material cannot be effectively utilized in the prior art is solved.

Example 3

A preparation method of a plant type high-efficiency environment-friendly deodorant comprises the following steps: step 1, sequentially adding chamomile, bidens, dandelion and low-striped bamboo into a culture substrate, standing for 15min, fishing for water control for 2 min; step 2, mixing the components obtained in the step 1 after water control, adding the mixture into a culture cavity, and simultaneously pouring 50% of ethanol by mass fraction for soaking; step 3, heating the soaked components in an environment of 35 ℃ for 6.5min, and standing for 3 s; step 4, standing, heating at 52 ℃ again, and standing for 2.5 s; step 5, after standing, adding KOH solution according to the proportion of 1:2.5, and then immediately adding the mixture into a water bath at 37 ℃ for soaking for 15 min; step 6, adding mushrooms and 85 mass percent of acetone solution after soaking, wherein the adding amount of the mushrooms and the acetone is 1:0.5, further heating the mixed solution at the heating temperature of 8.5 ℃ for 3 hours; step 7, carrying out fumigation treatment, carrying out condensation treatment after fumigation, and collecting after condensation treatment; and 8, circulating the steps 1 to 7 until the circulation is finished.

Wherein the step 1 specifically comprises the following steps: adding the mikania micrantha, the spanishneedles herb, the dandelion and the low-grain bamboo according to the proportion of 2:3:2.5:4, wherein the step 2 specifically comprises the following steps: the soaking duration is 44min, wherein intermittent stirring is required in the soaking process, the intermittent interval duration is 9.5min, the fumigating treatment duration in the step 7 is 25min, and the condensation duration is 1.5 h.

It should be noted that, the proportion of mikania micrantha, spanishneedles herb, dandelion and low-grain bamboo is specifically set, the soaking time is specifically set, and after continuous stirring, the raw materials and the extracted substances are uniformly distributed in the container, so that the separation of effective substances from the un-extracted parts of the raw materials in the mixed raw materials can be realized in a faster way, the extraction speed of the effective components is accelerated, and the time cost of production and processing is saved.

Comparative example 1

The preparation method comprises mixing herba Phyllanthi Urinariae, herba Sedi Sarmentosi, caulis et folium Stauntoniae, zinc ricinoleate deodorant and biological enzyme deodorant, soaking in culture medium for 10min, and heating and distilling the soaked mixture to obtain the preparation.

Comparative example 2

Mixing the extract of the pagodatree and the mulberry, the extract of the loquat nucleus, the extract of the wild peach nucleus and a biological enzyme deodorant, adding a culture medium, then adding a mixed solution of PVP and PEI, wherein the mass ratio of the PVP to the PEI is 0.5-15%, and mixing and soaking.

Based on the above examples, the application was compared with comparative examples 1 and 2 to obtain the data comparison results as follows:

	this application	Comparative example 1	Comparative example 2
				Removal rate of methyl mercaptan	98.66％	61.13％	69.30％
Utilization rate of raw material	80％-94％	41％-66％	47％-73％

The data can be analyzed and obtained on the basis, the application can effectively remove the methyl mercaptan in the odor, the utilization rate of raw materials can also reach 94%, and the problems that the methyl mercaptan removal effect is poor and the raw material utilization rate is small in the prior art are solved.

The previous description of the disclosed embodiments is provided to enable any person skilled in the art to make or use the present invention. Various modifications to these embodiments will be readily apparent to those skilled in the art, and the generic principles defined herein may be applied to other embodiments without departing from the spirit or scope of the invention. Thus, the present invention is not intended to be limited to the embodiments shown herein but is to be accorded the widest scope consistent with the principles and novel features disclosed herein.

Claims

1. A plant type efficient environment-friendly deodorant comprises a culture substrate and is characterized by further comprising the following components in percentage by mass: 10% -15% of chamomile, 2% -6% of spanishneedles, 32% -43% of dandelion, 21% -25% of low-grain bamboo and 19% -21% of cocoa bark extract; the culture substrate is filled with purified water at 37-41.5 ℃.

2. The plant-type efficient environment-friendly deodorant according to claim 1, characterized by further comprising 3-5 parts by mass of mushrooms, wherein the mushrooms are in a block shape.

3. A preparation method of a plant type high-efficiency environment-friendly deodorant, which is characterized in that the preparation method is based on the deodorant of any one of claims 1-2 and comprises the following steps:

step 4, standing, heating at 50-52 ℃ again, and standing for 2.5 s;

and 8, circulating the steps 1 to 7 until the circulation is finished.

4. The plant type efficient environment-friendly deodorant according to claim 3, wherein the step 1 specifically comprises: the mikania micrantha, the spanishneedles herb, the dandelion and the low-grain bamboo are added according to the proportion of 2:3:2.5: 4.

5. The plant-type efficient environment-friendly deodorant according to claim 3, wherein the step 2 specifically comprises: the soaking duration is 35min-44min, wherein intermittent stirring is required in the soaking process, and the intermittent interval duration is 8min-9.5 min.

6. The plant-type efficient environment-friendly deodorant according to claim 3, wherein the duration of the fumigation treatment in the step 7 is 15min to 25min, and the condensation duration is 1h to 1.5 h.