CN110169935A - A kind of compound for pore refining and preparation method thereof, application - Google Patents
A kind of compound for pore refining and preparation method thereof, application Download PDFInfo
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- CN110169935A CN110169935A CN201910458604.3A CN201910458604A CN110169935A CN 110169935 A CN110169935 A CN 110169935A CN 201910458604 A CN201910458604 A CN 201910458604A CN 110169935 A CN110169935 A CN 110169935A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9728—Fungi, e.g. yeasts
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/591—Mixtures of compounds not provided for by any of the codes A61K2800/592 - A61K2800/596
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- Medicines Containing Plant Substances (AREA)
- Cosmetics (AREA)
Abstract
The present invention relates to cosmetic field, a kind of compound for pore refining and preparation method thereof, application are provided, for solving the problems, such as that skin pore is coarse.A kind of compound for pore refining provided by the invention, comprising: purslane extract 2 ~ 40%, quinine fungus extract 2 ~ 40%, black extract of willow bark 2 ~ 40%.By the compounding of purslane, quinine fungus and black willow bark, can effective pore refining so that skin is more smooth.
Description
Technical field
The present invention relates to cosmetic fields, and in particular to a kind of compound for pore refining and preparation method thereof is answered
With.
Background technique
In the epoch now, everybody is walked on the road for pursuing beauty, and it is smooth, but hair that people, which are intended to oneself skin,
This coarse problem of hole is generally existing, has seriously affected the smooth fine and smooth degree of skin of face.Pore includes that naked eyes are sightless
Sweat gland opening, macroscopic pilosebaceous follicle opening, the visible pilosebaceous follicle opening etc. containing keratotic plug of naked eyes.According to multi-party research
And data surface, the reason for causing skin of face pore coarse mainly include heredity, skin quality, hormone secretion level, sebaceous glands oil
Rouge secretion is vigorous, and ultraviolet light irradiation causes skin lesion, skin aging, eating habit, skin care habit etc..The coarse problem of pore
It mostly occurs in the face of people, often has in nose and nose periphery cheek skin, chin position, and to belong to naked eyes visible containing angle more
The pilosebaceous follicle of bolt is open.Keratotic plug includes the secretion of skin grease itself, the residues such as extraneous dust/cosmetics mixing and
At.
Therefore, how effectively pore refining, and then be that skin is more smoothed in order to which number people big absolutely are of interest now
Problem.For this problem, the product of very more pore refinings, but product quality, effect and safety have been emerged on the market
Property is irregular.This patent passes through multiple experiment and clinical test, and the pore refining for a comprehensive effect of arranging in pairs or groups out extracts
Object can directly apply in a variety of basic cosmetics systems, including aqua class, creams class cosmetics.
Summary of the invention
Present invention solves the technical problem that the problem coarse for skin pore, provides a kind of compound for pore refining
And preparation method thereof, application.
In order to solve the above technical problem, the present invention provides technical solution are as follows:
A kind of compound for pore refining, comprising: purslane extract 2 ~ 40%, quinine fungus extract 2 ~ 40% are black
Extract of willow bark 2 ~ 40%.
Purslane, medicinal bracket fungus, black willow bark extract combination can sufficient pore refining；The stem of purslane and
Leaf can be clearing heat and detoxicating, cooling blood and hemostasis, is mainly used for treating the diseases such as hot dysentery purulence blood, heat gonorrhea, vaginal discharge diseases, Carbuncle swells dislikes sore, erysipelas；Medicine
It is mainly used for treating abdominal pain, flu, night sweat, chronic bronchitis and venomous snake bite with shelf fungus；Contain naturally in black willow bark
Salicylic acid can remove the hair follicle of blocking, prevent pore from blocking, and pre- anti-acne has the effect of certain pore refining.
By the compounding of purslane, quinine fungus and black willow bark, can effective pore refining so that skin
It is more smooth.
Preferably, comprising: purslane extract 30 ~ 40%, quinine fungus 35 ~ 40%, black extract of willow bark 35 ~ 40%.
It is preferred that purslane, quinine fungus, black willow bark content can further improve compound pore refining, promote skin flat
It is sliding.
Preferably, comprising: purslane extract 30%, quinine fungus 35%, black extract of willow bark 35%.The compound
It is especially suitable for pore refining.
Preferably, the purslane extract the preparation method comprises the following steps: using low-temperature extraction method from the stem and leaf of purslane
It is middle to obtain biologically active extract as purslane extract.It is the same quinine fungus of the extract of purslane stem and leaf, black
Extract of willow bark compounding, obtained compound have the effect of better pore refining.
Preferably, the quinine fungus extract and black extract of willow bark the preparation method comprises the following steps: auxiliary using ultrasonic wave
It helps method to extract quinine fungus and black willow bark, uses the ethyl alcohol of 70% concentration to extract as solvent, the weight of ethyl alcohol and medicinal material
Amount is than being 5:1；Active carbon is added in gained filtrate and carries out decolorization, chitosan, mistake after stirring flocculation are added after filtering
Ethyl alcohol is recycled in filter, and freeze-drying obtained solid is quinine fungus and black extract of willow bark.Quinine fungus is the same as black willow
Skin is extracted rear decoloring and flocculated with ethyl alcohol together removes carbohydrate impurity, can further remove the keratotic plug in pore, shrink
Pore, smooth skin.
A kind of compound for pore refining mentions purslane extract, quinine fungus extract and black willow bark
It takes object to be dissolved in solvent and is dried to obtain the compound for pore refining after mixing is uniformly dispersed.Three kinds of extract mixing can make
At compound, manufacture craft is simple, and production cost is low.
Preferably, purslane extract is mixed in equal volume with butanediol, obtains the first mixed liquor；Quinine fungus is mentioned
The mixed liquor obtained after taking object to mix with black extract of willow bark with the ethyl alcohol of 5 times of amounts is mixed with deionized water, and it is mixed to obtain second
Liquid is closed, the content of deionized water is 73 ~ 80% in second mixed liquor；It is dry after first and second mixed liquors are mixed, it obtains
To the compound for pore refining.
Preferably, compound is added to is in the cosmetics of basic solvent with water, and additive amount is 2 ~ 10%.Compound is same
It is used with the cosmetic combinations that water is basic solvent, can fully play its pore refining, the effect of firm skin.
Preferably, during compound being added to the cosmetics with water for basic solvent, control temperature is no more than 60
Degree Celsius, pH is controlled 2 ~ 9.In compound adding procedure, temperature is unsuitable excessively high, while the temperature and pH value are the same as the skin of human body
The temperature and pH value of skin are close, show that the compound is smaller to skin irritation.
Compared with prior art, the device have the advantages that are as follows: pass through purslane, quinine fungus and black willow bark
Compounding, can effective pore refining so that skin is more smooth；Compound is the same as the cosmetics for taking water as basic solvent
It is applied in combination, can fully play its pore refining, the effect of firm skin.
Specific embodiment
It the following examples are further illustrations of the invention, is not limitation of the present invention.
Embodiment 1
A kind of compound for pore refining, comprising: purslane extract 30%, quinine fungus 35%, black willow bark extract
Object 35%.The purslane extract the preparation method comprises the following steps: being had from the stem and leaf of purslane using low-temperature extraction method
The extract of bioactivity is purslane extract.The preparation method of the quinine fungus extract and black extract of willow bark
Are as follows: quinine fungus and black willow bark are extracted using ultrasonic wave auxiliary law, the ethyl alcohol of 70% concentration is used to be mentioned as solvent
It takes, the weight ratio of ethyl alcohol and medicinal material is 5:1；Active carbon is added in gained filtrate and carries out decolorization, adds shell after filtering
Glycan filters after stirring flocculation, recycles ethyl alcohol, freeze-drying obtained solid is quinine fungus and black extract of willow bark.
Purslane extract is mixed in equal volume with butanediol, obtains the first mixed liquor；By quinine fungus extract and black willow bark
Extract is mixed with the mixed liquor obtained after the ethyl alcohol mixing of 5 times of amounts with deionized water, obtains the second mixed liquor, described second is mixed
The content for closing deionized water in liquid is 73 ~ 80%；It is dry after first and second mixed liquors are mixed, it obtains for pore refining
It take water as additive amount 5% in the cosmetics of basic solvent that compound is added to by compound.Compound is added to and is with water
During the cosmetics of base solvent, control temperature is no more than 60 degrees Celsius, and pH is controlled 7.
Purslane, medicinal bracket fungus, black willow bark extract combination can sufficient pore refining；The stem of purslane and
Leaf can be clearing heat and detoxicating, cooling blood and hemostasis, is mainly used for treating the diseases such as hot dysentery purulence blood, heat gonorrhea, vaginal discharge diseases, Carbuncle swells dislikes sore, erysipelas；Medicine
It is mainly used for treating abdominal pain, flu, night sweat, chronic bronchitis and venomous snake bite with shelf fungus；Contain naturally in black willow bark
Salicylic acid can remove the hair follicle of blocking, prevent pore from blocking, and pre- anti-acne has the effect of certain pore refining.Pass through horse
The compounding of bitterroot, quinine fungus and black willow bark, can effective pore refining so that skin is more smooth.It is preferred that
Purslane, quinine fungus, black willow bark content can further improve compound pore refining, promote skin smooth.
The compound is especially suitable for pore refining.The same quinine fungus of the extract of purslane stem and leaf, black extract of willow bark
Compounding, the effect of obtained compound pore refining are more preferable.Quinine fungus extracts rear decoloring with ethyl alcohol together with black willow bark
And flocculate and remove carbohydrate impurity, it can further remove the keratotic plug in pore, pore refining, smooth skin.Three kinds of extractions
Object mixing can be made into compound, and manufacture craft is simple, and production cost is low.Compound is the same as the cosmetics group for taking water as basic solvent
It closes and uses, can fully play its pore refining, the effect of firm skin.In compound adding procedure, temperature is unsuitable excessively high,
Simultaneously the temperature and pH value it is close with the temperature and pH value of the skin of human body, show the compound to skin irritation compared with
It is small.
Embodiment 2
A kind of compound for pore refining, comprising: purslane extract 40%, quinine fungus 40%, black willow bark extract
Object 20%.The purslane extract the preparation method comprises the following steps: being had from the stem and leaf of purslane using low-temperature extraction method
The extract of bioactivity is purslane extract.The preparation method of the quinine fungus extract and black extract of willow bark
Are as follows: quinine fungus and black willow bark are extracted using ultrasonic wave auxiliary law, the ethyl alcohol of 70% concentration is used to be mentioned as solvent
It takes, the weight ratio of ethyl alcohol and medicinal material is 5:1；Active carbon is added in gained filtrate and carries out decolorization, adds shell after filtering
Glycan filters after stirring flocculation, recycles ethyl alcohol, freeze-drying obtained solid is quinine fungus and black extract of willow bark.
Purslane extract is mixed in equal volume with butanediol, obtains the first mixed liquor；By quinine fungus extract and black willow bark
Extract is mixed with the mixed liquor obtained after the ethyl alcohol mixing of 5 times of amounts with deionized water, obtains the second mixed liquor, described second is mixed
The content for closing deionized water in liquid is 73 ~ 80%；It is dry after first and second mixed liquors are mixed, it obtains for pore refining
Compound.It take water as additive amount 5% in the cosmetics of basic solvent that compound, which is added to,.Compound is added to and is with water
During the cosmetics of base solvent, control temperature is no more than 60 degrees Celsius, and pH is controlled 7.
Embodiment 3
A kind of compound for pore refining, comprising: purslane extract 40%, quinine fungus 20%, black willow bark extract
Object 40%.The purslane extract the preparation method comprises the following steps: being had from the stem and leaf of purslane using low-temperature extraction method
The extract of bioactivity is purslane extract.The preparation method of the quinine fungus extract and black extract of willow bark
Are as follows: quinine fungus and black willow bark are extracted using ultrasonic wave auxiliary law, the ethyl alcohol of 70% concentration is used to be mentioned as solvent
It takes, the weight ratio of ethyl alcohol and medicinal material is 5:1；Active carbon is added in gained filtrate and carries out decolorization, adds shell after filtering
Glycan filters after stirring flocculation, recycles ethyl alcohol, freeze-drying obtained solid is quinine fungus and black extract of willow bark.
Purslane extract is mixed in equal volume with butanediol, obtains the first mixed liquor；By quinine fungus extract and black willow bark
Extract is mixed with the mixed liquor obtained after the ethyl alcohol mixing of 5 times of amounts with deionized water, obtains the second mixed liquor, described second is mixed
The content for closing deionized water in liquid is 73 ~ 80%；It is dry after first and second mixed liquors are mixed, it obtains for pore refining
Compound.It take water as additive amount 5% in the cosmetics of basic solvent that compound, which is added to,.Compound is added to and is with water
During the cosmetics of base solvent, control temperature is no more than 60 degrees Celsius, and pH is controlled 7.
Comparative example 1
A kind of compound for pore refining, comprising: purslane extract 100%.
Comparative example 2
A kind of compound for pore refining, comprising: quinine fungus extract 100%.
Comparative example 3
A kind of compound for pore refining, comprising: black extract of willow bark 35%.
Comparative example 4
A kind of compound for pore refining, comprising: purslane extract 45%, quinine fungus 55%.
Comparative example 5
A kind of compound for pore refining, comprising: purslane extract 45%, black extract of willow bark 55%.
Comparative example 6
A kind of compound for pore refining, comprising: quinine fungus 50%, black extract of willow bark 50%.
Comparative example 7
Commercial product A
Comparative example 8
Commercial product B
Experimental example
Engage the practical cosmetics for being doped with the compound recorded in embodiment 1 ~ 3 and comparative example of several volunteers, volunteer year
Age: 18-45 years old, male or female, face skin no acute inflammation and skin disease, no cosmetic allergic contact dermatitis history, without ginseng in one month
It is tested with excessively similar, not in the gestational period and nursing period, the coarse person of face skin pore (judgment method: with tester at a distance of 0.5m
Observation, hence it is evident that visible pore).The subject to take one's test is 35.
Experimental group and experimental method
Experimental group: each subject's face is punished from the bridge of the nose as the right and left face skin, at random respectively using different
Product.
Experimental method: it is tested in constant temperature and humidity (25 degrees Celsius of temperature, humidity 60%) laboratory.Subject per surveys
Facial skin is cleaned using warm water before examination, face's remnants water droplet is gently wiped with paper handkerchief, test product is then evenly coated in list
Side nose and facial skin guarantee left and right sides skin using product without intersection.It is each using once daily morning and evening, 30 are used altogether
It.It once every three days scores, scores after every third day has used product ten minutes at night.
Evaluation rule and standard
Subject's self-assessment and instrument analysis assessment.Standards of grading: 0 point is to become larger without improvement or skin deterioration, pore；1 point
Slightly to improve；2 points improve for moderate；3 points are obviously improved；4 points hardly may be used for improvement, pore completely in the case where visually observing
See.
Subject's self-assessment: it is voluntarily evaluated by subject；
Instrument analysis assessment: using DIGIMIC800 type skin image analyzer, amplifies 10 times to same position skin, receives every time
Collect image three times, obtains pore pore size, be averaged as final data.
Experimental result
After continuous use product 60 days, the average mark of the evaluation to each product of tested volunteer and the diminution value in pore aperture
It is shown in Table 1.
1 product evaluation result of table
As known from Table 1, in embodiment 1 ~ 3 volunteer scoring highest, show comprising a certain proportion of purslane, quinine fungus
And the cosmetics of the compound of black willow bark can have good user experience, meanwhile, three compounds the compound generated and passes through
Certain way is added in cosmetics, can effective pore refining.
It include three kinds of extracts in embodiment 1 ~ 3, and one be then single use in comparative example 1 ~ 3 in three kinds of extracts
Kind, and the corresponding volunteer of comparative example 1 ~ 3 experience and the contractive effect of pore are weaker than embodiment 1 ~ 3, show be three
Compounding could obtain the effect of good pore refining according to a certain percentage.Volunteer's evaluation and aperture in comparative example 2 and 3
Diminution value is smaller with the difference of embodiment；Volunteer's evaluation and significant difference of the diminution value in aperture with embodiment, table in comparative example 1
In bright the application, the extract of quinine fungus and black willow bark may be larger to the effect for reducing pore, and purslane is extracted
The effect of object is the effect of significantly promoting this diminution pore.
It is compounded two-by-two in comparative example 4 ~ 6 using two kinds in three kinds of extracts, effect is also weaker than embodiment, shows
Only two kinds of compound compoundings not can obviously improve the effect of compound reduces pore.
Above-listed detailed description is illustrating for possible embodiments of the present invention, and above embodiments are not to limit this
The scope of the patents of invention, all equivalence enforcements or change without departing from carried out by the present invention, is intended to be limited solely by the scope of the patents of this case.
Claims (9)
1. a kind of compound for pore refining characterized by comprising purslane extract 2 ~ 40%, quinine fungus mentions
Take object 2 ~ 40%, black extract of willow bark 2 ~ 40%.
2. a kind of compound for pore refining according to claim 1 characterized by comprising purslane is extracted
Object 30 ~ 40%, quinine fungus 35 ~ 40%, black extract of willow bark 35 ~ 40%.
3. a kind of compound for pore refining according to claim 2 characterized by comprising purslane is extracted
Object 30%, quinine fungus 35%, black extract of willow bark 35%.
4. a kind of compound for pore refining according to claim 1, which is characterized in that the purslane extract
The preparation method comprises the following steps: obtained from the stem and leaf of purslane using low-temperature extraction method biologically active extract be dent
Amaranth extract.
5. a kind of compound for pore refining according to claim 1, which is characterized in that the quinine fungus mentions
Take object and black extract of willow bark the preparation method comprises the following steps: extracts quinine fungus and black willow bark using ultrasonic wave auxiliary law, makes
The ethyl alcohol of 70% concentration is used to extract as solvent, the weight ratio of ethyl alcohol and medicinal material is 5:1；Activity is added in gained filtrate
Charcoal carries out decolorization, and chitosan is added after filtering, is filtered after stirring flocculation, recycles ethyl alcohol, and freeze-drying obtained solid is
For quinine fungus and black extract of willow bark.
6. a kind of preparation method of the compound for pore refining, which is characterized in that by purslane extract, quinine fungus
Extract and black extract of willow bark are dissolved in solvent and are dried to obtain the compound for pore refining after mixing is uniformly dispersed.
7. a kind of preparation method of compound for pore refining according to claim 6, which is characterized in that by dent
Amaranth extract mixes in equal volume with butanediol, obtains the first mixed liquor；By quinine fungus extract and black extract of willow bark
It is mixed with obtained mixed liquor after the ethyl alcohol mixing of 5 times of amounts with deionized water, obtains the second mixed liquor, in second mixed liquor
The content of deionized water is 73 ~ 80%；It is dry after first and second mixed liquors are mixed, it obtains for the compound of pore refining
Object.
8. a kind of application of the compound for pore refining, which is characterized in that being added to compound with water as basic solvent
Cosmetics in, additive amount be 2 ~ 10%.
9. a kind of compound for pore refining according to claim 8, which is characterized in that by compound be added to
During water is the cosmetics of basic solvent, control temperature is no more than 60 degrees Celsius, and pH is controlled 2 ~ 9.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111450000A (en) * | 2020-04-08 | 2020-07-28 | 深圳市大美仁生物科技有限公司 | Formula for instantly and long-acting shrinking pores and application |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106963697A (en) * | 2017-05-19 | 2017-07-21 | 广州蜜妆生物科技有限公司 | It is a kind of that there is oil-control, the facial mask liquid of pore refining effect |
| CN109528582A (en) * | 2018-12-10 | 2019-03-29 | 澳宝化妆品（惠州）有限公司 | A kind of skin care compositions containing black extract of willow bark |
-
2019
- 2019-05-29 CN CN201910458604.3A patent/CN110169935A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106963697A (en) * | 2017-05-19 | 2017-07-21 | 广州蜜妆生物科技有限公司 | It is a kind of that there is oil-control, the facial mask liquid of pore refining effect |
| CN109528582A (en) * | 2018-12-10 | 2019-03-29 | 澳宝化妆品（惠州）有限公司 | A kind of skin care compositions containing black extract of willow bark |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111450000A (en) * | 2020-04-08 | 2020-07-28 | 深圳市大美仁生物科技有限公司 | Formula for instantly and long-acting shrinking pores and application |
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Application publication date: 20190827 |