CN110613641A - Zero-corrosion-resistance composition and application thereof in cosmetics - Google Patents
Zero-corrosion-resistance composition and application thereof in cosmetics Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/74—Biological properties of particular ingredients
- A61K2800/75—Anti-irritant
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Abstract
The invention discloses a zero-corrosion-resistance composition and application thereof in cosmetics. The zero-corrosion-resistant composition comprises the following components in percentage by weight: 0.01-20% of zanthoxylum bungeanum fruit extract, 0.01-20% of forsythia suspensa fruit extract, 0.01-20% of purslane extract and the balance of water. The zero-preservative composition disclosed by the invention is simple in formula composition, can achieve self-preservative capability on the premise of not adding any preservative, ensures that a product is not infected by bacteria or fungi, is low in irritation, can greatly reduce skin burden, and has profound significance in application in cosmetics; meanwhile, the composition also has the obvious effects of relieving and anti-allergy, moisturizing and resisting aging.
Description
Technical Field
The invention relates to the field of cosmetics, and particularly relates to a zero-corrosion-resistant composition and application thereof in cosmetics.
Background
Preservatives are substances which prevent the growth of microbial action. The preservation of the cosmetics is to protect the finished products of the cosmetics from being polluted by bacteria, mould and microzyme within the shelf life. Related components are chemically changed under the irradiation of sunlight, so that people can feel light, and the skin becomes red, black and painful; causing allergy to people and causing symptoms of red and oxygen; or cause skin burn. Excessive or improper preservative can lead epidermal cells to develop immature and loose structure, so that the epidermal layer becomes thin and easy to be stimulated by the outside and the defense ability is reduced; can damage cell DNA, gradually lose the elasticity of the skin and easily generate relaxation and fine lines; skin cells damaged by the preservative are continuously defectively propagated, so that the skin quality is poorer and poorer. Therefore, the research on the cosmetics which have high safety performance, are mild and do not irritate and reduce the skin burden has important significance.
Disclosure of Invention
In order to overcome the defects of the prior art, the invention provides a zero-corrosion-resistant composition and application thereof in cosmetics.
Specifically, the invention provides a zero-corrosion-resistant composition which comprises the following components in percentage by weight: 0.01-20% of zanthoxylum bungeanum fruit extract, 0.01-20% of forsythia suspensa fruit extract, 0.01-20% of purslane extract and the balance of water.
In another preferred embodiment, the invention provides a zero corrosion protection composition, which comprises the following components in percentage by weight: 0.01-20% of zanthoxylum bungeanum fruit extract, 0.01-20% of forsythia suspensa fruit extract, 0.01-20% of purslane extract and the balance of water.
In another preferred embodiment, the present invention provides a zero-preservative cosmetic composition comprising the following components in percentage by weight: 0.5% of zanthoxylum bungeanum fruit extract, 0.3% of forsythia suspensa fruit extract, 0.5% of purslane herb extract and the balance of water.
Preferably, the purslane extract mainly contains chemical components such as alkaloids, terpenoids, coumarins, flavonoids, organic acids, volatile oil, polysaccharides and the like.
Preferably, the zanthoxylum bungeanum fruit extract contains active ingredients such as limonene, cumic alcohol, chinolol, phytosterol, benzoic acid, unsaturated organic acid, diosmin, alkaloid and the like.
Preferably, the fructus forsythiae extract contains hypericin, triterpenoid saponin, phytosterol, phillyrin, alkaloid, saponin, oleanolic acid, coumarins, abundant vitamins, a small amount of volatile oil and other active ingredients.
In another preferred embodiment, the zanthoxylum bungeanum maxim fruit extract can be extracted by a steam distillation method, a vegetable oil extraction method, an edible alcohol extraction method, an anhydrous ether extraction method and a supercritical carbon dioxide fluid extraction method, wherein the content and the extraction rate of active ingredients of a product obtained by the supercritical carbon dioxide extraction are the highest, and the extraction rates of the zanthoxylum bungeanum maxim volatile oil and the ephedrine reach 100 percent and 94.6 percent respectively.
Preferably, the forsythia suspense extract is extracted by supercritical CO2The extraction technology has the optimal process conditions that: the extraction pressure is 27MPa, and the temperature is 60 ℃; the pressure of the resolution kettle I is 14MPa, and the temperature is 64 ℃; the pressure of the resolution kettle II is 6MPa, and the temperature is 50 ℃; CO 22The flow rate is 25kg/kg raw material.h; the extraction time is 5 h; the carrying agent is alcohol.
Preferably, the purslane extract is extracted by a solvent extraction method, an ultrasonic-assisted extraction method, a microwave-assisted extraction method, an enzyme extraction method, a high-voltage pulse electric field extraction method and a homogenization/hot water extraction method.
Preferably, the cosmetic composition forms include, but are not limited to, essence, emulsion, cream, gel, dressing.
The invention also provides a preparation method of the zero-corrosion-resistant composition, which sequentially comprises the following steps:
(1) weighing the raw materials according to the weight percentage for later use;
(2) and respectively adding the purslane extract, the pricklyash peel extract and the forsythia suspense extract into water, and uniformly stirring and dissolving to obtain the zero-preservative composition.
Preferably, the temperature of step (2) of the preparation method of the zero corrosion prevention composition is 35-55 ℃, and the stirring speed is 60-80 rpm.
In another preferred embodiment, the zanthoxylum bungeanum maxim fruit extract can be extracted by a steam distillation method, a vegetable oil extraction method, an edible alcohol extraction method, an anhydrous ether extraction method and a supercritical carbon dioxide fluid extraction method, wherein the effective component content and the extraction rate of a product obtained by the supercritical carbon dioxide extraction are highest, and the extraction rates of the zanthoxylum bungeanum maxim volatile oil and the ephedrine reach 100 percent and 94.6 percent respectively.
Preferably, the forsythia suspense extract is extracted by supercritical CO2The extraction technology has the optimal process conditions that: the extraction pressure is 27MPa, and the temperature is 60 ℃; analysis ofThe pressure of a kettle I is 14MPa, and the temperature is 64 ℃; the pressure of the resolution kettle II is 6MPa, and the temperature is 50 ℃; CO 22The flow rate is 25kg/kg raw material.h; the extraction time is 5 h; the carrying agent is alcohol.
The invention also provides application of the zero-preservative composition in preparing skin care products for external application of skin.
Preferably, the zero preservative composition of the present invention has a simple formulation and low irritation, and can greatly reduce the skin burden.
Preferably, the preservative-free composition of the present invention does not contain a preservative, and has significant soothing, anti-allergy, moisturizing and anti-aging effects.
Compared with the prior art, the invention has the beneficial effects that:
first, the zero-preservative composition of the invention can really ensure that the product is not infected by bacteria or fungi on the premise of not adding any preservative, and really realizes zero-preservative.
Secondly, the zero-preservative composition disclosed by the invention has a remarkable soothing and anti-allergy effect and small irritation by utilizing the synergistic effect of the purslane extract, the zanthoxylum fruit extract and the forsythia suspensa extract, and also has the effects of moisturizing and resisting aging.
Thirdly, the preparation method of the zero-corrosion-resistant composition is safe and simple, and can be used for large-scale production.
Drawings
Fig. 1 is a red area image taken by a VISIA skin tester after the subject first cleans his/her cheek.
FIG. 2 is a red area image taken by a VISIA skin tester after the subject had cleaned their cheeks for the second time.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention. The examples, in which specific conditions are not specified, were conducted under conventional conditions or conditions recommended by the manufacturer. The reagents or instruments used are not indicated by the manufacturer, and are all conventional products available commercially.
The phytosterol in the zanthoxylum bungeanum maxim fruit extract has the function of regulating the level of human hormone and has special effects on the aspects of aging resistance and the like.
Fructus forsythiae extract has certain moisture keeping effect, moderate moisture absorption effect, and can be used for improving xerosis cutis and pachylosis; has good comprehensive oxidation resistance, and has effects of promoting skin activity and resisting aging by combining with promotion effect on epithelial proliferation factor.
Purslane is rich in a large amount of flavonoids, adrenalines, polysaccharides, various vitamins, amino acids and other compounds. In cosmetics, the acne removing cream is mainly used for resisting allergy, inflammation and inflammation, resisting various external irritation to skin and also has an acne removing function. Especially has obvious anti-allergic effect on skin allergy caused by long-term use of hormone cosmetics.
The composition has the effects of safely relieving and anti-allergy by utilizing the synergistic effect of the purslane extract, the pricklyash peel extract and the fructus forsythiae extract, can calm and relieve the skin, enhances the skin barrier, plays a role in diminishing inflammation, and also has the effects of moisturizing and resisting aging.
Example of implementation 1
This example contains the zero corrosion inhibiting composition of the present invention: and (3) Chinese prickly ash fruit extract: 0.5g, forsythia suspense extract: 0.3g, purslane extract: 0.5g, glycerin: 5g, and further comprises the following raw materials: carbomer: 0.1g, pH adjuster, arginine: 0.08g, xanthan gum: 0.1g, water: 94 g.
The preparation method of the zero corrosion prevention composition described in this embodiment includes the following steps:
(1) weighing the raw materials according to the weight of the raw materials for later use;
(2) dispersing carbomer with glycerol, adding xanthan gum and water, heating to 80 deg.C, stirring at 60rpm for 15min, cooling to 40 deg.C to obtain mixed solution A;
(3) and uniformly mixing the mixed solution A with arginine serving as a pH regulator, and adding a pricklyash peel fruit extract, a fructus forsythiae extract and a purslane extract to obtain the product of the embodiment.
Example of implementation 2
This example contains the zero corrosion inhibiting composition of the present invention: and (3) Chinese prickly ash fruit extract: 0.6g, forsythia suspense extract: 0.4g, purslane extract: 0.6g, glycerin: 6g, and further comprises the following raw materials: carbomer: 0.12g, pH adjuster, arginine: 0.096g, xanthan gum: 0.15g, water: 92 g.
The preparation method of the zero corrosion protection composition described in this example includes the following steps:
(1) weighing the raw materials according to the weight of the raw materials for later use;
(2) dispersing carbomer with glycerol, adding xanthan gum and water, heating to 80 deg.C, stirring at 60rpm for 15min, cooling to 40 deg.C to obtain mixed solution A;
(3) and uniformly mixing the mixed solution A with arginine serving as a pH regulator, and adding a pricklyash peel fruit extract, a fructus forsythiae extract and a purslane extract to obtain the product of the embodiment.
Example of implementation 3
This example contains the zero corrosion inhibiting composition of the present invention: and (3) Chinese prickly ash fruit extract: 0.4g, forsythia suspense extract: 0.2g, purslane extract: 0.4g, glycerin: 4g, and further comprises the following raw materials: carbomer: 0.13g, pH adjuster, arginine: 0.104g, xanthan gum: 0.2g, water: 95 g.
The preparation method of the zero corrosion protection composition described in this example includes the following steps:
(1) weighing the raw materials according to the weight of the raw materials for later use;
(2) dispersing carbomer with glycerol, adding xanthan gum and water, heating to 80 deg.C, stirring at 60rpm for 15min, cooling to 40 deg.C to obtain mixed solution A;
(3) and uniformly mixing the mixed solution A with arginine serving as a pH regulator, and adding a pricklyash peel fruit extract, a fructus forsythiae extract and a purslane extract to obtain the product of the embodiment.
Example of implementation 4
This example contains the zero corrosion inhibiting composition of the present invention: and (3) Chinese prickly ash fruit extract: 0.7g, forsythia suspense extract: 0.5g, purslane extract: 0.7g, glycerin: 6g, and further comprises the following raw materials: carbomer: 0.14g, pH adjuster, arginine: 0.112g, xanthan gum: 0.25g, water: 92 g.
The preparation method of the zero corrosion protection composition described in this example includes the following steps:
(1) weighing the raw materials according to the weight of the raw materials for later use;
(2) dispersing carbomer with glycerol, adding xanthan gum and water, heating to 80 deg.C, stirring at 60rpm for 15min, cooling to 40 deg.C to obtain mixed solution A;
(3) and uniformly mixing the mixed solution A with arginine serving as a pH regulator, and adding a pricklyash peel fruit extract, a fructus forsythiae extract and a purslane extract to obtain the product of the embodiment.
Example of implementation 5
This example contains the zero corrosion inhibiting composition of the present invention: and (3) Chinese prickly ash fruit extract: 0.7g, forsythia suspense extract: 0.5g, purslane extract: 0.7g, butanediol: 6g, and further comprises the following raw materials: hydrolyzing sclerotium rolfsii gum: 0.1g, hydroxyethyl cellulose: 0.1g, water: 92 g.
The preparation method of the zero corrosion prevention composition described in this embodiment includes the following steps:
(1) weighing the raw materials according to the weight of the raw materials for later use;
(2) dispersing hydrolyzed sclerotium rolfsii gum and hydroxyethyl cellulose by using butanediol, then adding water, heating to 80 ℃, keeping the temperature and stirring for 15min at the stirring speed of 60rpm, and cooling to 40 ℃ to obtain a mixed solution A;
(3) and adding the zanthoxylum bungeanum fruit extract, the forsythia suspensa fruit extract and the purslane extract into the mixed solution A to obtain the product of the embodiment.
Example of implementation 6
This example contains the zero corrosion inhibiting composition of the present invention: and (3) Chinese prickly ash fruit extract: 0.6g, forsythia suspense extract: 0.4g, purslane extract: 0.6g, butanediol: 5g, and further comprises the following raw materials: hydrolyzing sclerotium rolfsii gum: 0.15g, hydroxyethyl cellulose: 0.15g, water: 93 g.
The preparation method of the preservative-free cosmetic composition described in this example includes the following steps:
(1) weighing the raw materials according to the weight of the raw materials for later use;
(2) dispersing hydrolyzed sclerotium rolfsii gum and hydroxyethyl cellulose by using butanediol, then adding water, heating to 80 ℃, keeping the temperature and stirring for 15min at the stirring speed of 60rpm, and cooling to 40 ℃ to obtain a mixed solution A;
(3) and adding the zanthoxylum bungeanum fruit extract, the forsythia suspensa fruit extract and the purslane extract into the mixed solution A to obtain the product of the embodiment.
Example 7 of implementation
This example contains the zero preservative cosmetic composition of the present invention: and (3) Chinese prickly ash fruit extract: 0.5g, forsythia suspense extract: 0.3g, purslane extract: 0.5g, butanediol: 4g, and further comprises the following raw materials: hydrolyzing sclerotium rolfsii gum: 0.2g, hydroxyethyl cellulose: 0.2g, water: 94 g.
The preparation method of the zero-preservative cosmetic composition comprises the following steps:
(1) weighing the raw materials according to the weight of the raw materials for later use;
(2) dispersing hydrolyzed sclerotium rolfsii gum and hydroxyethyl cellulose by using butanediol, then adding water, heating to 80 ℃, keeping the temperature and stirring for 15min at the stirring speed of 60rpm, and cooling to 40 ℃ to obtain a mixed solution A;
(3) and adding the zanthoxylum bungeanum fruit extract, the forsythia suspensa fruit extract and the purslane extract into the mixed solution A to obtain the product of the embodiment.
Example of implementation 8
This example contains the zero preservative cosmetic composition of the present invention: and (3) Chinese prickly ash fruit extract: 0.4g, forsythia suspense extract: 0.35g, purslane extract: 0.4g, butanediol: 9g, and further comprises the following raw materials: hydrolyzing sclerotium rolfsii gum: 0.25g, hydroxyethyl cellulose: 0.25g, water: 90 g.
The preparation method of the zero-preservative cosmetic composition comprises the following steps:
(1) weighing the raw materials according to the weight of the raw materials for later use;
(2) dispersing hydrolyzed sclerotium rolfsii gum and hydroxyethyl cellulose by using butanediol, then adding water, heating to 80 ℃, keeping the temperature and stirring for 15min at the stirring speed of 60rpm, and cooling to 40 ℃ to obtain a mixed solution A;
(3) and adding the zanthoxylum bungeanum fruit extract, the forsythia suspensa fruit extract and the purslane extract into the mixed solution A to obtain the product of the embodiment.
Example of application 9 test analysis of safety and efficacy of zero preservative cosmetic compositions
CTFA bacteria-adding antiseptic challenge test
The zero-preservative cosmetic of example 1 was subjected to the aseptic challenge test by repeating the aseptic challenge test method for 3 additions of bacteria for 42 days as recommended by CTFA, and the results are shown in table 1, in which B represents the inoculum size of bacteria and F represents the inoculum size of fungi.
TABLE 1 test results
TABLE 2 evaluation criteria
By referring to the evaluation criteria in table 2, it can be seen that the zero-preservative composition of embodiment 1 has excellent preservative effect after 42 days of microbial challenge test, which indicates that the zero-preservative cosmetic product has broad-spectrum bacteriostatic and bactericidal effects without adding any preservative.
2. Irritation test for preservative-free cosmetic compositions
The chick embryo chorioallantoic membrane test (CAMVA) in cosmetic testing is a standard assessment of the potential ocular irritation of an evaluated substance by testing the ability of the test substance to induce toxic changes in the chick embryo chorioallantoic membrane (which has a structure similar to that of the conjunctival tissue). The results of the chick embryo chorioallantoic membrane test performed on the zero preservative composition of example 1 are shown in Table 3. Table 3 shows the chick embryo chorioallantoic membrane test results for the zero preservative cosmetic composition of example 1.
TABLE 3
Scoring and evaluation reference criteria
As can be seen from Table 3, the zero antiseptic composition of example 1 acted on the chick chorioallantoic membrane, the total score was 0, and the reference score and evaluation criteria indicated that the intra-loop blood vessels on the chick chorioallantoic membrane were unchanged and non-responsive, the chick chorioallantoic membrane was normal, the obtained NC value was 0, and the chick chorioallantoic membrane was stressed, i.e., non-traumatic stimulation, and no blood damage was observed in the capillaries. The results of the chick embryo chorioallantoic membrane test of the zero-preservative composition of example 1 demonstrate that the zero-preservative cosmetic composition is extremely mild and non-irritating, and thus, the composition can be evaluated for minimal ocular irritation.
3. Efficacy testing analysis of zero preservative cosmetic compositions
The VISIA skin detector is an instrument capable of quantitatively analyzing pathological characteristics of skin, and can be used for detecting 8 skin health indexes such as surface spots, wrinkles, textures, pores, ultraviolet red spots, brown spots, red areas, purpurins and the like at one time by quantitatively analyzing the problems hidden in a skin basal layer. The red zone reflects the condition of the capillaries, the presence of blood vessels and heme in the dermal papilla layer of the skin, giving these tissues a red color, red blood streak, inflammatory acne, rosacea, spider nevi, etc., all detectable.
A plurality of skin-sensitive testers are searched, the red area condition of the testers is detected by a VISIA skin detector after the testers clean the cheeks, then the testers are coated with a facial mask prepared by the zero-preservative composition in the embodiment 1 for 15min, the facial mask is removed after 15min, the cheeks are tapped by hands to fully absorb essence, and then the testers detect the red area condition of the testers by the VISIA skin detector after the testers clean the cheeks. The red area map of one of the subjects was selected, with fig. 1 showing the red area map after the first cheek cleaning and fig. 2 showing the red area map after the second cheek cleaning.
The red area can reflect the inflammatory condition of the skin of the testee, and the smaller the characteristic count is, the better the inflammatory condition of the testee is. As can be seen by comparing fig. 1 and fig. 2, the characteristic count of the red area of the cheek of the subject was significantly decreased after the application of the zero antiseptic mask, indicating that the zero antiseptic mask can relieve the inflammatory condition of the skin, and has the effects of diminishing inflammation and tranquilizing.
The foregoing shows and describes the general principles, essential features, and advantageous features of the invention. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, which are described in the specification and illustrated only to illustrate the principle of the present invention, but that various changes and modifications may be made therein without departing from the spirit and scope of the present invention, which fall within the scope of the invention as claimed. The scope of the invention is defined by the appended claims and equivalents thereof.
Claims (9)
1. The zero-corrosion-resistance composition is characterized by comprising the following components in percentage by weight: 0.01-20% of zanthoxylum bungeanum fruit extract, 0.01-20% of forsythia suspensa fruit extract, 0.01-20% of purslane extract and the balance of water.
2. The zero-corrosion-resistance composition is characterized by comprising the following components in percentage by weight: 0.01-20% of zanthoxylum bungeanum fruit extract, 0.01-20% of forsythia suspensa fruit extract, 0.01-20% of purslane extract and the balance of water.
3. Zero-rot composition according to claim 1 or 2, wherein the components of zanthoxylum bungeanum maxim extract in the zero-rot composition comprise limonene, cumic alcohol, dinosaur alcohol, phytosterols, benzoic acid, unsaturated organic acids, diosmin and alkaloids.
4. The zero-preservative composition according to claim 1 or 2, wherein the ingredients of the forsythia suspense extract in the zero-preservative composition comprise hypericin, triterpenoid saponin, phytosterol, forsythol, alkaloid, saponin, oleanolic acid, coumarins, vitamins and volatile oil.
5. The zero-preservative composition according to claim 1 or 2, wherein the components of the purslane extract in the zero-preservative composition comprise alkaloids, terpenes, coumarins, flavonoids, organic acids, volatile oils and polysaccharides.
6. A process for preparing a zero corrosion inhibiting composition according to claim 1, comprising the steps of, in order:
(1) weighing the raw materials according to the weight percentage for later use;
(2) and respectively adding the purslane extract, the pricklyash peel extract and the forsythia suspense extract into water, and stirring and dissolving to obtain the zero-preservative composition.
7. The preparation method of the zero-antiseptic composition as claimed in claim 6, wherein the extraction method of the zanthoxylum bungeanum fruit extract is any one of steam distillation method, vegetable oil extraction method, edible alcohol extraction method, anhydrous ether extraction method and supercritical carbon dioxide fluid extraction method.
8. Preparation of the zero-preservative composition of claim 6The method is characterized in that the forsythia suspense extract is extracted by supercritical CO2The extraction technology is characterized in that the extraction pressure is 27MPa, and the temperature is 60 ℃; the pressure of the resolution kettle I is 14MPa, and the temperature is 64 ℃; the pressure of the resolution kettle II is 6MPa, and the temperature is 50 ℃; CO 22The flow rate is 25kg/kg raw material.h; the extraction time is 5 h; the carrying agent is alcohol.
9. Use of the zero preservative composition of claim 1 or 2 for the preparation of a skin care product for external application to the skin.
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110974775A (en) * | 2019-12-30 | 2020-04-10 | 湖南炎帝生物工程有限公司 | Allergy-relieving composition containing nostoc sphaeroides and preparation method and application thereof |
| CN111920715A (en) * | 2020-08-13 | 2020-11-13 | 广州品域美妆创新科技有限公司 | Composition containing soapberry extract and preparation method and application thereof |
| CN112057378A (en) * | 2020-08-25 | 2020-12-11 | 中北大学 | Botanical cosmetic preservative and preparation method thereof |
| CN112402272A (en) * | 2020-11-27 | 2021-02-26 | 陈珲 | White cream and manufacturing equipment thereof |
| CN112791020A (en) * | 2020-12-29 | 2021-05-14 | 陕西省石油化工研究设计院 | Plant source-based preservative for cosmetics and preparation method thereof |
| CN113797129A (en) * | 2021-09-30 | 2021-12-17 | 珠海美逸生物科技有限公司 | Antibacterial composition and preparation method and application thereof |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20130074983A (en) * | 2011-12-27 | 2013-07-05 | 주식회사 제닉 | Composition of preservatives for cosmetic and cosmetic composition comprising the same |
| US20140120190A1 (en) * | 2012-10-20 | 2014-05-01 | Dong-Qing WEI | Methods of preparing prickly-ash peel extracts and cosmetic compositions incorporating prickly-ash peel extracts |
| CN104223317A (en) * | 2014-09-29 | 2014-12-24 | 郭秀珍 | Preservative and preparation method thereof |
| CN104800113A (en) * | 2015-04-07 | 2015-07-29 | 广州菲梵生物科技有限公司 | Preservative-free herbal composition with corrosion-resistant effect, prepared from plant extract and humectant, and application thereof in daily cosmetics |
| CN107308064A (en) * | 2017-08-08 | 2017-11-03 | 广州蜜妆生物科技有限公司 | A kind of compound natural preservative |
| CN107582459A (en) * | 2017-10-11 | 2018-01-16 | 广州市禾基生物科技有限公司 | A kind of preservative containing the capsule of weeping forsythia and preparation method thereof |
-
2019
- 2019-09-17 CN CN201910875398.6A patent/CN110613641A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20130074983A (en) * | 2011-12-27 | 2013-07-05 | 주식회사 제닉 | Composition of preservatives for cosmetic and cosmetic composition comprising the same |
| US20140120190A1 (en) * | 2012-10-20 | 2014-05-01 | Dong-Qing WEI | Methods of preparing prickly-ash peel extracts and cosmetic compositions incorporating prickly-ash peel extracts |
| CN104223317A (en) * | 2014-09-29 | 2014-12-24 | 郭秀珍 | Preservative and preparation method thereof |
| CN104800113A (en) * | 2015-04-07 | 2015-07-29 | 广州菲梵生物科技有限公司 | Preservative-free herbal composition with corrosion-resistant effect, prepared from plant extract and humectant, and application thereof in daily cosmetics |
| CN107308064A (en) * | 2017-08-08 | 2017-11-03 | 广州蜜妆生物科技有限公司 | A kind of compound natural preservative |
| CN107582459A (en) * | 2017-10-11 | 2018-01-16 | 广州市禾基生物科技有限公司 | A kind of preservative containing the capsule of weeping forsythia and preparation method thereof |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110974775A (en) * | 2019-12-30 | 2020-04-10 | 湖南炎帝生物工程有限公司 | Allergy-relieving composition containing nostoc sphaeroides and preparation method and application thereof |
| CN111920715A (en) * | 2020-08-13 | 2020-11-13 | 广州品域美妆创新科技有限公司 | Composition containing soapberry extract and preparation method and application thereof |
| CN112057378A (en) * | 2020-08-25 | 2020-12-11 | 中北大学 | Botanical cosmetic preservative and preparation method thereof |
| CN112402272A (en) * | 2020-11-27 | 2021-02-26 | 陈珲 | White cream and manufacturing equipment thereof |
| CN112791020A (en) * | 2020-12-29 | 2021-05-14 | 陕西省石油化工研究设计院 | Plant source-based preservative for cosmetics and preparation method thereof |
| CN113797129A (en) * | 2021-09-30 | 2021-12-17 | 珠海美逸生物科技有限公司 | Antibacterial composition and preparation method and application thereof |
| CN113797129B (en) * | 2021-09-30 | 2023-02-03 | 珠海美逸生物科技有限公司 | Antibacterial composition and preparation method and application thereof |
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Application publication date: 20191227 |