CN107669792A - The preparation method of cordate houttuynia disinfectant - Google Patents
The preparation method of cordate houttuynia disinfectant Download PDFInfo
- Publication number
- CN107669792A CN107669792A CN201711059173.0A CN201711059173A CN107669792A CN 107669792 A CN107669792 A CN 107669792A CN 201711059173 A CN201711059173 A CN 201711059173A CN 107669792 A CN107669792 A CN 107669792A
- Authority
- CN
- China
- Prior art keywords
- powder
- disinfectant
- cordate houttuynia
- environment
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
- A61K36/282—Artemisia, e.g. wormwood or sagebrush
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/54—Lauraceae (Laurel family), e.g. cinnamon or sassafras
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/75—Rutaceae (Rue family)
- A61K36/752—Citrus, e.g. lime, orange or lemon
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/78—Saururaceae (Lizard's-tail family)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/333—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using mixed solvents, e.g. 70% EtOH
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/39—Complex extraction schemes, e.g. fractionation or repeated extraction steps
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/51—Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
Landscapes
- Health & Medical Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Alternative & Traditional Medicine (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Medical Informatics (AREA)
- Medicinal Chemistry (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Pharmacology & Pharmacy (AREA)
- Epidemiology (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of preparation method of cordate houttuynia disinfectant, including：Step 1: Heartleaf Houttuynia Herb is made；Step 2: by Heartleaf Houttuynia Herb, wrapped up with masking foil, it is put into 200~250 DEG C of environment and stops 10~15 seconds, then Heartleaf Houttuynia Herb is taken out, and it is put into the reactor equipped with the ethanol solution that mass fraction is 30%, 200kPa is forced into reactor and is kept for 15~20 minutes, extraction, obtains Herba Houttuyniae extract；Step 3: blend of essential oils is made；Step 4: solid powder is made；Step 5: adding methylcellulose into Herba Houttuyniae extract, it is stirred well to and is completely dissolved, then adds blend of essential oils and solid powder, stir to solid powder suspension, obtain cordate houttuynia disinfectant.For the present invention mainly using Herba Houttuyniae extract as raw material, smell is suitable and nonirritant, more to skin zero damage, suitable population.
Description
Technical field
The present invention relates to a kind of disinfectant.A kind of it is more particularly related to preparation method of cordate houttuynia disinfectant.
Background technology
Used skin sterilization disinfectant is mostly chemical reagent in the market, such as boric acid, Iodophor, potassium permanganate
Deng although these disinfectant disinfection effects are preferable, the smell is awful and has certain excitant, and may cause skin
Damage.Therefore, need badly and design a kind of suitable, small to the skin damage disinfectant of smell.
The content of the invention
It is an object of the present invention to provide a kind of preparation method of cordate houttuynia disinfectant, it is mainly with Herba Houttuyniae extract
For raw material, smell is suitable and nonirritant, more to skin zero damage, suitable population.
In order to realize according to object of the present invention and further advantage, there is provided a kind of preparation side of cordate houttuynia disinfectant
Method, including：
Step 1: taking cordate houttuynia, dry in the shade, crush, obtain Heartleaf Houttuynia Herb；
Step 2: by Heartleaf Houttuynia Herb, wrapped up with masking foil, be put into 200~250 DEG C of environment and stop 10~15 seconds, so
Heartleaf Houttuynia Herb is taken out afterwards, and is put into the reactor equipped with the ethanol solution that mass fraction is 30%, is added into reactor
It is depressed into 200kPa and is kept for 15~20 minutes, heating extraction 2~3 times, merging filtrate, heating concentration filtrate to relative density is
1.2~1.3, the first extract solution is obtained, filter residue is mixed with the ethanol solution that mass fraction is 10%, extracts 2~3 times, merges filter
Liquid, it is 1.2~1.3 that heating, which is concentrated into relative density, the second extract solution is obtained, by the first extract solution and the second extract solution with 3:1
Volume ratio mixes, and obtains Herba Houttuyniae extract；
Step 3: taking mugwort leaf, lemon, lavender, Chinese cassia tree, argy wormwood essential oil, lemon are obtained with steam distillation respectively
Essential oil, Lavender and cinnamon essential oil, mixing, obtain blend of essential oils；
Step 4: taking Herba Menthae powder, camphor powder and calcium carbonate powder, mix, obtain solid powder；
Step 5: adding methylcellulose into Herba Houttuyniae extract, it is stirred well to and is completely dissolved, then adds essential oil
Mixture and solid powder, stir to solid powder suspension, obtain suspension, suspension is put into container made of loadstone
It is interior, sealing, it is put into 50~60 DEG C of environment and stops 30~40 minutes, is then placed in 5~10 DEG C of environment and stops 10~15
Minute, repetition is put into 50~60 DEG C of environment and is put into 5~10 DEG C of environment 3~5 times, takes out suspension, obtains cordate houttuynia sterilization
Agent；Wherein, when being stopped in 5~10 DEG C of environment, with 20kHz ultrasonic irradiation.
Preferably, the preparation method of described cordate houttuynia disinfectant, it is 30% by mass fraction in the step 2
Ethanol solution be heated to 30~40 DEG C and extracted, the ethanol solution that mass fraction is 30% is heated to 50~60 DEG C of progress
Extraction.
Preferably, the preparation method of described cordate houttuynia disinfectant, in the step 4, Herba Menthae powder, camphor powder and
Calcium carbonate powder crosses 400 mesh sieves respectively.
Preferably, the preparation method of described cordate houttuynia disinfectant, in the step 3, argy wormwood essential oil, lemon extract
The mass ratio of oil, Lavender and cinnamon essential oil is 1:1:2.5:1.
Preferably, the preparation method of described cordate houttuynia disinfectant, in the step 4, Herba Menthae powder, camphor powder and
The weight ratio of calcium carbonate powder is 1:0.5:2.
Preferably, the preparation method of described cordate houttuynia disinfectant, Herba Houttuyniae extract, blend of essential oils, solid powder
The weight ratio of end and methylcellulose is 1:0.4:0.08:0.1.
The present invention comprises at least following beneficial effect：
1st, the Main Ingredients and Appearance of disinfectant of the invention is plant extracts, and chemical levels are few, and smell is small, and skin is hindered
Evil degree is less than second alcohol disinfectant.
2nd, the high temperature that the present invention is carried out in short-term after Heartleaf Houttuynia Herb is wrapped up with masking foil is burned, and quickly makes Heartleaf Houttuynia Herb
In desiccation, it is subsequently placed into the reactor equipped with ethanol solution and carries out HIGH PRESSURE TREATMENT so that ethanol solution can enter fish
Raw meat grass meal end is internal and is continuously in high pressure conditions, thus largely destroys cordate houttuynia cell so that cordate houttuynia contains
Fungicidal substance can be by being entered sufficiently into extraction process in Herba Houttuyniae extract, followed by the ethanol solution of low concentration
Filter residue is extracted at relatively high temperatures, the Fungicidal substance for making to remain in filter residue enters Herba Houttuyniae extract as far as possible, utilizes
The content that the extracting method of the present invention obtains Fungicidal substance in Herba Houttuyniae extract is significantly more than conventional water extraction or alcohol extracting.
3rd, blend of essential oils, Herba Menthae powder, camphor powder and calcium carbonate are mixed into Herba Houttuyniae extract by the present invention, and utilize first
Suspension is made in base cellulose, and blend of essential oils improves the disinfecting power of the present invention, and makes the present invention more pure and fresh pleasant,
Herba Menthae powder and camphor powder further increase the disinfecting power of the present invention, and one side Herba Menthae powder, camphor powder and calcium carbonate group
Into solid powder can play a part of improving adhesive force, extend action time of the disinfectant on skin, it is on the other hand solid
Body powder can attract other sterilization compositions in disinfectant to reunite around it to a certain degree, and so, these compositions can be with
Solid powder is attached on skin simultaneously so that disinfectant has stronger disinfective action to solid powder adhering zone.
4th, suspension is put into made of loadstone in container, repetition is put into 50~60 DEG C of environment and is put into 5~10
DEG C environment, on the one hand can extend the suspension time of suspension, avoid the too fast sedimentation of disinfectant, on the other hand cause solid powder
It is more various around last, more evenly around sterilization composition, further improve sterilizing power.
Further advantage, target and the feature of the present invention embodies part by following explanation, and part will also be by this
The research and practice of invention and be understood by the person skilled in the art.
Embodiment
With reference to embodiment, the present invention is described in further detail, to make those skilled in the art with reference to specification
Word can be implemented according to this.
Embodiment 1
A kind of preparation method of cordate houttuynia disinfectant, including：
Step 1: taking cordate houttuynia, dry in the shade, crush, obtain Heartleaf Houttuynia Herb；
Step 2: by Heartleaf Houttuynia Herb, wrapped up with masking foil, be put into 200 DEG C of environment and stop 10 seconds, then by cordate houttuynia
Powder is taken out, and is put into the reactor equipped with the ethanol solution that mass fraction is 30%, and 200kPa is forced into reactor
And kept for 15 minutes, heating extraction 2 times, merging filtrate, heating concentration filtrate to relative density is 1.2, obtains the first extract solution, will
Filter residue mixes with the ethanol solution that mass fraction is 10%, extracts 2 times, merging filtrate, and it is 1.2 that heating, which is concentrated into relative density,
The second extract solution is obtained, by the first extract solution and the second extract solution with 3:1 volume ratio mixing, obtains Herba Houttuyniae extract；
Step 3: taking mugwort leaf, lemon, lavender, Chinese cassia tree, argy wormwood essential oil, lemon are obtained with steam distillation respectively
Essential oil, Lavender and cinnamon essential oil, mixing, obtain blend of essential oils；
Step 4: taking Herba Menthae powder, camphor powder and calcium carbonate powder, mix, obtain solid powder；
Step 5: adding methylcellulose into Herba Houttuyniae extract, it is stirred well to and is completely dissolved, then adds essential oil
Mixture and solid powder, stir to solid powder suspension, obtain suspension, suspension is put into container made of loadstone
It is interior, sealing, it is put into 50 DEG C of environment and stops 30 minutes, be then placed in 5 DEG C of environment and stop 10 minutes, repetition is put into 50 DEG C
Environment and be put into 5 DEG C of environment 3 times, take out suspension, obtain cordate houttuynia disinfectant；Wherein, when being stopped in 5 DEG C of environment,
With 20kHz ultrasonic irradiation.
In the step 2, the ethanol solution that mass fraction is 30% is heated to 30 DEG C and extracted, by quality point
The ethanol solution that number is 30% is heated to 50 DEG C and extracted.
In the step 4, Herba Menthae powder, camphor powder and calcium carbonate powder cross 400 mesh sieves respectively.
In the step 3, argy wormwood essential oil, lemon, the mass ratio of Lavender and cinnamon essential oil are 1:1:
2.5:1。
In the step 4, the weight ratio of Herba Menthae powder, camphor powder and calcium carbonate powder is 1:0.5:2.
Herba Houttuyniae extract, blend of essential oils, the weight ratio of solid powder and methylcellulose are 1:0.4:0.08:0.1.
Embodiment 2
A kind of preparation method of cordate houttuynia disinfectant, including：
Step 1: taking cordate houttuynia, dry in the shade, crush, obtain Heartleaf Houttuynia Herb；
Step 2: by Heartleaf Houttuynia Herb, wrapped up with masking foil, be put into 250 DEG C of environment and stop 15 seconds, then by cordate houttuynia
Powder is taken out, and is put into the reactor equipped with the ethanol solution that mass fraction is 30%, and 200kPa is forced into reactor
And kept for 20 minutes, heating extraction 3 times, merging filtrate, heating concentration filtrate to relative density is 1.3, obtains the first extract solution, will
Filter residue mixes with the ethanol solution that mass fraction is 10%, extracts 3 times, merging filtrate, and it is 1.3 that heating, which is concentrated into relative density,
The second extract solution is obtained, by the first extract solution and the second extract solution with 3:1 volume ratio mixing, obtains Herba Houttuyniae extract；
Step 3: taking mugwort leaf, lemon, lavender, Chinese cassia tree, argy wormwood essential oil, lemon are obtained with steam distillation respectively
Essential oil, Lavender and cinnamon essential oil, mixing, obtain blend of essential oils；
Step 4: taking Herba Menthae powder, camphor powder and calcium carbonate powder, mix, obtain solid powder；
Step 5: adding methylcellulose into Herba Houttuyniae extract, it is stirred well to and is completely dissolved, then adds essential oil
Mixture and solid powder, stir to solid powder suspension, obtain suspension, suspension is put into container made of loadstone
It is interior, sealing, it is put into 60 DEG C of environment and stops 40 minutes, be then placed in 10 DEG C of environment and stop 15 minutes, repetition is put into 60
DEG C environment and be put into 10 DEG C of environment 5 times, take out suspension, obtain cordate houttuynia disinfectant；Wherein, stopped in 10 DEG C of environment
When, with 20kHz ultrasonic irradiation.
In the step 2, the ethanol solution that mass fraction is 30% is heated to 40 DEG C and extracted, by quality point
The ethanol solution that number is 30% is heated to 60 DEG C and extracted.
In the step 4, Herba Menthae powder, camphor powder and calcium carbonate powder cross 400 mesh sieves respectively.
In the step 3, argy wormwood essential oil, lemon, the mass ratio of Lavender and cinnamon essential oil are 1:1:
2.5:1。
In the step 4, the weight ratio of Herba Menthae powder, camphor powder and calcium carbonate powder is 1:0.5:2.
Herba Houttuyniae extract, blend of essential oils, the weight ratio of solid powder and methylcellulose are 1:0.4:0.08:0.1.
Embodiment 3
A kind of preparation method of cordate houttuynia disinfectant, including：
Step 1: taking cordate houttuynia, dry in the shade, crush, obtain Heartleaf Houttuynia Herb；
Step 2: by Heartleaf Houttuynia Herb, wrapped up with masking foil, be put into 230 DEG C of environment and stop 13 seconds, then by cordate houttuynia
Powder is taken out, and is put into the reactor equipped with the ethanol solution that mass fraction is 30%, and 200kPa is forced into reactor
And kept for 18 minutes, heating extraction 3 times, merging filtrate, heating concentration filtrate to relative density is 1.3, obtains the first extract solution, will
Filter residue mixes with the ethanol solution that mass fraction is 10%, extracts 3 times, merging filtrate, and it is 1.3 that heating, which is concentrated into relative density,
The second extract solution is obtained, by the first extract solution and the second extract solution with 3:1 volume ratio mixing, obtains Herba Houttuyniae extract；
Step 3: taking mugwort leaf, lemon, lavender, Chinese cassia tree, argy wormwood essential oil, lemon are obtained with steam distillation respectively
Essential oil, Lavender and cinnamon essential oil, mixing, obtain blend of essential oils；
Step 4: taking Herba Menthae powder, camphor powder and calcium carbonate powder, mix, obtain solid powder；
Step 5: adding methylcellulose into Herba Houttuyniae extract, it is stirred well to and is completely dissolved, then adds essential oil
Mixture and solid powder, stir to solid powder suspension, obtain suspension, suspension is put into container made of loadstone
It is interior, sealing, it is put into 55 DEG C of environment and stops 35 minutes, be then placed in 7 DEG C of environment and stop 12 minutes, repetition is put into 55 DEG C
Environment and be put into 7 DEG C of environment 4 times, take out suspension, obtain cordate houttuynia disinfectant；Wherein, when being stopped in 7 DEG C of environment,
With 20kHz ultrasonic irradiation.
In the step 2, the ethanol solution that mass fraction is 30% is heated to 38 DEG C and extracted, by quality point
The ethanol solution that number is 30% is heated to 58 DEG C and extracted.
In the step 4, Herba Menthae powder, camphor powder and calcium carbonate powder cross 400 mesh sieves respectively.
In the step 3, argy wormwood essential oil, lemon, the mass ratio of Lavender and cinnamon essential oil are 1:1:
2.5:1。
In the step 4, the weight ratio of Herba Menthae powder, camphor powder and calcium carbonate powder is 1:0.5:2.
Herba Houttuyniae extract, blend of essential oils, the weight ratio of solid powder and methylcellulose are 1:0.4:0.08:0.1.
Comparative example 1
Burned without high temperature in short-term and HIGH PRESSURE TREATMENT, remaining parameter is with identical in embodiment 3, technical process
Also it is identical.
Comparative example 2
Without aaerosol solution is repeated to be put into 50~60 DEG C of environment and is put into the operation of 5~10 DEG C of environment, remaining
For parameter with identical in embodiment 3, technical process is also identical.
Experiment
Disinfectant is made in the technical scheme for being utilized respectively embodiment 3, comparative example 1 and comparative example 2, and skin surface is disappeared
Poison, the front and rear total plate count of sterilization is surveyed, every kind of disinfectant surveys 3 groups, experimental data such as table 1, table 2 and table 3.
Table 1
| Clump count (cfu/cm before sterilization3) | Clump count (cfu/cm after sterilization3) | |
| Embodiment 3 | 11.2 | 0.3 |
| Comparative example 1 | 11.2 | 4.5 |
| Comparative example 2 | 12.8 | 1.7 |
Table 2
| Clump count (cfu/cm before sterilization3) | Clump count (cfu/cm after sterilization3) | |
| Embodiment 3 | 30.7 | 0.9 |
| Comparative example 1 | 35.2 | 15.3 |
| Comparative example 2 | 33.3 | 3.2 |
Table 3
| Clump count (cfu/cm before sterilization3) | Clump count (cfu/cm after sterilization3) | |
| Embodiment 3 | 71.6 | 2.0 |
| Comparative example 1 | 71.9 | 29.9 |
| Comparative example 2 | 72.4 | 6.6 |
From table 1, table 2 and table 3, the killing rate of the disinfectant of embodiment 3 is significantly higher than comparative example 1 and comparative example 2, can
See, preparation method of the invention can significantly improve the sterilizing power of disinfectant.
Although embodiment of the present invention is disclosed as above, it is not restricted in specification and embodiment listed
With it can be applied to various suitable the field of the invention completely, can be easily for those skilled in the art
Other modification is realized, therefore under the universal limited without departing substantially from claim and equivalency range, it is of the invention and unlimited
In specific details and shown here as the embodiment with description.
Claims (6)
- A kind of 1. preparation method of cordate houttuynia disinfectant, it is characterised in that including：Step 1: taking cordate houttuynia, dry in the shade, crush, obtain Heartleaf Houttuynia Herb；Step 2: by Heartleaf Houttuynia Herb, wrapped up with masking foil, be put into 200~250 DEG C of environment and stop 10~15 seconds, then will Heartleaf Houttuynia Herb takes out, and is put into the reactor equipped with the ethanol solution that mass fraction is 30%, is forced into reactor 200kPa simultaneously keep 15~20 minutes, heating extraction 2~3 times, merging filtrate, heating concentration filtrate to relative density be 1.2~ 1.3, the first extract solution is obtained, filter residue is mixed with the ethanol solution that mass fraction is 10%, extracts 2~3 times, merging filtrate, adds It is 1.2~1.3 that heat, which is concentrated into relative density, the second extract solution is obtained, by the first extract solution and the second extract solution with 3:1 volume ratio Mixing, obtains Herba Houttuyniae extract；Step 3: take mugwort leaf, lemon, lavender, Chinese cassia tree, respectively with steam distillation obtain argy wormwood essential oil, lemon, Lavender and cinnamon essential oil, mixing, obtain blend of essential oils；Step 4: taking Herba Menthae powder, camphor powder and calcium carbonate powder, mix, obtain solid powder；Step 5: adding methylcellulose into Herba Houttuyniae extract, it is stirred well to and is completely dissolved, then adds essential oil mixing Thing and solid powder, stir to solid powder suspension, obtain suspension, suspension is put into made of loadstone in container, it is close Envelope, is put into 50~60 DEG C of environment and stops 30~40 minutes, be then placed in 5~10 DEG C of environment and stop 10~15 minutes, Repetition is put into 50~60 DEG C of environment and is put into 5~10 DEG C of environment 3~5 times, takes out suspension, obtains cordate houttuynia disinfectant；Its In, when being stopped in 5~10 DEG C of environment, with 20kHz ultrasonic irradiation.
- 2. the preparation method of cordate houttuynia disinfectant as claimed in claim 1, it is characterised in that in the step 2, by matter The ethanol solution that amount fraction is 30% is heated to 30~40 DEG C and extracted, and the ethanol solution that mass fraction is 30% is heated to 50~60 DEG C are extracted.
- 3. the preparation method of cordate houttuynia disinfectant as claimed in claim 1, it is characterised in that in the step 4, peppermint Powder, camphor powder and calcium carbonate powder cross 400 mesh sieves respectively.
- 4. the preparation method of cordate houttuynia disinfectant as claimed in claim 1, it is characterised in that in the step 3, argy wormwood Essential oil, lemon, the mass ratio of Lavender and cinnamon essential oil are 1:1:2.5:1.
- 5. the preparation method of cordate houttuynia disinfectant as claimed in claim 4, it is characterised in that in the step 4, peppermint The weight ratio of powder, camphor powder and calcium carbonate powder is 1:0.5:2.
- 6. the preparation method of cordate houttuynia disinfectant as claimed in claim 5, it is characterised in that Herba Houttuyniae extract, essential oil mix The weight ratio of compound, solid powder and methylcellulose is 1:0.4:0.08:0.1.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711059173.0A CN107669792A (en) | 2017-11-01 | 2017-11-01 | The preparation method of cordate houttuynia disinfectant |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711059173.0A CN107669792A (en) | 2017-11-01 | 2017-11-01 | The preparation method of cordate houttuynia disinfectant |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107669792A true CN107669792A (en) | 2018-02-09 |
Family
ID=61144018
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711059173.0A Withdrawn CN107669792A (en) | 2017-11-01 | 2017-11-01 | The preparation method of cordate houttuynia disinfectant |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107669792A (en) |
-
2017
- 2017-11-01 CN CN201711059173.0A patent/CN107669792A/en not_active Withdrawn
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102145970A (en) | Multifunctional substrate modifier for aquaculture and preparation method thereof | |
| CN106701851A (en) | Method for extracting allicin | |
| CN107744535A (en) | The preparation method of honeysuckle disinfectant | |
| CN105396165A (en) | Preparation method for environmentally-friendly biomass deodorant | |
| CN110180378A (en) | A kind of efficient deodorizing composition and its production method | |
| CN106538629A (en) | A kind of livestock-raising disinfectant and preparation method thereof | |
| CN108849875A (en) | A kind of biology base porous carbon plants essential oil controlled release agent, preparation method and applications preventing and treating soil-borne disease of crop | |
| CN107669792A (en) | The preparation method of cordate houttuynia disinfectant | |
| Deo et al. | Standardization of Brahmi Ghrita with special reference to its pharmaceutical study | |
| CN108935536A (en) | A kind of natural drug and preparation method thereof inhibiting wawter bloom | |
| CN107582688A (en) | The preparation method of argy wormwood disinfectant | |
| CN101292670A (en) | Method for preparing plant jatropha curcas insecticide | |
| CN107670008A (en) | The preparation method of ginger disinfectant | |
| KR101833719B1 (en) | Manufachturing method for deodorant compounding using the waste pine cone | |
| KR101477078B1 (en) | Natural deodorant and germicide comprising crude drugs and manufacturaring process for the same | |
| KV et al. | Optimization of ultrasound-assisted extraction of watermelon seed oil using response surface methodology | |
| RU2348168C1 (en) | Method of processing fir tree greenery extraction wastes | |
| KR102314874B1 (en) | manufacturing method of disinfection and deodorant composition | |
| CN111838202A (en) | Novel deodorant | |
| CN109233889A (en) | A kind of Manufacturing approach and use of safe biologic matter gasification liquid | |
| JPWO2018235344A1 (en) | Antioxidant, tyrosinase activity inhibitor and whitening agent containing the antioxidant, and method for producing the antioxidant and the whitening agent | |
| CN113575617B (en) | Application of costus root in biological control, biological control medicament and preparation method thereof | |
| KR102655621B1 (en) | Soil conditioner and methods for manufacturing the same | |
| CN106266170A (en) | The preparation method of Fructus Schisandrae Chinensis extrat under a kind of room temperature | |
| CN106309699A (en) | Preparation method of prepared rehmannia root extracts at normal temperature |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20180209 |