CN109865423A - One Plant Extracts and the compound deodorizer of biological enzyme and preparation method thereof - Google Patents
One Plant Extracts and the compound deodorizer of biological enzyme and preparation method thereof Download PDFInfo
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- CN109865423A CN109865423A CN201910326852.2A CN201910326852A CN109865423A CN 109865423 A CN109865423 A CN 109865423A CN 201910326852 A CN201910326852 A CN 201910326852A CN 109865423 A CN109865423 A CN 109865423A
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/20—Air quality improvement or preservation, e.g. vehicle emission control or emission reduction by using catalytic converters
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Abstract
The present invention relates to the compound deodorizers of a Plant Extracts and biological enzyme, it include: 5 parts of plant extract composition including following component by weight, 20 parts of biological enzymatic compositions, 2-4 parts of zinc ricinate, 0.01-0.05 parts of potassium sorbate, 3-6 parts of ethyl alcohol, 5-8 parts of fatty glyceride, 56.95-64.99 parts of deionized water, special biological enzyme contained by product of the present invention, it can be with the group cream sulfydryl in odorous substance, amino, aldehyde radical, amido etc. neutralizes, condensation reaction, polluter in foul smell is converted to harmless carbohydrate, plant extracts mainly passes through absorption foul smell and reacts with foul smell molecule, foul smell is changed into odorless harmless carbohydrate, to reach quick deodorizing effect, the effective component of plant extracts in product of the present invention is all from day It is extracted in right plant, it is without any side effects to human body, skin is not stimulated, toxicity on inhalation is extremely low, will not cause any secondary pollution.
Description
Technical field
The present invention relates to deodorant production technical field more particularly to the composite deodurizings of a Plant Extracts and biological enzyme
Agent and preparation method thereof.
Background technique
In recent years, room air pollution was increasingly severe, and the case for influencing people's health is also more and more, or even draws
Send out major disease or death.In especially new decorating house, new car, there are the harmful substances such as a large amount of formaldehyde, benzene, TVOC.Its
It is mainly derived from the finishing materials such as wood-based plate, coating, furniture, the glue that new decorating house uses.It hangs up one's hat in formaldehyde, benzene etc.
Under the exceeded environment of harmful substance, it is easy to cause respiratory disease, leukaemia, neonatal chromosome disorder and teenager's memory
The major diseases such as power decline.
And currently, removing the air harmful substances such as formaldehyde, benzene, ammonia, TVOC is mainly the following type: physical deodorization
Agent, chemical deodorizing agent, microbial deodorant, plant deodorant etc..
Physical deodorization agent mainly passes through the physics modes deodorization such as absorption or covering, and this deodorant simultaneously has not been changed foul smell point
Son still can cause a degree of damage to the health of people.
Chemical deodorizing agent is to utilize oxidation, reduction decomposition, neutralization reaction, addition reaction, condensation reaction, ion-exchange reactions
Odorous substance is become odorless substance to reach elimination foul smell by equal chemical modes.Product after this deodorant after chemical reaction
New environmental contaminants are likely to result in, generate new destruction to human health, while chemical deodorizing agent is to human body rdativery sensitive,
It may cause human allergy, human mechanism caused to damage.
Plant deodorant mainly uses the natural disinfection deodorization factor in plant to extract, and can decompose removal foul smell,
The main stereochemical structure by changing odor molecules, slackens the chemical combination key in foul smell molecule, ultimately produces tasteless, nontoxic object
Matter.But that there are extraction processes is complicated for plant deodorant, production cost is higher, has the deficiencies of limitation for foul smell molecule.
Biological deodorant is the metabolin using beneficial microbe colony, using microbial fermentation, abstraction technique production, energy
The odorous substance being dissolved in the water is absorbed in microbial body, its degradation is made by bacteria metabolism activity.It is micro- simultaneously
Biological energy source secretes a variety of biological enzyme, the organic matters such as foul smell can thoroughly be synthesized tasteless substance, water and carbon dioxide.This deodorization
Agent safety is high, will not cause secondary pollution, and can reach and continue deodorization, low production cost for a long time.But there is also micro-
Biological mixed fermentation is difficult, unstable product quality, and biological enzyme is easy inactivation, and microorganism has certain adaptability of existence and life
Long period cannot reach fast deodorization.
The improvement of people's living standards, the requirement to living environment is higher and higher, also increasingly payes attention to health.
Therefore, the exploitation and use of the deodorant with efficient deodorizing effect & Safety has great market and life
State meaning.The compound deodorizer of exploitation plant extracts and biological enzyme gives full play to the fast deodorization advantage of plant extracts, more
Kind biological enzyme synergistic effect widens the type that can eliminate foul smell, and can keep its activity for a long time.
Plant extracts of the present invention and biological enzyme compound deodorizer have unique advantage, by various plants extract and
A variety of biological enzyme compoundings can quickly, persistently remove foul smell molecule.Accessible foul smell molecule mainly include formaldehyde, benzene, dimethylbenzene,
Ammonia, sulfur dioxide, hydrogen sulfide etc..The product is particularly suitable for the rapidly and efficiently deodorization requirement such as new decorating house, new car.To human body
It is safe and non-toxic, it is nonirritant, it is incombustible, it is biodegradable, it not will cause secondary pollution, after direct 10-20 times is diluted with water
Sprinkling, it is easy to use.
Summary of the invention
The purpose of the present invention is to solve the one kind existed in the prior art in powder containing moisture, and proposed
Plant extracts and the compound deodorizer of biological enzyme and preparation method thereof.
To achieve the goals above, present invention employs following technical solutions:
The compound deodorizer of a Plant Extracts and biological enzyme is designed, including following component by weight includes: that plant mentions
Take 5 parts of composition, biological 20 parts of enzymatic compositions, 2-4 parts of zinc ricinate, 0.01-0.05 parts of potassium sorbate, 3-6 parts of ethyl alcohol, rouge
5-8 parts of fatty acid glyceride, 56.95-64.99 parts of deionized water.
Preferably, the compound deodorizer of the plant extracts and biological enzyme includes plant extract group by optimal components by weight percent
Close 5 parts of object, biological 20 parts of enzymatic compositions, 2 parts of zinc ricinate, 0.02 part of potassium sorbate, 5 parts of ethyl alcohol, fatty glyceride 8
Part, 59.98 parts of deionized water.
Preferably, plant extract composition component by weight includes 3-5 parts of camellia, 2-3 parts of aloe, orange peel 1-
2 parts of co-grindings are as the extract for extracting raw material.
Preferably, the plant extract composition includes 4 parts of camellia, 3 parts of aloe, orange peel 2 by optimal components by weight percent
The ratio mixing of part is smashed as the extracting solution for extracting raw material.
Preferably, the biological enzymatic compositions component by weight includes 6-8 parts of protease, 8-12 parts of lipase, amylase
6-10 parts, 10-13 parts, -15 parts of oxido-reductase 10 of cellulase.
Preferably, the biological enzymatic compositions include 6 parts of protease, 10 parts of lipase, amylase 8 by optimal components by weight percent
Part, 12 parts of cellulase, 15 parts of oxidoreducing enzyme.
The preparation method of the compound deodorizer of one Plant Extracts and biological enzyme, includes the following steps:
S1: plant extract composition and zinc ricinate, ethyl alcohol, fatty glyceride are proportionally mixed, and added
It adjusts into high speed shear dispersion emulsifying machine, and by high speed shear dispersion emulsifying machine to the emulsified 60min of 8000r/min, is made
Emulsified solution is spare；
S2: the biological enzymatic compositions of corresponding proportion, potassium sorbate, deionization are added in emulsified solution obtained above
Water adjusts the emulsified 30min of high speed shear dispersion emulsifying machine 8000r/min, and compound deodorizer is made.
Preferably, the preparation method of the plant extract composition includes the following steps:
A1: camellia, aloe, orange peel are weighed in proportion, and their co-grindings are spare；
A2: 18-24h is impregnated with the petroleum ether (60-90) of 10-30 times of quality of raw material after co-grinding, is then carried out true
Empty pump filter, it is spare to obtain first time filtered fluid, and filter residue is repeated to impregnate filtering 2 times, is filtered by vacuum, and respectively obtains second
Filtered fluid and third time filtered fluid are spare；
A3: first time filtered fluid, second of filtered fluid and third time filtered fluid are sufficiently mixed filtrate and mixed, rotation is passed through
Petroleum ether therein is recycled in evaporator rectification, obtains plant extract composition.
Preferably, the preparation method of the biological enzymatic compositions includes the following steps:
B1: proportionally weighing protease, lipase, amylase, cellulase, and oxidoreducing enzyme is added to mixing vessel
It is interior, and be uniformly mixed spare；
B2: at 30 DEG C, protease, lipase, amylase, cellulase, oxidoreducing enzyme are added into mixing vessel
The deionized water of 30 times of quality is stirred dissolution 40min, stands 3h at 25 DEG C；
B3: under the conditions of 0.5mpa, unit of activity 2000U/ml, PH6 is made in the filter membrane for being 0.01um by membrane aperture
Biological enzyme combine liquid.
B4: in biological enzyme obtained combination liquid, sucrose 5-10 parts, 1-3 parts of sodium chloride, sodium thiosulfate is added by quality
0.002-0.004 parts, 5min is stirred to whole dissolutions, obtains biological enzymatic compositions.
A Plant Extracts and the compound deodorizer of biological enzyme proposed by the present invention and preparation method thereof, beneficial effect exists
In:
Special biological enzyme contained by 1 product of the present invention, can be with group cream sulfydryl, amino, the aldehyde radical, amido in odorous substance
Polluter in foul smell, is converted to harmless carbohydrate, will cause any secondary by equal generations neutralization, condensation reaction
Pollution.
2 pass through preferred enzymes, and optimum organization ratio assesses its deodorization, to include formaldehyde, dimethylbenzene, ammonia,
Various odor pollutants including hydrogen sulfide etc. show good removal effect.
3 plant extracts mainly pass through absorption foul smell and react with foul smell molecule, foul smell are changed into odorless harmless
Carbohydrate, to reach quick deodorizing effect, 24 hours deodorizing rates are 2 times of pure compound biological enzyme deodorizing rate.
4 plant extracts are reduced with respect to type, but all have deodorizing capability, generate strong scent compared with by addition essence
Unsoundness meaning is had more to cover the deodorant of foul smell.Product odour clear and natural, without blaming after the mixing of a variety of extracts
The acceptance level of the phenomenon that taste, penetrating odor, Market Consumer are bigger.
The effective component of plant extracts in 5 product of the present invention is all extracted from natural plants, to human body without any
Toxic side effect does not stimulate skin, and toxicity on inhalation is extremely low, will not cause any secondary pollution.
6 zinc ricinates can form very strong chemical combination key with nitrogen, the sulphur atom in foul smell using active zinc atom, thus
Thoroughly eliminate stink.Meanwhile zinc is essential element in human body, safety with higher.
7 this products directly adopt that biological enzyme is compound, will not be by microorganism growth conditions and period compared to microbial fermentation
Limitation, the vigor of enzyme will not be influenced by microorganism concn, will not be by the growth suppression of bacteriostatic preservative in deodorant
System, largely improves production efficiency and odor removal efficient.
The selection of 8 this products uses potassium sorbate bacteriostatic preservative, has very high safety, in addition to being capable of antisepsis and sterilization energy
Power, while can also maintain and stablize the vigor of biological enzyme.
Sucrose, sodium chloride are added in 9 biological enzymatic compositions, sodium thiosulfate can be good at the vigor for stablizing biological enzyme,
Extend the duration and persistence of its deodorization.Sucrose and sodium chloride can make cellulase keep rock-steady structure in aqueous solution,
Mutability does not lose activity.Sodium thiosulfate can prevent the oxidation of protease and lose activity.
The preparation method of 10 plant deodorization extracts, by the way of simple, filtering and distillation, by the deodorization in plant at
Divide and extract, extraction process is simple and easy, and petroleum ether is selected to do Extraction solvent, extracts compared to ethyl alcohol, substantially increases extraction
Efficiency and recovery rate.
The dissolution of 11 biological enzyme is improved biological enzyme solution rate, is simplified biological enzyme group using the method for stirring hydrotropy
The preparation process for closing object, has saved production time cost.
12 deodorization ranges are wider, and the compound and a variety of biological enzyme of various plants extraction is compound, can eliminate a variety of foul smell molecules, more
The deodorization limitation of plant extract deodorant and biological enzyme deodorant is mended.
Specific embodiment
It is next combined with specific embodiments below that the present invention will be further described.
Embodiment 1
The compound deodorizer of one Plant Extracts and biological enzyme, including following component by weight include: plant extract group
Close 5 parts of object, biological 20 parts of enzymatic compositions, 2 parts of zinc ricinate, 0.04 part of potassium sorbate, 6 parts of ethyl alcohol, fatty glyceride 8
Part, 58.96 parts of deionized water.
The plant extract composition in optimal components by weight percent include 5 parts of camellia, 3 parts of aloe, 2 parts of orange peel ratio
Mixing is smashed as the extracting solution for extracting raw material.
The biology enzymatic compositions include 6 parts of protease, 8 parts of lipase, 6 parts of amylase, fiber by optimal components by weight percent
10 parts of plain enzyme, oxido-reductase 10 part.
The preparation method of the compound deodorizer of one Plant Extracts and biological enzyme, includes the following steps:
S1: plant extract composition and zinc ricinate, ethyl alcohol, fatty glyceride are proportionally mixed, and added
It adjusts into high speed shear dispersion emulsifying machine, and by high speed shear dispersion emulsifying machine to the emulsified 60min of 8000r/min, is made
Emulsified solution is spare；
S2: the biological enzymatic compositions of corresponding proportion, potassium sorbate, deionization are added in emulsified solution obtained above
Water adjusts the emulsified 30min of high speed shear dispersion emulsifying machine 8000r/min, and compound deodorizer is made.
The preparation method of the plant extract composition includes the following steps:
A1: camellia, aloe, orange peel are weighed in proportion, and their co-grindings are spare；
A2: 18h is impregnated with the petroleum ether (60-90) of 200 parts of quality, is then filtered by vacuum, obtains filtering for the first time
Liquid is spare, and filter residue is repeated to impregnate filtering 2 times, is filtered by vacuum, respectively obtains second of filtered fluid and third time filtered fluid
It is spare；
A3: first time filtered fluid, second of filtered fluid and third time filtered fluid are sufficiently mixed filtrate and mixed, rotation is passed through
Petroleum ether therein is recycled in evaporator rectification, obtains plant extract composition.
The preparation method of the biology enzymatic compositions includes the following steps:
B1: proportionally weighing protease, lipase, amylase, cellulase, and oxidoreducing enzyme is added to mixing vessel
It is interior, and be uniformly mixed spare；
B2: at 30 DEG C, into mixing vessel, the deionized water of 1200 parts of addition, which is stirred, dissolves 40min, at 25 DEG C
Stand 3h；
B3: under the conditions of 0.5mpa, unit of activity 2000U/ml, PH6 is made in the filter membrane for being 0.01um by membrane aperture
Biological enzyme combine liquid.
B4: in biological enzyme obtained combination liquid, 5 parts of sucrose, 1 part of sodium chloride, sodium thiosulfate 0.002 is added by quality
Part, 5min is stirred to whole dissolutions, obtains biological enzymatic compositions.
Embodiment 2
The compound deodorizer of one Plant Extracts and biological enzyme, including following component by weight include: plant extract group
Close 5 parts of object, biological 20 parts of enzymatic compositions, 2 parts of zinc ricinate, 0.02 part of potassium sorbate, 5 parts of ethyl alcohol, fatty glyceride 8
Part, 59.98 parts of deionized water.
Plant extract composition component by weight includes 2 parts of 4 parts of camellia, 3 parts of aloe, orange peel co-grindings works
For the extract for extracting raw material.
The biology enzymatic compositions component by weight includes 6 parts of protease, 10 parts of lipase, amylase 8 part, cellulase
12 parts, 15 parts of oxidoreducing enzyme.
The preparation method of the compound deodorizer of one Plant Extracts and biological enzyme, includes the following steps:
S1: plant extract composition and zinc ricinate, ethyl alcohol, fatty glyceride are proportionally mixed, and added
It adjusts into high speed shear dispersion emulsifying machine, and by high speed shear dispersion emulsifying machine to the emulsified 60min of 8000r/min, is made
Emulsified solution is spare；
S2: the biological enzymatic compositions of corresponding proportion, potassium sorbate, deionization are added in emulsified solution obtained above
Water adjusts the emulsified 30min of high speed shear dispersion emulsifying machine 8000r/min, and compound deodorizer is made.
The preparation method of the plant extract composition includes the following steps:
A1: camellia, aloe, orange peel are weighed in proportion, and their co-grindings are spare；
A2: 20h is impregnated with the petroleum ether (60-90) of 180 parts of quality, is then filtered by vacuum, obtains first time filtered fluid
It is spare, filter residue is repeated to impregnate filtering 2 times, is filtered by vacuum, is respectively obtained second of filtered fluid and third time filtered fluid is spare；
A3: first time filtered fluid, second of filtered fluid and third time filtered fluid are sufficiently mixed filtrate and mixed, rotation is passed through
Petroleum ether therein is recycled in evaporator rectification, obtains plant extract composition.
The preparation method of the biology enzymatic compositions includes the following steps:
B1: proportionally weighing protease, lipase, amylase, cellulase, and oxidoreducing enzyme is added to mixing vessel
It is interior, and be uniformly mixed spare；
B2: at 30 DEG C, into mixing vessel, the deionized water of 1530 parts of addition, which is stirred, dissolves 40min, at 25 DEG C
Stand 3h；
B3: under the conditions of 0.5mpa, unit of activity 2000U/ml, PH6 is made in the filter membrane for being 0.01um by membrane aperture
Biological enzyme combine liquid.
B4: in biological enzyme obtained combination liquid, 8 parts of sucrose, 1 part of sodium chloride, sodium thiosulfate 0.004 is added by quality
Part, 5min is stirred to whole dissolutions, obtains biological enzymatic compositions.
Embodiment 3
The compound deodorizer of one Plant Extracts and biological enzyme, including following component by weight include: plant extract group
Close 5 parts of object, biological 20 parts of enzymatic compositions, 1 part of zinc ricinate, 0.01 part of potassium sorbate, 3 parts of ethyl alcohol, fatty glyceride 5
Part, 65.99 parts of deionized water.
Plant extract composition component by weight includes 1 part of 3 parts of camellia, 2 parts of aloe, orange peel co-grinding work
For the extract for extracting raw material.
The biology enzymatic compositions component by weight includes proteinase 8 part, 12 parts of lipase, 10 parts of amylase, cellulose
13 parts of enzyme, 14 parts of oxidoreducing enzyme.
The preparation method of the compound deodorizer of one Plant Extracts and biological enzyme, includes the following steps:
S1: plant extract composition and zinc ricinate, ethyl alcohol, fatty glyceride are proportionally mixed, and added
It adjusts into high speed shear dispersion emulsifying machine, and by high speed shear dispersion emulsifying machine to the emulsified 60min of 8000r/min, is made
Emulsified solution is spare；
S2: the biological enzymatic compositions of corresponding proportion, potassium sorbate, deionization are added in emulsified solution obtained above
Water adjusts the emulsified 30min of high speed shear dispersion emulsifying machine 8000r/min, and compound deodorizer is made.
The preparation method of the plant extract composition includes the following steps:
A1: camellia, aloe, orange peel are weighed in proportion, and their co-grindings are spare；
A2: it is impregnated for 24 hours with the petroleum ether (60-90) of 60 parts of quality, is then filtered by vacuum, obtains first time filtered fluid
It is spare, filter residue is repeated to impregnate filtering 2 times, is filtered by vacuum, is respectively obtained second of filtered fluid and third time filtered fluid is spare；
A3: first time filtered fluid, second of filtered fluid and third time filtered fluid are sufficiently mixed filtrate and mixed, rotation is passed through
Petroleum ether therein is recycled in evaporator rectification, obtains plant extract composition.
The preparation method of the biology enzymatic compositions includes the following steps:
B1: proportionally weighing protease, lipase, amylase, cellulase, and oxidoreducing enzyme is added to mixing vessel
It is interior, and be uniformly mixed spare；
B2: at 30 DEG C, into mixing vessel, the deionized water of 1710 parts of addition, which is stirred, dissolves 40min, at 25 DEG C
Stand 3h；
B3: under the conditions of 0.5mpa, unit of activity 2000U/ml, PH6 is made in the filter membrane for being 0.01um by membrane aperture
Biological enzyme combine liquid.
B4: in biological enzyme obtained combination liquid, 10 parts of sucrose, 3 parts of sodium chloride, sodium thiosulfate is added by quality
0.004 part, 5min is stirred to whole dissolutions, obtains biological enzymatic compositions.
Embodiment 4
The compound deodorizer of one Plant Extracts and biological enzyme, including following component by weight include: plant extract group
Close 5 parts of object, biological 20 parts of enzymatic compositions, 1 part of zinc ricinate, 0.03 part of potassium sorbate, 6 parts of ethyl alcohol, fatty glyceride 6
Part, 61.97 parts of deionized water.
Plant extract composition component by weight includes 2 parts of 5 parts of camellia, 3 parts of aloe, orange peel co-grindings works
For the extract for extracting raw material.
The biology enzymatic compositions component by weight includes 7 parts of protease, 11 parts of lipase, 9 parts of amylase, cellulase
11 parts, oxido-reductase 12 part.
The preparation method of the compound deodorizer of one Plant Extracts and biological enzyme, includes the following steps:
S1: plant extract composition and zinc ricinate, ethyl alcohol, fatty glyceride are proportionally mixed, and added
It adjusts into high speed shear dispersion emulsifying machine, and by high speed shear dispersion emulsifying machine to the emulsified 60min of 8000r/min, is made
Emulsified solution is spare；
S2: the biological enzymatic compositions of corresponding proportion, potassium sorbate, deionization are added in emulsified solution obtained above
Water adjusts the emulsified 30min of high speed shear dispersion emulsifying machine 8000r/min, and compound deodorizer is made.
The preparation method of the plant extract composition includes the following steps:
A1: camellia, aloe, orange peel are weighed in proportion, and their co-grindings are spare；
A2: 18h is impregnated with the petroleum ether (60-90) of 300 parts of quality, is then filtered by vacuum, obtains first time filtered fluid
It is spare, filter residue is repeated to impregnate filtering 2 times, is filtered by vacuum, is respectively obtained second of filtered fluid and third time filtered fluid is spare；
A3: first time filtered fluid, second of filtered fluid and third time filtered fluid are sufficiently mixed filtrate and mixed, rotation is passed through
Petroleum ether therein is recycled in evaporator rectification, obtains plant extract composition.
The preparation method of the biology enzymatic compositions includes the following steps:
B1: proportionally weighing protease, lipase, amylase, cellulase, and oxidoreducing enzyme is added to mixing vessel
It is interior, and be uniformly mixed spare；
B2: at 30 DEG C, into mixing vessel, the deionized water of 1500 parts of addition, which is stirred, dissolves 40min, at 25 DEG C
Stand 3h；
B3: under the conditions of 0.5mpa, unit of activity 2000U/ml, PH6 is made in the filter membrane for being 0.01um by membrane aperture
Biological enzyme combine liquid.
B4: in biological enzyme obtained combination liquid, 6 parts of sucrose, 1 part of sodium chloride, sodium thiosulfate 0.003 is added by quality
Part, 5min is stirred to whole dissolutions, obtains biological enzymatic compositions.
Comparative example 1
Other conditions are with embodiment 1, in addition to petroleum ether 200g is changed to ethyl alcohol 200g.
Comparative example 2
Other conditions are with embodiment 2, in addition to sucrose 0g, sodium chloride 0g, sodium thiosulfate 0g.
Comparative example 3
Other conditions are with embodiment 3, in addition to soaking time is 18 hours.
Comparative example 4
Other conditions are with embodiment 2, in addition to plant extract composition 25g, biological enzyme 0g.
Comparative example 5
Other conditions are with embodiment 2, in addition to plant extract composition 0g, biological enzyme 25g.
Removing and harmful gas test
1. preparing 30 air Laboratory Module (0.9m*0.9m*1.85m=1.5m3), it is specifically used as follows.
Experimental condition carries out under normal temperature and pressure conditions.
2. discharging source preparation.
It is solid with cotton thread by 5 layers of the medical absorbent cotton/gauze volume of 17cm*40cm on 30 diameter 5mm, the glass bar of long 30cm
Determine and be uprightly placed on it in reagent bottle of 500ml, is packed into 200 milliliters of pollutant, wherein 10 reagent bottles of formaldehyde, dimethylbenzene
10 reagent bottles, 10 reagent bottles of ammonia, concentration are respectively formaldehyde 0.2%, and ammonia 1%, dimethylbenzene 0.4%, various reagents are analysis
It is pure, after gauze is completely wet, it can come into operation.
2.1 hang on untreated base paper in blank assay cabin A0, B0, C0, by all groups of deodorization dilution agent
20 times, spray test base paper, and hang in each group experimental cabin.
Each reagent bottle equipped with the formaldehyde pollutants source of release prepared is respectively placed in blank assay cabin A0 and each group examination by 2.2
In hatch checking, hatch door is closed immediately.
Reagent bottle equipped with the xylene pollution object source of release prepared is respectively placed in blank assay cabin B0 and each group examination by 2.3
In hatch checking, hatch door is closed immediately.
Reagent bottle equipped with the ammonia contaminant source of release prepared is respectively placed in blank assay cabin C0 and each group experimental cabin by 2.4
In, hatch door is closed immediately.
2.5 open the fan of blank cabin and all experimental cabins, stir 1min, mix air and the pollutant of release in cabin
Afterwards, fan is simultaneously closed off, to air sampling is carried out in blank cabin A0, B0, C0, measures pollutants in air concentration value in blank cabin
For initial concentration.
The concentration of air pollutants in all cabins is sampled respectively after 2.6 2h, is tested respectively, after as deodorization 2h
The concentration value of each blank cabin and experimental cabin records data.
2.7 for 24 hours afterwards respectively sample the concentration of air pollutants in all cabins, test respectively, and as deodorization is for 24 hours
The concentration value of each blank cabin and experimental cabin afterwards records data.
The concentration of air pollutants in all cabins is sampled respectively after 2.8 7d, is tested respectively, after as deodorization 7d
The concentration value of each blank cabin and experimental cabin records data.
The sampling of 3 absorbing liquids and sampled result analysis:
The detection method of Pollutant Formaldehyde is carried out by GB/T 18204.26-2000；The detection method of dimethylbenzene presses GB/T
11737-1989 is carried out；The detection method of ammonia is carried out by GB/T 18883-2002.
Calculating of 4 deodorant to pollutants removal rate
As a result it records；Unit mg/m3
Except formaldehyde test result
| Test group | Concentration after 2h | Removal rate | Concentration after for 24 hours | Removal rate | Concentration after 7d | Removal rate |
| Blank cabin | 0.3 | / | 1.1 | / | 3.5 | / |
| Embodiment 1 | 0.018 | 94 | 0.012 | 98.91 | 0.4 | 88.57 |
| Embodiment 2 | 0.012 | 96 | 0.006 | 99.45 | 0.342 | 90.23 |
| Embodiment 3 | 0.022 | 92.67 | 0.02 | 98.08 | 0.36 | 89.71 |
| Embodiment 4 | 0.015 | 95 | 0.008 | 99.27 | 0.352 | 89.94 |
| Comparative example 1 | 0.04 | 86.67 | 0.02 | 98.18 | 0.375 | 89.29 |
| Comparative example 2 | 0.013 | 95.67 | 0.015 | 98.64 | 0.86 | 75.41 |
| Comparative example 3 | 0.035 | 88.33 | 0.022 | 98 | 0.386 | 88.98 |
| Comparative example 4 | 0.008 | 97.33 | 0.05 | 95.45 | 1.3 | 62.86 |
| Comparative example 5 | 0.08 | 73.33 | 0.046 | 95.82 | 0.39 | 88.86 |
Except dimethylbenzene test result
| Test group | Concentration after 2h | Removal rate | Concentration after for 24 hours | Removal rate | Concentration after 7d | Removal rate |
| Blank cabin | 0.72 | / | 2.16 | / | 6.43 | / |
| Embodiment 1 | 0.08 | 88.89 | 0.05 | 97.69 | 0.76 | 88.18 |
| Embodiment 2 | 0.06 | 91.67 | 0.03 | 98.61 | 0.62 | 90.36 |
| Embodiment 3 | 0.095 | 86.81 | 0.12 | 94.44 | 0.71 | 88.96 |
| Embodiment 4 | 0.066 | 90.83 | 0.05 | 97.69 | 0.68 | 89.42 |
| Comparative example 1 | 0.2 | 72.22 | 0.096 | 95.56 | 0.72 | 88.8 |
| Comparative example 2 | 0.013 | 90.56 | 0.086 | 96.02 | 2.02 | 68.58 |
| Comparative example 3 | 0.065 | 90.97 | 0.11 | 94.91 | 0.78 | 87.87 |
| Comparative example 4 | 0.05 | 93.06 | 0.05 | 97.69 | 2.5 | 61.12 |
| Comparative example 5 | 0.22 | 69.44 | 0.162 | 92.5 | 0.8 | 87.56 |
Except ammonia test result
| Test group | Concentration after 2h | Removal rate | Concentration after for 24 hours | Removal rate | Concentration after 7d | Removal rate |
| Blank cabin | 1.24 | / | 4.82 | / | 12.07 | / |
| Embodiment 1 | 0.15 | 87.9 | 0.163 | 96.62 | 1.53 | 87.32 |
| Embodiment 2 | 0.104 | 91.61 | 0.08 | 98.34 | 1.18 | 90.22 |
| Embodiment 3 | 0.175 | 85.89 | 0.261 | 94.59 | 1.42 | 88.24 |
| Embodiment 4 | 0.13 | 89.52 | 0.122 | 97.47 | 1.37 | 88.65 |
| Comparative example 1 | 0.32 | 74.19 | 0.19 | 96.06 | 1.4 | 88.4 |
| Comparative example 2 | 0.116 | 90.65 | 0.225 | 95.33 | 4.6 | 61.89 |
| Comparative example 3 | 0.12 | 90.32 | 0.23 | 95.23 | 1.56 | 87.08 |
| Comparative example 4 | 0.14 | 88.71 | 0.16 | 96.68 | 5.31 | 56.01 |
| Comparative example 5 | 0.492 | 60.32 | 0.334 | 93.07 | 1.73 | 85.67 |
Available from above-mentioned test result, the compound deodorizer of plant extraction liquid and biological enzyme has not only been gathered plant and has been mentioned
Take object deodorant and biological enzyme deodorant a little, moreover it is possible to generate the more excellent deodorizing effect in the two advantage, indices
All it is significantly increased.
Available from embodiment 1 and 1 result of comparative example, when vegetation water is extracted, petroleum ether extraction efficiency is extracted than ethyl alcohol
Effect is more excellent, and odor removal efficient is also faster.
It is available from embodiment 2 and 2 result of comparative example, although adding biological enzyme stabilizers on short time odor removal efficient
There is no significant difference, but with the extension of time, the bioenzyme activity of inanimate object enzyme stabilizers reduces, deodorizing effect weakens.Face
To environment such as new house finishing, new cars, meeting last very long discharges harmful substance, this completely new improvement is more able to satisfy this part of need
It asks.
Available from embodiment 3 and 3 result of comparative example, the length of soaking time influences plant extract purity and concentration,
To will affect the efficiency of fast deodorization.
Available from embodiment 2 and 4 result of comparative example, although simple plant extracts can be realized fast deodorization,
But it can not show a candle to the compound deodorizer of plant extracts and biological enzyme in deodorization persistence.
Available from embodiment 2 and 5 result of comparative example, the deodorization early period speed of simple biological enzyme compound deodorizer is not
And the compound deodorizer of plant extracts and biological enzyme, but after the time extends, the persistence deodorizing capability of biological enzyme is showed
Out, good deodorizing effect still can also be reached.The innovation of the compound deodorizer of plant extracts and biological enzyme is more able to satisfy
Present new house finishing, the market demand quickly moved in.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto,
Anyone skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (9)
1. the compound deodorizer of a Plant Extracts and biological enzyme, which is characterized in that including following component by weight include: plant
Object extracts 5 parts of composition, biological 20 parts of enzymatic compositions, 2-4 parts of zinc ricinate, 0.01-0.05 parts of potassium sorbate, ethyl alcohol 3-6
Part, 5-8 parts of fatty glyceride, 56.95-64.99 parts of deionized water.
2. the compound deodorizer of a Plant Extracts and biological enzyme according to claim 1, it is characterised in that: the plant
The compound deodorizer of object extract and biological enzyme includes 5 parts of plant extract composition, biological enzymatic compositions by optimal components by weight percent
20 parts, 2 parts of zinc ricinate, 0.02 part of potassium sorbate, 5 parts of ethyl alcohol, 8 parts of fatty glyceride, 59.98 parts of deionized water.
3. the compound deodorizer of a Plant Extracts and biological enzyme according to claim 1, which is characterized in that the plant
It includes 1-2 parts of 3-5 parts of camellia, 2-3 parts of aloe, orange peel co-grindings as extraction original that object, which extracts composition component by weight,
The extract of material.
4. the compound deodorizer of a Plant Extracts and biological enzyme according to claim 3, which is characterized in that the plant
Object extraction composition is smashed to be used as and be mentioned in the ratio mixing that optimal components by weight percent includes 4 parts of camellia, 3 parts of aloe, 2 parts of orange peel
Take the extracting solution of raw material.
5. the compound deodorizer of a Plant Extracts and biological enzyme according to claim 1, which is characterized in that the life
Object enzymatic compositions component by weight includes 6-8 parts of protease, 8-12 parts of lipase, 6-10 parts of amylase, cellulase 10-13
Part, -15 parts of oxido-reductase 10.
6. the compound deodorizer of a Plant Extracts and biological enzyme according to claim 5, which is characterized in that the life
Object enzymatic compositions include 6 parts of protease, 10 parts of lipase, amylase 8 part, 12 parts of cellulase, oxidation by optimal components by weight percent
Reductase 15 part.
7. a kind of preparation method of the compound deodorizer of plant extracts as described in claim 1 and biological enzyme, feature exist
In including the following steps:
S1: plant extract composition and zinc ricinate, ethyl alcohol, fatty glyceride are proportionally mixed, and are added to height
In fast shear dispersion emulsifying machine, and high speed shear dispersion emulsifying machine is adjusted to the emulsified 60min of 8000r/min, emulsification is made
Solution for standby；
S2: adding the biological enzymatic compositions of corresponding proportion, potassium sorbate in emulsified solution obtained above, and deionized water is adjusted
Compound deodorizer is made in the emulsified 30min of whole high speed shear dispersion emulsifying machine 8000r/min.
8. the according to claim 1, compound deodorizer of a Plant Extracts and biological enzyme described in 3 or 4, which is characterized in that
The preparation method of the plant extract composition includes the following steps:
A1: camellia, aloe, orange peel are weighed in proportion, and their co-grindings are spare；
A2: 18-24h is impregnated with the petroleum ether (60-90) of 10-30 times of quality of raw material after co-grinding, then carries out vacuum pumping
Filter, it is spare to obtain first time filtered fluid, and filter residue is repeated to impregnate filtering 2 times, is filtered by vacuum, respectively obtains second of filtering
Liquid and third time filtered fluid are spare；
A3: first time filtered fluid, second of filtered fluid and third time filtered fluid are sufficiently mixed filtrate and mixed, rotary evaporation is passed through
Petroleum ether therein is recycled in device rectification, obtains plant extract composition.
9. the according to claim 1, compound deodorizer of a Plant Extracts and biological enzyme described in 5 or 6, which is characterized in that
The preparation method of the biology enzymatic compositions includes the following steps:
B1: proportionally weighing protease, lipase, amylase, cellulase, and oxidoreducing enzyme is added in mixing vessel,
And it is uniformly mixed spare；
B2: at 30 DEG C, protease, lipase, amylase, cellulase, 30 times of oxidoreducing enzyme are added into mixing vessel
The deionized water of quality is stirred dissolution 40min, stands 3h at 25 DEG C；
B3: under the conditions of 0.5mpa, the life of unit of activity 2000U/ml, PH6 is made in the filter membrane for being 0.01um by membrane aperture
Object enzyme combines liquid.
B4: in biological enzyme obtained combination liquid, sucrose 5-10 parts, 1-3 parts of sodium chloride, sodium thiosulfate is added by quality
0.002-0.004 parts, 5min is stirred to whole dissolutions, obtains biological enzymatic compositions.
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| CN110585879A (en) * | 2019-09-23 | 2019-12-20 | 华川技术有限公司 | Pure natural water hyacinth deodorant liquid and preparation method thereof |
| CN110721572A (en) * | 2019-10-24 | 2020-01-24 | 深圳市绿藤环保科技有限公司 | Preparation method of extract for degrading triphenyl and triphenyl purifying agent |
| CN110833759A (en) * | 2019-10-21 | 2020-02-25 | 周加荣 | Compound enzyme and plant extract two-in-one deodorant formula and preparation method thereof |
| CN110876811A (en) * | 2019-12-03 | 2020-03-13 | 深圳市三林生物科技工程有限公司 | Water-soluble plant extract deodorant and preparation method thereof |
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| CN110585879A (en) * | 2019-09-23 | 2019-12-20 | 华川技术有限公司 | Pure natural water hyacinth deodorant liquid and preparation method thereof |
| CN110833759A (en) * | 2019-10-21 | 2020-02-25 | 周加荣 | Compound enzyme and plant extract two-in-one deodorant formula and preparation method thereof |
| CN110721572A (en) * | 2019-10-24 | 2020-01-24 | 深圳市绿藤环保科技有限公司 | Preparation method of extract for degrading triphenyl and triphenyl purifying agent |
| CN110721572B (en) * | 2019-10-24 | 2022-04-29 | 深圳如帆科技有限公司 | Preparation method of extract for degrading triphenyl and triphenyl purifying agent |
| CN110917377A (en) * | 2019-11-28 | 2020-03-27 | 北京易可多环境科技有限公司 | Novel deodorant prepared by compounding multiple plant extracts and preparation method thereof |
| CN112642284A (en) * | 2019-12-02 | 2021-04-13 | 河北福赛生物科技发展有限公司 | Process for producing deodorant by compounding biological enzyme and bamboo extract |
| CN110876811A (en) * | 2019-12-03 | 2020-03-13 | 深圳市三林生物科技工程有限公司 | Water-soluble plant extract deodorant and preparation method thereof |
| CN111298639A (en) * | 2020-03-30 | 2020-06-19 | 亚太森博（山东）浆纸有限公司 | Composition for reducing peculiar smell of wood chip storage yard, preparation method and application thereof |
| CN113170800A (en) * | 2021-04-26 | 2021-07-27 | 鹤莲祥生物医药科技有限公司 | Natural super-green biological enzyme disinfection and mildew removal deodorant |
| CN114130185A (en) * | 2021-12-06 | 2022-03-04 | 深圳市汇尚科科技有限公司 | Biological deodorant for pets and preparation method thereof |
| CN114767556A (en) * | 2022-03-31 | 2022-07-22 | 河北登尚科技有限公司 | Pet deodorant |
| CN114651732A (en) * | 2022-04-26 | 2022-06-24 | 湖南普泰尔环境股份有限公司 | Cat litter with deodorization and disinfection functions and preparation method thereof |
| CN114831137A (en) * | 2022-05-24 | 2022-08-02 | 湖南普泰尔环境股份有限公司 | Deodorant with antibacterial effect |
| CN114831137B (en) * | 2022-05-24 | 2023-06-16 | 湖南普泰尔环境股份有限公司 | Deodorant with antibacterial effect |
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Application publication date: 20190611 |