CN110574961A - Preparation method of lemon essence for cigarettes, and bead blasting cigarettes for cigarettes - Google Patents
Preparation method of lemon essence for cigarettes, and bead blasting cigarettes for cigarettes Download PDFInfo
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- CN110574961A CN110574961A CN201810586879.0A CN201810586879A CN110574961A CN 110574961 A CN110574961 A CN 110574961A CN 201810586879 A CN201810586879 A CN 201810586879A CN 110574961 A CN110574961 A CN 110574961A
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- lemon
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
Abstract
The invention discloses a preparation method of lemon essence for cigarettes, and beads and bead-blasting cigarettes for cigarettes, wherein the preparation method of the lemon essence for cigarettes comprises the following steps: (1) grinding dry lemon slices into lemon powder serving as a raw material, taking a solvent for tobacco as a dispersing agent, and carrying out high-pressure homogenization treatment on a mixed solution of the raw material and the dispersing agent to obtain a homogenized solution; wherein the mass ratio of the raw material to the dispersing agent is 1 per thousand-10%, the temperature of the high-pressure homogenization treatment is-20-0 ℃, and the pressure is 10 MPa-200 MPa; (2) and centrifuging the homogeneous solution, and collecting the centrifuged supernatant to obtain the lemon essence for the cigarettes.
Description
Technical Field
The invention relates to a preparation method of lemon essence for cigarettes, and beads and bead-blasting cigarettes for cigarettes, and belongs to the field of preparation of essence spices for cigarettes.
Background
The filter tip of the cigarette is added with the bead blasting to be made into bead blasting cigarette, which becomes a product popular in the market in recent years. The most critical experience of the bead-blasting cigarette in the smoking process is the style conversion, and the conversion needs to be right, namely the bead-blasting cigarette needs to be coordinated with the cigarette fragrance and is smooth and excessive, so that a smoker feels the right experience. The essence for popping beads has various tastes, such as the widely known mint taste, and the product has the Wanbao Luo of Juxin, Feimo in Japan. At present, the method is limited by the wall materials of the blasting beads, and most of the blasting beads are oil-soluble essence blasting beads. In recent years, the application of natural flavors is more and more emphasized in the flavor and fragrance for cigarettes, natural flavors of different styles are screened, and a proper processing method is applied to obtain the special and natural bead-popping cigarettes with good harmony with the fragrance of the cigarettes, so that the flavor and fragrance for cigarettes is one of the important directions of the research on the bead-popping cigarettes at present.
Disclosure of Invention
The invention solves the technical problem that the solvent suitable for the tobacco bead blasting is used as a dispersing agent, dry lemon slices or fresh lemons are ground or subjected to wall breaking cooking, the mixed solution is subjected to high-pressure homogenization treatment and centrifugation, and the natural lemon bead blasting essence is directly obtained.
The technical scheme of the invention is to provide a preparation method of lemon essence for cigarettes, which comprises the following steps:
(1) Grinding dry lemon slices into lemon powder serving as a raw material, taking a solvent for tobacco as a dispersing agent, and carrying out high-pressure homogenization treatment on a mixed solution of the raw material and the dispersing agent to obtain a homogenized solution; wherein the mass ratio of the raw material to the dispersing agent is 1 per thousand-10%, the temperature of the high-pressure homogenization treatment is-20-0 ℃, and the pressure is 10 MPa-200 MPa;
(2) and centrifuging the homogeneous solution, and collecting the centrifuged supernatant to obtain the lemon essence for the cigarettes.
Preferably, the mass ratio of the raw material to the dispersing agent is 5 per thousand to 5 percent. The mass percentage of the raw material of the dry lemon slice and the dispersing agent is determined according to the minimum identification concentration of lemon flavor sensed by a consumer and the coordination tolerance of the lemon flavor and the tobacco fragrance. The lemon concentration is higher, the lemon flavor is stronger, and is easier to be identified by consumers, but the stronger the lemon flavor is, the better the lemon flavor is, and whether the lemon flavor is coordinated with the tobacco flavor or not and the cost are also considered. The percentage of the two is 1 per thousand to 10 percent, preferably 5 per thousand to 5 percent through repeated experiments and sensory evaluation.
Preferably, the solvent for tobacco is caprylic capric glyceride or edible vegetable oil.
Preferably, the temperature of the high-pressure homogenization treatment is-20 ℃ to-10 ℃, and the pressure of the high-pressure homogenization treatment is 10MPa to 150 MPa.
Preferably, a two-stage homogenization process is used for high-pressure homogenization, and the number of times of high-pressure homogenization is 5-18. High-pressure homogenization is carried out at the temperature of 0 ℃ to-20 ℃ under circulating cooling, and the temperature of the whole homogenized liquid is ensured not to exceed 50 ℃. In the high-pressure homogenizing process, the local instantaneous high pressure of the homogenizing valve can reach 200MPa, so if a low-temperature cooling circulating device is not arranged, the local temperature overheating can influence the quality of the natural lemons, and the conclusion is also obtained through multiple tests and sensory evaluation.
The homogenization treatment of the present invention is substantially high-pressure homogenization. The high-pressure homogenization is two-stage homogenization, and each sample is generally homogenized for 5-18 times, preferably 10-15 times. Two-stage homogenization makes the final dispersion more uniform, and the number of homogenization times of each sample is verified through multiple experiments. Too few homogenization times or too large maximum particle size are not favorable for dissolving out aroma components in the lemon raw material, and too many homogenization times consume energy and time.
Preferably, the mesh number of the raw material is not less than 30 meshes.
Preferably, the raw materials further comprise black tea and/or green tea powder. The raw materials can also be lemon and black tea or lemon and green tea, respectively grinding dried lemon slice and dried tea into powder, dispersing with dispersant, or dispersing fresh lemon, mixing with tea powder/tea dust, and homogenizing under high pressure.
Preferably, fresh lemons are used as raw materials to replace the lemon powder, the mixed solution of the fresh lemons and the dispersing agent is subjected to wall breaking treatment, and then the mixed solution obtained after the wall breaking treatment is subjected to high-pressure homogenization treatment.
The used lemon raw material can also be fresh lemon or green lemon, dispersing with a dispersant, breaking the wall, and performing high-pressure homogenization treatment on the obtained mixed solution. At present, the wall material of the blasting bead is only suitable for oil-soluble solvent essence, so that dry lemon slices are preferably used as raw materials at the present stage, and the dry lemon slices obtained by low-temperature quick drying are preferably selected, so that the natural fragrance of the lemon is kept from being damaged; the wall material of the blasting bead can be further improved in the future, and the blasting bead is suitable for water-soluble and alcohol-soluble essence and spice, and fresh lemon or green lemon can be used as the raw material of lemon essence at the moment.
The invention also provides the lemon essence for cigarettes prepared by the preparation method.
The invention also provides a bead for blasting cigarettes, which consists of a sealed shell consisting of wall materials and liquid essence in the shell, wherein the liquid essence contains the lemon essence for the cigarettes.
the invention also provides a bead blasting cigarette, wherein the bead blasting cigarette is arranged in the tobacco filter tip.
The technical core of the invention is high-pressure homogenization treatment of lemon raw materials under a dispersion system, grinding dry lemon slices into powder as a raw material, taking an explosion bead applicable solvent as a dispersing agent, carrying out high-pressure homogenization treatment, carrying out instant high-pressure (up to 200MPa) slit extrusion on the dispersion system (raw materials plus the dispersing agent) through a valve assembly under high pressure, carrying out repeated high-pressure slit extrusion for many times, carrying out instant high-pressure extrusion to break cell walls, wherein the particle diameter of the lemon particles is smaller and smaller, and effective aroma components in the lemon particles can be fully dissolved and separated out. The mass ratio of the raw material to the dispersing agent is 1 per thousand to 10 percent, the solid phase and the liquid phase are stirred and dispersed into a uniform suspension state, the solid phase and the liquid phase are subjected to high-pressure homogenization treatment at the low temperature of 0 ℃ to-20 ℃, the temperature of the homogenized liquid is not more than 50 ℃, the homogenized liquid is subjected to repeated circulation homogenization, the supernatant is taken to obtain the lemon essence, 10 mul to 25 mul of bead blasting is prepared according to the requirement, and the lemon essence is added to a cigarette filter tip to prepare the bead blasting cigarette.
Preferably, the "solvent for tobacco" is a solvent suitable for use in making a bead for a cigarette. The preparation of the prior popping beads is only suitable for oil-soluble essence, the solvent (dispersant) is mainly caprylic/capric glyceride and various edible vegetable oils, and under the condition, the preparation of the lemon essence takes the oil-soluble solvent caprylic/capric glyceride, olive oil, salad oil, soybean oil and the like as the dispersant; with the improvement of the wall material of the blasting bead, the water-soluble essence is also used for manufacturing the blasting bead, and at this time, the dispersant of the invention can also be a water-soluble dispersant (such as water, ethanol, glycerol, propylene glycol or a mixture of two, three or four of the water, ethanol, glycerol and propylene glycol), which mainly depends on the applicability of the wall material of the blasting bead.
The pressure of the high-pressure homogenizing treatment is less than 200MPa, and the pressure is generally controlled to be 10 MPa-150 MPa. When homogenizing under high pressure, the pressure is gradually increased from 10 MPa.
The lemon essence has the beneficial effects that the lemon essence is obtained through a simple and easily-obtained preparation process under mild conditions, the natural lemon raw materials are not damaged by high-temperature heating, and the fragrance is not lost due to complex processes such as concentration, air extraction and the like, so that the lemon essence is natural and pure, is harmonious and natural with the tobacco fragrance, and gives people fresh and cool smoking experience.
Detailed Description
The invention is further described with reference to specific examples. The following examples are intended to illustrate the invention without further limiting it.
Example 1
Comparative experiments were made on control and test samples: grinding 200g of dry lemon slices into lemon powder with the mesh number of 80 meshes by using a low-temperature grinding machine, dispersing 9900g of caprylic-capric glyceride, rotating at high speed to disperse the lemon powder into a uniform suspension, weighing the lemon powder and equally dividing the lemon powder into two parts, and using one part as a control sample; and (3) performing high-pressure homogenization treatment on the other part: the homogenizing pressure is gradually increased from 10MPa to 130MPa, the homogenization is circulated for 10 times, the homogenizing component is placed in the low-temperature cooling circulation at the temperature of 0 ℃ to-5 ℃, and the homogenized sample is used as a test sample. The soaking time of the control sample and the test sample in the dispersing agent is completely the same, and the experimental result shows that: the control sample directly smells the smell and is light; the test sample is directly smelled to have obvious lemon flavor. Further processing, respectively centrifuging the control sample and the test sample, removing residues, collecting the clear liquid, making into bead blasting cigarette. The evaluation of smoking evaluation shows that after the control sample is pinched and broken, the lemon flavor is not obvious, while the test sample can feel more obvious lemon flavor. The high-pressure homogenization treatment can well dissolve and separate out the aroma components in the lemon, and the lemon flavor can be well reflected.
Example 2
Grinding 50g of dry lemon slices into lemon powder with the mesh number of 100 meshes by using a low-temperature grinding machine, dispersing 4900g of caprylic capric glyceride, rotating and dispersing at high speed to form a uniform suspension shape, homogenizing for 15 times at high pressure, gradually applying force from 10MPa to 150MPa, placing a homogenizing assembly in a low-temperature cooling circulation at the temperature of-10 to-20 ℃, pouring supernatant after homogenizing, centrifuging a part containing a small amount of suspended matters at the lower layer to obtain supernatant, combining the supernatants, and making the supernatant into 20 mu l of bead blasting standard to prepare the lemon bead blasting cigarette. Sensory evaluation shows that the oral cavity has obvious salivation promoting effect.
Example 3
Grinding 250g of black tea and 50g of dry lemon slices into black tea lemon powder with the mesh number of 60 meshes by using a low-temperature grinding machine, dispersing by using 4700g of caprylic capric glyceride, rotating at a high speed to disperse the black tea lemon powder into a uniform suspension, homogenizing for 12 times at a high pressure, gradually applying force from 10MPa to 140MPa, placing a homogenizing component in a low-temperature cooling circulation at the temperature of between-5 and-10 ℃, pouring supernatant liquid after the homogenization is finished, centrifuging a part of the lower layer containing a small amount of suspended matters to obtain clear liquid, combining the clear liquid, and making the clear liquid into 22 mu l of specification of popping beads to prepare the lemon black tea popping bead cigarette. Sensory evaluation shows that the broken bead is pinched during the smoking process, and the comfortable lemon tea can be obviously felt and is harmonious and natural with the tobacco fragrance.
Example 4
Grinding 250g of green tea and 50g of dry lemon slices into green tea lemon powder with the mesh number of 60 meshes by using a low-temperature grinding machine, dispersing the green tea lemon powder with 4700g of caprylic capric glyceride, rotating and dispersing the green tea lemon powder into a uniform suspension state at a high speed, homogenizing the green tea lemon powder for 12 times at a high pressure, gradually applying force from 10MPa to 140MPa, placing a homogenizing component in a low-temperature cooling circulation at the temperature of between-5 and-10 ℃, pouring supernatant liquid after homogenization, centrifuging a part containing a small amount of suspended matters at the lower layer, taking the supernatant liquid, combining the supernatant liquid, and making the supernatant liquid into 22 mu l of poplocks to prepare the lemon green tea pop. According to sensory evaluation, the bead breaking during smoking is achieved, and compared with example 3, the lemon green tea is slightly poorer in coordination than the lemon black tea.
Example 5
Grinding 50g of dry lemon slices into lemon powder with the mesh number of 100 meshes by using a low-temperature grinding machine, dispersing 4900g of caprylic capric glyceride, rotating and dispersing at high speed to form a uniform suspension shape, homogenizing for 15 times at high pressure, gradually applying force from 10MPa to 150MPa, placing a homogenizing assembly in a low-temperature cooling circulation at the temperature of-10 to-20 ℃, pouring supernatant after homogenizing, centrifuging a part containing a small amount of suspended matters at the lower layer to obtain supernatant, combining the supernatants, and making the supernatant into 20 mu l of bead blasting standard to prepare the lemon bead blasting cigarette. Sensory evaluation shows that compared with the example 2, the sensory difference is small, the lemon flavor bead blasting is obvious in body fluid generation, and the lemon flavor bead blasting is harmonious and natural with the tobacco fragrance.
Claims (11)
1. The preparation method of the lemon essence for cigarettes is characterized by comprising the following steps:
(1) Grinding dry lemon slices into lemon powder serving as a raw material, taking a solvent for tobacco as a dispersing agent, and carrying out high-pressure homogenization treatment on a mixed solution of the raw material and the dispersing agent to obtain a homogenized solution; wherein the mass ratio of the raw material to the dispersing agent is 1 per thousand-10%, the temperature of the high-pressure homogenization treatment is-20-0 ℃, and the pressure is 10 MPa-200 MPa;
(2) And centrifuging the homogeneous solution, and collecting the centrifuged supernatant to obtain the lemon essence for the cigarettes.
2. The production method according to claim 1, wherein the mass ratio of the raw material to the dispersant is 5% o to 5%.
3. The method according to claim 1, wherein the solvent for tobacco is caprylic/capric glyceride or edible vegetable oil.
4. The method according to claim 1, wherein the temperature of the high-pressure homogenization treatment is from-20 ℃ to-10 ℃, and the pressure of the high-pressure homogenization treatment is from 10MPa to 150 MPa.
5. The method according to claim 1, wherein the high-pressure homogenization is performed by a two-stage homogenization process, and the number of times of the high-pressure homogenization is 5 to 18.
6. The method of claim 1, wherein the mesh size of the starting material is not less than 30 mesh.
7. The method of claim 1, wherein the raw material further comprises black tea and/or green tea powder.
8. The preparation method according to claim 1, wherein fresh lemon is used as a raw material instead of the lemon powder, the mixed solution of the fresh lemon and the dispersing agent is subjected to wall breaking treatment, and then the mixed solution obtained after the wall breaking treatment is subjected to high-pressure homogenization treatment.
9. the lemon essence for cigarettes prepared by the preparation method of any one of claims 1 to 8.
10. a bead for blasting cigarettes, which consists of a sealed shell consisting of a wall material and liquid essence in the shell, and is characterized in that the liquid essence contains the lemon essence for the cigarettes as claimed in claim 9.
11. A bead blasting cigarette characterized in that the bead blasting for cigarette according to claim 10 is provided in a tobacco filter.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810586879.0A CN110574961A (en) | 2018-06-08 | 2018-06-08 | Preparation method of lemon essence for cigarettes, and bead blasting cigarettes for cigarettes |
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| CN201810586879.0A CN110574961A (en) | 2018-06-08 | 2018-06-08 | Preparation method of lemon essence for cigarettes, and bead blasting cigarettes for cigarettes |
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| CN110574961A true CN110574961A (en) | 2019-12-17 |
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| CN101558143A (en) * | 2006-12-13 | 2009-10-14 | 日本烟草产业株式会社 | Perfumed beads and filter for cigarette |
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| CN106617253A (en) * | 2015-11-04 | 2017-05-10 | 立场电子科技发展（上海）有限公司 | Method for preparing electronic cigarette essence from green tea |
| CN106666822A (en) * | 2016-11-29 | 2017-05-17 | 将军烟草集团有限公司 | Cigarette blast bead and preparation method thereof |
| CN107223757A (en) * | 2017-04-26 | 2017-10-03 | 江西九草铁皮石斛科技协同创新有限公司 | A kind of chewing gum containing dendrobium candidum and preparation method thereof |
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2018
- 2018-06-08 CN CN201810586879.0A patent/CN110574961A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101558143A (en) * | 2006-12-13 | 2009-10-14 | 日本烟草产业株式会社 | Perfumed beads and filter for cigarette |
| US20160374388A1 (en) * | 2015-06-03 | 2016-12-29 | Andrew Jon Thomson | Terpene profile replication blends and their applications |
| CN106617253A (en) * | 2015-11-04 | 2017-05-10 | 立场电子科技发展（上海）有限公司 | Method for preparing electronic cigarette essence from green tea |
| CN106108106A (en) * | 2016-06-30 | 2016-11-16 | 云南中烟工业有限责任公司 | A kind of cloud produces the high static pressure of essential oil of tobaccos and extracts the method with sterilization fresh and application simultaneously |
| CN106047487A (en) * | 2016-07-19 | 2016-10-26 | 湖北中烟工业有限责任公司 | Fruit sweet scent essence for cigarette dripping pills and application |
| CN106666822A (en) * | 2016-11-29 | 2017-05-17 | 将军烟草集团有限公司 | Cigarette blast bead and preparation method thereof |
| CN107223757A (en) * | 2017-04-26 | 2017-10-03 | 江西九草铁皮石斛科技协同创新有限公司 | A kind of chewing gum containing dendrobium candidum and preparation method thereof |
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Application publication date: 20191217 |