CN103271960A - Preparation method of ginseng cream richly containing scare ginsenosides Rg3 and Rh2 - Google Patents
Preparation method of ginseng cream richly containing scare ginsenosides Rg3 and Rh2 Download PDFInfo
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- CN103271960A CN103271960A CN2013102450978A CN201310245097A CN103271960A CN 103271960 A CN103271960 A CN 103271960A CN 2013102450978 A CN2013102450978 A CN 2013102450978A CN 201310245097 A CN201310245097 A CN 201310245097A CN 103271960 A CN103271960 A CN 103271960A
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- 235000003140 Panax quinquefolius Nutrition 0.000 title claims abstract description 59
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 title claims abstract description 57
- 235000008434 ginseng Nutrition 0.000 title claims abstract description 57
- 239000006071 cream Substances 0.000 title claims abstract description 20
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- 241000208340 Araliaceae Species 0.000 title claims description 56
- 229930182494 ginsenoside Natural products 0.000 title abstract description 6
- 238000000605 extraction Methods 0.000 claims abstract description 12
- 238000004945 emulsification Methods 0.000 claims abstract description 8
- 239000002994 raw material Substances 0.000 claims abstract description 8
- 238000012545 processing Methods 0.000 claims abstract description 5
- RWXIFXNRCLMQCD-JBVRGBGGSA-N (20S)-ginsenoside Rg3 Chemical compound O([C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@H]1CC[C@]2(C)[C@H]3C[C@@H](O)[C@H]4[C@@]([C@@]3(CC[C@H]2C1(C)C)C)(C)CC[C@@H]4[C@@](C)(O)CCC=C(C)C)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O RWXIFXNRCLMQCD-JBVRGBGGSA-N 0.000 claims description 14
- 238000003756 stirring Methods 0.000 claims description 12
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 12
- 239000008158 vegetable oil Substances 0.000 claims description 12
- 239000003921 oil Substances 0.000 claims description 11
- 235000019198 oils Nutrition 0.000 claims description 11
- 238000006243 chemical reaction Methods 0.000 claims description 9
- XIRZPICFRDZXPF-UHFFFAOYSA-N Ginsenoside Rg3 Natural products CC(C)=CCCC(C)(O)C1CCC(C2(CC(O)C3C4(C)C)C)(C)C1C(O)CC2C3(C)CCC4OC1OC(CO)C(O)C(O)C1OC1OC(CO)C(O)C(O)C1O XIRZPICFRDZXPF-UHFFFAOYSA-N 0.000 claims description 8
- 239000000706 filtrate Substances 0.000 claims description 8
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims description 8
- 239000012535 impurity Substances 0.000 claims description 8
- 238000006555 catalytic reaction Methods 0.000 claims description 7
- 230000001804 emulsifying effect Effects 0.000 claims description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- 210000000582 semen Anatomy 0.000 claims description 5
- 235000014676 Phragmites communis Nutrition 0.000 claims description 4
- 238000004140 cleaning Methods 0.000 claims description 4
- 239000004006 olive oil Substances 0.000 claims description 4
- 235000008390 olive oil Nutrition 0.000 claims description 4
- 238000002203 pretreatment Methods 0.000 claims description 4
- 238000010025 steaming Methods 0.000 claims description 4
- 235000021050 feed intake Nutrition 0.000 claims description 3
- ZEMPKEQAKRGZGQ-AAKVHIHISA-N 2,3-bis[[(z)-12-hydroxyoctadec-9-enoyl]oxy]propyl (z)-12-hydroxyoctadec-9-enoate Chemical compound CCCCCCC(O)C\C=C/CCCCCCCC(=O)OCC(OC(=O)CCCCCCC\C=C/CC(O)CCCCCC)COC(=O)CCCCCCC\C=C/CC(O)CCCCCC ZEMPKEQAKRGZGQ-AAKVHIHISA-N 0.000 claims description 2
- 235000019498 Walnut oil Nutrition 0.000 claims description 2
- 239000003549 soybean oil Substances 0.000 claims description 2
- 235000012424 soybean oil Nutrition 0.000 claims description 2
- 239000008170 walnut oil Substances 0.000 claims description 2
- 238000000034 method Methods 0.000 abstract description 13
- 240000005373 Panax quinquefolius Species 0.000 abstract description 5
- 239000003814 drug Substances 0.000 abstract description 5
- 235000013305 food Nutrition 0.000 abstract description 4
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 240000002234 Allium sativum Species 0.000 abstract 1
- 229940079593 drug Drugs 0.000 abstract 1
- 239000008157 edible vegetable oil Substances 0.000 abstract 1
- 235000004611 garlic Nutrition 0.000 abstract 1
- 239000010647 garlic oil Substances 0.000 abstract 1
- 239000001397 quillaja saponaria molina bark Substances 0.000 description 10
- 229930182490 saponin Natural products 0.000 description 10
- 150000007949 saponins Chemical class 0.000 description 10
- 238000005516 engineering process Methods 0.000 description 9
- 239000000047 product Substances 0.000 description 7
- 235000002791 Panax Nutrition 0.000 description 4
- 241000208343 Panax Species 0.000 description 4
- 238000009835 boiling Methods 0.000 description 3
- 229940089161 ginsenoside Drugs 0.000 description 3
- 230000000844 anti-bacterial effect Effects 0.000 description 2
- 230000000259 anti-tumor effect Effects 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 239000004519 grease Substances 0.000 description 2
- 230000036039 immunity Effects 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000012856 packing Methods 0.000 description 2
- 238000012958 reprocessing Methods 0.000 description 2
- 238000005070 sampling Methods 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 1
- 241000233866 Fungi Species 0.000 description 1
- 102000005744 Glycoside Hydrolases Human genes 0.000 description 1
- 108010031186 Glycoside Hydrolases Proteins 0.000 description 1
- 230000001133 acceleration Effects 0.000 description 1
- 230000000975 bioactive effect Effects 0.000 description 1
- 230000004071 biological effect Effects 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000011344 liquid material Substances 0.000 description 1
- 238000003754 machining Methods 0.000 description 1
- 239000012567 medical material Substances 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000009834 vaporization Methods 0.000 description 1
- 230000008016 vaporization Effects 0.000 description 1
Abstract
The invention discloses a preparation method of a ginseng cream richly containing scare ginsenosides Rg3 and Rh2. The method comprises the following steps: taking fresh ginseng or panax quinquefolium radix, garlic and edible vegetable oil as raw materials, wherein the pressure of the raw materials in a seal pot is kept at minus 0.03-0.05 MPa; performing vacuum catalyzing, vacuum extraction and vacuum emulsification at the temperature of 20-50 DEG C, so as to prepare the ginseng cream richly containing the scare ginsenosides Rg3 and Rh2. The preparation method is advanced in process, simple and feasible, and suitable for large-scale technical production. The product can be used for medicines, foods and health products directly or after being subjected to simple processing.
Description
Technical field
The invention belongs to modern Chinese traditional medicine field,, specifically refer to a kind of preparation method that is rich in rare ginsenoside Rg3, Rh2 Radix Ginseng cream.
Background technology
Radix Ginseng (Panax giseng C.A.Mey.), Radix Panacis Quinquefolii (Panax quinquefolium L.) are Araliaceae (Araliaceae) Panax (Panax) plant.Wherein, the implication of Panax Greek is " catholicon ", and the full language pronunciation of Radix Ginseng is the meaning of " king of BAICAO " for " Ao Er is thick to be reached ".As traditional medical material, has the history in thousands of years, in the countries in the world extensive use.The active component of generally acknowledging main in Radix Ginseng, the Radix Panacis Quinquefolii is the ginsenoside.Wherein, ginsenoside Rg3, Rh2 become the research focus in this field as the rare saponin of antitumor, resisting fatigue, raising immunity the best among the ginsenoside.Yet these two kinds of rare saponin exist in the common processed goods water ginseng of Radix Ginseng, Radix Panacis Quinquefolii, Radix Ginseng, active ginseng hardly, also only exist with small content in Radix Ginseng Rubra, black ginseng and Herba Salviae Chinensis, and the existing medicine, food, health product of being used for is also rare.
Summary of the invention
The objective of the invention is to overcome the existing in prior technology shortcoming provides a kind of preparation method that is rich in rare ginsenoside Rg3, Rh2 Radix Ginseng cream, and this preparation method technology advanced person is simple for process, is applicable to the big production of technology.Its product can directly or after simple reprocessing be used for medicine, food, health product.
Technical scheme of the present invention is as follows:
A kind of preparation method that is rich in rare ginsenoside Rg3, Rh2 Radix Ginseng cream may further comprise the steps:
A, raw material pre-treatment: fresh ginseng or bright Radix Panacis Quinquefolii clean remove impurity, cleaning, 40 ℃ ~ 70 ℃ oven dry, it is standby to go reed to cut into 3 ~ 5mm thin slice; The vegetable oil fine straining is standby; Bulbus Allii clean the peeling remove impurity, with the water of 1 ~ 5 times of weight under 100 ℃ ~ 130 ℃, 0.1 ~ 1MPa condition steaming processing 1 ~ 8h, to get Bulbus Allii juice standby;
B, vacuum catalysis: the fresh ginseng that a step is standby or the section of bright Radix Panacis Quinquefolii and Bulbus Allii juice feed intake in hermetically sealed can with the part by weight of 5 ~ 20:1, jar internal pressure maintenance-0.03 ~-0.05MPa, 20 ℃ ~ 50 ℃ of temperature, stirring reaction 1 ~ 5 day;
C, vacuum hydro-extraction: the vegetable oil that a step is standby joins in the interior system of jar of b step, and the part by weight that feeds intake is vegetable oil: fresh ginseng or Radix Panacis Quinquefolii section 1 ~ 5:1, and jar internal pressure maintenance-0.03 ~-0.05MPa, 20 ℃ ~ 50 ℃ of temperature, stir extraction 10 ~ 30 days, filter filtrate for later use;
D, vacuum emulsification: the filtrate that obtains in the c step is placed in the hermetically sealed can, jar internal pressure maintenance-0.03 ~-0.05MPa, 20 ℃ ~ 50 ℃ of temperature, stirring and emulsifying 5 ~ 10 days gets Radix Ginseng cream.
Described vegetable oil is Oleum Ricini, Oleum Brassicae campestris, soybean oil, olive oil, walnut oil, Oleum Arachidis hypogaeae semen, Oleum Helianthi, Testa oryzae oil, Oleum Gossypii semen, germ oil, Oleum pini koraiensis, Semen Maydis oil or tempered oil.
The present invention is directed to common Radix Ginseng, Radix Panacis Quinquefolii processed goods at present, as in water ginseng, Radix Ginseng, active ginseng, Radix Ginseng Rubra, Herba Salviae Chinensis, the black ginseng have than powerful antitumor, resisting fatigue, the bioactive rare saponin Rg3 of raising immunity, Rh2 exists hardly or trace exists.In order to improve rare saponin Rg3, the Rh2 content in Radix Ginseng, the Radix Panacis Quinquefolii processed goods, improve the biological activity of processed goods, improve added value of product; Be raw material with fresh ginseng or bright Radix Panacis Quinquefolii, Bulbus Allii and vegetable oil, according to experimental data, invented a kind of production technology of utilizing vacuum catalysis, vacuum hydro-extraction, the preparation of vacuum emulsification technology to be rich in rare saponin Rg3, Rh2 Radix Ginseng cream.
Reduction along with air pressure descends according to the boiling point of liquid, and vacuum can cause principles such as liquid seethes with excitement rapidly, vaporization.Adopt technology such as vacuum catalysis, vacuum hydro-extraction, vacuum emulsification as advanced cutting edge technology of modern times, utilize pressure to be reduced to nearly vacuum state, the most liquid material can seethe with excitement under lower temperature, the movement velocity of molecule is sharply accelerated, thereby improved the efficient of chemical reaction, extraction, emulsifying.The present invention considers that just nearly vacuum state can make Yi Shui, oil for solvent, the reaction system that is participated in by fresh ginseng or bright Radix Panacis Quinquefolii, Bulbus Allii, vegetable oil, in lower temperature, also be under the optimum temperature of whole production, can remain on the state of boiling, thus the acceleration that accelerated reaction changes.In this process, the ginsenoside's constituents in Radix Ginseng or the Radix Panacis Quinquefolii under the effect of the intrinsic glycoside hydrolase of Radix Ginseng or Radix Panacis Quinquefolii, is degraded to rare saponin Rg3, Rh2, and is extracted by vegetable oil under the low-temperature boiling state and emulsifying combines together.In entire reaction course, Bulbus Allii grease after treatment has on the one hand very strong, broad-spectrum antibacterial activity, can suppress whole reaction system under eutrophic state, the long-time placement, growing of antibacterial and fungus causes the degraded of nutrient substance and effective ingredient; On the other hand, this grease can be worked in coordination with extraction and the emulsifying of finishing rare saponin Rg3, Rh2 with vegetable oil.
Low even the problem that almost do not have of the present invention's rare saponin content from the product that has solved Radix Ginseng, Radix Panacis Quinquefolii conventional machining process gained in essence utilizes vacuum catalysis, vacuum hydro-extraction, the vacuum emulsification technology to process the Radix Ginseng cream that is rich in rare ginsenoside Rg3, Rh2.Its product can directly or after simple reprocessing be used for medicine, food, health product.
Be raw material with fresh ginseng, Bulbus Allii, Fructus Maydis oil, the income earner joins processed goods evaluation to various processes.Experimental data such as following table:
Can be drawn by above data, contain rare saponin Rh2 and Rg3 hardly in fresh ginseng, Radix Ginseng, active ginseng, content in the Radix Ginseng Rubra is 0.005 ~ 0.049mg/g only also, and the content of these two kinds of rare saponin exceeds 2 ~ 8 times than content in the Radix Ginseng Rubra in the Radix Ginseng cream.
The specific embodiment
Embodiment 1:
A, raw material pre-treatment: fresh ginseng 20kg cleans remove impurity, cleaning, 60 ℃ of oven dry, it is standby to go reed to cut into the 5mm thin slice, and Fructus Maydis oil 40L fine straining is standby, Bulbus Allii 2kg cleans the peeling remove impurity, with 120 ℃/0.5MPa of 1 times of water steaming processing 4h, to get Bulbus Allii juice standby;
B, vacuum catalysis: the fresh ginseng of a step process gained or the section of bright Radix Panacis Quinquefolii and Bulbus Allii juice are fed intake in hermetically sealed can jar internal pressure maintenance-0.05MPa, 30 ℃ of temperature, stirring reaction 3 days;
C, vacuum hydro-extraction: the Fructus Maydis oil of a step process gained is joined in the jar of b step process gained in the system, jar internal pressure maintenances-0.03MPa, 40 ℃ of temperature stir and extracted filtration, filtrate for later use 30 days;
D, vacuum emulsification: will handle the filtrate that obtains through c and place in the hermetically sealed can, jar internal pressure maintenance-0.05MPa, 20 ℃ of temperature, stirring and emulsifying 5 days gets Radix Ginseng cream;
E, detection: sampling Radix Ginseng cream is tested;
F, packing: the Radix Ginseng cream through being up to the standards is packed by specification, seals up for safekeeping.
Embodiment 2:
A, raw material pre-treatment: bright Radix Panacis Quinquefolii 20kg cleans remove impurity, cleaning, 50 ℃ of oven dry, it is standby to go reed to cut into the 3mm thin slice, and olive oil 50L fine straining is standby, Bulbus Allii 4kg cleans the peeling remove impurity, with 110 ℃/0.2MPa of 2 times of water steaming processing 6h, to get Bulbus Allii juice standby;
B, vacuum catalysis: will feed intake in hermetically sealed can jar internal pressure maintenance-0.03MPa, 40 ℃ of temperature, stirring reaction 2 days through the fresh ginseng of a step process gained or the section of bright Radix Panacis Quinquefolii and Bulbus Allii juice;
C, vacuum hydro-extraction: will join through the olive oil of a step process gained in the jar of b step process gained in the system, jar internal pressure maintenances-0.05MPa, 50 ℃ of temperature stir and extracted filtration, filtrate for later use 20 days;
D, vacuum emulsification: will place through the filtrate that the c step process obtains in the hermetically sealed can, jar internal pressure maintenance-0.05MPa, 25 ℃ of temperature, stirring and emulsifying 10 days gets Radix Ginseng cream;
E, detection: sampling Radix Ginseng cream is tested;
F, packing: the Radix Ginseng cream through being up to the standards is packed by specification, seals up for safekeeping.
Claims (2)
1. preparation method that is rich in rare ginsenoside Rg3, Rh2 Radix Ginseng cream may further comprise the steps:
A, raw material pre-treatment: fresh ginseng or bright Radix Panacis Quinquefolii clean remove impurity, cleaning, 40 ℃ ~ 70 ℃ oven dry, it is standby to go reed to cut into 3 ~ 5mm thin slice; The vegetable oil fine straining is standby; Bulbus Allii clean the peeling remove impurity, with the water of 1 ~ 5 times of weight under 100 ℃ ~ 130 ℃, 0.1 ~ 1MPa condition steaming processing 1 ~ 8h, to get Bulbus Allii juice standby;
B, vacuum catalysis: the fresh ginseng that a step is standby or the section of bright Radix Panacis Quinquefolii and Bulbus Allii juice feed intake in hermetically sealed can with the part by weight of 5 ~ 20:1, jar internal pressure maintenance-0.03 ~-0.05MPa, 20 ℃ ~ 50 ℃ of temperature, stirring reaction 1 ~ 5 day;
C, vacuum hydro-extraction: the vegetable oil that a step is standby joins in the interior system of jar of b step, and the part by weight that feeds intake is vegetable oil: fresh ginseng or Radix Panacis Quinquefolii section 1 ~ 5:1, and jar internal pressure maintenance-0.03 ~-0.05MPa, 20 ℃ ~ 50 ℃ of temperature, stir extraction 10 ~ 30 days, filter filtrate for later use;
D, vacuum emulsification: the filtrate that obtains in the c step is placed in the hermetically sealed can, jar internal pressure maintenance-0.03 ~-0.05MPa, 20 ℃ ~ 50 ℃ of temperature, stirring and emulsifying 5 ~ 10 days gets Radix Ginseng cream.
2. a kind of preparation method that is rich in rare ginsenoside Rg3, Rh2 Radix Ginseng cream according to claim 1 is characterized in that described vegetable oil is Oleum Ricini, Oleum Brassicae campestris, soybean oil, olive oil, walnut oil, Oleum Arachidis hypogaeae semen, Oleum Helianthi, Testa oryzae oil, Oleum Gossypii semen, germ oil, Oleum pini koraiensis, Fructus Maydis tempered oil.
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| CN201310245097.8A CN103271960B (en) | 2013-06-20 | 2013-06-20 | Preparation method of ginseng cream richly containing scare ginsenosides Rg3 and Rh2 |
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| CN201310245097.8A CN103271960B (en) | 2013-06-20 | 2013-06-20 | Preparation method of ginseng cream richly containing scare ginsenosides Rg3 and Rh2 |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103989719A (en) * | 2014-05-23 | 2014-08-20 | 吉林农业大学 | Ginseng flat-soluble part and application thereof for alleviating hangover |
| CN104644658A (en) * | 2013-11-22 | 2015-05-27 | 富力 | Application of ginsenoside Rg3 in preparation of medicine for relieving and/or treating dementia disease and medicine |
| CN104957714A (en) * | 2015-05-26 | 2015-10-07 | 高健铭 | Compound American ginseng essential oil drink to prevent neuronal damage in elderly |
| CN107751419A (en) * | 2017-11-10 | 2018-03-06 | 哈尔滨美森食品制造有限公司 | A kind of preparation method of baby walnut powdered oil |
| CN109223582A (en) * | 2018-10-31 | 2019-01-18 | 延边大学 | Diol type ginsenoside nano-emulsion with anti aging effect function and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
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| CN104957714A (en) * | 2015-05-26 | 2015-10-07 | 高健铭 | Compound American ginseng essential oil drink to prevent neuronal damage in elderly |
| CN107751419A (en) * | 2017-11-10 | 2018-03-06 | 哈尔滨美森食品制造有限公司 | A kind of preparation method of baby walnut powdered oil |
| CN109223582A (en) * | 2018-10-31 | 2019-01-18 | 延边大学 | Diol type ginsenoside nano-emulsion with anti aging effect function and preparation method thereof |
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Effective date of registration: 20240307 Address after: Room 601, Unit 2, Building 3, Industrial and Commercial Bank Community, Zhongyin Hutong, Bohai Street, Dunhua City, Yanbian Korean Autonomous Prefecture, Jilin Province, 133700 Patentee after: Liu Junsen Country or region after: China Address before: 133700, No.14 Ziyou Road, Bohai Street, Dunhua City, Yanbian Korean Autonomous Prefecture, Jilin Province Patentee before: Dunhua Guangsheng Biotechnology Oil Co.,Ltd. Country or region before: China |
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