CN110833759A - Compound enzyme and plant extract two-in-one deodorant formula and preparation method thereof - Google Patents
Compound enzyme and plant extract two-in-one deodorant formula and preparation method thereof Download PDFInfo
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- CN110833759A CN110833759A CN201911008744.7A CN201911008744A CN110833759A CN 110833759 A CN110833759 A CN 110833759A CN 201911008744 A CN201911008744 A CN 201911008744A CN 110833759 A CN110833759 A CN 110833759A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/74—General processes for purification of waste gases; Apparatus or devices specially adapted therefor
- B01D53/84—Biological processes
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/74—General processes for purification of waste gases; Apparatus or devices specially adapted therefor
- B01D53/77—Liquid phase processes
- B01D53/78—Liquid phase processes with gas-liquid contact
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2251/00—Reactants
- B01D2251/95—Specific microorganisms
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2257/00—Components to be removed
- B01D2257/90—Odorous compounds not provided for in groups B01D2257/00 - B01D2257/708
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/20—Air quality improvement or preservation, e.g. vehicle emission control or emission reduction by using catalytic converters
Abstract
The invention discloses a compound enzyme and plant extract two-in-one deodorant formula and a preparation method thereof, wherein the compound enzyme and plant extract two-in-one deodorant formula comprises the following components in parts by weight: 2.0-7.5 parts of plant essential oil, 15.0-29.0 parts of plant extract composition, 10.0-23.0 parts of complex enzyme composition, 1.8-5.2 parts of alkyl glycoside, 9.5-10.0 parts of water-soluble chitosan quaternary ammonium salt, 3.0-10.0 parts of n-octanol and 30.0-250.0 parts of deionized water. The invention can effectively absorb and convert ammonia and organic amine compounds in the air, and can effectively absorb and convert malodorous gas molecules such as nitrogen compounds, sulfur compounds and the like into substances without toxicity, harm and odor. The invention has safe, green and high-efficiency components, does not produce secondary pollution and realizes zero emission.
Description
Technical Field
The invention belongs to the field of biological deodorization, and relates to a formula and a preparation method of a two-in-one deodorant containing complex enzyme and plant extracts.
Background
With the rapid development of social economy and the continuous acceleration of urbanization process, the problem of indoor and outdoor environmental pollution is increasingly prominent, and at present, more than 4000 malodorous substances can be sensed by human olfaction, which are paid more and more attention to people. The malodorous substance is a substance capable of causing odor of olfactory organsSubstances, which usually contain certain atoms or groups of atoms, also called malodorous groups, e.g. organic malodorous substances often contain hydroxyl (-OH), carbonyl (C ═ O), carboxyl (-COOH), amino (-NH)2) And mercapto (-SH) groups. In addition to functional groups, the local structure, the skeletal structure, the steric structure, etc. of the molecule often have a decisive influence on the odor. Malodorous substances are often mixtures of gaseous substances, with various interactions (e.g., additive, synergistic, counteracting, masking, etc.) between the substances. The malodorous substances directly affect the life quality of people and harm the health of people, so that how to quickly and durably remove the odor becomes the popular direction of the current research on the premise of ensuring safety.
The natural plant extract is used for deodorizing by utilizing the good decomposition and removal effect of natural active ingredients in plants on malodorous substances such as nitrogen compounds, sulfur compounds and the like. The plant extract contains abundant biological alcohol, polyphenol and terpenoid substances, and can perform chemical reactions such as oxidation reduction, neutralization and esterification with malodorous substances and physical reactions such as adsorption and dissolution to finally generate tasteless and nontoxic substances; the complex enzyme deodorization can thoroughly change organic matters such as odor and the like into tasteless substances, water and carbon dioxide. The complex enzyme has extremely high deodorization safety, does not cause secondary pollution, and can achieve long-term continuous deodorization. However, both deodorizing methods also have some disadvantages, such as the limitation of plant extract products to odor molecules; the complex enzyme can not achieve rapid deodorization and the like. Therefore, the development and the use of the deodorant with high-efficiency deodorization effect and safety have great market and ecological significance. The advantage of rapid deodorization of the plant extract is fully exerted by developing the two-in-one deodorant of the complex enzyme and the plant extract, and the variety of malodorous substances capable of being purified is increased by the synergistic effect of a plurality of complex enzymes.
The composite enzyme and plant extract two-in-one deodorant has unique advantages, the purpose of quickly and continuously removing most odor molecules is achieved through compounding of various plant extracts and the composite enzyme, and the comfort and pleasure of a user are improved due to the addition of the plant essential oil. The deodorant disclosed by the invention is safe and non-toxic to a human body, free of irritation, biodegradable, free of secondary pollution and convenient to use.
Disclosure of Invention
The invention aims to provide a composite enzyme and plant extract two-in-one deodorant, which is friendly to human beings, animals and the environment, free of toxicity or irritation, free of secondary pollution and convenient to match with other equipment.
In order to achieve the purpose of the invention, the invention provides the following technical scheme:
a complex enzyme and plant extract two-in-one deodorant is designed, and is characterized by comprising the following raw materials in parts by weight: 2.0-7.5 parts of plant essential oil, 15.0-29.0 parts of plant extract composition, 10.0-23.0 parts of complex enzyme composition, 1.8-5.2 parts of alkyl glycoside, 9.5-10.0 parts of water-soluble chitosan quaternary ammonium salt, 3.0-10.0 parts of n-octanol and 30.0-250.0 parts of deionized water.
The plant essential oil disclosed by the invention comprises one or more of the following components in parts by weight: 1.5-3.1 parts of immature bitter orange essential oil, 1.8-3.5 parts of juniper essential oil, 1.5-3.1 parts of turmeric essential oil, 0.3-1.2 parts of dill essential oil and 0.5-5.6 parts of oak bark essential oil.
The plant extract composition comprises the following components in parts by weight: 2.5-9.0 parts of cedar extract, 1.0-5.0 parts of chloranthus japonicus extract, 4.0-6.0 parts of citronella extract, 1.5-6.0 parts of sisal extract and 1.5-3.0 parts of geranium extract.
Wherein the optimal weight part combination proportion is as follows: cedar extract, chloranthus japonicus extract and geranium extract are 4: 3: 1.5.
The complex enzyme composition comprises the following components in parts by weight: 1.0-4.3 parts of polyphenol oxidase, 0.2-2.6 parts of cellulase, 0.9-5.0 parts of chymosin, 1.3-6.6 parts of mannase, 1.5-8.5 parts of subtilisin, 0.2-5.7 parts of bromelain, 1.5-4.8 parts of naringinase and 0.1-0.8 part of papain.
Wherein the optimal weight part combination proportion is as follows: cellulase, mannanase and naringinase are 2: 5: 3.
The composite enzyme and plant extract two-in-one deodorant provided by the invention comprises the following preparation steps:
(1) weighing each single enzyme according to the proportion of the prescription, and uniformly mixing in a container.
(2) Adding 15 times of deionized water to dissolve, and shaking on a water bath constant temperature shaking table at 35 ℃ for 4 h.
(3) Adding the solution into an ultrafiltration centrifugal tube (30kDa) at 3000rpm for 30min for concentration, passing through a filter membrane with the aperture of 0.01 μm under the condition of 0.3MPa to obtain a complex enzyme composition with the enzyme activity of more than 2500U/mg and the pH value of 6.0, and standing for later use.
(4) Weighing each plant extract according to the prescription, dissolving in ethanol, and mixing in a container.
(5) Stirring and mixing the plant essential oil and the alkyl glycoside uniformly at the temperature of 45 ℃, standing to room temperature, adding the mixture into the n-octanol solution in the step (4), stirring and mixing uniformly.
(6) And (3) adding the uniformly mixed solution prepared in the step (5) into the prepared complex enzyme composition solution, adding the water-soluble chitosan quaternary ammonium salt, and stirring and uniformly mixing to obtain the deodorant.
Compared with the prior art, the invention has the following beneficial effects:
the invention adopts the combination of complex enzyme and plant extract for deodorization, and is green, environment-friendly, efficient and safe. Compared with a single deodorant, the deodorant not only can increase the types of the malodorous substances removed, but also can quickly and durably exert the deodorizing effect; the deodorant is added with plant essential oil, is an extracted concentrate of natural plants, is green and safe, and can add comfortable and pleasant fragrance while deodorizing.
According to the optimal combination proportion of the single enzymes in the complex enzyme, the complex enzyme has the best removal effect on sulfur dioxide, methyl mercaptan, nitrogen oxide and the like, and also has better removal effect on escherichia coli and staphylococcus aureus.
The compound enzyme adopted by the invention is a composition of biological enzymes, so that the period of preparing the enzymes by fermenting plants or microorganisms is saved, and the enzyme activity cannot be influenced by the composition; the plant extract composition saves the extraction time and working procedure, is efficient and time-saving, and greatly improves the production efficiency.
Detailed Description
The present invention will be further described with reference to specific examples, which are set forth merely to illustrate the invention and are not to be construed as limiting the invention.
Specific example 1:
1. a composite enzyme and plant extract two-in-one deodorant comprises the following components in parts by weight:
(1) plant essential oil: 2.5 parts of immature bitter orange essential oil and 1.0 part of dill essential oil.
(2) Plant extract composition: 4.0 parts of cedar extract, 3.0 parts of chloranthus japonicus extract, 5.0 parts of citronella extract, 3.5 parts of sisal hemp extract and 1.5 parts of geranium extract.
(3) The compound enzyme composition comprises the following components: 2.0 parts of polyphenol oxidase, 2.0 parts of cellulase, 3.0 parts of chymosin, 5.0 parts of mannase, 4.4 parts of subtilisin, 3.0 parts of bromelain, 3.0 parts of naringinase and 0.4 part of papain.
(4) 3.5 parts of alkyl glycoside, 10.0 parts of water-soluble chitosan quaternary ammonium salt, 8.0 parts of n-octanol and 200.0 parts of deionized water.
2. The preparation method of the deodorant comprises the following steps:
(1) weighing each single enzyme according to the proportion of the prescription, and uniformly mixing in a container.
(2) Adding 15 times of deionized water to dissolve, and shaking on a water bath constant temperature shaking table at 35 ℃ for 4 h.
(3) Adding the solution into an ultrafiltration centrifugal tube (30kDa) at 3000rpm for 30min for concentration, passing through a filter membrane with the aperture of 0.01 μm under the condition of 0.3MPa to obtain a complex enzyme composition with the enzyme activity of more than 2500U/mg and the pH value of 6.0, and standing for later use.
(4) Weighing each plant extract according to the prescription, dissolving in n-octanol, and mixing uniformly in a container.
(5) Stirring and mixing the plant essential oil and the alkyl glycoside uniformly at the temperature of 45 ℃, standing to room temperature, adding the mixture into the n-octanol solution in the step (4), stirring and mixing uniformly.
(6) And (3) adding the uniformly mixed solution prepared in the step (5) into the prepared complex enzyme composition solution, adding the water-soluble chitosan quaternary ammonium salt, and stirring and uniformly mixing to obtain the deodorant.
Example 2:
1. a composite enzyme and plant extract two-in-one deodorant comprises the following components in parts by weight:
(1) plant essential oil: 3.4 parts of juniper essential oil, 0.3 part of dill essential oil and 0.5 part of oak bark essential oil.
(2) Plant extract composition: 6.4 parts of cedar extract, 4.8 parts of chloranthus japonicus extract, 4.5 parts of citronella extract, 3.5 parts of sisal hemp extract and 2.4 parts of geranium extract.
(3) The compound enzyme composition comprises the following components: 3.0 parts of polyphenol oxidase, 1.2 parts of cellulase, 0.9 part of chymosin, 3.0 parts of mannase, 1.5 parts of subtilisin, 3.2 parts of bromelain, 1.8 parts of naringinase and 0.5 part of papain.
(4) 1.8 parts of alkyl glycoside, 9.5 parts of water-soluble chitosan quaternary ammonium salt, 3.0 parts of n-octanol and 130.0 parts of deionized water.
2. The preparation method of the deodorant comprises the following steps:
(1) weighing each single enzyme according to the proportion of the prescription, and uniformly mixing in a container.
(2) Adding 15 times of deionized water to dissolve, and shaking on a water bath constant temperature shaking table at 35 ℃ for 4 h.
(3) Adding the solution into an ultrafiltration centrifugal tube (30kDa) at 3000rpm for 30min for concentration, passing through a filter membrane with the aperture of 0.01 μm under the condition of 0.3MPa to obtain a complex enzyme composition with the enzyme activity of more than 2500U/mg and the pH value of 6.0, and standing for later use.
(4) Weighing each plant extract according to the prescription, dissolving in n-octanol, and mixing uniformly in a container.
(5) Stirring and mixing the plant essential oil and the alkyl glycoside uniformly at the temperature of 45 ℃, standing to room temperature, adding the mixture into the n-octanol solution in the step (4), stirring and mixing uniformly.
(6) And (3) adding the uniformly mixed solution prepared in the step (5) into the prepared complex enzyme composition solution, adding the water-soluble chitosan quaternary ammonium salt, and stirring and uniformly mixing to obtain the deodorant.
Example 3:
1. a composite enzyme and plant extract two-in-one deodorant comprises the following components in parts by weight:
(1) plant essential oil: 1.6 parts of immature bitter orange essential oil, 3.1 parts of turmeric essential oil, 0.4 part of dill essential oil and 1.6 parts of oak bark essential oil.
(2) Plant extract composition: 6.4 parts of cedar extract, 4.8 parts of chloranthus japonicus extract, 5.0 parts of citronella extract, 4.0 parts of sisal hemp extract and 2.4 parts of geranium extract.
(3) The compound enzyme composition comprises the following components: 4.3 parts of polyphenol oxidase, 2.2 parts of cellulase, 1.0 part of chymosin, 5.5 parts of mannase, 3.5 parts of subtilisin, 1.7 parts of bromelain, 3.3 parts of naringinase and 0.8 part of papain.
(4) 5.2 parts of alkyl glycoside, 10.0 parts of water-soluble chitosan quaternary ammonium salt, 10.0 parts of n-octanol and 210.0 parts of deionized water.
2. The preparation method of the deodorant comprises the following steps:
(1) weighing each single enzyme according to the proportion of the prescription, and uniformly mixing in a container.
(2) Adding 15 times of deionized water to dissolve, and shaking on a water bath constant temperature shaking table at 35 ℃ for 4 h.
(3) Adding the solution into an ultrafiltration centrifugal tube (30kDa) at 3000rpm for 30min for concentration, passing through a filter membrane with the aperture of 0.01 μm under the condition of 0.3MPa to obtain a complex enzyme composition with the enzyme activity of more than 2500U/mg and the pH value of 6.0, and standing for later use.
(4) Weighing each plant extract according to the prescription, dissolving in n-octanol, and mixing uniformly in a container.
(5) Stirring and mixing the plant essential oil and the alkyl glycoside uniformly at the temperature of 45 ℃, standing to room temperature, adding the mixture into the n-octanol solution in the step (4), stirring and mixing uniformly.
(6) And (3) adding the uniformly mixed solution prepared in the step (5) into the prepared complex enzyme composition solution, adding the water-soluble chitosan quaternary ammonium salt, and stirring and uniformly mixing to obtain the deodorant.
Claims (7)
1. A compound enzyme and plant extract two-in-one deodorant formula is characterized in that the deodorant contains the following raw materials in parts by weight: 2.0-7.5 parts of plant essential oil, 15.0-29.0 parts of plant extract composition, 10.0-23.0 parts of complex enzyme composition, 1.8-5.2 parts of alkyl glycoside, 9.5-10.0 parts of water-soluble chitosan quaternary ammonium salt, 3.0-10.0 parts of n-octanol and 30.0-250.0 parts of deionized water.
2. The plant essential oil according to claim 1, characterized by comprising one or more of the following components in parts by weight: 1.5-3.1 parts of immature bitter orange essential oil, 1.8-3.5 parts of juniper essential oil, 1.5-3.1 parts of turmeric essential oil, 0.3-1.2 parts of dill essential oil and 0.5-5.6 parts of oak bark essential oil.
3. The plant extract composition according to claim 1, characterized by comprising the following components in parts by weight: 2.5-9.0 parts of cedar extract, 1.0-5.0 parts of chloranthus japonicus extract, 4.0-6.0 parts of citronella extract, 1.5-6.0 parts of sisal extract and 1.5-3.0 parts of geranium extract.
4. The plant extract composition of claim 3, wherein: wherein the optimal weight part combination ratio of the cedar extract, the chloranthus japonicus extract and the geranium extract is 4: 3: 1.5.
5. The complex enzyme composition of claim 1, which is characterized by comprising the following components in parts by weight: 1.0-4.3 parts of polyphenol oxidase, 0.2-2.6 parts of cellulase, 0.9-5.0 parts of chymosin, 1.3-6.6 parts of mannase, 1.5-8.5 parts of subtilisin, 0.2-5.7 parts of bromelain, 1.5-4.8 parts of naringinase and 0.1-0.8 part of papain.
6. The complex enzyme composition according to claim 5, characterized in that: wherein the optimal weight part combination proportion of the cellulase, the mannase and the naringinase is 2: 5: 3.
7. The compound enzyme and plant extract two-in-one deodorant formula according to claim 1, characterized in that the preparation method comprises the following steps:
(1) weighing each single enzyme according to the proportion of the prescription, and uniformly mixing in a beaker;
(2) adding 15 times of deionized water for dissolution, and shaking on a water bath constant temperature shaking table at 35 ℃ for 4 h;
(3) adding the solution into an ultrafiltration centrifugal tube (30kDa) at 3000rpm for 30min for concentration, passing through a filter membrane with the aperture of 0.01 μm under the condition of 0.3MPa to obtain a complex enzyme composition with the enzyme activity of more than 2500U/mg and the pH value of 6.0, and standing for later use;
(4) weighing each plant extract according to a prescription, dissolving in n-octanol, and mixing uniformly in a container;
(5) stirring and mixing the plant essential oil and the alkyl glycoside uniformly at the temperature of 45 ℃, standing to room temperature, adding the mixture into the n-octanol solution in the step (4), stirring and adding the mixture uniformly;
(6) and (3) adding the uniformly mixed solution prepared in the step (5) into the prepared complex enzyme composition solution, adding the water-soluble chitosan quaternary ammonium salt, and stirring and uniformly mixing to obtain the deodorant.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112603864A (en) * | 2020-12-23 | 2021-04-06 | 江苏雅博动物健康科技有限责任公司 | Deodorization spray for pets and preparation method thereof |
| CN113209812A (en) * | 2021-05-10 | 2021-08-06 | 江苏雅博动物健康科技有限责任公司 | Biological deodorization particle for pet and preparation method thereof |
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| CN109045999A (en) * | 2018-08-21 | 2018-12-21 | 南京创灵环保科技有限公司 | Compound biological enzyme deodorant and preparation method thereof |
| CN109173644A (en) * | 2018-09-21 | 2019-01-11 | 湖北煜韩环境科技有限公司 | One Plant Extracts are except formaldehyde formulations and preparation method thereof |
| CN109865423A (en) * | 2019-04-23 | 2019-06-11 | 惠州市铭铠防霉抗菌科技有限公司 | One Plant Extracts and the compound deodorizer of biological enzyme and preparation method thereof |
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Patent Citations (4)
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| CN106912503A (en) * | 2015-12-25 | 2017-07-04 | 北京绿伞化学股份有限公司 | A kind of indoor air disinfection agent and preparation method thereof |
| CN109045999A (en) * | 2018-08-21 | 2018-12-21 | 南京创灵环保科技有限公司 | Compound biological enzyme deodorant and preparation method thereof |
| CN109173644A (en) * | 2018-09-21 | 2019-01-11 | 湖北煜韩环境科技有限公司 | One Plant Extracts are except formaldehyde formulations and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112603864A (en) * | 2020-12-23 | 2021-04-06 | 江苏雅博动物健康科技有限责任公司 | Deodorization spray for pets and preparation method thereof |
| CN113209812A (en) * | 2021-05-10 | 2021-08-06 | 江苏雅博动物健康科技有限责任公司 | Biological deodorization particle for pet and preparation method thereof |
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Application publication date: 20200225 |