CN108703899B - Skin-care massage essential oil - Google Patents
Skin-care massage essential oil Download PDFInfo
- Publication number
- CN108703899B CN108703899B CN201811010155.8A CN201811010155A CN108703899B CN 108703899 B CN108703899 B CN 108703899B CN 201811010155 A CN201811010155 A CN 201811010155A CN 108703899 B CN108703899 B CN 108703899B
- Authority
- CN
- China
- Prior art keywords
- parts
- oil
- skin
- care massage
- essential oil
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/347—Phenols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/63—Steroids; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/522—Antioxidants; Radical scavengers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
Abstract
The invention discloses skin-care massage essential oil which comprises the following raw materials: jojoba oil, menthol, rosemary oil, wheat germ oil, polydimethylsiloxane, iodopropynyl butylcarbamate, hyaluronic acid, EDTA disodium, an antioxidant and a solubilizer. The skin-care massage essential oil disclosed by the invention has the effects that the effective components can rapidly permeate into the skin to be absorbed, the proliferation and metabolic capacity of cells are enhanced, the skin environment can be effectively regulated, pores are dredged, the skin is moistened, the skin elasticity is recovered, the skin barrier function is improved, and the damaged skin is repaired. Also can relieve nervous emotion, relax mood, promote sleep, and improve sleep quality. Has effects of resisting oxidation, scavenging free radicals, and delaying aging.
Description
Technical Field
The invention relates to a skin-care massage essential oil.
Background
Because the skin is the first line of defense of the human body against the invasion of harmful substances, bacteria, viruses and the like, the skin becomes the organ which is most easily attacked by the outside and is most frequently attacked and damaged by the outside. Meanwhile, the skin is also an important component for showing the external aesthetic feeling and characteristics of the human body. Therefore, a good local environment is created for the skin, which is beneficial to the damage repair of the skin, the skin aging is delayed, and the formation of pox and acne is reduced. However, with the aging, the body's ability to scavenge free radicals is continuously reduced, so that free radicals are accumulated in the body, lipid peroxides such as MDA and the like are crosslinked with proteins, nucleic acids or lipids to form insoluble substances, the abnormal crosslinking causes the living environment of skin cells to be changed, the structure of the skin cells is destroyed and killed, and the skin shows aging and inflammation phenomena such as dryness, roughness, looseness and the like. In the aging process of the skin, the epidermis of the skin is deteriorated with the aging of keratinocytes, and wrinkles are also generated.
The essential oil is volatile aromatic substance extracted from flower, leaf, stem, root or fruit of plant by steam distillation, extrusion, cold soaking or solvent extraction. The essential oil is divided into diluted (compound essential oil) and undiluted (single essential oil). Not all plants produce essential oils, only plants containing the sebaceous glands are likely to produce essential oils. The sebaceous glands of different plants are distributed differently, some are petals, leaves, rhizomes or trunks. The sachet is extracted to obtain the plant essential oil. Essential oils contain many different components, and some essential oils, such as roses, can be made up of more than 250 different molecules. Essential oils are lipophilic and very soluble in oils and fats, because the molecular chains of essential oils are usually relatively short, which makes them very permeable to the skin and enter the body via the abundant capillaries under the subcutaneous fat. The essential oil is composed of a plurality of very small molecules, and the high volatile substances can be absorbed by nasal mucosa tissues to enter the body, so that messages are directly sent to the brain, and the emotion and the physiological function of the body are regulated through the peripheral system of the brain. Therefore, in aromatherapy, the essential oils can strengthen physiological and psychological functions.
The traditional skin care essential oil contains a large amount of chemical compounds and solvents, has high irritation to the skin and is easy to damage the skin. With the increasing living standard of people, the skin care concept of pursuing green environmental protection and returning to nature is also enhanced, so that the pursuing of natural products without toxicity and side effects as active additives and cosmetic raw materials becomes a hot point of the skin care essential oil industry. The traditional essential oil also has the problems of high volatility, short fragrance retention time, large volatilization loss of functional components, high waste rate and reduced efficacy. In addition, the existing essential oil in the market at present has single effect, and people often need to buy various essential oils to meet various requirements.
Disclosure of Invention
The invention provides a skin-care massage essential oil. The invention adopts the following technical scheme:
a skin-care massage essential oil comprises the following raw materials:
jojoba oil, menthol, rosemary oil, wheat germ oil, polydimethylsiloxane, iodopropynyl butylcarbamate, hyaluronic acid, EDTA disodium, an antioxidant and a solubilizer.
The skin-care massage essential oil comprises the following raw materials in parts by weight:
30-60 parts of jojoba oil, 1-5 parts of menthol, 10-20 parts of rosemary oil, 700 parts of sweet orange oil, 30-60 parts of wheat germ oil, 0.03-0.1 part of iodopropynyl butylcarbamate, 3-6 parts of hyaluronic acid, 0.3-1 part of EDTA disodium, 0.1-0.6 part of antioxidant and 0.1-0.6 part of solubilizer.
The skin-care massage essential oil comprises the following raw materials in parts by weight:
30-60 parts of jojoba oil, 1-5 parts of menthol, 10-20 parts of rosemary oil, 700 parts of sweet orange oil, 30-60 parts of wheat germ oil, 0.03-0.1 part of iodopropynyl butylcarbamate, 3-6 parts of hyaluronic acid, 0.3-1 part of EDTA disodium, 3-6 parts of litsea cubeba oil, 3-6 parts of weeping forsythia oil, 3-8 parts of grassleaf sweelflag rhizome oil, 0.1-0.6 part of antioxidant and 0.1-0.6 part of solubilizer.
The skin-care massage essential oil comprises the following raw materials in parts by weight:
30-60 parts of jojoba oil, 1-5 parts of menthol, 10-20 parts of rosemary oil, 700 parts of sweet orange oil, 30-60 parts of wheat germ oil, 0.03-0.1 part of iodopropynyl butylcarbamate, 3-6 parts of hyaluronic acid, 0.3-1 part of EDTA disodium, 1.5-5 parts of pollen extract, 3-6 parts of litsea cubeba oil, 3-6 parts of weeping forsythia oil, 3-8 parts of grassleaf sweelflag rhizome oil, 0.1-0.6 part of antioxidant and 0.1-0.6 part of solubilizer.
The skin-care massage essential oil comprises the following raw materials in parts by weight:
30-60 parts of jojoba oil, 1-5 parts of menthol, 10-20 parts of rosemary oil, 700 parts of sweet orange oil, 30-60 parts of wheat germ oil, 0.03-0.1 part of iodopropynyl butylcarbamate, 3-6 parts of hyaluronic acid, 0.3-1 part of EDTA disodium, 1.5-5 parts of pollen extract, 3-6 parts of litsea cubeba oil, 3-6 parts of weeping forsythia oil, 3-8 parts of grassleaf sweelflag rhizome oil, 1-5 parts of aescin sodium and/or albiflorin, 0.1-0.6 part of antioxidant and 0.1-0.6 part of solubilizer.
The skin-care massage essential oil comprises the following raw materials in parts by weight:
30-60 parts of jojoba oil, 1-5 parts of menthol, 10-20 parts of rosemary oil, 700 parts of sweet orange oil, 30-60 parts of wheat germ oil, 0.03-0.1 part of iodopropynyl butylcarbamate, 3-6 parts of hyaluronic acid, 0.3-1 part of EDTA disodium, 1.5-5 parts of pollen extract, 3-6 parts of litsea cubeba oil, 3-6 parts of weeping forsythia oil, 3-8 parts of grassleaf sweelflag rhizome oil, 0.1-0.6 part of antioxidant, 0.1-0.6 part of solubilizer, and 1-5 parts of a mixture of aescin sodium and albiflorin, wherein the mass ratio of the aescin sodium to the albiflorin is (1-3): (1-3).
The litsea cubeba oil, the forsythia fruit oil and the grassleaf sweelflag rhizome oil have good functions of soothing the nerves, resisting oxidation, diminishing inflammation and resisting bacteria, are mixed with the sweet orange oil and the jojoba oil, have good compatibility, are not layered and have harmonious fragrance.
The skin care massage essential oil comprises one or more of alpha-tocopherol, tea polyphenol, BHT, BHA and tocopherol acetate. The antioxidant is further preferably BHT and tocopherol acetate in a mass ratio of (1-2): the mixture of (1-2).
The skin care massage essential oil according to any one of the above, wherein the solubilizer is one or more of sucrose laurate, capric triglyceride, tocopheryl acetate and ethylhexyl methoxycinnamate. The solubilizer is further preferably ethylhexyl methoxycinnamate and triglyceride decanoate according to the mass ratio of (1-3): (1-3). The essential oil is very volatile, and can be quickly volatilized once contacting air, and all the components can be fully dissolved into a whole by using the solubilizer, so that the fragrance retention time is prolonged; when the skin-care product acts on skin, more functional components can be absorbed by the skin, the volatilization loss is reduced, and the effects of repairing the skin and soothing the nerves are better realized.
Preferably, the pollen is one of schisandra pollen, rape pollen and sweet clover pollen, preferably schisandra pollen. The pollen contains various volatile oils, has effects of enhancing essential oil fragrance, relieving nerve, tranquilizing mind, resisting oxidation, diminishing inflammation, and resisting bacteria.
The preparation method of the pollen extract comprises the following steps: and (2) performing supercritical carbon dioxide extraction on 5-8g of pollen at the extraction pressure of 25-35MPa and the extraction temperature of 45-55 ℃ for 2-4 hours at the carbon dioxide flow rate of 40-50L/h, at the temperature of 40-50 ℃ and the pressure of 10-15MPa in a separation kettle I, at the temperature of 25-35 ℃ and the pressure of 5-8MPa in a separation kettle II, and collecting the supercritical extract to obtain the pollen extract.
The skin care massage essential oil according to any one of the above, the preparation method thereof is as follows: weighing the raw materials according to the parts by weight, and stirring the raw materials at the temperature of between 25 and 35 ℃ and the rotating speed of between 300 and 600 revolutions per minute for 20 to 40 minutes to obtain the skin-care massage essential oil.
The invention provides skin-care massage essential oil, which has the effects that effective components can rapidly permeate into skin to be absorbed, the proliferation and metabolic capacity of cells are enhanced, the skin environment can be effectively adjusted, pores are dredged, the skin is moistened, the skin elasticity is recovered, the skin barrier function is improved, and the damaged skin is repaired. Also can relieve nervous emotion, relax mood, promote sleep, and improve sleep quality. Has effects of resisting oxidation, scavenging free radicals, and delaying aging.
On the basis of the common knowledge in the field, the above preferred conditions can be combined randomly to obtain the preferred embodiments of the invention.
Detailed Description
The invention is further illustrated by the following examples, which are not intended to limit the scope of the invention. The experimental methods without specifying specific conditions in the following examples were selected according to the conventional methods and conditions, or according to the commercial instructions.
Example 1
The skin-care massage essential oil comprises the following raw materials in parts by weight:
45 parts of jojoba oil, 2 parts of menthol, 15 parts of rosemary oil, 500 parts of sweet orange oil, 50 parts of wheat germ oil, 0.06 part of iodopropynyl butylcarbamate, 5 parts of hyaluronic acid, 0.5 part of EDTA disodium, 0.25 part of antioxidant and 0.2 part of solubilizer.
The antioxidant is BHT and tocopheryl acetate in a mass ratio of 2: 1. The solubilizer is ethylhexyl methoxycinnamate and capric triglyceride in a mass ratio of 3: 1.
The preparation method of the skin-care massage essential oil comprises the following steps: weighing the raw materials according to the parts by weight, and stirring the raw materials at the temperature of 30 ℃ for 30 minutes at the rotating speed of 500 revolutions per minute to obtain the skin-care massage essential oil.
Example 2
The skin-care massage essential oil comprises the following raw materials in parts by weight:
45 parts of jojoba oil, 2 parts of menthol, 15 parts of rosemary oil, 500 parts of sweet orange oil, 50 parts of wheat germ oil, 0.06 part of iodopropynyl butylcarbamate, 5 parts of hyaluronic acid, 0.5 part of EDTA disodium, 4 parts of litsea cubeba oil, 4 parts of weeping forsythia oil, 5 parts of grassleaf sweelflag rhizome oil, 0.25 part of antioxidant and 0.2 part of solubilizer.
The antioxidant is BHT and tocopheryl acetate in a mass ratio of 2: 1. The solubilizer is ethylhexyl methoxycinnamate and capric triglyceride in a mass ratio of 3: 1.
The preparation method of the skin-care massage essential oil comprises the following steps: weighing the raw materials according to the parts by weight, and stirring the raw materials at the temperature of 30 ℃ for 30 minutes at the rotating speed of 500 revolutions per minute to obtain the skin-care massage essential oil.
Example 3
The skin-care massage essential oil comprises the following raw materials in parts by weight:
45 parts of jojoba oil, 2 parts of menthol, 15 parts of rosemary oil, 500 parts of sweet orange oil, 50 parts of wheat germ oil, 0.06 part of iodopropynyl butylcarbamate, 5 parts of hyaluronic acid, 0.5 part of EDTA disodium, 3 parts of schisandra chinensis pollen extract, 4 parts of litsea cubeba oil, 4 parts of forsythia oil, 5 parts of grassleaf sweelflag rhizome oil, 0.25 part of antioxidant and 0.2 part of solubilizer.
The antioxidant is BHT and tocopheryl acetate in a mass ratio of 2: 1. The solubilizer is ethylhexyl methoxycinnamate and capric triglyceride in a mass ratio of 3: 1.
The preparation method of the schisandra chinensis pollen extract comprises the following steps: and (2) performing supercritical carbon dioxide extraction on 6g of schisandra pollen at the extraction pressure of 30MPa, the extraction temperature of 50 ℃, the extraction time of 3 hours, the carbon dioxide flow rate of 45L/h, the temperature of a separation kettle I of 45 ℃, the pressure of 12MPa, the temperature of a separation kettle II of 30 ℃ and the pressure of 6MPa, and collecting supercritical extracts to obtain the schisandra pollen extract.
The preparation method of the skin-care massage essential oil comprises the following steps: weighing the raw materials according to the parts by weight, and stirring the raw materials at the temperature of 30 ℃ for 30 minutes at the rotating speed of 500 revolutions per minute to obtain the skin-care massage essential oil.
Example 4
The skin-care massage essential oil comprises the following raw materials in parts by weight:
45 parts of jojoba oil, 2 parts of menthol, 15 parts of rosemary oil, 500 parts of sweet orange oil, 50 parts of wheat germ oil, 0.06 part of iodopropynyl butylcarbamate, 5 parts of hyaluronic acid, 0.5 part of EDTA disodium, 3 parts of rape pollen extract, 4 parts of litsea cubeba oil, 4 parts of weeping forsythia oil, 5 parts of grassleaf sweelflag rhizome oil, 0.25 part of antioxidant and 0.2 part of solubilizer.
The antioxidant is BHT and tocopheryl acetate in a mass ratio of 2: 1. The solubilizer is ethylhexyl methoxycinnamate and capric triglyceride in a mass ratio of 3: 1.
The preparation method of the rape pollen extract comprises the following steps: and (2) performing supercritical carbon dioxide extraction on 6g of rape pollen at the extraction pressure of 28MPa and the extraction temperature of 52 ℃ for 2.5 hours at the carbon dioxide flow rate of 42L/h, at the temperature of 45 ℃ in the separation kettle I and the pressure of 15MPa in the separation kettle II and at the temperature of 33 ℃ and the pressure of 7MPa, and collecting supercritical extracts to obtain the rape pollen extract.
The preparation method of the skin-care massage essential oil comprises the following steps: weighing the raw materials according to the parts by weight, and stirring the raw materials at the temperature of 30 ℃ for 30 minutes at the rotating speed of 500 revolutions per minute to obtain the skin-care massage essential oil.
Example 5
The skin-care massage essential oil comprises the following raw materials in parts by weight:
45 parts of jojoba oil, 2 parts of menthol, 15 parts of rosemary oil, 500 parts of sweet orange oil, 50 parts of wheat germ oil, 0.06 part of iodopropynyl butylcarbamate, 5 parts of hyaluronic acid, 0.5 part of EDTA disodium, 3 parts of sweet clover pollen extract, 4 parts of litsea cubeba oil, 4 parts of weeping forsythia oil, 5 parts of grassleaf sweelflag rhizome oil, 0.25 part of antioxidant and 0.2 part of solubilizer.
The antioxidant is BHT and tocopheryl acetate in a mass ratio of 2: 1. The solubilizer is ethylhexyl methoxycinnamate and capric triglyceride in a mass ratio of 3: 1.
The preparation method of sweet clover pollen extract comprises the following steps: and (3) carrying out supercritical carbon dioxide extraction on 6g of sweet clover pollen at the extraction pressure of 30MPa and the extraction temperature of 45 ℃ for 4 hours at the carbon dioxide flow rate of 48L/h, at the temperature of 45 ℃ and the pressure of 13MPa in a separation kettle I and at the temperature of 30 ℃ and the pressure of 6MPa in a separation kettle II, and collecting supercritical extract to obtain the sweet clover pollen extract.
The preparation method of the skin-care massage essential oil comprises the following steps: weighing the raw materials according to the parts by weight, and stirring the raw materials at the temperature of 30 ℃ for 30 minutes at the rotating speed of 500 revolutions per minute to obtain the skin-care massage essential oil.
Example 6
The skin-care massage essential oil comprises the following raw materials in parts by weight:
45 parts of jojoba oil, 2 parts of menthol, 15 parts of rosemary oil, 500 parts of sweet orange oil, 50 parts of wheat germ oil, 0.06 part of iodopropynyl butylcarbamate, 5 parts of hyaluronic acid, 0.5 part of EDTA disodium, 3 parts of schisandra pollen extract, 4 parts of litsea cubeba oil, 4 parts of forsythia oil, 5 parts of grassleaf sweelflag rhizome oil, 1.5 parts of aescine sodium, 0.25 part of antioxidant and 0.2 part of solubilizer.
The antioxidant is BHT and tocopheryl acetate in a mass ratio of 2: 1. The solubilizer is ethylhexyl methoxycinnamate and capric triglyceride in a mass ratio of 3: 1.
The preparation method of the schisandra pollen extract is the same as that of example 3.
The preparation method of the skin-care massage essential oil comprises the following steps: weighing the raw materials according to the parts by weight, and stirring the raw materials at the temperature of 30 ℃ for 30 minutes at the rotating speed of 500 revolutions per minute to obtain the skin-care massage essential oil.
Example 7
The skin-care massage essential oil comprises the following raw materials in parts by weight:
45 parts of jojoba oil, 2 parts of menthol, 15 parts of rosemary oil, 500 parts of sweet orange oil, 50 parts of wheat germ oil, 0.06 part of iodopropynyl butylcarbamate, 5 parts of hyaluronic acid, 0.5 part of EDTA disodium, 3 parts of schisandra pollen extract, 4 parts of litsea cubeba oil, 4 parts of forsythia oil, 5 parts of grassleaf sweelflag rhizome oil, 1.5 parts of albiflorin, 0.25 part of antioxidant and 0.2 part of solubilizer.
The antioxidant is BHT and tocopheryl acetate in a mass ratio of 2: 1. The solubilizer is ethylhexyl methoxycinnamate and capric triglyceride in a mass ratio of 3: 1.
The preparation method of the schisandra pollen extract is the same as that of example 3.
The preparation method of the skin-care massage essential oil comprises the following steps: weighing the raw materials according to the parts by weight, and stirring the raw materials at the temperature of 30 ℃ for 30 minutes at the rotating speed of 500 revolutions per minute to obtain the skin-care massage essential oil.
Example 8
The skin-care massage essential oil comprises the following raw materials in parts by weight:
45 parts of jojoba oil, 2 parts of menthol, 15 parts of rosemary oil, 500 parts of sweet orange oil, 50 parts of wheat germ oil, 0.06 part of iodopropynyl butylcarbamate, 5 parts of hyaluronic acid, 0.5 part of EDTA disodium, 3 parts of schisandra pollen extract, 4 parts of litsea cubeba oil, 4 parts of forsythia oil, 5 parts of grassleaf sweelflag rhizome oil, 0.75 part of sodium aescinate, 0.75 part of albiflorin, 0.25 part of antioxidant and 0.2 part of solubilizer.
The antioxidant is BHT and tocopheryl acetate in a mass ratio of 2: 1. The solubilizer is ethylhexyl methoxycinnamate and capric triglyceride in a mass ratio of 3: 1.
The preparation method of the schisandra pollen extract is the same as that of example 3.
The preparation method of the skin-care massage essential oil comprises the following steps: weighing the raw materials according to the parts by weight, and stirring the raw materials at the temperature of 30 ℃ for 30 minutes at the rotating speed of 500 revolutions per minute to obtain the skin-care massage essential oil.
The main raw materials used in the examples are as follows:
jojoba oil: CAS number: 61789-91-1, Jiangxi Baolin Natural aroma Co. Menthol: CAS number: 89-78-1. Rosemary oil, CAS: 8000-25-7, Jiangxi globulus Laboratae, Natural aroma, Inc. Wheat germ oil: CAS: 68917-73-7, Jiaye Biotech, Taian. Sweet orange oil: CAS: 8008-57-9, Shanghai commander Son Business ltd, product number: SS 000705. Iodopropynyl alcohol butyl carbamate: CAS: 55406-53-6. Hyaluronic acid: CAS number: 9004-61-9, molecular weight 80 KDa. Schisandra chinensis pollen: pollen of Schisandra chinensis (Turcz.) Baill. of Magnoliaceae. Rape pollen: pollen of Brassica napus L. of Brassicaceae and Brassica. Sweet clover powder: pollen of Melilotus officinalis (L.) of Melilotus of Papilionaceae. Litsea cubeba oil: CAS: 68855-99-2, Shanghai Shuaishui Son industries, Inc., product number: SS 000708. And (3) forsythia oil: CAS: 68917-49-7, Shanghai commander Son industries, Ltd., product number: SS 000612. Grassleaf sweelflag rhizome oil: CAS: 91745-11-8, commander Son industries ltd, product number: SS 000589. Sodium aescinate: CAS: 20977-05-3, commander Son practice ltd, product number: SS 005987. Albiflorin: CAS: 39011-90-0, commander Son industries ltd, product number: SS 005992. BHT: CAS number: 128-37-0. Tocopherol acetate: CAS number: 7695-91-2. Ethylhexyl methoxycinnamate: CAS: 5466-77-3. Capric acid triglyceride: CAS: 621-71-6.
Testing the acne treatment effect:
(I) inclusion criteria
640 acne patients meeting the conditions (the standard for curative effect of diagnosis of traditional Chinese medicine diseases (ZY/T001.8-94)) are randomly divided into 8 groups, and 80 patients in each group have no significant difference in sex, age and acne symptoms and are comparable.
(II) treatment methods
Groups 1-8 patients were treated with the skin-care massage essential oils of examples 1-8, respectively. The treatment method comprises the following steps: the skin care massage essential oil is uniformly applied to acne part before sleep every day, and the application amount is 0.05mL/cm2The treatment is continued for 30 days.
(III) therapeutic efficacy judgment criteria
The basic cure is as follows: the pimple disappears, the flushing completely fades, new acne does not grow any more, and no recurrence is observed for one year; the effect is shown: the pimple basically disappears, and new acne does not grow in half a year; the method has the following advantages: the pimple obviously disappears, but new acne occasionally grows out; and (4) invalidation: the symptoms are not improved. The test results are shown in Table 1.
Table 1: acne treatment effect test result table
| Basic recovery (case) | Obvious effect (example) | Effective (example) | Invalid (example) | |
| Example 1 | 31 | 14 | 16 | 19 |
| Example 2 | 37 | 15 | 13 | 15 |
| Example 3 | 49 | 16 | 8 | 7 |
| Example 4 | 45 | 15 | 11 | 9 |
| Example 5 | 47 | 13 | 9 | 11 |
| Example 6 | 59 | 12 | 5 | 4 |
| Example 7 | 54 | 13 | 8 | 5 |
| Example 8 | 67 | 7 | 4 | 2 |
Improving sleep effect test:
(I) case data: all cases were volunteers with insomnia symptoms, 180 men aged 62-74 years and with course of 1-2 years, 180 women aged 64-74 years and with course of 2-3 years. The treatment groups were randomized into 8 treatment groups and 1 control group, each group containing 40 patients (20 men and 20 women). The sex, age and insomnia symptom scores of 9 groups of patients have no significant difference (P is more than 0.05), and are comparable.
(II) inclusion standard: has typical symptoms of insomnia, lasts for more than one month, and meets the syndrome differentiation standard of traditional Chinese medicine. The medical diagnosis standard refers to the guiding principle of clinical research on new Chinese medicines issued by Ministry of health (1993) and has the following typical symptoms of insomnia: difficulty in falling asleep, frequent wakefulness, instability in sleep or inability to sleep again after waking up; early morning waking, no sleep at night, drowsiness in the daytime, sleep less than 5 hours, and recurrent attack history.
(III) exclusion criteria: eliminating general diseases such as pain, fever, cough, operation, etc., patients caused by external interference factors, mental patients, and patients with EKG, liver and kidney function, blood, urine, and stool abnormality.
(IV) a treatment method: the treatment groups 1 to 8 respectively use the skin-care massage essential oil of the examples 1 to 8, 0.5mL of the skin-care massage essential oil is taken before sleeping every day, and the skin-care massage essential oil is uniformly applied to temples, earlobes, behind ears and necks, massaged for 30 minutes and continuously used for 30 days. The control group was massaged for 30 minutes without using the skin care massage essential oil and continuously massaged for 30 days.
(V) observation of curative effect: and calculating the improvement rate and the curative effect judgment of obvious effect, effective effect and ineffective effect according to the clinical symptom scoring standard with the application number of 201110313259.8. The post-compress score P <0.05 for each group comparison. Has statistical significance.
The test results are shown in Table 2.
Table 2: test result table for improving sleep effect
DPPH cleaning effect test:
DPPH scavenging by skin care massage essential oils of examples 1-8The ability to function as a basis was tested: preparing a sample solution with the concentration of 0.5mg/mL by using absolute ethyl alcohol as a solvent and skin-care massage essential oil as a solute; to a 1cm quartz cuvette, 2.0mL of the sample solution and 2.0mL of a 1.0X 10 molar concentration4Uniformly mixing a DPPH solution in mol/L, standing in a dark place for 30 minutes, and measuring a light absorption value A at 517nm by taking an ethanol water solution with a volume fraction of 95% as a reference solution; measuring the light absorption value Ao of the mixed solution of 2.0mL of sample solution and 2.0mL of ethanol water solution with the volume fraction of 95% at 517nm by the same method; further, 2.0mL of the solution was measured to have a molar concentration of 1.0X 104The absorbance A1 at 517nm of a mixed solution of DPPH solution in mol/L and ethanol aqueous solution with the volume fraction of 95% is calculated according to the following formula: the clearance (%) {1- (a-Ao)/a1} × 100. The test results are shown in Table 3.
Table 3: DPPH cleaning effect test result table
| Clearance (%) | |
| Example 1 | 45.4 |
| Example 2 | 47.2 |
| Example 3 | 50.6 |
| Example 4 | 49.5 |
| Example 5 | 48.7 |
| Example 6 | 53.7 |
| Example 7 | 54.2 |
| Example 8 | 57.5 |
The skin-care massage essential oil disclosed by the invention can relieve nervous emotion, relax mood, promote sleep and improve sleep quality. Can effectively regulate skin environment, dredge pores, improve skin barrier function, repair damaged skin and have good efficacy on acne. Has effects of resisting oxidation, scavenging free radicals, and delaying aging.
The foregoing detailed description of the preferred embodiments of the invention has been presented. It should be understood that numerous modifications and variations could be devised by those skilled in the art in light of the present teachings without departing from the inventive concepts. Therefore, the technical solutions available to those skilled in the art through logic analysis, reasoning and limited experiments based on the prior art according to the concept of the present invention should be within the scope of protection defined by the claims.
Claims (4)
1. The skin-care massage essential oil is characterized by comprising the following raw materials in parts by weight:
30-60 parts of jojoba oil, 1-5 parts of menthol, 10-20 parts of rosemary oil, 700 parts of sweet orange oil, 30-60 parts of wheat germ oil, 0.03-0.1 part of iodopropynyl butylcarbamate, 3-6 parts of hyaluronic acid, 0.3-1 part of EDTA disodium, 1.5-5 parts of pollen extract, 3-6 parts of litsea cubeba oil, 3-6 parts of weeping forsythia oil, 3-8 parts of grassleaf sweelflag rhizome oil, 0.1-0.6 part of antioxidant, 0.1-0.6 part of solubilizer, and 1-5 parts of a mixture of aescin sodium and albiflorin, wherein the mass ratio of the aescin sodium to the albiflorin is (1-3): (1-3);
the pollen is one of fructus Schisandrae pollen, rape pollen, and sweet clover pollen;
the preparation method of the pollen extract comprises the following steps: and (2) performing supercritical carbon dioxide extraction on 5-8g of pollen at the extraction pressure of 25-35MPa and the extraction temperature of 45-55 ℃ for 2-4 hours at the carbon dioxide flow rate of 40-50L/h, at the temperature of 40-50 ℃ and the pressure of 10-15MPa in a separation kettle I, at the temperature of 25-35 ℃ and the pressure of 5-8MPa in a separation kettle II, and collecting the supercritical extract to obtain the pollen extract.
2. The essential oil for skin care massage according to claim 1, wherein the antioxidant is one or more of alpha-tocopherol, tea polyphenol, BHT, BHA, and tocopherol acetate.
3. The skin-care massage essential oil as claimed in claim 2, wherein the antioxidant is BHT and tocopherol acetate in a mass ratio of (1-2): the mixture of (1-2).
4. The skin care massage essential oil of claim 1, wherein the solubilizer is one or more of sucrose laurate, capric triglyceride, tocopheryl acetate, ethylhexyl methoxycinnamate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811010155.8A CN108703899B (en) | 2018-08-31 | 2018-08-31 | Skin-care massage essential oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811010155.8A CN108703899B (en) | 2018-08-31 | 2018-08-31 | Skin-care massage essential oil |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN108703899A CN108703899A (en) | 2018-10-26 |
| CN108703899B true CN108703899B (en) | 2021-02-02 |
Family
ID=63873581
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811010155.8A Active CN108703899B (en) | 2018-08-31 | 2018-08-31 | Skin-care massage essential oil |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108703899B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115813975B (en) * | 2021-12-31 | 2023-12-12 | 亿艾(河南)生物科技有限公司 | Plant essential oil for resolving depression and aiding sleep and application thereof |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2777205B1 (en) * | 1998-04-10 | 2000-06-30 | Lhs | POLLEN EXTRACTION PROCESS AND COSMETIC, DERMO-COSMETIC OR PHARMACEUTICAL APPLICATIONS OF THE EXTRACT OBTAINED BY THIS PROCESS |
| US7235265B2 (en) * | 2005-10-31 | 2007-06-26 | Ross Rosen | Herbal skin formulation |
| CN102366501B (en) * | 2011-10-16 | 2013-04-03 | 广东养美医药投资有限公司 | Self-heated traditional Chinese medicine (TCM) emplastrum for improving sleep quality |
| CN102871925B (en) * | 2012-10-22 | 2013-08-28 | 上海韬鸿投资管理咨询有限公司 | Firming and massaging essential oil |
| FR3042118B1 (en) * | 2015-10-08 | 2017-11-24 | Laboratoires Chemineau | COMPOSITION BASED ON NATURAL VEGETABLE OIL AND LIME WATER FOR TOPICAL APPLICATION |
| CN107929101B (en) * | 2017-11-17 | 2021-03-26 | 泰合玺健康科技南京有限公司 | Firming massage essential oil and preparation method thereof |
-
2018
- 2018-08-31 CN CN201811010155.8A patent/CN108703899B/en active Active
Non-Patent Citations (1)
| Title |
|---|
| "The Efficacy of Sodium Aescinate on CutaneousWound Healing in Diabetic Rats";Zonglin Zhang 等;《Inflammation》;20151031;第38卷(第5期);第1942-1948页 * |
Also Published As
| Publication number | Publication date |
|---|---|
| CN108703899A (en) | 2018-10-26 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106726965B (en) | Anti-allergy and soothing skin care product composition and preparation method thereof | |
| CN108670943A (en) | A kind of moisturizing, whitening, light spot composition of plant extracts | |
| KR101908978B1 (en) | A aromatic composition having anti-stress and fatigue relaxing, and a cosmetic composition containing the same | |
| CN109044941B (en) | Skin firming, nourishing and moisturizing composition and preparation method and application thereof | |
| CN105596277A (en) | Cactus face cream for treating acne and preparation method thereof | |
| KR101810229B1 (en) | Cosmetic composition for improving acne containing teatree leaves spicule powder | |
| CN111329981B (en) | Antibacterial, anti-inflammatory and blood circulation-promoting microcapsule Chinese herbal medicine composition and preparation method thereof | |
| KR101332215B1 (en) | Cosmetic composition containing fermentated complex of extracts with cryptomeria japonica and nelumbo nucifera for acne improvement and enhancing immune system | |
| KR102330465B1 (en) | Composition for skin comprising pine bark extract reducing edema, cellulite, breaking down body fat, promoting blood circulation and skin cream comprising thereof | |
| CN107184483A (en) | High penetration camellia massage essential oil promoting blood circulation and removing obstruction in channels and preparation method thereof | |
| CN109939193A (en) | A kind of composition for treating skin eczema, preparation and preparation method and application | |
| CN109303724A (en) | A kind of novel maintenance stoste composition of releiving containing folium artemisiae argyi | |
| CN108703899B (en) | Skin-care massage essential oil | |
| CN109288884B (en) | Preparation method and application of sunflower extract with soothing and repairing effects | |
| CN111643610A (en) | Plant composite liquid and preparation method and application thereof | |
| Lee et al. | A Study on the Effect of Eclipta Prostrata Extract and MTS on the Improvement of Scalp Health and Prevention of Hair Loss for Workers in Their 20s and 30s. | |
| KR101810230B1 (en) | A aromatic composition containing honey extract, and a cosmetic composition containing the same | |
| CN115518127A (en) | Antibacterial, anti-inflammatory, detumescence and itching relieving cream and preparation method thereof | |
| CN109010572A (en) | A kind of Chinese medicine composition and its preparation method and application with sun-proof synergy and anti-aging effects | |
| CN114515304A (en) | Plant composition for preventing and treating and repairing skin sensitivity and preparation method thereof | |
| CN108078886A (en) | A kind of compound Thief zone moisturizing elite and its preparation process | |
| CN111481487B (en) | Whitening skin care composition containing herba Violae extract and preparation method thereof | |
| CN114587767A (en) | Cold compress cover, eye cold compress eye patch and preparation process thereof | |
| CN107375613A (en) | A kind of Chinese medical extract and its external preparation that red blood trace on face effect is removed with Eradicates | |
| CN110302132A (en) | A kind of reparation spray and preparation method thereof of the filtrate of secretion containing snail |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| TA01 | Transfer of patent application right | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20210107 Address after: 438300 south of Jinguang Avenue, Huanggang Economic Development Zone, Hubei Province Applicant after: SANFEIME (HUBEI) BIOTECHNOLOGY Co.,Ltd. Address before: Room 201d, 201e, 205, 2 / F, building 11, innovation and Technology Park, Songshanhu high tech Industrial Development Zone, Dongguan, Guangdong 523000 (cluster registration) Applicant before: DONGGUAN XUANMO BIOTECHNOLOGY Co.,Ltd. |
|
| GR01 | Patent grant | ||
| GR01 | Patent grant |