CN110810680A - 一种含玉米黄质的明目枸杞饮料 - Google Patents
一种含玉米黄质的明目枸杞饮料 Download PDFInfo
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- CN110810680A CN110810680A CN201911217110.2A CN201911217110A CN110810680A CN 110810680 A CN110810680 A CN 110810680A CN 201911217110 A CN201911217110 A CN 201911217110A CN 110810680 A CN110810680 A CN 110810680A
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- China
- Prior art keywords
- zeaxanthin
- extract
- medlar
- fructus lycii
- extraction
- Prior art date
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Links
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Classifications
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- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
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- A—HUMAN NECESSITIES
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- A—HUMAN NECESSITIES
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- A—HUMAN NECESSITIES
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- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
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- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
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Abstract
本发明公开了一种含玉米黄质的明目枸杞饮料,以鲜枸杞、复水枸杞打浆得到枸杞果浆、酶解、亚临界液态萃取、真空脱溶得到玉米黄质双棕榈酸酯提取物,然后加工制作成不同含量的玉米黄质双棕榈酸酯微囊粉末和玉米黄质微囊,以此作为明目功能成分制备枸杞饮料,饮料的配比为:枸杞汁或发酵枸杞汁5—50%、白砂糖5—10%、牛磺酸0.01—1%、决明子提取物0.1—5%、菊花提取物0.1—5%、蓝莓汁0—5%、葡萄籽提取物0.1—5%、维生素C0.01—1%、低聚糖0.1—1%,叶黄素0.001—0.01%、阿拉伯糖若干、玉米黄质双棕榈酸酯微囊或玉米黄质微囊若干、酸味剂、稳定剂、乳化剂若干。
Description
本发明是申请号为2017110746110、发明名称为“一种从液态枸杞原料中提取玉米黄质双棕榈酸酯的方法”的分案申请,原申请日为2017-11-05。
技术领域:
本发明属于生物提取领域,具体地说是涉及一种含玉米黄质的明目枸杞饮料。
技术背景:
枸杞中含有丰富的类胡萝卜素、枸杞黄酮、枸杞多糖、甜菜碱、单糖、双糖、核黄素、牛磺酸、不饱和脂肪酸,及十八种氨基酸和十九种必需微量元素。类胡萝卜素包括玉米黄素及其酯类、酸浆果红素、隐黄质、β-胡萝卜素,其中具有明目功能的玉米黄质是所有水果中最高者。
关于枸杞的深加工及综合利用,已公开的技术有《超临界枸杞渣粕萃取物及其生产方法》(CN 100400133C),其技术方案采用超临界萃取技术,萃取物的主要成分是枸杞籽油,油酸和亚油酸等脂肪酸占到萃取物的90%以上,玉米黄质仅含0.6%~0.7%,提取成本高,效率较低。授权公告日为2016.03.16发明专利“从枸杞、枸杞废渣中提取玉米黄质的方法”(CN103130698B)发明专利,该技术方案将枸杞或枸杞渣粕分离成枸杞籽和枸杞果肉,分别萃取可以得到高浓度玉米黄质提取物和高纯度的枸杞籽,该方法以固体原料进行提取,鲜果需要干燥才能提取,加大提取成本。目前还没有发现直接以鲜枸杞或枸杞汁、枸杞浆为原料进行综合提取玉米黄质双棕榈酸酯和玉米黄质、黄酮、多糖、甜菜碱的报道,也未见到从枸杞中分离膳食纤维和枸杞蛋白质的报道,也未见到利用枸杞制作枸杞糖浆的报道,更未见到用枸杞加工残留糖类进行饲料酵母培养的报道。现有提取方法生产成本较高,枸杞原料的综合利用率较低。
发明内容:
原发明提供一种从液态枸杞原料中提取玉米黄质双棕榈酸酯的方法,解决了现有技术提取成本高,效率低的技术问题,改进玉米黄质双棕榈酸酯的提取工艺,解决了以鲜枸杞或以液态原料进行提取的技术问题,提高枸杞的综合利用率。
本发明提供一种利用液态枸杞原料中提取的玉米黄质双棕榈酸酯以及玉米黄质来制备明目枸杞饮料方法。
从液态枸杞原料中提取玉米黄质双棕榈酸酯的步骤如下:
1)枸杞原料预处理得枸杞浆,然后在得到的枸杞浆中添加果胶酶、纤维素酶进行酶解;
进一步地,述所述枸杞原料预处理是指干枸杞复水、枸杞渣复水,打浆去籽得枸杞浆;
进一步地,述所述枸杞原料预处理是指鲜枸杞清洗、打浆去籽,浓缩得枸杞浆;
进一步地,述所述枸杞原料预处理是指鲜枸杞、复水枸杞、复水枸杞渣打浆去籽得枸杞果浆,在枸杞果浆中加入原料重量0—100%的枸杞全粉,搅拌均匀得枸杞浆;
更进一步地,所加的枸杞全粉为粒度在300目以上的破壁枸杞粉。
进一步地,鲜枸杞和一定比例的干枸杞一起打浆得枸杞浆。
2)将酶解后的枸杞浆加入萃取系统,加入萃取剂,密闭萃取,萃取压力保持在0.4—0.5Mpa,萃取系统可设置回流喷淋,也可设置搅拌;达到平衡时将萃取剂回收进解析罐,解压使提取物析出,回收萃取剂,收集玉米黄质双棕榈酸酯提取物,经过若干级萃取,完成萃取的枸杞浆则从萃取罐底放出。
也可进行多级逆流萃取,将酶解后的枸杞果浆加入多级逆流萃取系统的第一个萃取罐中,加入来自下一级(新鲜萃取剂)的萃取剂,进行密闭萃取,萃取时可进行搅拌,也可回流,萃取压力保持在0.4—0.5Mpa,达到平衡时将萃取剂回收进解析罐,解压使提取物析出,回收萃取剂,收集玉米黄质双棕榈酸酯提取物,果浆则进入下一级萃取罐,加入来自下一级(新鲜萃取剂)的萃取剂进行萃取,达到平衡时将含有提取物的萃取剂回收进暂存罐,通入第一萃取罐进行萃取,果浆则进入第三级萃取罐。如此经过若干级萃取,完成萃取的枸杞浆则从最后一级萃取罐底放出;枸杞浆的流向与萃取剂的流向相反,从进入萃取系统到排出萃取系统,玉米黄质双棕榈酸酯的含量逐步降低,经若干级萃取后直至为零;萃取剂则相反,经过若干级萃取后其中的玉米黄质双棕榈酸酯的含量逐步升高,直至第一级萃取后达到最高而解压析出。萃取剂进入萃取罐的输送和萃取时压力保持在0.4—0.5Mpa。
进一步的,所述萃取剂是亚临界流体,是丙烷、丁烷、异丁烷(R600a)、1,1,1,2-四氟乙烷(R134a)、二甲醚(DME)、液化石油气(LPG)和六氟化硫中的一种。
进一步的,萃取剂回收是通过压缩机进行回收。
进一步的,在加入新鲜萃取剂时加入原料重量0—10%的乙酸乙酯。
3)收集到的玉米黄质双棕榈酸酯提取物进行真空脱溶,直到提取物中萃取剂残留量低于8ppm,收集玉米黄质双棕榈酸酯提取物;
4)得到的玉米黄质双棕榈酸酯提取物制作成不同含量的玉米黄质双棕榈酸酯微囊粉末;
一种提取枸杞中玉米黄质的方法,玉米黄质双棕榈酸酯提取物进行皂化、分离、结晶、干燥得到纯品玉米黄质,得到的纯品玉米黄质制作成不同玉米黄质含量的微囊粉末。
一种含有玉米黄质的明目枸杞饮料,其特征在于具有以下重量百分比的组成:
枸杞汁或发酵枸杞汁5—50%、白砂糖5—10%、牛磺酸0.01—1%、决明子提取物0.1—5%、菊花提取物0.1—5%、蓝莓汁1—5%、葡萄籽提取物0.1—5%、维生素C0.01—1%、低聚糖0.1—1%,叶黄素0.001—0.1%、阿拉伯糖若干、上述玉米黄质双棕榈酸酯微囊或玉米黄质微囊若干、酸味剂、稳定剂、乳化剂若干,其余为水。进一步地,所述阿拉伯糖的添加量是白砂糖的3—5%;进一步地,所述明目枸杞饮料中玉米黄质和叶黄素的含量比是1:5。
本发明取得以下有益效果:
1.本发明以枸杞鲜果或枸杞干果、枸杞渣复水制得的枸杞浆,枸杞浓缩汁为原料,从液态原料中提取玉米黄质双棕榈酸酯及其玉米黄质,扩大了玉米黄质提取的原料范围,降低了提取成本。
2.本发明鲜枸杞和干枸杞结合使用,省却了浓缩的工艺,实现节能降耗,降低了生产成本。
3.鲜枸杞、复水枸杞、复水枸杞渣打浆去籽得枸杞果浆,在枸杞果浆中加入原料重量0—100%的枸杞全粉的枸杞原料的预处理方案,既达到了枸杞汁浓缩的目的,实现节能降耗,又使提取物含有一定量的脂肪酸,更方便提取物玉米黄质双棕榈酸酯的收集。
4.本发明萃取剂采用亚临界流体,萃取效率高,萃取剂回收是通过压缩机进行,同现有技术相比节约能耗。
具体实施例
实施例1
从液态枸杞原料中提取玉米黄质双棕榈酸酯的步骤如下:
1)枸杞原料预处理,干枸杞或枸杞渣加入1-5倍的水进行复水打浆,除去枸杞籽得到枸杞果浆,浆中添加果胶酶、纤维素酶进行酶解,然后高压均质。
2)将酶解后的枸杞浆加入萃取系统,加入萃取剂,密闭萃取,萃取压力保持在0.4—0.5Mpa,萃取系统可设置回流喷淋,也可设置搅拌;达到平衡时将萃取剂回收进解析罐,解压使提取物析出,回收萃取剂,收集玉米黄质双棕榈酸酯提取物,经过若干级萃取,完成萃取的枸杞浆则从萃取罐底放出。所用萃取剂是丙烷、丁烷、异丁烷(R600a)、1,1,1,2-四氟乙烷(R134a)、二甲醚(DME)、液化石油气(LPG)和六氟化硫中的一种,本实施例采用丁烷作为萃取剂。萃取剂回收是通过压缩机进行回收。为了便于提取物的收集,在加入新鲜萃取剂时加入原料重量0%的乙酸乙酯。
3)收集到的玉米黄质双棕榈酸酯提取物进行真空脱溶,直到提取物中萃取剂残留量低于8ppm,收集玉米黄质双棕榈酸酯提取物。
4)得到的玉米黄质双棕榈酸酯提取物溶解,乳化,选择食品胶作为壁材通过喷雾干燥制作成不同含量的玉米黄质双棕榈酸酯微囊粉末。
将上面所得的玉米黄质双棕榈酸酯提取物进行皂化、分离、结晶、干燥得到纯品玉米黄质,得到的纯品玉米黄质溶解,乳化,以纤维素或食品胶作为壁材进行喷雾干燥制作成不同玉米黄质含量的微囊粉末。
一种含有玉米黄质的明目枸杞饮料,具有以下重量百分比的组成:枸杞汁5%、白砂糖10%、牛磺酸0.1%、决明子提取物0.1%、菊花提取物0.5%、蓝莓汁1.5%、葡萄籽提取物0.15%、维生素C0.01%、低聚糖0.11%,叶黄素0.0008%、阿拉伯糖0.15%、提取得到的玉米黄质双棕榈酸酯微囊或玉米黄质微囊若干,使饮料中玉米黄质和叶黄素的含量比是1:5,酸味剂、稳定剂、乳化剂若干,其余为水。
一种含有玉米黄质的明目枸杞饮料,其特征在于具有以下重量百分比的组成:发酵枸杞汁5%、白砂糖10%、牛磺酸0.1%、决明子提取物0.1%、菊花提取物0.5%、蓝莓汁1.5%、葡萄籽提取物0.15%、维生素C0.01%、低聚糖0.11%,叶黄素0.0005%、阿拉伯糖0.15%、玉米黄质双棕榈酸酯微囊或玉米黄质微囊若干,使饮料中玉米黄质和叶黄素的含量比是1:5,酸味剂、稳定剂、乳化剂若干,其余为水。
实施例2
从液态枸杞原料中提取玉米黄质双棕榈酸酯的步骤如下:
2)枸杞原料预处理,干枸杞或枸杞渣加入1-5倍的水进行复水打浆,除去枸杞籽得到枸杞果浆,浆中添加果胶酶、纤维素酶进行酶解,然后高压均质。
2)将酶解后的枸杞果浆加入多级逆流萃取系统的第一个萃取罐中,加入来自下一级(新鲜萃取剂)的萃取剂,开启回流和搅拌进行密闭萃取,萃取压力保持在0.4—0.5Mpa,达到平衡时将萃取剂回收进解析罐,解压使提取物析出,回收萃取剂,收集玉米黄质双棕榈酸酯提取物,果浆则进入下一级萃取罐,加入来自下一级(新鲜萃取剂)的萃取剂进行萃取,达到平衡时将含有提取物的萃取剂回收进暂存罐,通入第一萃取罐进行萃取,果浆则进入第三级萃取罐。如此经过若干级萃取,完成萃取的枸杞浆则从最后一级萃取罐底放出;枸杞浆的流向与萃取剂的流向相反,从进入萃取系统到排出萃取系统,玉米黄质双棕榈酸酯的含量逐步降低,经若干级萃取后直至为零;萃取剂则相反,经过若干级萃取后其中的玉米黄质双棕榈酸酯的含量逐步升高,直至第一级萃取后达到最高而解压析出。萃取剂进入萃取罐的输送和萃取时压力保持在0.4—0.5Mpa。所用萃取剂是丙烷、丁烷、异丁烷(R600a)、1,1,1,2-四氟乙烷(R134a)、二甲醚(DME)、液化石油气(LPG)和六氟化硫中的一种,本实施例采用丁烷作为萃取剂。萃取剂回收是通过压缩机进行回收。为了便于提取物的收集,在加入新鲜萃取剂时加入原料重量0%的乙酸乙酯。
3)收集到的玉米黄质双棕榈酸酯提取物进行真空脱溶,直到提取物中萃取剂残留量低于8ppm,收集玉米黄质双棕榈酸酯提取物。
4)得到的玉米黄质双棕榈酸酯提取物溶解,乳化,选择食品胶作为壁材通过喷雾干燥制作成不同含量的玉米黄质双棕榈酸酯微囊粉末。
将上面所得的玉米黄质双棕榈酸酯提取物进行皂化、分离、结晶、干燥得到纯品玉米黄质,得到的纯品玉米黄质溶解,乳化,以纤维素或食品胶作为壁材进行喷雾干燥制作成不同玉米黄质含量的微囊粉末。
一种含有玉米黄质的明目枸杞饮料,其特征在于具有以下重量百分比的组成:枸杞汁5%、白砂糖10%、牛磺酸0.1%、决明子提取物0.1%、菊花提取物0.5%、蓝莓汁1.5%、葡萄籽提取物0.15%、维生素C0.01%、低聚糖0.11%,叶黄素0.0008%、阿拉伯糖0.15%、提取得到的玉米黄质双棕榈酸酯微囊或玉米黄质微囊若干,使饮料中玉米黄质和叶黄素的含量比是1:5,酸味剂、稳定剂、乳化剂若干,其余为水。
一种含有玉米黄质的明目枸杞饮料,其特征在于具有以下重量百分比的组成:发酵枸杞汁5%、白砂糖10%、牛磺酸0.1%、决明子提取物0.1%、菊花提取物0.5%、蓝莓汁1.5%、葡萄籽提取物0.15%、维生素C0.01%、低聚糖0.11%,叶黄素0.0005%、阿拉伯糖0.15%、玉米黄质双棕榈酸酯微囊或玉米黄质微囊若干,使饮料中玉米黄质和叶黄素的含量比是1:5,酸味剂、稳定剂、乳化剂若干,其余为水。
实施例3
从液态枸杞原料中提取玉米黄质双棕榈酸酯的步骤如下:
1)枸杞原料预处理,鲜枸杞清洗打浆除去枸杞籽后浓缩得枸杞浆,添加果胶酶、纤维素酶进行酶解,然后高压均质。
2)将酶解后的枸杞果浆加入多级逆流萃取系统的第一个萃取罐中,加入来自下一级(新鲜萃取剂)的萃取剂,开启回流和搅拌进行密闭萃取,萃取压力保持在0.4—0.5Mpa,达到平衡时将萃取剂回收进解析罐,解压使提取物析出,回收萃取剂,收集玉米黄质双棕榈酸酯提取物,果浆则进入下一级萃取罐,加入来自下一级(新鲜萃取剂)的萃取剂进行萃取,达到平衡时将含有提取物的萃取剂回收进暂存罐,通入第一萃取罐进行萃取,果浆则进入第三级萃取罐。如此经过若干级萃取,完成萃取的枸杞浆则从最后一级萃取罐底放出;枸杞浆的流向与萃取剂的流向相反,从进入萃取系统到排出萃取系统,玉米黄质双棕榈酸酯的含量逐步降低,经若干级萃取后直至为零;萃取剂则相反,经过若干级萃取后其中的玉米黄质双棕榈酸酯的含量逐步升高,直至第一级萃取后达到最高而解压析出。萃取剂进入萃取罐的输送和萃取时压力保持在0.4—0.5Mpa。所用萃取剂是丙烷、丁烷、异丁烷(R600a)、1,1,1,2-四氟乙烷(R134a)、二甲醚(DME)、液化石油气(LPG)和六氟化硫中的一种,本实施例采用丁烷作为萃取剂。萃取剂回收是通过压缩机进行回收。为了便于提取物的收集,在加入新鲜萃取剂时加入原料重量10%的乙酸乙酯。
3)收集到的玉米黄质双棕榈酸酯提取物进行真空脱溶,直到提取物中萃取剂残留量低于8ppm,收集玉米黄质双棕榈酸酯提取物。
4)得到的玉米黄质双棕榈酸酯提取物溶解,乳化,选择食品胶作为壁材通过喷雾干燥制作成不同含量的玉米黄质双棕榈酸酯微囊粉末。
将上面所得的玉米黄质双棕榈酸酯提取物进行皂化、分离、结晶、干燥得到纯品玉米黄质,得到的纯品玉米黄质溶解,乳化,以纤维素或食品胶作为壁材进行喷雾干燥制作成不同玉米黄质含量的微囊粉末。
一种含有玉米黄质的明目枸杞饮料,其特征在于具有以下重量百分比的组成:枸杞汁10%、白砂糖8%、牛磺酸0.1%、决明子提取物0.2%、菊花提取物0.5%、蓝莓汁0.5%、葡萄籽提取物0.15%、维生素C0.01%、低聚糖0.11%,叶黄素0.0009%、阿拉伯糖0.15%、提取得到的玉米黄质双棕榈酸酯微囊或玉米黄质微囊若干,使饮料中玉米黄质和叶黄素的含量比是1:5,酸味剂、稳定剂、乳化剂若干,其余为水。
一种含有玉米黄质的明目枸杞饮料,其特征在于具有以下重量百分比的组成:发酵枸杞汁10%、白砂糖10%、牛磺酸0.15%、决明子提取物0.21%、菊花提取物0.5%、蓝莓汁0.5%、葡萄籽提取物0.45%、维生素C0.02%、低聚糖0.11%,叶黄素0.0006%、阿拉伯糖0.15%、玉米黄质双棕榈酸酯微囊或玉米黄质微囊若干,使饮料中玉米黄质和叶黄素的含量比是1:5,酸味剂、稳定剂、乳化剂若干,其余为水。
实施例4
从液态枸杞原料中提取玉米黄质双棕榈酸酯的步骤如下:
1)枸杞原料预处理,鲜枸杞、复水枸杞、复水枸杞渣打浆去籽,得枸杞果浆,加入原料重量0—100%的枸杞全粉,搅拌溶解得到枸杞浆,添加果胶酶、纤维素酶进行酶解,然后高压均质,所用枸杞全粉为粒度在300目以上的破壁枸杞粉。
2)将酶解后的枸杞果浆加入多级逆流萃取系统的第一个萃取罐中,加入来自下一级(新鲜萃取剂)的萃取剂,开启回流和搅拌进行密闭萃取,萃取压力保持在0.4—0.5Mpa,达到平衡时将萃取剂回收进解析罐,解压使提取物析出,回收萃取剂,收集玉米黄质双棕榈酸酯提取物,果浆则进入下一级萃取罐,加入来自下一级(新鲜萃取剂)的萃取剂进行萃取,达到平衡时将含有提取物的萃取剂回收进暂存罐,通入第一萃取罐进行萃取,果浆则进入第三级萃取罐。如此经过若干级萃取,完成萃取的枸杞浆则从最后一级萃取罐底放出;枸杞浆的流向与萃取剂的流向相反,从进入萃取系统到排出萃取系统,玉米黄质双棕榈酸酯的含量逐步降低,经若干级萃取后直至为零;萃取剂则相反,经过若干级萃取后其中的玉米黄质双棕榈酸酯的含量逐步升高,直至第一级萃取后达到最高而解压析出。萃取剂进入萃取罐的输送和萃取时压力保持在0.4—0.5Mpa。所用萃取剂是丙烷、丁烷、异丁烷(R600a)、1,1,1,2-四氟乙烷(R134a)、二甲醚(DME)、液化石油气(LPG)和六氟化硫中的一种,本实施例采用丁烷作为萃取剂。萃取剂回收是通过压缩机进行回收。为了便于提取物的收集,在加入新鲜萃取剂时加入原料重量5%的乙酸乙酯。
3)收集到的玉米黄质双棕榈酸酯提取物进行真空脱溶,直到提取物中萃取剂残留量低于8ppm,收集玉米黄质双棕榈酸酯提取物。
4)得到的玉米黄质双棕榈酸酯提取物溶解,乳化,选择食品胶作为壁材通过喷雾干燥制作成不同含量的玉米黄质双棕榈酸酯微囊粉末。
将上面所得的玉米黄质双棕榈酸酯提取物进行皂化、分离、结晶、干燥得到纯品玉米黄质,得到的纯品玉米黄质溶解,乳化,以纤维素或食品胶作为壁材进行喷雾干燥制作成不同玉米黄质含量的微囊粉末。
一种含有玉米黄质的明目枸杞饮料,其特征在于具有以下重量百分比的组成:枸杞汁20%、白砂糖7%、牛磺酸0.15%、决明子提取物0.3%、菊花提取物0.25%、蓝莓汁1.5%、葡萄籽提取物0.25%、维生素C0.01%、低聚糖0.11%,叶黄素0.005%、阿拉伯糖0.15%、提取得到的玉米黄质双棕榈酸酯微囊或玉米黄质微囊若干,使饮料中玉米黄质和叶黄素的含量比是1:5,酸味剂、稳定剂、乳化剂若干,其余为水。
一种含有玉米黄质的明目枸杞饮料,其特征在于具有以下重量百分比的组成:发酵枸杞汁25%、白砂糖8%、牛磺酸0.21%、决明子提取物0.31%、菊花提取物0.45%、蓝莓汁1.25%、葡萄籽提取物0.25%、维生素C0.01%、低聚糖0.11%,叶黄素0.0005%、阿拉伯糖0.15%、玉米黄质双棕榈酸酯微囊或玉米黄质微囊若干,使饮料中玉米黄质和叶黄素的含量比是1:5,酸味剂、稳定剂、乳化剂若干,其余为水。
实施例5
从液态枸杞原料中提取玉米黄质双棕榈酸酯的步骤如下:
1)枸杞原料预处理,鲜枸杞和干枸杞按1:1的比例一起打浆得枸杞浆,在上述枸杞浆中添加果胶酶、纤维素酶进行酶解,然后高压均质。
2)将酶解后的枸杞果浆加入多级逆流萃取系统的第一个萃取罐中,加入来自下一级(新鲜萃取剂)的萃取剂,开启回流和搅拌进行密闭萃取,萃取压力保持在0.4—0.5Mpa,达到平衡时将萃取剂回收进解析罐,解压使提取物析出,回收萃取剂,收集玉米黄质双棕榈酸酯提取物,果浆则进入下一级萃取罐,加入来自下一级(新鲜萃取剂)的萃取剂进行萃取,达到平衡时将含有提取物的萃取剂回收进暂存罐,通入第一萃取罐进行萃取,果浆则进入第三级萃取罐。如此经过若干级萃取,完成萃取的枸杞浆则从最后一级萃取罐底放出;枸杞浆的流向与萃取剂的流向相反,从进入萃取系统到排出萃取系统,玉米黄质双棕榈酸酯的含量逐步降低,经若干级萃取后直至为零;萃取剂则相反,经过若干级萃取后其中的玉米黄质双棕榈酸酯的含量逐步升高,直至第一级萃取后达到最高而解压析出。萃取剂进入萃取罐的输送和萃取时压力保持在0.4—0.5Mpa。所用萃取剂是丙烷、丁烷、异丁烷(R600a)、1,1,1,2-四氟乙烷(R134a)、二甲醚(DME)、液化石油气(LPG)和六氟化硫中的一种,本实施例采用丁烷作为萃取剂。萃取剂回收是通过压缩机进行回收。为了便于提取物的收集,在加入新鲜萃取剂时加入原料重量7%的乙酸乙酯。
3)收集到的玉米黄质双棕榈酸酯提取物进行真空脱溶,直到提取物中萃取剂残留量低于8ppm,收集玉米黄质双棕榈酸酯提取物。
4)得到的玉米黄质双棕榈酸酯提取物溶解,乳化,选择食品胶作为壁材通过喷雾干燥制作成不同含量的玉米黄质双棕榈酸酯微囊粉末。
将上面所得的玉米黄质双棕榈酸酯提取物进行皂化、分离、结晶、干燥得到纯品玉米黄质,得到的纯品玉米黄质溶解,乳化,以纤维素或食品胶作为壁材进行喷雾干燥制作成不同玉米黄质含量的微囊粉末。
一种含有玉米黄质的明目枸杞饮料,其特征在于具有以下重量百分比的组成:发酵枸杞汁50%、白砂糖5%、牛磺酸0.21%、决明子提取物0.3%、菊花提取物0.25%、蓝莓汁0.5%、葡萄籽提取物0.85%、维生素C0.01%、低聚糖0.21%,叶黄素0.005%、阿拉伯糖0.15%、玉米黄质双棕榈酸酯微囊或玉米黄质微囊若干,使饮料中玉米黄质和叶黄素的含量比是1:5,酸味剂、稳定剂、乳化剂若干,其余为水。
一种枸杞粉丝,含枸杞(干基)10%,含提取出的玉米黄质双棕榈酸酯或玉米黄质中的一种或两种,其添加量以控制枸杞粉丝中的玉米黄质的含量(质量百分比)在0.0009%,将枸杞粉碎成300目以上的枸杞粉,在淀粉中加入枸杞粉和玉米黄质双棕榈酸酯,混合,加水打糊、调粉、真空脱气、漏粉、煮粉、冷却、冷冻、解冻、干燥而成枸杞粉丝。
本发明不仅限于上述实施例。
上述实施例虽然对本发明的具体实施方案进行了描述,但是,本领域技术人员应该认识到,在不偏离本发明的精神和范围的前提下,可以对本发明进行多种改变与修饰,其结果都在本发明的保护范围之内。
Claims (1)
1.一种含玉米黄质的明目枸杞饮料,其重量百分比组成:枸杞汁或发酵枸杞汁5—50%、白砂糖5—10%、牛磺酸0.01—1%、决明子提取物0.1—5%、菊花提取物0.1—5%、蓝莓汁0—5%、葡萄籽提取物0.1—5%、维生素C0.01—1%、低聚糖0.1—1%,叶黄素0.001—0.01%、阿拉伯糖若干、玉米黄质双棕榈酸酯微囊或玉米黄质微囊若干、酸味剂、稳定剂、乳化剂若干,其余为水;所述阿拉伯糖的添加量是白砂糖的3—5%;所述玉米黄质和叶黄素的含量比是1:5;所述玉米黄质双棕榈酸酯微囊和玉米黄质微囊的制备方法如下:
1)枸杞原料预处理,包括干枸杞复水、枸杞渣复水,打浆去籽得枸杞浆;鲜枸杞清洗、打浆去籽得枸杞浆;鲜枸杞、复水枸杞、复水枸杞渣打浆去籽得枸杞果浆,在枸杞果浆中加入原料重量0—100%的枸杞全粉,搅拌均匀得枸杞浆;鲜枸杞和一定比例的干枸杞一起打浆得枸杞浆;枸杞全粉溶解得枸杞浆;然后在得到的枸杞浆中添加果胶酶、纤维素酶进行酶解;
2)将酶解后的枸杞浆加入萃取系统,加入萃取剂,进行密闭萃取,萃取压力保持在0.1—10Mpa,达到平衡时将萃取剂回收进解析罐,解压使提取物析出,回收萃取剂,收集玉米黄质双棕榈酸酯提取物,经过若干级萃取,完成萃取的枸杞浆则从萃取罐底放出;所述萃取剂回收是通过压缩机进行回收;所述萃取剂是丙烷、丁烷、异丁烷(R600a)、1,1,1,2-四氟乙烷(R134a)、二甲醚(DME)、液化石油气(LPG)、二氧化碳和六氟化硫中的一种;
3)收集到的玉米黄质双棕榈酸酯提取物进行真空脱溶,直到提取物萃取剂残留量低于8ppm,收集得到玉米黄质双棕榈酸酯提取物;
4)得到的玉米黄质双棕榈酸酯提取物制作成不同含量的玉米黄质双棕榈酸酯微囊粉末;
5)得到的玉米黄质双棕榈酸酯提取物进行皂化、分离、结晶、干燥得到纯品玉米黄质;纯品玉米黄质进一步制作成不同玉米黄质含量的微囊粉末。
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