CN107744535A - The preparation method of honeysuckle disinfectant - Google Patents
The preparation method of honeysuckle disinfectant Download PDFInfo
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- CN107744535A CN107744535A CN201711058463.3A CN201711058463A CN107744535A CN 107744535 A CN107744535 A CN 107744535A CN 201711058463 A CN201711058463 A CN 201711058463A CN 107744535 A CN107744535 A CN 107744535A
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- honeysuckle
- powder
- disinfectant
- preparation
- solution
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/12—Ketones
- A61K31/122—Ketones having the oxygen directly attached to a ring, e.g. quinones, vitamin K1, anthralin
- A61K31/125—Camphor; Nuclear substituted derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/35—Caprifoliaceae (Honeysuckle family)
- A61K36/355—Lonicera (honeysuckle)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
- A61K36/534—Mentha (mint)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
- A61K47/30—Macromolecular organic or inorganic compounds, e.g. inorganic polyphosphates
- A61K47/36—Polysaccharides; Derivatives thereof, e.g. gums, starch, alginate, dextrin, hyaluronic acid, chitosan, inulin, agar or pectin
- A61K47/38—Cellulose; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/10—Dispersions; Emulsions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
Abstract
The invention discloses a kind of preparation method of honeysuckle disinfectant, including：Step 1: extracting honeysuckle, freezes, is put into white wine steam ambient and stops 10~15 minutes, repeat lyophilized, white wine steam ambient to stop 3~5 times, obtained honeysuckle is extracted 2~3 times with water, merging filtrate, obtain the first extract solution, by filter residue alcohol solution dipping, immersion process microwave irradiation, filtering, obtain the second extract solution, first extract solution is mixed with the second extract solution, heating concentration, obtains Flos Lonicerae extractive solution；Step 2: blend of essential oils is made；Step 3: solid powder is made；Step 4: adding methylcellulose into Flos Lonicerae extractive solution, it is stirred well to and is completely dissolved, then adds blend of essential oils and solid powder, stir to solid powder suspension, obtain suspension, obtain honeysuckle disinfectant.For the present invention mainly using Flos Lonicerae extractive solution as raw material, smell is suitable and nonirritant, more to skin zero damage, suitable population.
Description
Technical field
The present invention relates to a kind of disinfectant.A kind of it is more particularly related to preparation method of honeysuckle disinfectant.
Background technology
Used skin sterilization disinfectant is mostly chemical reagent in the market, such as boric acid, Iodophor, potassium permanganate
Deng although these disinfectant disinfection effects are preferable, the smell is awful and has certain excitant, and may cause skin
Damage.Therefore, need badly and design a kind of suitable, small to the skin damage disinfectant of smell.
The content of the invention
It is an object of the present invention to provide a kind of preparation method of honeysuckle disinfectant, it is mainly with Flos Lonicerae extractive solution
For raw material, smell is suitable and nonirritant, more to skin zero damage, suitable population.
In order to realize according to object of the present invention and further advantage, there is provided a kind of preparation side of honeysuckle disinfectant
Method, including：
Step 1: extracting honeysuckle, freezes, be put into white wine steam ambient and stop 10~15 minutes, repeat lyophilized, white wine and steam
Vapour environment is stopped 3~5 times, and obtained honeysuckle is extracted 2~3 times with water, merging filtrate, the first extract solution is obtained, filter residue is used
Mass fraction is 70% alcohol solution dipping 3~5 hours, and it with power density is 200mW/ that 30 minutes are spaced in immersion process
cm2Microwave irradiation 80 seconds, filtering, obtain the second extract solution, the first extract solution mixed with the second extract solution, heat and be concentrated into phase
It is 1.4~1.5 to density, obtains Flos Lonicerae extractive solution；White wine steam is obtained by heating 50 degree of white wine；
Step 2: taking mugwort leaf, lemon, lavender, Chinese cassia tree, argy wormwood essential oil, lemon are obtained with steam distillation respectively
Essential oil, Lavender and cinnamon essential oil, mixing, obtain blend of essential oils；
Step 3: taking Herba Menthae powder, camphor powder and calcium carbonate powder, mix, obtain solid powder；
Step 4: adding methylcellulose into Flos Lonicerae extractive solution, it is stirred well to and is completely dissolved, then adds essential oil
Mixture and solid powder, stir to solid powder suspension, obtain suspension, suspension is put into container made of loadstone
It is interior, sealing, it is put into 50~60 DEG C of environment and stops 30~40 minutes, is then placed in 5~10 DEG C of environment and stops 10~15
Minute, repetition is put into 50~60 DEG C of environment and is put into 5~10 DEG C of environment 3~5 times, takes out suspension, obtains honeysuckle sterilization
Agent；Wherein, when being stopped in 5~10 DEG C of environment, with 20kHz ultrasonic irradiation.
Preferably, the preparation method of described honeysuckle disinfectant, in the step 1, by honeysuckle with 40~50
DEG C water extracted.
Preferably, the preparation method of described honeysuckle disinfectant, in the step 3, Herba Menthae powder, camphor powder and
Calcium carbonate powder crosses 400 mesh sieves respectively.
Preferably, the preparation method of described honeysuckle disinfectant, in the step 2, argy wormwood essential oil, lemon extract
The mass ratio of oil, Lavender and cinnamon essential oil is 1:1:2.5:1.
Preferably, the preparation method of described honeysuckle disinfectant, in the step 3, Herba Menthae powder, camphor powder and
The weight ratio of calcium carbonate powder is 1:0.5:2.
Preferably, the preparation method of described honeysuckle disinfectant, Flos Lonicerae extractive solution, blend of essential oils, solid powder
The weight ratio of end and methylcellulose is 1:0.5:0.08:0.1.
The present invention comprises at least following beneficial effect：
1st, the Main Ingredients and Appearance of disinfectant of the invention is plant extracts, and chemical levels are few, and smell is small, and skin is hindered
Evil degree is less than second alcohol disinfectant.
2nd, the present invention repeats to freeze, operation is stopped in white wine steam ambient to Honeysuckle Flower so that honeysuckle powder
End absorbs white wine steam repeatedly, largely to destroy honeysuckle cell, subsequent extracting in water so that contain in honeysuckle
Fungicidal substance can by being entered sufficiently into extraction process in Flos Lonicerae extractive solution, and using ethanol solution coordinate microwave
Filter residue is extracted again, the Fungicidal substance that can make to remain in filter residue as far as possible enters Flos Lonicerae extractive solution, utilizes this hair
The content that bright extracting method obtains Fungicidal substance in Flos Lonicerae extractive solution is significantly more than conventional water extraction and alcohol extracting.
3rd, blend of essential oils, Herba Menthae powder, camphor powder and calcium carbonate are mixed into Flos Lonicerae extractive solution by the present invention, and utilize first
Suspension is made in base cellulose, and blend of essential oils improves the disinfecting power of the present invention, and makes the present invention more pure and fresh pleasant,
Herba Menthae powder and camphor powder further increase the disinfecting power of the present invention, and one side Herba Menthae powder, camphor powder and calcium carbonate group
Into solid powder can play a part of improving adhesive force, extend action time of the disinfectant on skin, it is on the other hand solid
Body powder can attract other sterilization compositions in disinfectant to reunite around it to a certain degree, and so, these compositions can be with
Solid powder is attached on skin simultaneously so that disinfectant has stronger disinfective action to solid powder adhering zone.
4th, suspension is put into made of loadstone in container, repetition is put into 50~60 DEG C of environment and is put into 5~10
DEG C environment, on the one hand can extend the suspension time of suspension, avoid the too fast sedimentation of disinfectant, on the other hand cause solid powder
It is more various around last, more evenly around sterilization composition, further improve sterilizing power.
Further advantage, target and the feature of the present invention embodies part by following explanation, and part will also be by this
The research and practice of invention and be understood by the person skilled in the art.
Embodiment
With reference to embodiment, the present invention is described in further detail, to make those skilled in the art with reference to specification
Word can be implemented according to this.
Embodiment 1
A kind of preparation method of honeysuckle disinfectant, including：
Step 1: extracting honeysuckle, freezes, be put into white wine steam ambient and stop 10 minutes, lyophilized, white wine steam ring is repeated
Border is stopped 3 times, and obtained honeysuckle is extracted 2 times with water, merging filtrate, the first extract solution is obtained, is with mass fraction by filter residue
70% alcohol solution dipping 3 hours, it with power density is 200mW/cm that 30 minutes are spaced in immersion process2Microwave irradiation 80
Second, filtering, the second extract solution is obtained, the first extract solution is mixed with the second extract solution, it is 1.4 that heating, which is concentrated into relative density, is obtained
Flos Lonicerae extractive solution；White wine steam is obtained by heating 50 degree of white wine；
Step 2: taking mugwort leaf, lemon, lavender, Chinese cassia tree, argy wormwood essential oil, lemon are obtained with steam distillation respectively
Essential oil, Lavender and cinnamon essential oil, mixing, obtain blend of essential oils；
Step 3: taking Herba Menthae powder, camphor powder and calcium carbonate powder, mix, obtain solid powder；
Step 4: adding methylcellulose into Flos Lonicerae extractive solution, it is stirred well to and is completely dissolved, then adds essential oil
Mixture and solid powder, stir to solid powder suspension, obtain suspension, suspension is put into container made of loadstone
It is interior, sealing, it is put into 50 DEG C of environment and stops 30 minutes, be then placed in 5 DEG C of environment and stop 10 minutes, repetition is put into 50 DEG C
Environment and be put into 5 DEG C of environment 3 times, take out suspension, obtain honeysuckle disinfectant；Wherein, when being stopped in 5 DEG C of environment,
With 20kHz ultrasonic irradiation.
In the step 1, honeysuckle is extracted with 40 DEG C of water.
In the step 3, Herba Menthae powder, camphor powder and calcium carbonate powder cross 400 mesh sieves respectively.
In the step 2, argy wormwood essential oil, lemon, the mass ratio of Lavender and cinnamon essential oil are 1:1:
2.5:1。
In the step 3, the weight ratio of Herba Menthae powder, camphor powder and calcium carbonate powder is 1:0.5:2.
Flos Lonicerae extractive solution, blend of essential oils, the weight ratio of solid powder and methylcellulose are 1:0.5:0.08:0.1.
Embodiment 2
A kind of preparation method of honeysuckle disinfectant, including：
Step 1: extracting honeysuckle, freezes, be put into white wine steam ambient and stop 15 minutes, lyophilized, white wine steam ring is repeated
Border is stopped 5 times, and obtained honeysuckle is extracted 3 times with water, merging filtrate, the first extract solution is obtained, is with mass fraction by filter residue
70% alcohol solution dipping 5 hours, it with power density is 200mW/cm that 30 minutes are spaced in immersion process2Microwave irradiation 80
Second, filtering, the second extract solution is obtained, the first extract solution is mixed with the second extract solution, it is 1.5 that heating, which is concentrated into relative density, is obtained
Flos Lonicerae extractive solution；White wine steam is obtained by heating 50 degree of white wine；
Step 2: taking mugwort leaf, lemon, lavender, Chinese cassia tree, argy wormwood essential oil, lemon are obtained with steam distillation respectively
Essential oil, Lavender and cinnamon essential oil, mixing, obtain blend of essential oils；
Step 3: taking Herba Menthae powder, camphor powder and calcium carbonate powder, mix, obtain solid powder；
Step 4: adding methylcellulose into Flos Lonicerae extractive solution, it is stirred well to and is completely dissolved, then adds essential oil
Mixture and solid powder, stir to solid powder suspension, obtain suspension, suspension is put into container made of loadstone
It is interior, sealing, it is put into 60 DEG C of environment and stops 40 minutes, be then placed in 10 DEG C of environment and stop 15 minutes, repetition is put into 60
DEG C environment and be put into 10 DEG C of environment 5 times, take out suspension, obtain honeysuckle disinfectant；Wherein, stopped in 10 DEG C of environment
When, with 20kHz ultrasonic irradiation.
In the step 1, honeysuckle is extracted with 50 DEG C of water.
In the step 3, Herba Menthae powder, camphor powder and calcium carbonate powder cross 400 mesh sieves respectively.
In the step 2, argy wormwood essential oil, lemon, the mass ratio of Lavender and cinnamon essential oil are 1:1:
2.5:1。
In the step 3, the weight ratio of Herba Menthae powder, camphor powder and calcium carbonate powder is 1:0.5:2.
Flos Lonicerae extractive solution, blend of essential oils, the weight ratio of solid powder and methylcellulose are 1:0.5:0.08:0.1.
Embodiment 3
A kind of preparation method of honeysuckle disinfectant, including：
Step 1: extracting honeysuckle, freezes, be put into white wine steam ambient and stop 12 minutes, lyophilized, white wine steam ring is repeated
Border is stopped 4 times, and obtained honeysuckle is extracted 3 times with water, merging filtrate, the first extract solution is obtained, is with mass fraction by filter residue
70% alcohol solution dipping 4 hours, it with power density is 200mW/cm that 30 minutes are spaced in immersion process2Microwave irradiation 80
Second, filtering, the second extract solution is obtained, the first extract solution is mixed with the second extract solution, it is 1.4 that heating, which is concentrated into relative density, is obtained
Flos Lonicerae extractive solution；White wine steam is obtained by heating 50 degree of white wine；
Step 2: taking mugwort leaf, lemon, lavender, Chinese cassia tree, argy wormwood essential oil, lemon are obtained with steam distillation respectively
Essential oil, Lavender and cinnamon essential oil, mixing, obtain blend of essential oils；
Step 3: taking Herba Menthae powder, camphor powder and calcium carbonate powder, mix, obtain solid powder；
Step 4: adding methylcellulose into Flos Lonicerae extractive solution, it is stirred well to and is completely dissolved, then adds essential oil
Mixture and solid powder, stir to solid powder suspension, obtain suspension, suspension is put into container made of loadstone
It is interior, sealing, it is put into 55 DEG C of environment and stops 35 minutes, be then placed in 7 DEG C of environment and stop 12 minutes, repetition is put into 55 DEG C
Environment and be put into 7 DEG C of environment 4 times, take out suspension, obtain honeysuckle disinfectant；Wherein, when being stopped in 7 DEG C of environment,
With 20kHz ultrasonic irradiation.
In the step 1, honeysuckle is extracted with 47 DEG C of water.
In the step 3, Herba Menthae powder, camphor powder and calcium carbonate powder cross 400 mesh sieves respectively.
In the step 2, argy wormwood essential oil, lemon, the mass ratio of Lavender and cinnamon essential oil are 1:1:
2.5:1。
In the step 3, the weight ratio of Herba Menthae powder, camphor powder and calcium carbonate powder is 1:0.5:2.
Flos Lonicerae extractive solution, blend of essential oils, the weight ratio of solid powder and methylcellulose are 1:0.5:0.08:0.1.
Comparative example 1
Do not repeat to freeze, operation stopped in white wine steam ambient, remaining parameter with identical in embodiment 3,
Technical process is also identical.
Comparative example 2
Without aaerosol solution is repeated to be put into 50~60 DEG C of environment and is put into the operation of 5~10 DEG C of environment, remaining
For parameter with identical in embodiment 3, technical process is also identical.
Experiment
Disinfectant is made in the technical scheme for being utilized respectively embodiment 3, comparative example 1 and comparative example 2, and skin surface is disappeared
Poison, the front and rear total plate count of sterilization is surveyed, every kind of disinfectant surveys 3 groups, experimental data such as table 1, table 2 and table 3.
Table 1
| Clump count (cfu/cm before sterilization3) | Clump count (cfu/cm after sterilization3) | |
| Embodiment 3 | 15.3 | 0.3 |
| Comparative example 1 | 13.7 | 5.2 |
| Comparative example 2 | 15.5 | 1.7 |
Table 2
| Clump count (cfu/cm before sterilization3) | Clump count (cfu/cm after sterilization3) | |
| Embodiment 3 | 37.5 | 1.0 |
| Comparative example 1 | 36.4 | 14.5 |
| Comparative example 2 | 38.2 | 4.2 |
Table 3
| Clump count (cfu/cm before sterilization3) | Clump count (cfu/cm after sterilization3) | |
| Embodiment 3 | 74.4 | 2.3 |
| Comparative example 1 | 74.3 | 27.6 |
| Comparative example 2 | 75.5 | 8.1 |
From table 1, table 2 and table 3, the killing rate of the disinfectant of embodiment 3 is significantly higher than comparative example 1 and comparative example 2, can
See, preparation method of the invention can significantly improve the sterilizing power of disinfectant.
Although embodiment of the present invention is disclosed as above, it is not restricted in specification and embodiment listed
With it can be applied to various suitable the field of the invention completely, can be easily for those skilled in the art
Other modification is realized, therefore under the universal limited without departing substantially from claim and equivalency range, it is of the invention and unlimited
In specific details and shown here as the embodiment with description.
Claims (6)
- A kind of 1. preparation method of honeysuckle disinfectant, it is characterised in that including：Step 1: extracting honeysuckle, freezes, be put into white wine steam ambient and stop 10~15 minutes, lyophilized, white wine steam ring is repeated Border is stopped 3~5 times, and obtained honeysuckle is extracted 2~3 times with water, merging filtrate, the first extract solution is obtained, by filter residue quality Fraction is 70% alcohol solution dipping 3~5 hours, and it with power density is 200mW/cm that 30 minutes are spaced in immersion process2's Microwave irradiation 80 seconds, filtering, obtains the second extract solution, the first extract solution is mixed with the second extract solution, and heating is concentrated into relatively close Spend for 1.4~1.5, obtain Flos Lonicerae extractive solution；Step 2: take mugwort leaf, lemon, lavender, Chinese cassia tree, respectively with steam distillation obtain argy wormwood essential oil, lemon, Lavender and cinnamon essential oil, mixing, obtain blend of essential oils；Step 3: taking Herba Menthae powder, camphor powder and calcium carbonate powder, mix, obtain solid powder；Step 4: adding methylcellulose into Flos Lonicerae extractive solution, it is stirred well to and is completely dissolved, then adds essential oil mixing Thing and solid powder, stir to solid powder suspension, obtain suspension, suspension is put into made of loadstone in container, it is close Envelope, is put into 50~60 DEG C of environment and stops 30~40 minutes, be then placed in 5~10 DEG C of environment and stop 10~15 minutes, Repetition is put into 50~60 DEG C of environment and is put into 5~10 DEG C of environment 3~5 times, takes out suspension, obtains honeysuckle disinfectant；Its In, when being stopped in 5~10 DEG C of environment, with 20kHz ultrasonic irradiation.
- 2. the preparation method of honeysuckle disinfectant as claimed in claim 1, it is characterised in that in the step 1, by gold Honeysuckle flower is extracted with 40~50 DEG C of water.
- 3. the preparation method of honeysuckle disinfectant as claimed in claim 1, it is characterised in that in the step 3, peppermint Powder, camphor powder and calcium carbonate powder cross 400 mesh sieves respectively.
- 4. the preparation method of honeysuckle disinfectant as claimed in claim 1, it is characterised in that in the step 2, argy wormwood Essential oil, lemon, the mass ratio of Lavender and cinnamon essential oil are 1:1:2.5:1.
- 5. the preparation method of honeysuckle disinfectant as claimed in claim 4, it is characterised in that in the step 3, peppermint The weight ratio of powder, camphor powder and calcium carbonate powder is 1:0.5:2.
- 6. the preparation method of honeysuckle disinfectant as claimed in claim 5, it is characterised in that Flos Lonicerae extractive solution, essential oil mix The weight ratio of compound, solid powder and methylcellulose is 1:0.5:0.08:0.1.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201711058463.3A CN107744535A (en) | 2017-11-01 | 2017-11-01 | The preparation method of honeysuckle disinfectant |
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|---|---|---|---|
| CN201711058463.3A CN107744535A (en) | 2017-11-01 | 2017-11-01 | The preparation method of honeysuckle disinfectant |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108324933A (en) * | 2018-04-08 | 2018-07-27 | 山东鲁北药业有限公司 | Lysozyme disinfecting liquid and its preparation method and application |
| CN111034746A (en) * | 2019-11-21 | 2020-04-21 | 周明臻 | Disinfectant for silkworm eating mulberry leaves and preparation method thereof |
| CN111066829A (en) * | 2019-11-21 | 2020-04-28 | 周明臻 | Disinfectant for rearing instrument in rearing room and preparation method thereof |
-
2017
- 2017-11-01 CN CN201711058463.3A patent/CN107744535A/en not_active Withdrawn
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108324933A (en) * | 2018-04-08 | 2018-07-27 | 山东鲁北药业有限公司 | Lysozyme disinfecting liquid and its preparation method and application |
| CN111034746A (en) * | 2019-11-21 | 2020-04-21 | 周明臻 | Disinfectant for silkworm eating mulberry leaves and preparation method thereof |
| CN111066829A (en) * | 2019-11-21 | 2020-04-28 | 周明臻 | Disinfectant for rearing instrument in rearing room and preparation method thereof |
| CN111066829B (en) * | 2019-11-21 | 2021-11-30 | 周明臻 | Disinfectant for rearing instrument in rearing room and preparation method thereof |
| CN111034746B (en) * | 2019-11-21 | 2022-02-01 | 周明臻 | Disinfectant for silkworm eating mulberry leaves and preparation method thereof |
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