CN110240419B - 锂铝硅玻璃、锂铝硅化学强化玻璃及其制备方法与应用 - Google Patents
锂铝硅玻璃、锂铝硅化学强化玻璃及其制备方法与应用 Download PDFInfo
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- CN110240419B CN110240419B CN201910491063.4A CN201910491063A CN110240419B CN 110240419 B CN110240419 B CN 110240419B CN 201910491063 A CN201910491063 A CN 201910491063A CN 110240419 B CN110240419 B CN 110240419B
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- Prior art keywords
- glass
- lithium
- lithium aluminum
- chemically strengthened
- sio
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- 239000011521 glass Substances 0.000 title claims abstract description 149
- -1 Lithium aluminum silicon Chemical compound 0.000 title claims abstract description 114
- 239000005345 chemically strengthened glass Substances 0.000 title claims abstract description 72
- 238000002360 preparation method Methods 0.000 title claims abstract description 19
- 239000006018 Li-aluminosilicate Substances 0.000 claims abstract description 111
- 238000005342 ion exchange Methods 0.000 claims abstract description 85
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 56
- 229910052681 coesite Inorganic materials 0.000 claims abstract description 38
- 229910052906 cristobalite Inorganic materials 0.000 claims abstract description 38
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 38
- 229910052682 stishovite Inorganic materials 0.000 claims abstract description 38
- 238000005728 strengthening Methods 0.000 claims abstract description 38
- 229910052905 tridymite Inorganic materials 0.000 claims abstract description 38
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims abstract description 33
- XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 claims abstract description 32
- FUJCRWPEOMXPAD-UHFFFAOYSA-N Li2O Inorganic materials [Li+].[Li+].[O-2] FUJCRWPEOMXPAD-UHFFFAOYSA-N 0.000 claims abstract description 31
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims abstract description 31
- XUCJHNOBJLKZNU-UHFFFAOYSA-M dilithium;hydroxide Chemical compound [Li+].[Li+].[OH-] XUCJHNOBJLKZNU-UHFFFAOYSA-M 0.000 claims abstract description 31
- 229910052593 corundum Inorganic materials 0.000 claims abstract description 30
- 229910001845 yogo sapphire Inorganic materials 0.000 claims abstract description 30
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N titanium dioxide Inorganic materials O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 25
- 229910000272 alkali metal oxide Inorganic materials 0.000 claims abstract description 11
- VWDWKYIASSYTQR-UHFFFAOYSA-N sodium nitrate Chemical compound [Na+].[O-][N+]([O-])=O VWDWKYIASSYTQR-UHFFFAOYSA-N 0.000 claims description 58
- 150000003839 salts Chemical class 0.000 claims description 40
- KKCBUQHMOMHUOY-UHFFFAOYSA-N Na2O Inorganic materials [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 claims description 34
- 235000010344 sodium nitrate Nutrition 0.000 claims description 26
- 239000004317 sodium nitrate Substances 0.000 claims description 26
- JFBZPFYRPYOZCQ-UHFFFAOYSA-N [Li].[Al] Chemical compound [Li].[Al] JFBZPFYRPYOZCQ-UHFFFAOYSA-N 0.000 claims description 15
- 239000005368 silicate glass Substances 0.000 claims description 14
- 229910001960 metal nitrate Inorganic materials 0.000 claims description 12
- 229910000502 Li-aluminosilicate Inorganic materials 0.000 claims description 9
- 230000001681 protective effect Effects 0.000 claims description 8
- 229910052710 silicon Inorganic materials 0.000 claims description 7
- 239000010703 silicon Substances 0.000 claims description 7
- 238000002844 melting Methods 0.000 claims description 6
- 230000008018 melting Effects 0.000 claims description 6
- 239000005357 flat glass Substances 0.000 claims description 5
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 238000003825 pressing Methods 0.000 claims description 4
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 claims 2
- 229910052744 lithium Inorganic materials 0.000 claims 2
- 238000003426 chemical strengthening reaction Methods 0.000 abstract description 18
- CPLXHLVBOLITMK-UHFFFAOYSA-N Magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 38
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 description 22
- 239000000395 magnesium oxide Substances 0.000 description 20
- 238000000034 method Methods 0.000 description 15
- 239000010410 layer Substances 0.000 description 14
- 238000009826 distribution Methods 0.000 description 13
- 230000002829 reductive effect Effects 0.000 description 13
- 229910001416 lithium ion Inorganic materials 0.000 description 12
- 229910001415 sodium ion Inorganic materials 0.000 description 12
- BITYAPCSNKJESK-UHFFFAOYSA-N potassiosodium Chemical compound [Na].[K] BITYAPCSNKJESK-UHFFFAOYSA-N 0.000 description 11
- VVNXEADCOVSAER-UHFFFAOYSA-N lithium sodium Chemical compound [Li].[Na] VVNXEADCOVSAER-UHFFFAOYSA-N 0.000 description 10
- 230000008569 process Effects 0.000 description 9
- 239000006058 strengthened glass Substances 0.000 description 9
- 229910052783 alkali metal Inorganic materials 0.000 description 8
- 239000002131 composite material Substances 0.000 description 8
- 150000002500 ions Chemical class 0.000 description 8
- 229910052760 oxygen Inorganic materials 0.000 description 8
- 239000001301 oxygen Substances 0.000 description 8
- 239000000126 substance Substances 0.000 description 8
- 150000001340 alkali metals Chemical class 0.000 description 7
- 238000000137 annealing Methods 0.000 description 7
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 7
- 230000000052 comparative effect Effects 0.000 description 7
- 239000011734 sodium Substances 0.000 description 7
- 238000003723 Smelting Methods 0.000 description 5
- 229910001413 alkali metal ion Inorganic materials 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- 235000010333 potassium nitrate Nutrition 0.000 description 5
- 239000004323 potassium nitrate Substances 0.000 description 5
- 238000004031 devitrification Methods 0.000 description 4
- 238000011160 research Methods 0.000 description 4
- 239000005341 toughened glass Substances 0.000 description 4
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 3
- 230000008901 benefit Effects 0.000 description 3
- 238000005520 cutting process Methods 0.000 description 3
- 230000007547 defect Effects 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 229910001414 potassium ion Inorganic materials 0.000 description 3
- LIVNPJMFVYWSIS-UHFFFAOYSA-N silicon monoxide Chemical compound [Si-]#[O+] LIVNPJMFVYWSIS-UHFFFAOYSA-N 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 description 2
- 229910052782 aluminium Inorganic materials 0.000 description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 2
- 239000011449 brick Substances 0.000 description 2
- 238000002425 crystallisation Methods 0.000 description 2
- 230000008025 crystallization Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000000227 grinding Methods 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 229910052749 magnesium Inorganic materials 0.000 description 2
- 239000011777 magnesium Substances 0.000 description 2
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 150000002823 nitrates Chemical class 0.000 description 2
- 230000003287 optical effect Effects 0.000 description 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
- 230000002195 synergetic effect Effects 0.000 description 2
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 244000137852 Petrea volubilis Species 0.000 description 1
- 238000006124 Pilkington process Methods 0.000 description 1
- FKNQFGJONOIPTF-UHFFFAOYSA-N Sodium cation Chemical compound [Na+] FKNQFGJONOIPTF-UHFFFAOYSA-N 0.000 description 1
- AFCIMSXHQSIHQW-UHFFFAOYSA-N [O].[P] Chemical compound [O].[P] AFCIMSXHQSIHQW-UHFFFAOYSA-N 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 238000004220 aggregation Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 1
- 150000001342 alkaline earth metals Chemical class 0.000 description 1
- 239000005354 aluminosilicate glass Substances 0.000 description 1
- 238000000149 argon plasma sintering Methods 0.000 description 1
- 239000006121 base glass Substances 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000008395 clarifying agent Substances 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 238000005034 decoration Methods 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000000670 limiting effect Effects 0.000 description 1
- 239000004579 marble Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 238000007500 overflow downdraw method Methods 0.000 description 1
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 1
- 238000005191 phase separation Methods 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 238000013001 point bending Methods 0.000 description 1
- 238000005498 polishing Methods 0.000 description 1
- 239000002861 polymer material Substances 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000002441 reversible effect Effects 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 229910052814 silicon oxide Inorganic materials 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000006133 sodium aluminosilicate glass Substances 0.000 description 1
- 238000003892 spreading Methods 0.000 description 1
- 230000007480 spreading Effects 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 239000002344 surface layer Substances 0.000 description 1
- 238000010408 sweeping Methods 0.000 description 1
- 238000005496 tempering Methods 0.000 description 1
- 238000002834 transmittance Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C21/00—Treatment of glass, not in the form of fibres or filaments, by diffusing ions or metals in the surface
- C03C21/001—Treatment of glass, not in the form of fibres or filaments, by diffusing ions or metals in the surface in liquid phase, e.g. molten salts, solutions
- C03C21/002—Treatment of glass, not in the form of fibres or filaments, by diffusing ions or metals in the surface in liquid phase, e.g. molten salts, solutions to perform ion-exchange between alkali ions
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/076—Glass compositions containing silica with 40% to 90% silica, by weight
- C03C3/089—Glass compositions containing silica with 40% to 90% silica, by weight containing boron
- C03C3/091—Glass compositions containing silica with 40% to 90% silica, by weight containing boron containing aluminium
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/076—Glass compositions containing silica with 40% to 90% silica, by weight
- C03C3/097—Glass compositions containing silica with 40% to 90% silica, by weight containing phosphorus, niobium or tantalum
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Ceramic Engineering (AREA)
- Glass Compositions (AREA)
Abstract
Description
Claims (12)
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CN201910491063.4A CN110240419B (zh) | 2019-06-06 | 2019-06-06 | 锂铝硅玻璃、锂铝硅化学强化玻璃及其制备方法与应用 |
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CN201910491063.4A CN110240419B (zh) | 2019-06-06 | 2019-06-06 | 锂铝硅玻璃、锂铝硅化学强化玻璃及其制备方法与应用 |
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CN110240419A CN110240419A (zh) | 2019-09-17 |
CN110240419B true CN110240419B (zh) | 2021-11-05 |
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Families Citing this family (12)
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---|---|---|---|---|
CN110746112B (zh) * | 2019-10-24 | 2022-07-29 | 重庆鑫景特种玻璃有限公司 | 低钠素玻璃、化学强化玻璃及化学强化玻璃的制备方法 |
CN113929308B (zh) * | 2019-12-03 | 2023-09-22 | 重庆鑫景特种玻璃有限公司 | 一种具有超高分叉阈值的微晶玻璃 |
CN111410439B (zh) * | 2020-03-24 | 2021-04-20 | 武汉理工大学 | 一种基于玻璃应力驰豫的化学钢化方法及钢化玻璃 |
CN114075046B (zh) * | 2020-08-18 | 2023-01-24 | 重庆鑫景特种玻璃有限公司 | 具有高压应力和高安全性的强化玻璃及其加工方法 |
CN114075044B (zh) * | 2020-08-18 | 2023-01-24 | 重庆鑫景特种玻璃有限公司 | 一种具有安全应力状态的强化玻璃及其加工方法 |
CN114075045B (zh) * | 2020-08-18 | 2023-01-24 | 重庆鑫景特种玻璃有限公司 | 一种具有高安全应力的化学强化玻璃及测试方法 |
KR102509484B1 (ko) * | 2020-10-29 | 2023-03-13 | (주)유티아이 | 플렉시블 커버 윈도우 및 그 제조방법 |
CN112592056A (zh) * | 2020-10-30 | 2021-04-02 | 重庆鑫景特种玻璃有限公司 | 具有低变化幅度的张应力区的安全强化玻璃及制法和应用 |
CN112661405A (zh) * | 2020-12-25 | 2021-04-16 | 醴陵旗滨电子玻璃有限公司 | 一种锂铝硅玻璃及其制备方法、智能终端及显示器 |
CN113121109A (zh) * | 2021-03-31 | 2021-07-16 | 彩虹集团(邵阳)特种玻璃有限公司 | 一种防蓝光高强度锂铝硅盖板玻璃及其制备方法和应用 |
CN113387598A (zh) * | 2021-06-29 | 2021-09-14 | 江苏铁锚玻璃股份有限公司 | 锂铝硅玻璃的新型强化工艺 |
CN114394745B (zh) * | 2022-01-07 | 2024-02-20 | 彩虹集团(邵阳)特种玻璃有限公司 | 铝硅酸盐玻璃及其制备方法和盖板玻璃 |
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US4119760A (en) * | 1975-08-15 | 1978-10-10 | Ppg Industries, Inc. | Chemical strengthening of glass |
CN102336521A (zh) * | 2011-06-14 | 2012-02-01 | 吴艺菲 | 铝硅酸盐玻璃及其制备方法 |
CN102795766A (zh) * | 2011-05-23 | 2012-11-28 | 旭硝子株式会社 | 制造化学强化的玻璃的方法 |
CN102815860A (zh) * | 2011-06-10 | 2012-12-12 | 肖特玻璃科技(苏州)有限公司 | 形成具有多个表面应力层钢化玻璃的方法及钢化玻璃制品 |
CN104591538A (zh) * | 2014-12-23 | 2015-05-06 | 中国南玻集团股份有限公司 | 铝硅酸盐玻璃、铝硅酸盐玻璃的强化方法及强化玻璃 |
CN107531550A (zh) * | 2015-03-31 | 2018-01-02 | 科立视材料科技有限公司 | 具有低介电常数的化学强化碱铝硼硅酸玻璃的玻璃组成物 |
CN108147657A (zh) * | 2017-12-29 | 2018-06-12 | 深圳市东丽华科技有限公司 | 一种素玻璃、强化玻璃及制备方法 |
CN108863050A (zh) * | 2018-06-20 | 2018-11-23 | 醴陵旗滨电子玻璃有限公司 | 锂铝硅酸盐玻璃及其制备方法 |
CN109071319A (zh) * | 2016-04-20 | 2018-12-21 | 康宁股份有限公司 | 包含金属氧化物浓度梯度的玻璃基制品 |
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JP5890393B2 (ja) * | 2011-03-31 | 2016-03-22 | 日本板硝子株式会社 | 低膨張ガラス、強化ガラス、及び強化ガラスの製造方法 |
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2019
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US4119760A (en) * | 1975-08-15 | 1978-10-10 | Ppg Industries, Inc. | Chemical strengthening of glass |
CN102795766A (zh) * | 2011-05-23 | 2012-11-28 | 旭硝子株式会社 | 制造化学强化的玻璃的方法 |
CN102815860A (zh) * | 2011-06-10 | 2012-12-12 | 肖特玻璃科技(苏州)有限公司 | 形成具有多个表面应力层钢化玻璃的方法及钢化玻璃制品 |
CN102336521A (zh) * | 2011-06-14 | 2012-02-01 | 吴艺菲 | 铝硅酸盐玻璃及其制备方法 |
CN104591538A (zh) * | 2014-12-23 | 2015-05-06 | 中国南玻集团股份有限公司 | 铝硅酸盐玻璃、铝硅酸盐玻璃的强化方法及强化玻璃 |
CN107531550A (zh) * | 2015-03-31 | 2018-01-02 | 科立视材料科技有限公司 | 具有低介电常数的化学强化碱铝硼硅酸玻璃的玻璃组成物 |
CN109071319A (zh) * | 2016-04-20 | 2018-12-21 | 康宁股份有限公司 | 包含金属氧化物浓度梯度的玻璃基制品 |
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