CN110574962B - Preparation method of tea-flavored essence for cigarettes and cigarette explosion beads and explosion bead cigarettes - Google Patents
Preparation method of tea-flavored essence for cigarettes and cigarette explosion beads and explosion bead cigarettes Download PDFInfo
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- CN110574962B CN110574962B CN201810587596.8A CN201810587596A CN110574962B CN 110574962 B CN110574962 B CN 110574962B CN 201810587596 A CN201810587596 A CN 201810587596A CN 110574962 B CN110574962 B CN 110574962B
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
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Abstract
The invention discloses a preparation method of tea-flavored essence for cigarettes and explosive beads and explosive bead cigarettes for cigarettes. The preparation method of the tea aroma essence for the cigarettes comprises the following steps: (1) Taking tea powder and/or tea dust as raw materials, taking a tobacco solvent as a dispersing agent, and carrying out high-pressure homogenization treatment on the obtained mixed solution to obtain a homogenized solution; wherein the mass ratio of the raw materials to the dispersing agent is 1 per mill-15%, the temperature of high-pressure homogenization treatment is-20-0 ℃ and the pressure is 10-200 MPa; (2) Centrifuging the homogenized liquid, and collecting supernatant after centrifugation to obtain the tea essence for cigarettes. The tea-flavored essence for cigarettes is used for manufacturing the cigarette bead-explosion cigarettes and manufacturing the tea-flavored bead-explosion cigarettes.
Description
Technical Field
The invention relates to a preparation method of tea-flavored essence for cigarettes, and explosive beads and explosive bead cigarettes for cigarettes, belonging to the field of essence and flavor preparation.
Background
Tea leaves and tobacco leaves belong to important stem leaf cash crops, so that the old people who smoke are always people who like tea, how to combine tea and tobacco together is always a dream of tobacco research workers. Tea is generally hot water for drinking, most of the tea is water-soluble substances, oral cavity feeling is dominant, nasal cavity feeling is secondary, smoke is absorbed through burning or heating, and nasal cavity feeling and oral cavity feeling are combined, so that the consumption modes of the tea and the cigarette are obviously different; in addition, the aroma and taste of the tea are relatively light, namely the concentration of aroma-causing components is not high, and the conventional tea extraction process usually involves a high-temperature heating extraction and concentration process, so that the aroma-causing components in the tea can be chemically changed or carried away by air flow, the aroma quality is changed, or the style is changed, and the original aroma characteristics of the tea are difficult to maintain. How to coordinate the tea and tobacco flavors is also critical for such research. The cigarette filter tip is added with the bursting beads to prepare bursting bead cigarettes, which become products popular in the market in recent years. The essence for bursting beads has various tastes such as the well-known peppermint taste, and the product has the seven stars in Japan and the Wanbao way of Feimo. At present, most of the oil-soluble essence explosion beads are limited by explosion bead wall materials. Screening different kinds of tea leaves, attempting to obtain tea leaf extracts through a simple and mild preparation process, keeping the original juice and flavor of the tea leaves, and making the tea leaves into pop beads is one of important research directions for realizing tea and smoke fusion.
Disclosure of Invention
The invention solves the technical problems that the solvent suitable for the tobacco bursting beads is used as a dispersing agent, tea is subjected to high-pressure homogenization treatment and centrifugation to directly obtain the tea essence, and the tea essence has the advantages of simple manufacturing process, mild conditions, light processing at low temperature, no complex processes of high-temperature heating extraction, concentration and the like, so that the obtained tea essence well maintains the original flavor of tea aroma, the original aroma of the tea is revealed, and the tea aroma and the tobacco aroma are coordinated and natural.
The technical scheme of the invention is that the preparation method of the tea aroma essence for cigarettes comprises the following steps:
(1) Taking tea powder and/or tea dust as raw materials, taking tobacco solvent as a dispersing agent, and carrying out high-pressure homogenization treatment on the mixed solution of the tobacco solvent to obtain homogenized solution; wherein the mass ratio of the raw materials to the dispersing agent is 1 per mill to 15 percent, the temperature of the homogenization treatment is-20 ℃ to 0 ℃ and the pressure is 10MPa to 200MPa;
(2) Centrifuging the homogenized liquid, and collecting supernatant after centrifugation to obtain the tea essence for cigarettes.
Preferably, the raw materials account for 1 to 8 percent of the mass of the dispersing agent. The mass ratio of tea powder or tea dust raw material to the dispersing agent is determined according to the minimum identification concentration for the consumers to perceive the tea flavor and the coordination tolerance of the tea flavor and the tobacco flavor. The higher the tea strength, the stronger the tea flavor and the tea taste, and the consumer can easily identify the tea flavor and the tea taste, but the stronger the tea flavor and the better the tea taste, and whether the tea flavor and the tea taste are coordinated with the tobacco flavor or not is considered. The percentage of the two components is 1 per mill to 15 percent, preferably 1 to 8 percent, obtained by repeated experiments and sensory evaluation.
Preferably, the dispersant is caprylic capric glyceride or edible vegetable oil.
Preferably, the temperature of the high-pressure homogenization treatment is-20 ℃ to-10 ℃.
Preferably, the mesh number of the raw material is not less than 30 mesh.
Preferably, the pressure of the high-pressure homogenizing treatment is gradually increased from small to large, and the range is 10MPa to 200MPa.
High-pressure homogenization is carried out at 0 ℃ to minus 20 ℃ in a circulating cooling way, so that the temperature of the whole homogenized liquid is ensured not to exceed 50 ℃. In the high-pressure homogenizing process, the local instantaneous high pressure of the homogenizing valve can reach 200MPa, so that if a low-temperature cooling circulation device is not added, the quality of the tea aroma is affected by local temperature overheating, and the conclusion is also obtained through multiple tests and sensory evaluation.
Preferably, the homogenization treatment is performed using a secondary homogenization process, with a number of homogenization between 5 and 18. The homogenization treatment of the present invention is essentially high pressure homogenization. The high-pressure homogenization is secondary homogenization, and is generally carried out 5 to 18 times, preferably 10 to 15 times, on each sample. The secondary homogenization makes the final dispersion system more uniform, and the homogenization times of each sample are obtained through multiple experimental verification. Too little homogenization or too large maximum particle size is unfavorable for dissolving out aroma components in the tea, and too much homogenization is energy-consuming and time-consuming.
Preferably, the preparation method of the tea aroma essence for cigarettes comprises the steps.
The invention provides the tea-flavored essence for cigarettes, which is prepared by the preparation method.
The invention provides a cigarette explosion bead which consists of a sealed shell formed by wall materials and liquid essence in the shell, wherein the liquid essence comprises the cigarette tea essence.
The invention provides a bead-blasting cigarette, wherein the bead-blasting cigarette is arranged in a tobacco filter tip.
The technical core of the invention is that the high-pressure homogenization treatment of tea raw materials under a dispersion system takes tea powder as raw materials, takes a solvent suitable for bursting beads as a dispersing agent, carries out the high-pressure homogenization treatment, and the high-pressure homogenization passes through a dispersion system (raw materials and dispersing agent) of the tea which is extruded by a slit under the instant high pressure (up to 200 MPa) of a valve component, and after repeated high-pressure slit extrusion, the cell wall is crushed under the instant high-pressure extrusion, the grain size of the tea is smaller and smaller, and the effective aroma components in the tea can be fully dissolved and separated out. The mass ratio of the raw materials to the dispersing agent is 1 per mill-15%, the solid phase and the liquid phase are stirred and dispersed into uniform suspension, the high pressure homogenization treatment is carried out under the low temperature of 0 ℃ to minus 20 ℃, the temperature of the homogenized liquid is not more than 50 ℃, the homogenization is carried out for multiple times, the centrifugation is carried out, the deslagging is carried out, the supernatant fluid is taken to obtain the tea-flavor essence substrate, 10 mul-25 ul standard bursting beads are manufactured according to the requirement, and the bursting beads are added into a cigarette holder rod to manufacture the bursting bead cigarette.
Preferably, the "tobacco solvent" is a solvent suitable for use in making tobacco popping beads. The preparation of the present pop beads is only suitable for oil-soluble essence, the solvent (dispersing agent) is usually mainly caprylic/capric glyceride and various edible vegetable oils, in this case, the preparation of the tea essence of the present invention uses the oil-soluble solvent caprylic/capric glyceride, olive oil, salad oil, soybean oil and the like as dispersing agents; with the improvement of the explosion bead wall material, the water-soluble essence is also used for manufacturing the explosion beads, and the dispersing agent can be water-soluble dispersing agent (such as water, ethanol, glycerol and propylene glycol) at the moment, which mainly depends on the applicability of the explosion bead wall material.
The pressure of high-pressure homogenization treatment is less than 200MPa, and the pressure is generally controlled to be 10-150 MPa. In the high-pressure homogenization, the pressure is gradually increased from 10 MPa.
Tea powder or tea dust including green tea, black tea, oolong tea, black tea, yellow tea, white tea, preferably green tea. According to the development requirement of the bead-bursting cigarettes, the tea leaves of various kinds can be prepared into the corresponding tea-flavored essence, and green tea is preferred from the aspects of tea-flavored tea flavor intensity, consumer identification, popular preference and the like.
The tea-flavored essence obtained by high-pressure homogenization can also be added with proper amount of tea-flavored characteristic spice or tea polyphenol to enhance the tea flavor of the tea-flavored essence; or adding tea aroma characteristic perfume and tea polyphenol into tea dust/tea powder dispersion system, and homogenizing under high pressure to obtain tea aroma essence.
The tea-flavored essence has the beneficial effects that the tea-flavored essence is obtained through the simple and easily-obtained preparation process with mild conditions, the tea flavor is not damaged by high-temperature heating, and the aroma is not lost due to the complicated process such as concentration, air extraction and the like, so that the tea-flavored essence well maintains the original flavor of tea, and is coordinated and natural with tobacco flavor.
Detailed Description
The invention is further described below in connection with specific embodiments. The following examples are intended to illustrate the invention and are not intended to be limiting.
Example 1
Control and test samples were prepared for comparative experiments: grinding 100g of green tea into 80-mesh green tea powder by a ball mill, dispersing with 9900g of caprylic/capric glyceride, rotating at high speed to disperse into uniform suspension, weighing and dividing into two parts, and one part of control sample; another part of high-pressure homogenization treatment: the homogenizing pressure is gradually increased from 10MPa to 150MPa, the homogenizing component is circularly homogenized for 10 times, and the homogenizing component is placed in a low-temperature cooling circulation at 0 ℃ to minus 5 ℃ to be used as a test sample after homogenization. The soaking time of the control sample and the test sample in the dispersing agent is completely the same, and the experimental result shows that: the color of the solvent of the control sample is basically colorless or light, and the control sample is directly smelled to be basically odorless; the color of the test sample solvent is obviously yellow-green, and the test sample solvent is directly smelled to find that the test sample solvent has obvious tea fragrance. Further processing, respectively centrifuging the control sample and the test sample to remove residues, taking clear liquid to prepare the explosion beads, and preparing the explosion beads into the cigarette. The evaluation shows that after the explosion beads of the control sample are broken, the tea flavor and tea taste are not obvious, and the test sample can feel the obvious tea flavor and tea taste. The high-pressure homogenization treatment can well dissolve and separate aroma components in the tea, and the tea aroma and tea taste can be well reflected.
Example 2
Grinding 100g of green tea into 100-mesh green tea powder by a ball mill, dispersing with 4900g of caprylic/capric glyceride, rotating at high speed to disperse into uniform suspension, homogenizing for 15 times under high pressure, gradually increasing the homogenizing pressure from 10MPa to 150MPa, placing a homogenizing component in a low-temperature cooling cycle of-10 ℃ to-20 ℃, pouring supernatant after homogenization, centrifuging a part of the supernatant containing a small amount of suspended matters, taking supernatant, mixing the supernatant, preparing 20 mu l of standard blasting beads from the supernatant, and preparing the green tea blasting bead cigarette. Through sensory evaluation and suction, the broken and burst beads are pinched in the suction process, and the tea has natural and comfortable tea flavor.
Example 3
Grinding 250g of black tea into 60-mesh black tea powder by a ball mill, dispersing 4750g of caprylic/capric glyceride, rotating at high speed, dispersing into a uniform suspension, homogenizing for 12 times under high pressure, gradually increasing the homogenizing pressure from 10MPa to 140MPa, placing a homogenizing component in a low-temperature cooling cycle of-5 ℃ to-10 ℃, pouring supernatant after homogenization, centrifuging a part of the supernatant containing a small amount of suspended matters, taking supernatant, mixing the supernatant, preparing 22 mu l of standard explosion beads from the supernatant, and preparing black tea explosion bead cigarettes. Through sensory evaluation and suction, the broken and burst beads are pinched in the suction process, and the tea flavor and the tea taste are coordinated with the tobacco flavor.
Example 4
Grinding 25g of oolong tea into 100-mesh black tea powder by a ball mill, dispersing 4975g of caprylic/capric glyceride, rotating at high speed, dispersing into uniform suspension, homogenizing for 15 times under high pressure, gradually applying force from 10MPa until a 110MPa homogenizing component is placed in a low-temperature cooling cycle of minus 10 ℃ to minus 15 ℃, pouring supernatant after homogenization, centrifuging a part of the supernatant containing a small amount of suspended matters, taking supernatant, mixing the supernatant, and preparing 22 mu l of standard explosion beads from the supernatant to prepare oolong tea explosion bead cigarettes. Through sensory evaluation and suction, the burst beads are pinched in the suction process, the tea flavor and tea flavor are coordinated with the tobacco flavor, and the tea flavor is slightly light.
Example 5
Grinding 100g of green tea into 100-mesh green tea powder by a ball mill, dispersing 4900g of olive oil, rotating at high speed to disperse into uniform suspension, homogenizing for 15 times under high pressure, gradually increasing the homogenizing pressure from 10MPa to 150MPa, placing a homogenizing component in a low-temperature cooling cycle of-10 ℃ to-20 ℃, pouring supernatant after homogenization, centrifuging a part of the lower layer containing a small amount of suspended matters to obtain clear liquid, mixing the clear liquid, preparing 20 mu l of clear liquid into explosive beads, and preparing the green tea explosive bead cigarette. Sensory evaluation shows that compared with example 2, the sensory difference is small, the tea aroma and the tea taste are natural, and the tea aroma and the tea taste are coordinated.
Example 6
Grinding 100g of green tea into 100-mesh green tea powder by a ball mill, adding 50g of tea polyphenol into the green tea powder, dispersing with 4900g of caprylic/capric glyceride, rotating and dispersing at high speed to form a uniform suspension, homogenizing for 15 times under high pressure, gradually increasing the homogenizing pressure from 10MPa to 150MPa, placing a homogenizing component in a low-temperature cooling cycle of minus 10 ℃ to minus 20 ℃, pouring supernatant after homogenizing, centrifuging a part of the supernatant containing a small amount of suspended matters at the lower layer to obtain supernatant, combining the supernatant, taking the supernatant as a base of tea essence, adding 20 mu l of bursting beads into the supernatant, and preparing the green tea bursting bead cigarette. Sensory evaluation showed that the tea flavor was more intense than in example 2.
Claims (5)
1. The preparation method of the tea-flavored essence for the cigarette pop beads is characterized by comprising the following steps of:
(1) Taking tea powder and/or tea dust as raw materials, taking tobacco solvent as a dispersing agent, and carrying out high-pressure homogenization treatment on the mixed solution of the raw materials and the dispersing agent to obtain homogenized solution; wherein the mass percentage of the raw materials and the dispersing agent is 1 per mill-8%, the temperature of high-pressure homogenization treatment is-20 ℃ to-10 ℃, and the homogenization pressure is gradually increased from 10MPa to 150MPa;
(2) Centrifuging the homogenized liquid, and collecting the supernatant after centrifugation to obtain the tea aroma essence for cigarettes;
the tobacco solvent is caprylic capric glyceride or edible vegetable oil;
carrying out high-pressure homogenization treatment by using a secondary homogenization process, wherein the high-pressure homogenization times are 5-18 times;
the tea powder and/or tea powder is green tea;
the mesh number of the raw materials is not less than 30 meshes.
2. The preparation method of claim 1, wherein tea polyphenol is added into the dispersion system of the step (2), and the tea aroma for cigarettes is obtained through high-pressure homogenization treatment.
3. The tea aroma for cigarettes obtained by the preparation method of any one of claims 1 to 2.
4. A bead for cigarettes, which consists of a sealed shell consisting of wall materials and liquid essence in the shell, and is characterized in that the liquid essence comprises the tea essence for cigarettes according to claim 3.
5. A bead-blasting cigarette characterized in that the bead-blasting cigarette of claim 4 is provided in a tobacco filter.
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| CN110574962B true CN110574962B (en) | 2023-06-13 |
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| CN111621363A (en) * | 2020-05-18 | 2020-09-04 | 云南中烟工业有限责任公司 | Cigarette-used glutinous rice essence bead and preparation method thereof |
| CN111961531B (en) * | 2020-09-10 | 2023-09-29 | 将军烟草集团有限公司济南包装材料分公司 | Bead-explosion essence for citrus parviflora and preparation method and application thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1781573A (en) * | 2004-12-03 | 2006-06-07 | 刘乡乡 | Super micro extracting technology |
| CN106551424A (en) * | 2016-11-29 | 2017-04-05 | 湖北中烟工业有限责任公司 | A kind of preparation method and applications of the Green tea essence for cigarette drop pill |
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| US9045244B2 (en) * | 2011-05-06 | 2015-06-02 | Altria Client Services Inc. | Apparatus and method for staining a tobacco pouch product |
| CN106108106B (en) * | 2016-06-30 | 2017-12-01 | 云南中烟工业有限责任公司 | A kind of high static pressure of cloud production essential oil of tobaccos is extracted simultaneously and the method for sterilization fresh |
| CN107223757A (en) * | 2017-04-26 | 2017-10-03 | 江西九草铁皮石斛科技协同创新有限公司 | A kind of chewing gum containing dendrobium candidum and preparation method thereof |
| CN106987314B (en) * | 2017-04-27 | 2021-01-08 | 河南中烟工业有限责任公司 | Citrus reticulata flavor essence for bead blasting of cigarettes and application of citrus reticulata flavor essence in cigarettes |
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1781573A (en) * | 2004-12-03 | 2006-06-07 | 刘乡乡 | Super micro extracting technology |
| CN106551424A (en) * | 2016-11-29 | 2017-04-05 | 湖北中烟工业有限责任公司 | A kind of preparation method and applications of the Green tea essence for cigarette drop pill |
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