CN111920715A

CN111920715A - Composition containing soapberry extract and preparation method and application thereof

Info

Publication number: CN111920715A
Application number: CN202010810264.9A
Authority: CN
Inventors: 段国梅
Original assignee: Guangzhou Pinyu Beauty Innovation Technology Co ltd
Current assignee: Guangzhou Pinyu Beauty Innovation Technology Co ltd
Priority date: 2020-08-13
Filing date: 2020-08-13
Publication date: 2020-11-13

Abstract

The invention discloses a composition containing a soapberry extract, and a preparation method and application thereof. The composition comprises soapberry extract, quillaja bark extract, zanthoxylum bungeanum fruit extract and forsythia suspensa fruit extract, and the mass ratio of the soapberry extract to the quillaja bark extract to the zanthoxylum bungeanum fruit extract is 0.0001-10: 0.0001-5: 0.0001-2: 0.0001-2, under the synergistic effect of the four components, the composition has excellent foaming, sterilizing and decontaminating effects, and the pure natural active matter is safe and mild, has a formula of a zero-additive preservative system, has no stimulation to the skin, and is suitable for various skin crowds.

Description

Composition containing soapberry extract and preparation method and application thereof

Technical Field

The invention belongs to the field of cleaning cosmetics, and relates to a composition containing a soapberry extract, and a preparation method and application thereof.

Background

It is known that there is a great deal of sweat, oil and fat on the skin of the human body, and also the loss of metabolic aged keratin. If the cleaning is not timely, bacteria, acne, pimples and the like can be generated. In order to achieve a better cleaning effect, consumers can select products with stronger cleaning capability, and although dirt, grease and the like on the surface of the skin are cleaned, the water-oil balance of the skin is easily damaged, so that the skin is dry and the like. In order to achieve the aim of cleaning and protecting the skin, the market has a large and high demand for cleaning cosmetic products. Currently, most cleansing products on the market are soap-based and amino acid cleansers. Because soap base cleansing power is strong but not mild, amino acid cleansing power is mild and cleansing power is weak. Therefore, milder cleansing with strong cleansing power is needed to satisfy the market and consumer needs.

Since the twenty-first century, the separation, extraction and identification of the pure natural plant sapindus saponin are more comprehensive and high-yield, and various internal and external biological activities are continuously proved, so that the application of the sapindus saponin in the fields of medicine, food health care, daily chemicals, agriculture and the like is accelerated. The invention provides a composition containing a soapberry extract, wherein the soapberry extract contains saponin and aglycone which are natural nonionic surfactants, can reduce the surface tension of water, has good foaming performance, and has the effects of resisting bacteria, sterilizing and diminishing inflammation on skin; in addition, the source of the cleansing cosmetic is natural, and the cleansing cosmetic has no stimulation to skin, and is a safe and high-efficacy cleansing cosmetic raw material. The invention particularly relates to a composition containing a pure natural soapberry extract, a preparation method of a cleansing bubble without adding a preservative and application of the cleansing bubble.

Disclosure of Invention

The invention aims to provide a composition containing soapberry extract, a preparation method and application thereof, in particular to application in cleaning cosmetics and a preparation method of cleansing bubbles. The tests on the dirt-removing power and the mildness of the cleansing foam product prove that the product has excellent foaming, sterilizing and dirt-removing effects.

In order to achieve the purpose, the invention adopts the technical scheme that:

in a first aspect, the present invention provides a composition containing a sapindus extract, wherein the composition comprises components including a sapindus extract, a quillaja bark extract, a zanthoxylum bungeanum fruit extract and a forsythia suspensa fruit extract, and the mass ratio of the components is 0.0001-10: 0.0001-5: 0.0001-2: 0.0001-2.

Preferably, the components of the composition are of natural plant origin.

Preferably, the sapindus mukorossi extract is a pure natural sapindus mukorossi extract.

Preferably, the fructus forsythiae extract contains effective components such as forsythol, sterol compounds, saponins, flavonol glycosides, and malvidin.

Preferably, the sapindus mukorossi extract contains effective components such as terpenes, steroidal saponins, amino acids, proteins, vitamins, oleic acid, oil and the like.

Preferably, the zanthoxylum bungeanum maxim fruit extract contains active ingredients such as limonene, cumic alcohol, geraniol, sterol and unsaturated organic acid.

Preferably, the quillaja bark extract contains effective components such as saponin, polyphenol, sterol compound, unsaturated organic acid, etc.

In another preferred embodiment, the present invention provides a composition comprising an extract of sapindus mukorossi, comprising the following components in percentage by weight: 0.0001-10% of soapberry extract, 0.0001-5% of quillaja bark extract, 0.0001-2% of zanthoxylum fruit extract and 0.0001-2% of forsythia extract.

In a second aspect, the present invention provides a cosmetic containing the soapberry extract, the cosmetic comprising a composition containing the soapberry extract.

Preferably, the cosmetic comprises 2-20% of the composition containing the soapberry extract.

Preferably, the cosmetics comprise cleansing bubbles, cleansing milk and cleansing cream.

Preferably, the cosmetic is a cleansing bubble.

Preferably, the cleansing bubble comprises 2-20% of a composition containing soapberry extract.

Preferably, the cleansing bubble comprises a composition of natural plant origin.

Preferably, the composition is of natural plant origin, the mass of which represents between 2 and 20% of the mass of the cosmetic product.

Preferably, the cleansing bubble further comprises the following components in percentage by mass: 5-60% of cosmetic matrix.

Preferably, the balance of the cleansing bubbles is deionized water.

Preferably, the cosmetic base comprises at least one of an emollient, a thickener, a humectant, and a neutralizing agent.

Preferably, the emollient includes at least one of esters, triglycerides, fatty alcohols, and the like.

Preferably, the thickener comprises at least one of high molecular water-soluble substances, synthetic resins, polyethylene glycol esters and the like.

Preferably, the humectant comprises at least one of polyols, natural moisturizing factors, amino acids, high molecular biochemicals and the like.

Preferably, the neutralizing agent comprises at least one of sodium hydroxide, potassium hydroxide, sodium bicarbonate, sodium acetate, sodium pyrophosphate, sodium carbonate, ammonia, hydrochloric acid, phosphoric acid, formic acid, acetic acid, diethanolamine, triethanolamine, arginine, glycine, and the like.

Preferably, the cleansing bubbles are liquid cosmetics without preservatives and essences.

In a third aspect, the present invention provides a method for preparing a cosmetic containing a sapindus mukorossi extract, the method comprising the steps of:

(1) mixing glycerol, xanthan gum, fructus Sapindi Mukouossi extract and water, heating to 75-85 deg.C, and stirring to obtain transparent liquid;

(2) cooling the liquid to be prepared in the step (1) to 55-60 ℃, adding the Quillaja saponaria bark extract, the Zanthoxylum bungeanum fruit extract and the weeping forsythia extract, and stirring to obtain a transparent liquid for later use;

(3) cooling the solution to be prepared in the step (2) to 45-50 ℃, adding at least one of emollient, thickener, humectant and neutralizer, stirring for 3-5min, cooling to below 45 ℃, and filtering to obtain the cosmetic containing the soapberry extract.

Preferably, the step (3) is specifically carried out by cooling the solution to be prepared in the step (2) to 45-50 ℃, adding decyl glucoside, dipotassium glycyrrhizinate and arginine, stirring for 3-5min, cooling to below 45 ℃, and filtering to obtain the cleansing foam.

Preferably, the cosmetic obtained in the step (3) is a cleansing bubble containing the soapberry extract.

In a fourth aspect, the present invention provides the use of a composition comprising an extract of soapberry fruit for the preparation of cleansing cosmetics.

Preferably, the soapberry extract is a natural nonionic surfactant, has rich and fine foam and strong detergency, and also has an antifungal effect.

Preferably, the quillaja bark extract is a natural skin cleanser and conditioner, has excellent cleansing ability and skin astringing effect, and also has antibacterial and bactericidal effects.

Preferably, the zanthoxylum bungeanum maxim fruit extract contains a large amount of limonene, and the main function of the zanthoxylum bungeanum maxim fruit extract is to inhibit the formation of dermatophytes, so that the effect of inhibiting bacteria is achieved.

Preferably, the fructus forsythiae extract contains effective components such as forsythol, sterol compounds, saponins, flavonol glycosides, maltesin and the like, has the main effects of resisting bacteria, inflammation and acne, and has high-performance repairing and healing effects. The inventor uses the soapberry extract, the quillaja bark extract, the zanthoxylum bungeanum fruit extract and the forsythia suspense extract in a combined way, and finds that the four components can achieve synergistic cleaning, bacteriostasis and anti-inflammation, and when the soapberry extract, the quillaja bark extract, the zanthoxylum bungeanum fruit extract and the forsythia suspense extract are mixed in a mass ratio of (0.0001-10): 0.0001-5: 0.0001-2: 0.0001-2, the composition has good decontamination capability, bacteriostasis and anti-inflammatory effects.

Compared with the prior art, the invention has the following advantages and beneficial effects:

(1) the composition has excellent cleaning ability, antibacterial and anti-inflammatory effects through the synergistic effect among the soapberry extract, the quillaja bark extract, the zanthoxylum bungeanum fruit extract and the forsythia suspensa fruit extract.

(2) The functional components in the composition are all derived from plants, are natural and safe, and can be applied to cosmetics, and the obtained cleansing bubbles have excellent cleaning capacity and bacteriostatic and anti-inflammatory effects; the cleansing bubble product is a formula without preservative, and is safe and reliable.

(3) The preparation method of the cleansing bubble is simple and is easy for industrial production.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention. The examples, in which specific conditions are not specified, were conducted under conventional conditions or conditions recommended by the manufacturer. The reagents or instruments used are not indicated by the manufacturer, and are all conventional products available commercially.

The soapberry extract is a natural nonionic surfactant, has rich and fine foam and strong detergency and also has an antifungal effect; the quillaja bark extract is a natural skin cleanser and conditioner, has excellent cleaning capability and skin astringency effect, and also has antibacterial and bactericidal effects; the zanthoxylum bungeanum maxim extract contains a large amount of limonene and has the main function of inhibiting the formation of dermatophytes so as to achieve the effect of inhibiting bacteria; the fructus forsythiae extract contains effective components such as forsythol, sterol compound, saponin, flavonol glycosides, and maltesin, and has antibacterial, antiinflammatory, acne removing, and high-performance repairing and healing effects. The inventor uses the soapberry extract, the quillaja bark extract, the zanthoxylum bungeanum fruit extract and the forsythia suspense extract in a combined way, and finds that the four components can be synergistically cleaned, bacteriostatic and anti-inflammatory, and when the soapberry extract, the quillaja bark extract, the zanthoxylum bungeanum fruit extract and the forsythia suspense extract are mixed in a mass ratio of (0.01-10): 0.01-5: 0.01-2: 0.01-2, the composition has good decontamination capability, bacteriostasis and anti-inflammatory effects.

The invention provides a technical scheme that: a composition containing pure natural fructus Sapindi Mukouossi extract and cleansing bubble without antiseptic comprises water, fructus Sapindi Mukouossi extract, decyl glucoside, glycerol, Quillaja saponaria bark extract, dipotassium glycyrrhizinate, xanthan gum, fructus Zanthoxyli extract, fructus forsythiae extract, and arginine.

Example 1

Preparing the cleansing bubbles without adding the preservative:

(1) mixing 3.0% glycerol, 0.05% xanthan gum, 1.5% fructus Sapindi Mukouossi extract and 89.0% water, heating to 75-85 deg.C, and stirring to obtain transparent liquid;

(2) cooling the solution to be prepared in the step (1) to 55-60 ℃, adding 1.0% of Quillaja saponaria bark extract, 0.5% of zanthoxylum bungeanum fruit extract and 0.5% of fructus forsythiae extract, and stirring to obtain a transparent liquid for later use;

(3) cooling the solution to be prepared in the step (2) to 45-50 ℃, adding 6.0% decyl glucoside, 0.05% dipotassium glycyrrhizinate and 0.1% arginine, stirring for 3-5min, cooling to below 45 ℃, and filtering to obtain the cleansing bubble.

Example 2

(1) Mixing 3.0% glycerol, 0.05% xanthan gum, 3.5% fructus Sapindi Mukouossi extract and 87.0% water, heating to 75-85 deg.C, and stirring to obtain transparent liquid;

Example 3

(1) Mixing 3.0% glycerol, 0.05% xanthan gum, 5.5% fructus Sapindi Mukouossi extract and 85.0% water, heating to 75-85 deg.C, and stirring to obtain transparent liquid;

The cleansing bubbles of examples 1, 2, 3 were selected for cleansing ability, foaming ability and safety and mildness evaluation tests:

the results of the trial tests of examples 1, 2, 3 and a commercial facial mousse (control) claiming to be cleaner are shown. Test objects: each experimental group was 50 women (25-50 years old); test area: a face; use of: the medicine is taken in the morning and evening respectively, and is continuously used for 4 weeks; and (3) testing items: cleaning effect, foaming ability and safety effect. The results of the trial are shown in table 1 below:

TABLE 1 statistical table for evaluation of efficacy of control group and cleansing bubbles of examples 1, 2 and 3

As can be seen from Table 1, the cleaning ability and foaming ability of the formulations of examples 1, 2 and 3 are improved with the increase of the soapberry content; however, in the examples 2 and 3, with the increase of the soapberry content, the cleaning capability and the foaming capability of the cleansing foam are not obviously improved; the cleansing and foaming abilities of examples 2 and 3 were superior to those of the control group, indicating that the cleansing foam of the present invention has significant cleansing and foaming abilities, resulting in a cleaner and brighter skin. Meanwhile, the mild people of the control group and the examples 1, 2 and 3 account for a large proportion of the mild people for the mild efficacy; compared with the slight prick degree, the number of people in the control group is far higher than that in examples 1, 2 and 3; none of the control group and examples 1, 2, 3 had a stimulating population; it is demonstrated that the cleansing foam of the present invention is mild and non-irritating.

Example 4

(1) Mixing 3.0% glycerol, 0.05% xanthan gum, 3.5% fructus Sapindi Mukouossi extract and 88.0% water, heating to 75-85 deg.C, and stirring to obtain transparent liquid;

(2) cooling the solution to be prepared in the step (1) to 55-60 ℃, adding 0.5% of Quillaja saponaria bark extract, 0.25% of zanthoxylum bungeanum fruit extract and 0.25% of fructus forsythiae extract, and stirring to obtain a transparent liquid for later use;

Example 5

Example 6

(1) Mixing 3.0% glycerol, 0.05% xanthan gum, 3.5% fructus Sapindi Mukouossi extract and 85.0% water, heating to 75-85 deg.C, and stirring to obtain transparent liquid;

(2) cooling the solution to be prepared in the step (1) to 55-60 ℃, adding 2.0% of Quillaja saponaria bark extract, 1.0% of zanthoxylum fruit extract and 1.0% of forsythia suspensa extract, and stirring to obtain a transparent liquid for later use;

The cleansing bubbles of examples 4, 5, 6 were selected for the preservative challenge test:

examples 1, 2, and 3 were tested for preservation challenge according to the method for detecting the total number of colonies in chapter 2 of the year 2015, the method for detecting mold and yeast in chapter 6 of the year 2015, and the microbial challenge test method recommended by CTFA for repeating the addition of 3 times for 42 days. The test data results are shown in table 2 below:

table 2 example 1, 2, 3 statistical table of the bactericidal test of cleansing bubbles

It can be seen from table 2 that the cleansing bubbles of examples 4, 5 and 6 have more significant bactericidal effect with the addition of the composition of quillaja bark extract, zanthoxylum bungeanum fruit extract and forsythia suspensa fruit extract. Wherein, in example 4, the bacteria, the mold and the yeast in the 3 rd time of bacteria addition are not up to the standard, and in examples 4 and 5, the antiseptic challenge test can be passed, which proves that the composition emphasizes the excellent sterilization effect.

Comparative example 1

(1) Mixing 3.0% of glycerol, 0.05% of xanthan gum and 85.0% of water, heating to 75-85 ℃, stirring to obtain a transparent liquid, and then cooling to 45-50 ℃ for later use;

(2) adding decyl glucoside 6.0%, dipotassium glycyrrhizinate 0.05% and arginine 0.1% into the solution of (1), stirring for 3-5min, cooling to below 45 deg.C, and filtering to obtain the final product.

The cleansing bubbles of example 2 and comparative example 1 were selected for cleansing power, foaming power and safety and mildness evaluation tests:

trial tests were performed on the effects of example 2 and comparative example 1. Test objects: each experimental group was 50 women (25-50 years old); test area: a face; use of: the medicine is taken in the morning and evening respectively, and is continuously used for 4 weeks; and (3) testing items: cleaning effect, foaming ability and safety effect. The results of the trial are shown in Table 3 below:

TABLE 3 statistical table for evaluation of efficacy of comparative example 1 and example 2 cleansing bubbles

As can be seen from table 3, in example 2, compared to comparative example 1, the cleaning ability and foaming ability of example 2 added with the sapindus mukorossi extract, the quillaja saponaria bark extract, the zanthoxylum bungeanum fruit extract and the forsythia suspensa extract were all stronger than those of comparative example 1, wherein most of the testers considered that the cleaning ability and foaming ability of comparative example 1 were general, and the cleaning ability and foaming ability were strong in contrast to example 2, which proved that the cleansing foam of the present invention had a fast foaming and powerful detergent effect. Both of them are safe and mild and have no irritation. The facial cleansing foam has the advantages that through the combination of the soapberry extract, the quillaja bark extract, the zanthoxylum bungeanum fruit extract and the forsythia suspensa extract, the facial cleansing foam with quick foaming and strong cleaning effects is invented, the composition also has excellent sterilization effect, the synergistic interaction effect among the soapberry extract, the quillaja bark extract, the zanthoxylum bungeanum fruit extract and the forsythia suspensa extract is achieved, and the novel point of the facial cleansing foam is also provided.

The foregoing examples are illustrative of embodiments of the present invention only and are not intended to be limiting in any way; those skilled in the art can make various changes and modifications to the disclosed technology, which are equivalent to those of the embodiments of the present invention, and it is within the scope of the present invention to make various changes and modifications of the invention based on the technical spirit of the present invention.

Claims

1. The composition containing the soapberry extract is characterized by comprising the components of the soapberry extract, the soapberry bark extract, the pricklyash peel extract and the weeping forsythia extract in a mass ratio of 0.0001-10: 0.0001-5: 0.0001-2: 0.0001-2.

2. The composition containing sapindus mukorossi extract according to claim 1, comprising the following components in percentage by weight: 0.0001-10% of soapberry extract, 0.0001-5% of quillaja bark extract, 0.0001-2% of zanthoxylum fruit extract and 0.0001-2% of forsythia extract.

3. A cosmetic containing a sapindus mukorossi extract, characterized by comprising the composition containing a sapindus mukorossi extract according to claim 1 or 2.

4. The cosmetic containing the sapindus mukorossi extract according to claim 3, wherein the cosmetic comprises 2 to 20% of the composition containing the sapindus mukorossi extract.

5. The cosmetic composition of claim 3, wherein the cosmetic composition is a cleansing bubble.

6. The cosmetic composition of claim 5, wherein the cleansing bubbles comprise 2-20% of the composition comprising the soapberry extract.

7. The cosmetic containing sapindus mukorossi extract as claimed in claim 5, wherein said cleansing bubbles further comprise the following components in mass percent: 5-60% of cosmetic matrix.

8. The cosmetic composition of claim 7, wherein the cosmetic base comprises at least one of an emollient, a thickener, a humectant and a neutralizing agent.

9. A method for preparing a cosmetic containing a soapberry extract, characterized by comprising the steps of:

(3) cooling the solution to be prepared in the step (2) to 45-50 ℃, adding at least one of an emollient, a thickener, a humectant and a neutralizer, stirring for 3-5min, cooling to below 45 ℃, and filtering to obtain the cosmetic containing the soapberry extract in the claim 3.

10. Use of the composition containing the soapberry extract according to claim 1 or 2 for preparing a cleansing cosmetic.