CN110812251A - 一种白茶自热面膜及其制备方法 - Google Patents
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Abstract
本发明公开的一种白茶自热面膜及其制备方法,包括压缩面膜基布、面膜精华液,所述面膜精华液包括1‑3份保湿剂、1‑3份渗透剂、20‑50份白茶提取物、5‑10份EGCG纳米脂质体、1‑3份植物精油、1‑3份pH缓冲剂、5‑10份增稠剂、0.5‑1份防腐剂、1‑3份复合增效剂,所述压缩面膜基布包括5‑20份小苏打、50‑70份果纤膜材,使用时能自产热,使用舒适,配合面膜精华液,提高皮肤对营养物质的吸收,抗氧化能力强、保湿性能强。
Description
技术领域
本发明涉及茶叶加工领域,具体涉及一种白茶自热面膜及其制备方法。
背景技术
白茶,属微发酵茶,是中国茶农创制的传统名茶,采摘后,不经杀青或揉捻,只经过晒或文火干燥后加工的茶,白茶提取物含有丰富的茶多酚、表没食子儿茶素没食子酸酯(EGCG)、黄酮等物质,具有治麻疹、抗癌、抗菌、抗氧化损伤、抗衰老调节免疫功能等药理活性,具有显著的抗肿瘤、抗癌、抗突变作用,但利用白茶的加工产品市面上较少。
EGCG 具有非常广泛的生物学功能,如抗氧化性、抗癌、抗心血管疾病等功效,然而由于 EGCG 本身的不稳定性,暴露在空气中易氧化变质,导致结构破坏,功能减弱。
面膜是重要的护肤、美白用品。面膜护肤的原理,就是利用覆盖在脸部的时间,暂时隔离外界空气与污染,提高肌肤温度,皮肤的毛孔扩张,促进汗腺分泌与新陈代谢,使肌肤的含氧量上升,面膜有利于肌肤排除表皮细胞新陈代谢的产物和积累的油脂类物质,面膜中的面膜液和水分渗入肌肤表皮的角质层中,皮肤变得柔软,增加弹性,但是冬天或温度低时,面膜温度过低,使得皮肤毛孔收缩,不利于皮肤对营养物质的吸收且使用面膜舒适度不高。
发明内容
为解决上述问题,本发明提供一种白茶自热面膜及其制备方法,使用时能自产热,使用舒适,配合面膜精华液,提高皮肤对营养物质的吸收,抗氧化能力强、保湿性能强。
本发明的解决的技术方案是,提供一种白茶自热面膜,包括压缩面膜基布、面膜精华液,所述面膜精华液包括1-3份保湿剂、1-3份渗透剂、20-50份白茶提取物、5-10份EGCG纳米脂质体、1-3份植物精油、1-3份pH缓冲剂、5-10份增稠剂、0.5-1份防腐剂、1-3份复合增效剂,所述压缩面膜基布包括5-20份小苏打、50-70份果纤膜材。
优选地,所述渗透剂包括透皮短肽。
优选地,所述pH缓冲剂包括羟乙基哌嗪乙烷磺酸,所述增稠剂为羧甲基纤维素钠,所述防腐剂包括山梨酸钾、尼泊金甲酯,所述保湿剂包括透明质酸、甘油。
优选地,所述复合增效剂包括维生素E、维生素B、水杨酸、烟酰胺、L-酪氨酸、海藻糖,所述植物精油包括玫瑰精油、茶树精油、熏衣草精油。
还提供一种白茶自热面膜的制备方法,包括以下步骤:S1、取苹果、香蕉、菠菜等纤维食品烘干、粉碎、过筛,得果蔬干粉;干粉经强碱浸泡、酶解、灭酶后,过滤,滤渣洗涤烘干得果纤膜材;加入小苏打溶液后混合,将混合液加入多针头静电纺丝箱中进行静电纺丝,纺丝后真空干燥后水刺加固,烘干后真空压缩,即得面膜基布;S2、取1-3份保湿剂、1-3份渗透剂、20-50份白茶提取物、5-10份EGCG纳米脂质体、1-3份植物精油、1-3份pH缓冲剂、5-10份增稠剂、0.5-1份防腐剂、1-3份复合增效剂混合均质搅拌,即得面膜精华液;
优选地,所述白茶提取物的制备方法包括以下步骤:将白茶粉碎加入至超临界萃取器中,进行超临界CO2萃取,萃取压力为27MPa、萃取温度为55℃、萃取时间为50min、65%乙醇的用量为1000mL,萃取结束后,打开超临界萃取器放油阀,收集所述白茶提取物。
优选地,所述EGCG纳米脂质体的制备方法包括以下步骤:混合吐温60、胆固醇、大豆卵磷脂及所述白茶提取物,分散均匀后,加入乙醇,在60℃下水浴至溶解,得混合液,将混合液快速注入到不断搅拌的PBS缓冲液中,搅拌10-30min,搅拌速度为90-100r/min,真空旋蒸除去乙醇,充入N2密封,置于4℃保存,即得EGCG纳米脂质体,脂质体是一种自组装胶束微粒,磷脂是最常见的脂质,常分散在水中自然形成闭合多层囊泡,每层均为脂质的双分子层,水溶性活性物质包埋于水或醇相中,脂溶性活性物质包埋在磷脂双分子层中,脂质体主要利用的是多层脂质结构对 EGCG实现包埋。
本方案的有益效果为:
1.面膜基布中的小苏打为碱性、与面膜精华液中酸性的白茶提取物茶多酚、保湿剂、pH缓冲剂等发生酸碱放热反应,使得使用时,将面膜基布浸泡于面膜精华液中,发生酸碱放热反应,贴于脸部时温度升高,使用舒适,保持皮肤毛孔打开;
2.面膜基布中的小苏打参与酸碱反应时,放出二氧化碳气体,面膜基布在浸泡面膜精华液后仍保持着细密且疏松的微孔结构,利于面膜精华液中营养成分的导入;
3.透皮短肽可通过生物学特异机制克服皮肤屏障,提高植物精油、黄酮或多酚等功能成分的透皮性,便于皮肤吸收,提高透明质酸钠、海藻糖的透皮性,保湿性能更为持久;
4.EGCG 具有非常广泛的生物学功能,如抗氧化性、抗癌、抗心血管疾病等功效,然而由于 EGCG 本身的不稳定性,暴露在空气中易氧化变质,导致结构破坏,功能减弱,利用纳米包埋技术制备EGCG纳米脂质体,以纳米脂质体作为载体,提高EGCG的稳定性及脂溶性,保护肌肤油脂层、亲肤能力更佳,且EGCG具有抗氧化功能,延缓皮肤衰老;
5.白茶提取物含有丰富的茶多酚、表没食子儿茶素没食子酸酯(EGCG)、黄酮等物质,具有治麻疹、抗癌、抗菌、抗氧化损伤、抗衰老调节免疫功能等药理活性,复合增效剂包括维生素E、维生素B、水杨酸、烟酰胺、L-酪氨酸、海藻糖,所述植物精油包括玫瑰精油、茶树精油、熏衣草精油,提高保湿性能、补充皮肤维生素、抗黑色素,并保持肌肤油脂层。
具体实施方式
为了使本发明所述的内容更加便于理解,下面结合具体实施方式对本发明所述的技术方案做进一步的说明,但是本发明不仅限于此。
实施例1
制备白茶提取物:将白茶粉碎加入至超临界萃取器中,进行超临界CO2萃取,萃取压力为27MPa、萃取温度为55℃、萃取时间为50min、65%乙醇的用量为1000mL,萃取结束后,打开超临界萃取器放油阀,收集所述白茶提取物,本实施例所用的超临界萃取器型号为SPTHA220-40-11的超临界CO2萃取装置。
实施例2
制备EGCG纳米脂质体:混合10ml吐温60、15mg胆固醇、5mg大豆卵磷脂及所述50mg白茶提取物,分散均匀后,加入乙醇,在60℃下水浴至溶解,得混合液,将混合液快速注入到不断搅拌的PBS缓冲液中,搅拌10-30min,搅拌速度为90-100r/min,真空旋蒸除去乙醇,充入N2密封,置于4℃保存,即得EGCG纳米脂质体。
实施例3
取50g苹果、50g香蕉、50g菠菜等纤维食品烘干、粉碎、过筛,得果蔬干粉;干粉经强碱浸泡、市售蛋白酶、市售水解酶40℃酶解2h、100℃灭酶后,过滤,滤渣洗涤烘干得果纤膜材;加入10g/ml的小苏打溶液后混合,将混合液加入多针头静电纺丝箱中进行静电纺丝,纺丝后真空干燥后水刺加固,烘干后真空压缩,即得面膜基布;取1g透明质酸、1g透皮短肽、20g白茶提取物、5gEGCG纳米脂质体、1g玫瑰精油、1g羟乙基哌嗪乙烷磺酸、5g羧甲基纤维素钠、0.5g山梨酸钾、1g复合增效剂,其中复合增效剂包括等质量份数的维生素E、维生素B、水杨酸、烟酰胺、L-酪氨酸、海藻糖混合均质搅拌,即得面膜精华液;
使用时,将独立包装的面膜精华液和面膜基布混合5min后再敷于脸部,保持10-20min。
实施例4
取50g苹果、50g香蕉、50g菠菜等纤维食品烘干、粉碎、过筛,得果蔬干粉;干粉经强碱浸泡、市售蛋白酶、市售水解酶40℃酶解2h、100℃灭酶后,过滤,滤渣洗涤烘干得果纤膜材;加入10g/ml的小苏打溶液后混合,将混合液加入多针头静电纺丝箱中进行静电纺丝,纺丝后真空干燥后水刺加固,烘干后真空压缩,即得面膜基布;取3g透明质酸、3g透皮短肽、50g白茶提取物、10gEGCG纳米脂质体、2g茶树精油、3g羟乙基哌嗪乙烷磺酸、10g羧甲基纤维素钠、1g尼泊金甲酯、3g复合增效剂,其中复合增效剂包括等质量份数的维生素E、维生素B、水杨酸、烟酰胺、L-酪氨酸、海藻糖混合均质搅拌,即得面膜精华液;
使用时,将独立包装的面膜精华液和面膜基布混合5min后再敷于脸部,保持10-20min。
实施例5
取50g苹果、50g香蕉、50g菠菜等纤维食品烘干、粉碎、过筛,得果蔬干粉;干粉经强碱浸泡、市售蛋白酶、市售水解酶40℃酶解2h、100℃灭酶后,过滤,滤渣洗涤烘干得果纤膜材;加入10g/ml的小苏打溶液后混合,将混合液加入多针头静电纺丝箱中进行静电纺丝,纺丝后真空干燥后水刺加固,烘干后真空压缩,即得面膜基布;取2g透明质酸、2g透皮短肽、30g白茶提取物、8gEGCG纳米脂质体、2g熏衣草精油、2g羟乙基哌嗪乙烷磺酸、8g羧甲基纤维素钠、0.8g尼泊金甲酯、2g复合增效剂,其中复合增效剂包括等质量份数的维生素E、维生素B、水杨酸、烟酰胺、L-酪氨酸、海藻糖混合均质搅拌,即得面膜精华液;
使用时,将独立包装的面膜精华液和面膜基布混合5min后再敷于脸部,保持10-20min。
以上所述仅为本发明的较佳实施例,凡依本发明申请专利范围所做的均等变化与修饰,皆应属本发明的涵盖范围。
Claims (7)
1.一种白茶自热面膜,其特征在于,包括压缩面膜基布、面膜精华液,所述面膜精华液包括1-3份保湿剂、1-3份渗透剂、20-50份白茶提取物、5-10份EGCG纳米脂质体、1-3份植物精油、1-3份pH缓冲剂、5-10份增稠剂、0.5-1份防腐剂、1-3份复合增效剂,所述压缩面膜基布包括5-20份小苏打、50-70份果纤膜材。
2.根据权利要求1所述的一种白茶自热面膜,其特征在于,所述渗透剂包括透皮短肽。
3.根据权利要求1所述的一种白茶自热面膜,其特征在于,所述pH缓冲剂包括羟乙基哌嗪乙烷磺酸,所述增稠剂为羧甲基纤维素钠,所述防腐剂包括山梨酸钾、尼泊金甲酯,所述保湿剂包括透明质酸、甘油。
4.根据权利要求1所述的一种白茶自热面膜,其特征在于,所述复合增效剂包括维生素E、维生素B、水杨酸、烟酰胺、L-酪氨酸、海藻糖,所述植物精油包括玫瑰精油、茶树精油、熏衣草精油。
5.一种如权利要求1所述白茶自热面膜的制备方法,其特征在于,包括以下步骤:S1、取苹果、香蕉、菠菜等纤维食品烘干、粉碎、过筛,得果蔬干粉;干粉经强碱浸泡、酶解、灭酶后,过滤,滤渣洗涤烘干得果纤膜材;加入小苏打溶液后混合,将混合液加入多针头静电纺丝箱中进行静电纺丝,纺丝后真空干燥后水刺加固,烘干后真空压缩,即得面膜基布;S2、取1-3份保湿剂、1-3份渗透剂、20-50份白茶提取物、5-10份EGCG纳米脂质体、1-3份植物精油、1-3份pH缓冲剂、5-10份增稠剂、0.5-1份防腐剂、1-3份复合增效剂混合均质搅拌,即得面膜精华液。
6.根据权利要求5所述的一种白茶自热面膜的制备方法,其特征在于,所述白茶提取物的制备方法包括以下步骤:将白茶粉碎加入至超临界萃取器中,进行超临界CO2萃取,萃取压力为27MPa、萃取温度为55℃、萃取时间为50min、65%乙醇的用量为1000mL,萃取结束后,打开超临界萃取器放油阀,收集所述白茶提取物。
7.根据权利要求6所述的一种白茶自热面膜的制备方法,其特征在于,所述EGCG纳米脂质体的制备方法包括以下步骤:混合吐温60、胆固醇、大豆卵磷脂及所述白茶提取物,分散均匀后,加入乙醇,在60℃下水浴至溶解,得混合液,将混合液快速注入到不断搅拌的PBS缓冲液中,搅拌10-30min,搅拌速度为90-100r/min,真空旋蒸除去乙醇,充入N2密封,置于4℃保存,即得EGCG纳米脂质体。
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