CN110770280B - 用于制备烷氧基官能有机氢硅氧烷低聚物的方法 - Google Patents

用于制备烷氧基官能有机氢硅氧烷低聚物的方法 Download PDF

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CN110770280B
CN110770280B CN201880038458.2A CN201880038458A CN110770280B CN 110770280 B CN110770280 B CN 110770280B CN 201880038458 A CN201880038458 A CN 201880038458A CN 110770280 B CN110770280 B CN 110770280B
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hydrocarbon group
sio
functional
formula
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CN110770280A (zh
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M·奥尔森
J·戈恩德隆
周晓源
W·约翰逊
C·马钱德
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Dow Silicones Corp
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Dow Corning Corp
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04—Polysiloxanes
    • C08G77/06—Preparatory processes
    • C08G77/08—Preparatory processes characterised by the catalysts used
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/24—Phosphines, i.e. phosphorus bonded to only carbon atoms, or to both carbon and hydrogen atoms, including e.g. sp2-hybridised phosphorus compounds such as phosphabenzene, phosphole or anionic phospholide ligands
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04—Polysiloxanes
    • C08G77/045—Polysiloxanes containing less than 25 silicon atoms
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04—Polysiloxanes
    • C08G77/12—Polysiloxanes containing silicon bound to hydrogen
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04—Polysiloxanes
    • C08G77/14—Polysiloxanes containing silicon bound to oxygen-containing groups
    • C08G77/18—Polysiloxanes containing silicon bound to oxygen-containing groups to alkoxy or aryloxy groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04—Polysiloxanes
    • C08G77/38—Polysiloxanes modified by chemical after-treatment
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L83/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon only; Compositions of derivatives of such polymers
    • C08L83/04—Polysiloxanes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2231/00—Catalytic reactions performed with catalysts classified in B01J31/00
    • B01J2231/40—Substitution reactions at carbon centres, e.g. C-C or C-X, i.e. carbon-hetero atom, cross-coupling, C-H activation or ring-opening reactions
    • B01J2231/44—Allylic alkylation, amination, alkoxylation or analogues
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/80—Complexes comprising metals of Group VIII as the central metal
    • B01J2531/82—Metals of the platinum group
    • B01J2531/822—Rhodium
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/48—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule in which at least two but not all the silicon atoms are connected by linkages other than oxygen atoms
    • C08G77/50—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule in which at least two but not all the silicon atoms are connected by linkages other than oxygen atoms by carbon linkages
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/70—Siloxanes defined by use of the MDTQ nomenclature

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • General Chemical & Material Sciences (AREA)
  • Silicon Polymers (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
CN201880038458.2A 2017-06-26 2018-06-26 用于制备烷氧基官能有机氢硅氧烷低聚物的方法 Active CN110770280B (zh)

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US201762524636P 2017-06-26 2017-06-26
US62/524636 2017-06-26
PCT/US2018/039377 WO2019005710A1 (en) 2017-06-26 2018-06-26 METHOD FOR HYDROSILYLATION OF ALIPHATICALLY UNSATURATED ALCOXYSILANES AND HYDROGENICALLY TERMINATED ORGANOSILOXANE OLIGOMERS FOR PREPARING ALCOXYSILYL-TERMINATED POLYMERS USEFUL FOR FUNCTIONALIZING POLYORGANOSILOXANES USING A RHODIUM CATALYST

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WO (1) WO2019005710A1 (enExample)

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EP3768793B1 (en) 2018-03-19 2023-09-27 Dow Silicones Corporation Polyorganosiloxane hot melt adhesive compositions containing polyolefin - polydiorganoosiloxane copolymers and methods for the preparation and use thereof
KR102798860B1 (ko) 2018-12-21 2025-04-25 다우 실리콘즈 코포레이션 다작용성 유기실록산, 이를 함유하는 조성물, 및 이의 제조 방법
WO2020131365A1 (en) 2018-12-21 2020-06-25 Dow Silicones Corporation Method for preparing a functionalized polyorganosiloxane
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KR102814239B1 (ko) 2018-12-21 2025-05-29 다우 실리콘즈 코포레이션 다작용성 유기실록산, 이를 함유하는 조성물, 및 이의 제조 방법
JP7121190B2 (ja) * 2019-09-11 2022-08-17 ダウ シリコーンズ コーポレーション アルコキシ官能性オルガノハイドロジェンシロキサンオリゴマーの調製方法及び当該オリゴマーの使用
CA3114661C (en) * 2019-09-11 2022-03-22 Dow Silicones Corporation Method for the preparation use of an alkoxy-functional organohydrogensiloxane oligomer using purified starting materials and use of the oligomer
US11466037B2 (en) * 2019-10-31 2022-10-11 Nata Semiconductor Materials Co., Ltd. Catalysis of dehydrocoupling reactions between amines and silanes
WO2021262492A1 (en) * 2020-06-24 2021-12-30 Dow Silicones Corporation Composition and method for silyl hydride reaction catalyzed by fluorinated arylborane lewis acids
CN116234858B (zh) * 2020-06-24 2025-05-06 美国陶氏有机硅公司 用于由氟化芳基硼烷路易斯酸催化的使有机硅化合物与硅基氢化物反应的组合物和方法
JP2023534152A (ja) * 2020-07-06 2023-08-08 ダウ シリコーンズ コーポレーション 触媒、レドックススイッチ触媒系、及びヒドロシリル化を伴う関連方法
JP7780513B2 (ja) * 2020-09-24 2025-12-04 ダウ シリコーンズ コーポレーション シリルエステル化合物の調製方法及び使用
CN114698378B (zh) * 2020-10-28 2023-04-14 美国陶氏有机硅公司 三烷氧基官能化支化硅氧烷组合物
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CN119053644A (zh) 2022-05-04 2024-11-29 美国陶氏有机硅公司 硅酮-聚醚共聚物、包含硅酮-聚醚共聚物的密封剂和相关方法
JP2025519575A (ja) 2022-06-15 2025-06-26 ダウ グローバル テクノロジーズ エルエルシー ホスホニウム塩を含む硬化性ポリオルガノシロキサン組成物並びにその調製方法及び使用
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CN110770280A (zh) 2020-02-07
JP7189157B2 (ja) 2022-12-13
WO2019005710A1 (en) 2019-01-03
EP3645606B1 (en) 2024-06-26
US20200140618A1 (en) 2020-05-07
JP2020525562A (ja) 2020-08-27
EP3645606A1 (en) 2020-05-06
US11098163B2 (en) 2021-08-24

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