CN110200856A - A kind of production technology preparing Chinese medicine medicine oil using Umbellales Araliaceae medicinal material - Google Patents
A kind of production technology preparing Chinese medicine medicine oil using Umbellales Araliaceae medicinal material Download PDFInfo
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- CN110200856A CN110200856A CN201910467434.5A CN201910467434A CN110200856A CN 110200856 A CN110200856 A CN 110200856A CN 201910467434 A CN201910467434 A CN 201910467434A CN 110200856 A CN110200856 A CN 110200856A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
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Abstract
The present invention relates to a kind of production technologies that Chinese medicine medicine oil is prepared using Umbellales Araliaceae medicinal material, steps are as follows: (1) raw material prerinse, drying, choosing Umbellales Araliaceae medicinal raw material need to be pre-processed, and medicinal material is cleaned, and is being dried at 60 degree；(2) raw material crushes, and plant material is ground into powdery using pulverizer, it is spare to cross 30-40 mesh；(3) it is impregnated before extracting, powder raw material is fitted into container, extractant is added and impregnates, solid-liquid ratio 1:1-50；(4) filling and sealing；(5) extraction vessel equipped with plant material is put into super-pressure compression chamber, starting device, processing pressure 50-800MPa, dwell time 1-60min by super-pressure broken wall treatment, while circular treatment 2-3 times；(6) secondary extraction；(7) it filters.After treatment process processing of the invention, the Chinese medicine medicine oil rich in saponin(e substance is obtained.
Description
Technical field
The invention belongs to cosmetic fields, are related to the production technology of Chinese medicine medicine oil, especially a kind of to utilize Umbellales slender acanthopanax
Section's medicinal material prepares the production technology of Chinese medicine medicine oil.
Background technique
Umbellales araliaceae ginseng plant is rare medicinal plant, known at least existing 4000 history.
Umbellales Araliaceae is used as medicine with rhizome, ginseng, Radix Notoginseng, the American Ginseng etc. of common medicinal material such as Panax.These Chinese medicines
In main active be dammarane type tetracyclic triterpene saponin(e, the substance have important physiological activity.Such as ginsenoside
With raising immunity of organisms, antibacterial, improve cardiovascular and cerebrovascular blood supply insufficiency, adjusting central nervous system, antifatigue, anti-aging
The effects of.
Common active ingredients from traditional Chinese medicinal extracting method have common infusion method, steam distillation, chemical solvent extraction,
Supercritical carbon dioxide extraction method etc..Steam distillation, be will the vegetable material containing volatile component and water condistillation, make to wave
Hair property ingredient distillates together with vapor, and the leach extraction method of volatile component is taken through condensation point.Temperature when due to steam distillation
Excessively high, Heat sensitive active ingredient such as may decompose, aoxidize at the reaction in medicinal material, and active component content is caused to lose.
Supercritical CO2Extracting process extract Chinese medicine active constituent, although can to avoid heat-sensitive substance decomposition, oxidation
The problems such as, but fluid is lost very greatly after compared with long circulating route, separating still in extraction process, therefore oil yield is not very high.Together
When method process specifications it is high, cost of equipment investment is big.It is especially high to equipment air-tightness requirement, easily cause catastrophic explosion
Accident, there are hidden dangers, and equipment is low to energy utilization rate, and big energy-consuming expends high.
The research of superhigh pressure technique starts from 1914, which is at home and abroad mainly used in grocery trade, in order to
It prevents the microbial contamination of food, extend the food storage time.Ultra high pressure extraction (ultrahigh-pressure
Extraction, UHPE), also referred to as superelevation isostatic cool pressing is extracted, and refers to the hydrostatic pressure masterpiece for using 100-1000MPa at normal temperature
For Extraction solvent and the mixed liquor for being extracted substance, and a period of time is kept under a predetermined, make inside and outside plant cell
Pressure reach balance after rapid release, since intraor extracellular osmotic pressure increases suddenly, the structure of cell membrane change so that
Intracellular effective component can pass through cell membrane and be transferred in extracellular Extraction medium, reach extract plant in effectively at
The purpose divided.
Relative to other traditional Chinese medicine ingredients methods, super-pressure method prepares Chinese medicine oil and has the following characteristics that
1, extraction efficiency is high: since pressure is higher, solvent can penetrate into the cell in very short time, keep effective component rapid
Up to dissolution equilibrium.
2, retain extract active constituent: although pressure rise, substance releases heat to the external world, due to high-pressure bottle and outside
Boundary's environment has good heat exchange, can maintain to carry out at room temperature throughout the extraction process substantially, can farthest protect
Active material in medicinal material has been stayed, the problems such as reducing because of thermally-induced effective component denaturation, loss and pharmacological activity is avoided.
3, it consumes energy low, highly-safe: ultra high pressure extraction process medium fluid deformation is smaller, the less energy intensive in fluid compression,
The consumption and transmitting of noenergy in pressure maintaining and stress-relief process.The lesser compress of fluid, will not generate in operation
The volume change of increasing greatly reduces device because of device leakproofness bring risk.Therefore, the safety of ultra high pressure extraction equipment
Property be much higher than supercritical CO2Extraction equipment.
Summary of the invention
It is an object of the invention to provide in place of overcome the deficiencies in the prior art, a kind of extraction time is short, and low energy consumption, effectively
Constituents extraction rate is high, and the production technology and application of Chinese medicine medicine oil are prepared using Umbellales Araliaceae medicinal material.
The present invention realizes that the technical solution of purpose is as follows:
1, a kind of production technology that Chinese medicine medicine oil is prepared using Umbellales Araliaceae medicinal material, after vegetable drug raw material crushes,
Extracted dose of immersion strengthens extraction process using super-pressure wall breaking technology, and processing step is as follows:
(1) raw material cleaning, drying
Umbellales Araliaceae raw medicinal material is eluted using deionized water, and using automatic drier under 60 degree of temperature
Medicinal material is subjected to drying and processing；
(2) raw material crushes
After medicinal material drying, medicinal raw material is ground into powdery using pulverizer, it is spare to cross 30-40 mesh；
(3) it is impregnated before extracting
Powder raw material is fitted into container, extractant is added and impregnates, is sufficiently stirred, impregnates 1-48h, obtains raw material sufficiently
Infiltration, solid-liquid ratio 1:1-50, extractant are caprylic/capric triglyceride, vegetable fat, lauryl alcohol lactate, palm acid ethyl
Mutatis mutandis liquid fat in one of own ester or a variety of cosmetics；
(4) filling and sealing
It will be fitted into packaging bag by the raw material sufficiently impregnated, be sealed using vacuum sealer；
(5) super-pressure broken wall treatment
Extraction vessel equipped with plant material is put into super-pressure compression chamber, starting device, processing pressure 50-
800MPa, dwell time 1-60min, circular treatment 2-3 times；
(6) secondary extraction
After ultra high pressure treatment, extraction vessel is placed in 30-80 DEG C of isoperibol and carries out secondary extraction, time 24-
72h, meanwhile, it was once ultrasonically treated every 4-6 hours, 10min per treatment, power 300w；
(8) it filters
It will treated obtains Chinese medicine medicine oil after feed liquid filtered using automatic deslagging filter.
Moreover, the solid-liquid ratio is 1:1-6.
Moreover, the super-pressure broken wall treatment dwell time is 15-30min.
Moreover, the isothermal holding temperature is 40-50 DEG C.
The advantages and positive effects of the present invention are:
1, the present invention is acted on by broken wall of the super-pressure to plant cell, and the effective component in medicinal material is made to be easier to be extracted agent
It takes out of, by householder methods such as heat preservation, ultrasounds, the extraction efficiency of general ginsenoside can be greatly improved in the short time.
2, the present invention uses caprylic/capric triglyceride, and the cosmetics standard such as lauryl alcohol lactate has grease to be situated between as extraction
Matter avoids when extracting the substance using conventional organic solvents, and the problem of solvent residual that may cause improves products application
Safety in daily use chemicals industry, while also can guarantee the leaching efficiency of the effective component in plant.
3, the present invention is using ultra high pressure extraction technology there are many advantage, including extraction time is short, and low energy consumption, effective component mentions
Effective component inactivation, loss caused by taking rate high and avoidable fuel factor etc..It is easy to operate, it is suitable for industrialized production.
Specific embodiment
The method of the present invention is described below by specific embodiment.Unless stated otherwise, technology used in the present invention
Means are method known in those skilled in the art.In addition, embodiment is interpreted as illustrative, rather than this hair is limited
Bright range, the spirit and scope of the invention are limited only by the claims that follow.To those skilled in the art, it is not carrying on the back
Under the premise of from spirit and scope of the present invention, in these embodiments material component and dosage carry out various changes or change
It is dynamic to also belong to protection scope of the present invention.
The present invention provides a kind of production technology that Chinese medicine medicine oil is prepared using Umbellales Araliaceae medicinal material, specifically includes following
Step:
1, raw material cleaning, drying
Umbellales Araliaceae raw medicinal material is eluted using deionized water, and using automatic drier under 60 degree of temperature
Medicinal material is subjected to drying and processing.
2, raw material crushes
Medicinal material is cleaned, after drying, medicinal raw material is ground into powdery using pulverizer, it is spare to cross 40 meshes；
3, it is impregnated before extracting
Powder raw material is fitted into container, extractant is added, and (extractant should be cosmetics and use permits in raw material catalogue
Various greases, such as caprylic/capric triglyceride, lauryl alcohol lactate the combination grease used carries out in proportion) it impregnates, feed liquid
Than 1:1-1:50, more preferable 1:1-1:10, more preferable 1:1-1:6, and be sufficiently stirred, 1-48h is impregnated, (preferably 6-8h) makes original
Material is sufficiently infiltrated.
4, filling and sealing
It is fitted into packaging bag by the raw material sufficiently impregnated, is sealed using vacuum sealer；
5, super-pressure broken wall treatment
Container equipped with plant material is put into super-pressure compression chamber, starting device, processing pressure 50-800MPa, is protected
The pressure time is 1-60min, preferably 15-30min, while circular treatment 2-3 times.
6, secondary extraction
After ultra high pressure treatment, extraction vessel is placed higher than in the isoperibol of room temperature (30-80 DEG C), preferably 40-50 DEG C,
To avoid the destruction of the excessively high effective component to leaching of temperature, and the oxidation of extractant is avoided, keeps the temperature 24-72h.Meanwhile
It was once ultrasonically treated every 4-6 hours (per treatment 10min, power 300w).Crude drug cell is broken by super-pressure
Wall effect further leaches the liposoluble constituent in medicinal material using ultrasonic wave added method.Shorten the production cycle of medicine oil.
7, it filters
Chinese medicine medicine oil will be obtained after the filtering of treated feed liquid.
Here is that the embodiment of Chinese medicine medicine oil is prepared according to different ratio extracting solution and various extracting conditions, specific interior
Hold as follows:
Embodiment 1:
The preparation of ginseng oil: being extractant, material ratio 1:1, ultra-high pressure condition using caprylic/capric triglyceride
100MPa, dwell time 20min, 40 DEG C of isothermal holding 48h are during which primary every 6h ultrasonic treatment, 10min per treatment, mistake
Filter obtains product, total Ginsenosides Content 4.85mg/g.
Embodiment 2:
The preparation of ginseng oil: being extractant, material ratio 1:1, ultra-high pressure condition 200MPa, pressure maintaining using lauryl alcohol lactate
Time 20min, 40 DEG C of isothermal holding 48h, during which primary every 6h ultrasonic treatment, product, ginseng is obtained by filtration in each 10min
Total saponin content is 6.86mg/g.
Embodiment 3:
The preparation of ginseng oil: being extractant, object using caprylic/capric triglyceride, carbonic acid dibutyl ester compound lard (1:4)
During which material is ultrasonically treated one every 6h than 1:1, ultra-high pressure condition 300MPa, dwell time 20min, 40 DEG C of isothermal holding 48h
Secondary, product, total Ginsenosides Content 8.78mg/g is obtained by filtration in 10min per treatment.
Embodiment 4:
The preparation of Radix Notoginseng oil: being extractant using caprylic/capric triglyceride, lauryl alcohol lactate compound lard (1:2),
Material ratio 1:1, ultra-high pressure condition 400MPa, dwell time 20min, 40 DEG C of placement 48h are during which primary every 6h ultrasonic treatment,
Product, content of the total saponins in radix notoginseng 9.18mg/g is obtained by filtration in 10min per treatment.
Embodiment 5:
The preparation of Radix Notoginseng oil: being extractant using caprylic/capric triglyceride, lauryl alcohol lactate compound lard (1:3),
Material ratio 1:1, ultra-high pressure condition 400MPa, dwell time 20min, 40 DEG C of placement 48h are during which primary every 6h ultrasonic treatment,
Product, content of the total saponins in radix notoginseng 9.34mg/g is obtained by filtration in 10min per treatment.
Embodiment 6:
The preparation of American Ginseng oil: being to mention using caprylic/capric triglyceride, lauryl alcohol lactate compound lard (1:0.5)
Agent, material ratio 1:1, ultra-high pressure condition 400MPa are taken, during which dwell time 20min, 40 DEG C of placement 48h are ultrasonically treated every 6h
Once, product, total Ginsenosides Content 8.01mg/g is obtained by filtration in 10min per treatment.
Embodiment 7:
The preparation of American Ginseng oil: being to extract using caprylic/capric triglyceride, Parleam compound lard (1:1)
During which agent, material ratio 1:1, ultra-high pressure condition 500MPa, dwell time 20min, 40 DEG C of placement 48h are ultrasonically treated one every 6h
Secondary, product, total Ginsenosides Content 8.20mg/g is obtained by filtration in 10min per treatment.
Embodiment 8:
The preparation of American Ginseng oil: being to extract using caprylic/capric triglyceride, lauryl alcohol lactate compound lard (1:4)
During which agent, material ratio 1:1, ultra-high pressure condition 600MPa, dwell time 20min, 40 DEG C of placement 48h are ultrasonically treated one every 6h
Secondary, product, total Ginsenosides Content 8.45mg/g is obtained by filtration in each 10min.
The broken wall of plant cell is acted on by super-pressure, so that the effective component in medicinal material is easier to be extracted agent and is taken out of, leads to
The householder methods such as heat preservation, ultrasound are crossed, the extraction efficiency of general ginsenoside can be greatly improved in the short time.
The present invention uses caprylic/capric triglyceride, and the cosmetics standard such as lauryl alcohol lactate has grease as Extraction medium,
Avoid using conventional organic solvents extract the substance when, the problem of solvent residual that may cause, improve products application in
Safety in daily use chemicals industry, while also can guarantee the leaching efficiency of the effective component in plant.
Claims (4)
1. a kind of production technology for preparing Chinese medicine medicine oil using Umbellales Araliaceae medicinal material, after vegetable drug raw material crushes, through mentioning
It takes agent to impregnate, extraction process is strengthened using super-pressure wall breaking technology, it is characterised in that: processing step is as follows:
(1) raw material cleaning, drying
Umbellales Araliaceae raw medicinal material is eluted using deionized water, and uses automatic drier under 60 degree of temperature by medicine
Material carries out drying and processing；
(2) raw material crushes
After medicinal material drying, medicinal raw material is ground into powdery using pulverizer, it is spare to cross 30-40 mesh；
(3) it is impregnated before extracting
Powder raw material is fitted into container, extractant is added and impregnates, is sufficiently stirred, impregnates 1-48h, soaks raw material sufficiently
Profit, solid-liquid ratio 1:1-50, extractant be caprylic/capric triglyceride, vegetable fat, lauryl alcohol lactate, palm acid ethyl oneself
Mutatis mutandis liquid fat in one of ester or a variety of cosmetics；
(4) filling and sealing
It will be fitted into packaging bag by the raw material sufficiently impregnated, be sealed using vacuum sealer；
(5) super-pressure broken wall treatment
Extraction vessel equipped with plant material is put into super-pressure compression chamber, starting device, processing pressure 50-800MPa, is protected
The pressure time is 1-60min, circular treatment 2-3 times；
(6) secondary extraction
After ultra high pressure treatment, extraction vessel is placed in 30-80 DEG C of isoperibol and carries out secondary extraction, time 24-72h,
Meanwhile it being once ultrasonically treated every 4-6 hours, 10min per treatment, power 300w；
(7) it filters
It will treated obtains Chinese medicine medicine oil after feed liquid filtered using automatic deslagging filter.
2. a kind of production technology for preparing Chinese medicine medicine oil using Umbellales Araliaceae medicinal material according to claim 1, special
Sign is: the solid-liquid ratio is 1:1-6.
3. a kind of production technology for preparing Chinese medicine medicine oil using Umbellales Araliaceae medicinal material according to claim 1, special
Sign is: the super-pressure broken wall treatment dwell time is 15-30min.
4. a kind of production technology for preparing Chinese medicine medicine oil using Umbellales Araliaceae medicinal material according to claim 1, special
Sign is: the isothermal holding temperature is 40-50 DEG C.
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| CN201910467434.5A CN110200856A (en) | 2019-05-31 | 2019-05-31 | A kind of production technology preparing Chinese medicine medicine oil using Umbellales Araliaceae medicinal material |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110724594A (en) * | 2019-11-18 | 2020-01-24 | 刘俚扬 | Sectional type extraction process for high-concentration BITC papaya seed oil |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1629181A (en) * | 2004-09-03 | 2005-06-22 | 吉林大学 | Ginseng saponin superhigh pressure extraction process |
| CN104841156A (en) * | 2015-05-09 | 2015-08-19 | 东北师范大学 | Method for extracting effective components in plants by using ultrahigh pressure equipment |
| CN108096073A (en) * | 2017-12-27 | 2018-06-01 | 北京同德展科贸有限公司 | Production technology and the application of Chinese medicine medicine oil are prepared using Umbellales Umbelliferae medicinal material |
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2019
- 2019-05-31 CN CN201910467434.5A patent/CN110200856A/en not_active Withdrawn
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1629181A (en) * | 2004-09-03 | 2005-06-22 | 吉林大学 | Ginseng saponin superhigh pressure extraction process |
| CN104841156A (en) * | 2015-05-09 | 2015-08-19 | 东北师范大学 | Method for extracting effective components in plants by using ultrahigh pressure equipment |
| CN108096073A (en) * | 2017-12-27 | 2018-06-01 | 北京同德展科贸有限公司 | Production technology and the application of Chinese medicine medicine oil are prepared using Umbellales Umbelliferae medicinal material |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110724594A (en) * | 2019-11-18 | 2020-01-24 | 刘俚扬 | Sectional type extraction process for high-concentration BITC papaya seed oil |
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Application publication date: 20190906 |