CN109965089A - A kind of emulsifiable natural oil coating agent applied to granular mixed feed - Google Patents
A kind of emulsifiable natural oil coating agent applied to granular mixed feed Download PDFInfo
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/10—Animal feeding-stuffs obtained by microbiological or biochemical processes
- A23K10/16—Addition of microorganisms or extracts thereof, e.g. single-cell proteins, to feeding-stuff compositions
- A23K10/18—Addition of microorganisms or extracts thereof, e.g. single-cell proteins, to feeding-stuff compositions of live microorganisms
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/30—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/142—Amino acids; Derivatives thereof
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/158—Fatty acids; Fats; Products containing oils or fats
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/174—Vitamins
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/20—Inorganic substances, e.g. oligoelements
- A23K20/30—Oligoelements
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K40/00—Shaping or working-up of animal feeding-stuffs
- A23K40/30—Shaping or working-up of animal feeding-stuffs by encapsulating; by coating
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Abstract
The invention discloses a kind of emulsifiable natural oil coating agents applied to granular mixed feed, including natural animal-plant grease, concentrating soya lecithin oil, emulsifier, antioxidant, anti-mould fresh keeping agent, polar solvent, vitamin, chelating amino acids state microelement, probiotics and Chinese herbal medicine ultra-fine powder.After required raw material is mixed, sticky paste is made in agitated homogeneous dispersion to obtain the final product.Coating agent is blended into 5~10 times of clear water and stirs to form the medicine slurry with appropriate viscosity, medicament can be selected to prepare medicine slurry with this agent and this agent auxiliary, the medicine slurry can be watered after dilution for livestock and poultry cultivation subjects drank water, can also spray feeding cultivation object after mix granular mixed feed.When granular mixed feed after mix feeds aquaculture object, dust significantly reduces, the hydrophilelipophile parents characteristic of the molten phospholipid complexes lost in breeding water body, liposome, also it can reduce and feed area's water surface tension, mitigate cultivation object to ingest Stress responses, improves health care prophylactic treatment scheme implementation result in breeding production.
Description
Technical field
The invention belongs to coating agent field, especially a kind of emulsifiable natural oil applied to granular mixed feed is coated
Agent.
Background technique
Taking health care prophylactic treatment medicament orally to cultivation object in breeding production especially aquaculture production is common skill
How art measure adds drug with popularizing for granular mixed feed technology, in granular mixed feed and becomes pharmaceutical chemistry
It is the problem of must resolving.
Processing conditions is harsh and the residual pollution of production line medicine, feed situation complexity etc. due to, in advance in feedstuff
Middle mixing medicaments, the mode that then processing compressed granulate mixed feed prepares pharmaceutical chemistry become in breeding production in what is be gradually eliminated
Gesture.
Needs are used in order to meet pharmaceutical chemistry in breeding production in time, it is first will that is generallyd use at present, which prepares the mode of pharmaceutical chemistry,
Drug and appropriate pre-gelatinized starch or the medicine adhesives such as cellulose ether derivative or sodium alginate after mixing, are added to appropriate
It is stirring while adding in clear water, a period of time is stood after stirring evenly, when medical fluid becomes sticky, by manually or mechanically uniformly admixing
In appropriate granular mixed feed, dried in the cool for pharmaceutical chemistry.Even if using in pharmaceuticals industry or food industry by Multiple components
The film coating agent of composition replaces said medicine adhesive, except increase medicament expense cost, requires have preferable mixing equipment item
Outside part, can not equally altogether dispense with the defect of following several respects: a variety of drugs while the existing interaction of while using, having can
It can cause adverse reaction；The dissolution characteristics of drug will affect drug and the affinity of medical fluid causes the reduction of the medical fluid uniformity；Medical fluid
Lack retardation factor appropriate when contacting with granular mixed feed, the dosage for first contacting the feed granules absorption of medical fluid is high, also can
The uniformity reduction for influencing pharmaceutical chemistry feeds effect；After pharmaceutical chemistry dries, the feed clast of more medicament contg superelevation will form, influence
The safety fed.
It is therefore preferable that a variety of natural supplementary materials prepare the novel coating that production meets feed addictive statutory standard meticulously
Agent substitutes original medicine adhesive, film coating agent, reduces the labor intensity and expense branch of mixing granular mixed feed pharmaceutical chemistry
Out, the interaction being passivated between drug, the uniformity raising for improving pharmaceutical chemistry mixing feed effect, reduce and raise in pharmaceutical chemistry dry process
Material debris production quantity improves the safety of granular mixed feed mixing bait feeding in breeding production, it has also become the emphasis of research.
Summary of the invention
A kind of practical and convenient the technical problem to be solved by the present invention is in view of the deficiencies of the prior art, provide, safety is high
The coating agent applied to granular mixed feed mixing pharmaceutical chemistry of effect.
In order to solve the above-mentioned technical problem, the invention discloses a kind of emulsifiable natural oils applied to granular mixed feed
Rouge coating agent, the component including following parts by weight:
Specifically, the natural animal-plant grease is the lard, fish oil, vegetable seeds directly extracted from nature animals and plants
Oil, rice bran oil, soya-bean oil, peanut oil, any one or two or more compositions in palm oil.
The concentrating soya lecithin oil be it is conditioned by raw material of soybean oil sediment, vacuum dehydration and come commercially available production
Product, hydrophilic-hydrophobic balance value are 3~5, and water dispersible is poor, viscosity is stronger, is commonly called as raw phospholipid, and concentrating soya lecithin oil is established
The basis of this coating agent Major Nutrient physiological activity and important service performance is determined.
The emulsifier is food additives sucrose ester of the hydrophilic-hydrophobic balance value greater than 11, natural terpenoids tea soap
Any one in element, natural steroid compound hyodeoxycholic acid or two or more compositions.
The antioxidant is the composition of any one or two kinds of Vitwas E, tea polyphenols., raised to meet
The tocopherol or natural tocopherol of the chemical industry synthesis of feed additives specification, the natural polyphenol class compound extracted from tealeaves.
The vitamin be retinyl acetate, vitamine D3, menadione sodium bisulfite, thiamine mononitrate, riboflavin,
Puridoxine hydrochloride, chlorocobalamin, folic acid, D-Biotin, niacinamide, D-VB5 calcium, in vitamin C any one or it is two or more
Composition, can not also add.
The chelating amino acids state microelement is third generation trace mineral supplement, belongs to organic trace element model
Farmland, including iron, manganese, copper, zinc, iodine, selenium amino-acid chelate in any one or two or more compositions, can not also add
Add；It is pre- that other related components in this coating agent can improve this coating agent health-care assistance as chelating amino acids state microelement
Compatibility when anti-healing potion preparation medicine slurry between drug ingedient.
The probiotics be bacillus, saccharomycete, lactic acid bacteria, photosynthetic bacteria solid-state or liquid formulation any one or
Two or more compositions can not also add.
The Chinese herbal medicine ultra-fine powder is folium cortex eucommiae, rheum officinale, Cortex Phellodendri, radix scutellariae, folium isatidis, Radix Isatidis, kuh-seng, rhizoma zingiberis Ultramicro-powder
Any one in end or two or more compositions, can not also add；The effective component of Chinese herbal medicine ultra-fine powder is of the invention
It can effectively be extracted in coating agent.
Wherein, the partial size of the ultra-micro powder was 300 mesh classifying screens, oversize≤5%.
The anti-mould fresh keeping agent be garlic extracting juice, galic essential oil, in eucalyptus leaf essential oil any one or it is two or more
Composition can not also add.
Wherein, the garlic extracting juice is using stainless steel spiral juice extractor, by removing slag of squeezing of garlic
Natural garlic juice；
Wherein, the galic essential oil is the commercially available natural plant essential oils for meeting Code for Food Additives；
Wherein, the eucalyptus leaf essential oil is the commercially available natural plant essential oils for meeting Code for Food Additives.
The polar solvent is the composition of any one or two kinds of dehydrated alcohol and water, can not also be added.
This is applied to the optimum formula of the emulsifiable natural oil coating agent of granular mixed feed are as follows:
The present invention also provides the preparation methods of the above-mentioned emulsifiable natural oil coating agent applied to granular mixed feed: will
After required raw material mixing, sticky paste is made to obtain the final product in agitated homogeneous dispersion, and substantially the present invention is one kind with O/W/O type multiphase
Homogeneous mixture based on lotion.
Coating agent of the present invention is blended into 5~10 times of clear water and slightly mixes energy Phase inversion emulsification, being formed has appropriate viscosity
Medicine slurry, the substantially medicine slurry is the uniform mixing based on W/O/W type multi-phase emulsion containing phospholipid complexes, liposome
Object.This agent and this agent auxiliary select the medicine slurry spraying mix granular mixed feed of medicament preparation or feed cultivation after being watered dilution
Object is the usage mode of this agent, because of the interaction of each component physicochemical property as a result, granular mixed feed is handled through this agent
Afterwards, dust significantly reduces when feeding, the hydrophilelipophile parents characteristic of the molten phospholipid complexes lost in breeding water body, liposome,
It can reduce water surface tension, mitigate cultivation object and ingest Stress responses, it is real to improve health care prophylactic treatment scheme in breeding production
Apply effect.
The utility model has the advantages that
1, the present invention selects a variety of supplementary materials such as natural animal-plant grease, concentrating soya lecithin oil to be formulated meticulously, converts
Water can generate the micro-capsule of a large amount of active molecule membrane structures when preparing spice medicine slurry, allow in medicament polarity or nonpolarity element all
It obtains the interaction preferably between dissolution, drug to be passivated, medicine slurry adherency is opened up retardance time delay and optimized, for mixing
Conjunction granular mixed feed can improve the raising of pharmaceutical chemistry degree of mixing uniform and feed effect, reduce feed dust clast and generate quantity, guarantee
The safety fed, easy to operate specification, mixing granular mixed feed pharmaceutical chemistry are high-efficient.
2, the spice medicine slurry of coating agent preparation of the present invention, can be watered after dilution for livestock and poultry cultivation subjects drank water, can also spray
Feeding cultivation object especially has bitter taste to the medicament for mixing clothes in livestock and poultry cultivation production after applying mix granular mixed feed
Drug has ideal flavored action, can widen the administration route of drug；When feeding aquaculture object, the phosphatide of the molten mistake in part
Complex, liposome hydrophilelipophile parents characteristic facilitate bait throwing in region formed a metastable dipping area, reduce
The surface tension of water improves water body dissolved oxygen level, dredges office caused by a large amount of defecations, secreting mucus when ingesting in cultivation object set
Portion's water body seriously pollutes, and improves environment and slows down stress of ingesting, improves grazing rate.
3, coating agent of the present invention can effectively facilitate the operating of fat, digestion, absorption, and the liver and gallbladder for preventing cultivated animals are comprehensive
Disease, and unsaturated fatty acid can be supplemented, it boosts metabolism, accelerates growth, reduce feed coefficient.
4, the Chinese herbal medicines such as coating agent of the invention and anthelmintic, antibiotic and Sanhuang San, plate Huang dissipate, kuh-seng dissipates, removing toxic substances dissipates
Micro mist shares, and can generate a certain number of phospholipid complexes and liposome, enable drug absorption rate, bioavilability and drug pair
The directed forces of pathogen significantly improve, and synergy promotes disease cured.
Detailed description of the invention
The present invention is done with reference to the accompanying drawings and detailed description and is further illustrated, of the invention is above-mentioned
And/or otherwise advantage will become apparent.
Fig. 1 is concentrating soya lecithin oil microphoto；
Fig. 2 is coating agent microphoto prepared by embodiment 1；
Fig. 3 is that 200 grams of coating agent of the preparation of embodiment 1 are watered to medicine slurry static condition picture made from 2kg；
Fig. 4 is the medicine slurry microphoto that coating agent prepared by embodiment 1 is watered preparation；
Fig. 5 is that coating agent prepared by embodiment 1 stirs the effect photo after granular mixed feed.
Specific embodiment
According to following embodiments, the present invention may be better understood.
Embodiment 1
According to preparing natural oil coating agent as following formula:
Level-one edible soybean oil 39kg；
Concentrating soya lecithin oil 50kg；
The sucrose ester 2.5kg that hydrophilic-hydrophobic balance value is 12；
Vitwas E 200g；
Galic essential oil 300g；
Water 3kg；
Dehydrated alcohol 5kg.
Above-mentioned supplementary material presses " catalogue of feed additive varieties (2013) ", GB 1535-2003 soybean oil, GB/T 23878-
The standards such as 2009 feed addictive soybean lecithins, GB 8272-2009 food additives sucrose fatty ester, GB2760, CP2010
Apolegamy.
Above-mentioned each component is fed intake mixing according to certain sequence, sticky paste is made in agitated dispersion machine homogeneous to obtain the final product.
Specifically, it is made by following two step:
(1) it is greater than 2.2KW speed regulation vertical hydraulic using power and goes up and down stirring dispersion machine, selects 200 revs/min of revolving speed,
The polar solvent water and dehydrated alcohol, emulsifier hydrophilic-hydrophobic balance value that formula ratio is sequentially added in bucket A are drawn in stainless steel ingredient
The sucrose ester of value 12 promotes dispersing speed to 1000 revs/min, then the natural animal-plant grease of formula ratio 30% after stirring evenly
Level-one edible soybean oil is slowly added into ingredient and draws in bucket A, is prepared into O/W primary emulsified body.
(2) it is greater than 2.2KW speed regulation vertical hydraulic using power and goes up and down stirring dispersion machine, is drawn in bucket B first in stainless steel ingredient
The natural animal-plant grease level-one edible soybean oil of formula ratio 70% is added, selects 100 revs/min of revolving speed, being heated to 70
DEG C formula ratio concentrating soya lecithin oil be slowly added into and stir evenly after, then be successively slowly added into the antioxidant vitamin E of formula ratio
Acetate, anti-mould fresh keeping agent galic essential oil are made oily phase just mixed object, promote dispersing speed to 1000 revs/min, match above-mentioned
Material draws the O/W primary emulsified body prepared in bucket A to be slowly added into ingredient and draws in bucket B, continues to stir 15 minutes homogeneous after feeding intake
Sticky paste is made to obtain the final product, substantially the present invention is a kind of lotion based on O/W/O type multi-phase emulsion.
Fig. 1 is concentrating soya lecithin oil microphoto, and concentrating soya lecithin oil under room temperature, viscosity is strong, micro- through smear
Sem observation measures, and there are 100 microns of size > after a small amount of water swelling of phosphatide condensates in concentrating soya lecithin oil.
Fig. 2 is coating agent microphoto made from the present embodiment, the homogeneous good fluidity of the coating agent under room temperature, through applying
Piece microscope observes and measures, and there are 200 microns of size > after a large amount of water swellings of phosphatide condensates in the coating agent.
Fig. 3 is to be watered, standing 30 good to medicine slurry standing stability made from 2kg for 200 grams of coating agent made from the present embodiment
Minute or more it is not stratified.
Fig. 4 is that coating agent made from the present embodiment is watered the medicine slurry microphoto of preparation, medicine slurry color milk yellow,
Medicine slurry is observed and measured through smear microscopy, and emulsion droplet diameter is distributed in a few micrometers to hundreds of microns in medicine slurry
Between.
Medicine slurry mix granular mixed feed is prepared using above-mentioned coating agent:
S1: looking for the transparent polyester bottle (salad oil bottle) of a 5~10L, and more than ten handstones are placed in bottle, then uses
Electric drill bores the aperture of 5~8 1.2~2mm of diameter on bottle cap, and appropriate capacity graticule is finally marked in body with marking pen；
S2: every mix 40kg granular mixed feed is pressed, coating agent 200g is taken, is made into gross weight with adapted medicament and proper amount of clear water
The ratio of about 1.5~2kg medicine slurry.The clear water and coating agent that about 4 times of coating agent amounts are successively poured into dispensing bottle, cover bottle cap
It shakes up, medicament needed for adding, which shakes up, to be supplied clear water and shake up again to total amount, stands 15 minutes；
S3: it is inverted ingredient bottle, appropriate medicine slurry is slowly sprayed in Ou Ke medicine clothing machine according to body graticule when shaking and is centrifuged
On the granular mixed feed of tumbling motion, about 3~4 minutes mixs to particle uniform color light can be packed.
Fig. 5 is after coating agent obtained above stirs granular mixed feed, feed granules smooth in appearance, without dust clast
Effect photo.
Recommend to select this agent by the 0.5% of granular mixed feed weight.
This coating agent selects 5L PACKAGING BY POLYESTER BOTTLES, it is ensured that storage stability, following table 1 and table 2 are the coating agents batch
Organoleptic indicator, portion of techniques index and GB/T23878-2009 feed addictive after secondary product room temperature stored protected from light 500 days is big
The comparison of Fabaceous Lecithin corresponding index.
Table 1
Table 2
It is compared by above two table, can determine that the coating agent meets the standard requirements of feed addictive, and recommend agent
All supplementary materials that there are many conventional amount used in feed lower than concentrating soya lecithin oil for amount, prepare this agent meet related feed and add
Add agent code requirement, therefore coating agent of the invention is safe and reliable for granular mixed feed mixing pharmaceutical chemistry.
Embodiment 2
According to preparing natural oil coating agent as following formula:
Level-one edible soybean oil 10kg；
Concentrating soya lecithin oil 75kg；
Leached tea oil slag micro mist (natural terpenoids Tea Saponin >=10%) 3.6kg that hydrophilic-hydrophobic balance value is 15；
Vitwas E 500g；
Garlic oil extracting juice 5kg；
Dehydrated alcohol 4.9kg；
Water 1kg
Above-mentioned supplementary material presses " catalogue of feed additive varieties (2013) ", GB 1535-2003 soybean oil, GB/T 23878-
The standards such as 2009 feed addictive soybean lecithins, GB 8272-2009 food additives sucrose fatty ester, GB2760, CP2010
Apolegamy.
Above-mentioned each component is fed intake mixing according to certain sequence, sticky paste is made in agitated dispersion machine homogeneous to obtain the final product.
Specifically, it is made by following two step:
(1) it is greater than 2.2KW speed regulation vertical hydraulic using power and goes up and down stirring dispersion machine, selects 200 revs/min of revolving speed,
Polar solvent dehydrated alcohol, the emulsifier hydrophilic-hydrophobic balance value value 15 that formula ratio is sequentially added in bucket A are drawn in stainless steel ingredient
Leached tea oil slag micro mist (natural terpenoids Tea Saponin >=10%), stir after ten minutes addition polar solvent water, promoted dispersion
Machine revolving speed is to 300 revs/min, then the natural animal-plant grease level-one edible soybean oil of formula ratio 30% is slowly added into ingredient and is drawn
In bucket A, it is prepared into the homogeneous mixture based on O/W primary emulsified body.
(2) it is greater than 2.2KW speed regulation vertical hydraulic using power and goes up and down stirring dispersion machine, is drawn in bucket B first in stainless steel ingredient
The natural animal-plant grease level-one edible soybean oil of formula ratio 70% is added, selects 100 revs/min of revolving speed, being heated to 70
DEG C formula ratio concentrating soya lecithin oil be slowly added into and stir evenly after, then be successively slowly added into the antioxidant vitamin E of formula ratio
Acetate, anti-mould fresh keeping agent garlic oil extracting juice are made oily phase just mixed object, promote dispersing speed to 300 revs/min, upper
Stating ingredient draws the homogeneous mixture based on O/W primary emulsified body prepared in bucket A to be slowly added into ingredient drawing bucket B, feeds intake
After continue stir 15 minutes homogeneous sticky paste is made to obtain the final product, substantially the present invention be one kind with O/W/O type multi-phase emulsion
Based on homogeneous mixture.
Recommend to select this agent by the 0.5% of granular mixed feed weight.
This coating agent selects multi-layer co-extruded plastics thin-film barrier bag to do inner packing, per packed amount 10kg, makes of plastic barrel outer
Packaging, 1 bag of every barrelage, it is ensured that storage stability, following table 3 and table 4 are that the coating agent batch products room temperature is protected from light storage
Organoleptic indicator, portion of techniques index and GB/T 23878-2009 feed addictive soybean lecithin corresponding index after depositing 500
Comparison.
Table 3
Table 4
It is compared by above two table, can determine that the coating agent meets the standard requirements of feed addictive, and recommend agent
All supplementary materials that there are many conventional amount used in feed lower than concentrating soya lecithin oil for amount, prepare this agent meet related feed and add
Add agent code requirement, therefore coating agent of the invention is safe and reliable for granular mixed feed mixing pharmaceutical chemistry.
Embodiment 3
Level-one edible soybean oil 75kg；
Concentrating soya lecithin oil 20kg；
The hyodeoxycholic acid 500g that hydrophilic-hydrophobic balance value is 18
98% content tea polyphenols 20g；
Eucalyptus leaf essential oil 100g；
Water 3.2kg；
Dehydrated alcohol 1kg.
Above-mentioned supplementary material presses " catalogue of feed additive varieties (2013) ", GB 1535-2003 soybean oil, GB/T 23878-
The standards such as 2009 feed addictive soybean lecithins, GB 8272-2009 food additives sucrose fatty ester, GB2760, CP2010
Apolegamy.
Above-mentioned each component is fed intake mixing according to certain sequence, sticky paste is made in agitated dispersion machine homogeneous to obtain the final product.
Specifically, it is made by following two step:
(1) it is greater than 2.2KW speed regulation vertical hydraulic using power and goes up and down stirring dispersion machine, selects 200 revs/min of revolving speed,
The polar solvent water and dehydrated alcohol, emulsifier hydrophilic-hydrophobic balance value that formula ratio is sequentially added in bucket A are drawn in stainless steel ingredient
The sucrose ester of value 12 promotes dispersing speed to 1000 revs/min, then the natural animal-plant grease of formula ratio 30% after stirring evenly
Level-one edible soybean oil is slowly added into ingredient and draws in bucket A, is prepared into O/W primary emulsified body.
(2) it is greater than 2.2KW speed regulation vertical hydraulic using power and goes up and down stirring dispersion machine, is drawn in bucket B first in stainless steel ingredient
The natural animal-plant grease level-one edible soybean oil of formula ratio 70% is added, selects 100 revs/min of revolving speed, being heated to 70
DEG C formula ratio concentrating soya lecithin oil be slowly added into and stir evenly after, then be successively slowly added into the antioxidant vitamin E of formula ratio
Acetate, anti-mould fresh keeping agent galic essential oil are made oily phase just mixed object, promote dispersing speed to 1000 revs/min, match above-mentioned
Material draws the O/W primary emulsified body prepared in bucket A to be slowly added into ingredient and draws in bucket B, continues to stir 15 minutes homogeneous after feeding intake
Sticky paste is made to obtain the final product, substantially the present invention is a kind of lotion based on O/W/O type multi-phase emulsion.
Recommend to select this agent by the 0.5% of granular mixed feed weight.
This coating agent selects 5L PACKAGING BY POLYESTER BOTTLES, it is ensured that storage stability, following table 5 and table 6 are the coating agents batch
Organoleptic indicator, portion of techniques index and GB/T 23878-2009 feed addictive after secondary product room temperature stored protected from light 500 days is big
The comparison of Fabaceous Lecithin corresponding index.
Table 5
Table 6
It is compared by above two table, can determine that the coating agent meets the standard requirements of feed addictive, and recommend agent
All supplementary materials that there are many conventional amount used in feed lower than concentrating soya lecithin oil for amount, prepare this agent meet related feed and add
Add agent code requirement, therefore coating agent of the invention is safe and reliable for granular mixed feed mixing pharmaceutical chemistry.
Embodiment 4
By 1 bag of every mix granular mixed feed (40kg), take coating agent 200g, with the health care prophylactic treatment medicament of adapted and
Proper amount of clear water, which is made into, always weighs about 2kg medicine slurry and every barrel of medicine slurry gross weight is no more than the ratio standard of 20kg, take respectively embodiment 1,
Coating agent prepared by embodiment 2, embodiment 3 into the clean plastic barrel equipped with 4 times of weight clear water, is then covered tightly or is tightened in right amount
It is not run out coating agent packaging bottleneck and sack；With thin stick or electronic splash bar agitation lotion and formed with natural for clear water 1~2 minute
The milk yellow medicine slurry of viscosity, is then added other required medicaments and supplies clear water to total amount, continue to be made for stirring 1~2 minute
Medicine slurry；It can be used within medicine slurry standing 15 minutes or more rod-shaped spray gun to extract weighing medicine slurry spray while stirring and stir shape to mix is in
On the granular mixed feed of state, appearance to medicine slurry adherency is opened up uniformly；The 5-10L for being packed into more than ten pebbles can also be used
Transparent polyester bottle manually shakes prepare medicine slurry standing 15 minutes according to the above ratio, is inverted after covering the bottle cap for being drilled with several apertures
Body sprays medicine slurry when shaking, and in time according to medicine slurry quantity needed for the containing mark line metering marked in advance on body.
Above-mentioned medicine slurry, which continues to be watered 40 times, can also be used for livestock and fowl drinking water.
To mitigate spice labor intensity, the cultivation object relative to certain overall weight, which can keep mixing, takes health care prophylactic treatment
The constant appropriate reduction spice total amount of medicament total amount, the granular mixed feed mix for for safety selecting partial size smaller as far as possible.For
Aquaculture, 1 bag of daily mix granular mixed feed (40kg) feed for the cultivation object of total weight 5000kg, mix clothes and drive
Then suggest only feeding for the cultivation object of 2500~3000kg of total weight when worm medicine.For the livestock and poultry of fed granules mixed feed,
Feed-mixing amount can be determined by the 50% of every Day feeding amount.The feed of daily mix is ingested the situation preferable period point in one day
It has fed for 1~2 time.
The coating agent of coating agent of the present invention, especially embodiment 1 preparation has preferable user experience.Pass through observation
The discovery of spice situation is taken in terms of weighing coating agent, and coating agent prepared by embodiment 1, embodiment 3 is compared with packet prepared by embodiment 2
Clothing agent is convenient；The spice medicine slurry stability aspect prepared with coating agent, coating agent prepared by embodiment 1 is than embodiment 2, embodiment
3 preparation coating agent it is good, under normal circumstances medicine slurry stand 30 minutes it is not stratified, show in medicine slurry have a large amount of bioactive molecule film knots
The micro-capsule of structure, allow in medicine slurry polarity or nonpolarity element all preferably to be dissolved and formed a certain number of phospholipid complexes with
Interaction between liposome, drug is weakened；Retardance time delay is opened up in the spice medicine slurry spice adherency prepared with coating agent
Energy aspect separately invents about 3 points of mix granular mixed feed of pharmaceutical chemistry coating doffer (medicine clothing machine) of production using the present inventor
Clock, coating agent performance prepared by embodiment 1 is optimal, and the granular mixed feed particle surface uniform color of mix is bright, feed meal
Dirt is less, and coating agent prepared by embodiment 2 shows slightly have stick to each other phenomenon between the granular mixed feed particle of mix, leads to
Crossing the appropriate dosage for reducing coating agent and extending duration of mixing can solve, and coating agent prepared by embodiment 3 shows as mix
Granular mixed feed particle surface color uniformity, feed dust it is slightly poor compared with embodiment 1, solution, which has, appropriate increases packet
The dosage of clothing agent improves two kinds of medicine slurry spraying effect of spraying method raising.
Embodiment 5
On August 5th, 2017, certain coastal Large-scale pig farm of Dongtai City, 10, every column, 50 columns of meter newly into 2 monthly age piglets hair
The raw diarrhea state of an illness of having loose bowels is pig blood dysentery caused by Treponema Hyodysenteriae infects through Elisa In The Diagnosis.Wherein 44
Column rule of thumb starts to stop feeding certain brand piglet granular mixed feed, changes and feed autogamy powdery compound feed, feeding per ton for August 6th
The coating Enrofloxacin powder 1kg of material 10% determining enrofloxacin content of addition；Remaining 6 column, 5 afternoon of August start using 10% grace
Air-flow Ultramicro-powder Enrofloxacin powder drinking-water, the mix granular mixed feed pharmaceutical chemistry of promise sand star content respectively handle 3 columns, drinking-water, mix
Granular mixed feed pharmaceutical chemistry operation using embodiment 1 prepare coating agent by aforementioned ratio standard carry out, it is per ton drink water, every bag
The dosage of 40kg brand granular mixed feed, the air-flow Ultramicro-powder Enrofloxacin powder of 10% determining enrofloxacin content is respectively
0.4kg, 32g, piglet drinking-water, situation of ingesting are normal.When to August afternoon 6 on the 8th, drinking-water, mix granular mixed feed pharmaceutical chemistry are taken
6 column meter, 60 piglets of operation all disappear without death, dysentery symptom, and recovery from illness is transferred to normal feeding management；It extremely washes in a pan on remaining 44 column
16, also more piglet appetite is depressed, symptom of having loose bowels is more serious in column, and August 9th start, and stops feeding added with coating grace promise
The autogamy powdery compound feed of Sha Xing, refeeding brand granular mixed feed, using embodiment 1 prepare coating agent with
The air-flow Ultramicro-powder Enrofloxacin powder of 10% determining enrofloxacin content prepares drinking water administration treatment, until on 11 afternoon of August, add up newly-increased
Extremely naughty piglet 6, livestock on hand piglet health status restore good, and dysentery symptom all disappears, and recovery from illness is transferred to normal feeding management.
Since Enrofloxacin bitter taste is larger, using drinking water, mixing feeding administration, swinery can generate food refusal phenomenon, generally use coating En Nuosha
Feeding, Enrofloxacin injection two kinds of administration routes of injection are mixed, but there is conversion feed and cause swinery stress reaction, repeatedly batch injection
Cumbersome defect.By this diagnosis and treatment activity, to mixing clothes when showing the coating agent prepared using embodiment 1 preparation medicine slurry
Medicament especially has the drug of bitter taste to have effects that certain flavoring, has widened route of administration, reduces dosage, improves
Therapeutic effect.
Embodiment 6
200 mu of the port the Jianggang town village Dun Men, Dongtai City adult fish of crucian culture pond mouth, the equidistant placement 4 in the pool slope Kou Xi north-south
Autoamtic bait putting machine is No.1, No. two, No. three, No. four device for feeding fish bait, No. two, No. three device for feeding fish bait material charging regions by Nan Zhibei number consecutively
Domain edge is also mounted with the probe floating drum of automatic dissolved oxygen measurement and control instrument respectively.On July 6th, 2018 is that the pool mouthful customary per half a month is continuous
Last 1 day of fish body health care is carried out with coating agent mix brand granular mixed feed prepared by embodiment 1 within 6 days, 17 when starts
Before last meal is fed, because considering that same day weather is fine, pool surface is calm, and automatic dissolved oxygen measurement and control instrument display screen is shown in feed canopy
No. two, No. three device for feeding fish bait region dissolved oxygen that feeds intake be respectively 16.0mg/l, 16.1mg/l, therefore offhand decision adds 2 bags of throwing to count 80kg
Grain mixed feed is in No. three device for feeding fish bait (close to feed canopy), in other three device for feeding fish bait respectively plus at 2 bags of meter 80kg coating agents
The granular mixed feed managed, during feeding No. three device for feeding fish bait feed intake region fish situation of ingesting compared with other three regions that feed intake
Difference, 30 divide that automatic dissolved oxygen measurement and control instrument display screen shows No. two, No. three device for feeding fish bait feed intake region dissolved oxygen point when feeding half an hour to 17
Not Wei 5.8mg/l, 3.2mg/l, until feeding terminates 10 to divide when the 18 of 10 minutes, automatic dissolved oxygen measurement and control instrument display screen show No. two,
No. three device for feeding fish bait region dissolved oxygen that feeds intake is respectively 13.5mg/l, 13.3mg/l..According to the analysis, the particle handled by coating agent
When mixed feed is fed, phospholipid complexes, liposomal fraction with hydrophilelipophile parents characteristic are molten to be lost in bait throwing in region, can shape
At a metastable dipping area, the surface tension of water is reduced, crucian is dredged and a large amount of defecations, secreting mucus when ingesting is concentrated to make
At local water body seriously pollute, improve water body dissolved oxygen level, in addition crucian to the processed particle of coating agent cooperate
The predisposing factors of ingesting of feed are that other the three region crucian situations of ingesting that feed intake are better than No. three batch chargers region crucian that feeds intake and take the photograph
The main reason for food situation.
Embodiment 7
There is the spot fork that the first and second two cultivating conditions are similar, the water surface is 200 mu in the area the Yancheng City great Feng culture zone Chuan Dong
The Wei Channel-catfish adult fish culture pool mouthful, puts end in a suitable place to breed in by the end of April, 2016, and stocking model is to put 8.5 tail of average size/kilogram Channel-catfish in a suitable place to breed per acre
1000 tail of fingerling, 2.2 tail of average size/kilogram 50 tail of Variegated, 3 tail of average size/kilogram 30 tail of silver carp kind.It cultivated
First and second liang of pool same periods feed same brand with the granular mixed feed of model in journey, and identical regular water transfer is taken to change the cultivation at bottom
Water body management measure, the first pool also adhere to that continuous 6 days of per half a month was carried out with coating agent mix granular mixed feed prepared by embodiment 1
The customary aquaculture management measure of fish body health care.Respectively enteritis occurs for the second pool He " Channel-catfish fish covers enteropathy mid-May and late September " epidemic disease
Feelings, first pool situation does not have fish disease normally during cultivation.After second pool epidemic situation occurs, corresponding pesticide and disinfectant measure is taken,
And pharmaceutical chemistry to the ill is fed on the basis of drug sensitive test, give certain brand feed factory to process drug foods treatment enteritis with Enrofloxacin,
The coating agent scene mixing drug foods treatment " Channel-catfish prepared with embodiment 1 is dissipated with florfenicol powder, doxycycline soluble powder, plate Huang
Fish covers enteropathy ", epidemic situation sprawling is controlled, preferable therapeutic effect is achieved, the second pool is fallen ill twice to be added up to skim Si Wang Channel-catfish fish
More than 1900 tails.To late November current year, on the basis of Channel-catfish fish export and processing enterprise Dui Channel-catfish fish sample detection medicine is residual qualified, first
Two pool mouth fishing sale of second terminate, and first pool bighead silver carp adult fish specification is larger, and the first pool increases production 3000kg than the second pool；Channel-catfish fish at
Fish average size, the first pool are 752g/ tail, and the second pool is 686g/ tail；Feed coefficient, the first pool are 1.42, and the second pool is 1.59；It is overall net
Income, the first pool are 18.7 ten thousand yuan higher than the second pool；10 Wei Channel-catfish fishes are respectively dissected on first and second liang of pools when fishing, and Jia Tang Channel-catfish fish liver appearance is compared with the second pool
Ruddy compact, after measured, the first pool is 2.81 to average liver body ratio, and the second pool is 3.03, significant difference.Production practices prompt embodiment 1
The coating agent of preparation has the operating for promoting fat, digestion, absorption, prevents the liver and gall syndrome of cultivated animals, promotes new old generation
It thanks, accelerates growth, reduce the multi-efficiency of feed coefficient.
Embodiment 8
In by the end of April, 2015, the fish pond of 180 mu of Dongtai City's port Jianggang town a bite water surface, and furuncle occurs for the carassius auratus gibelio species put in a suitable place to breed
Sore disease until multiple pesticide and disinfectant measure had been taken on the pool mouthful when May 8 saw and treated patients, and has fed the saliferous of 5 days feed factories processing
The granular mixed feed (having stopped medicine feed bait when seeing and treating patients 3 days) of sour Enrofloxacin, the pool mouthful dead fish increase day by day, from initial daily dead fish
More than ten tails, develop to the same day of seeing and treating patients 3500 are a plurality of, sampling of fishing of casting net, and pond fish kind the incidence of infection is deposited 80% in the discovery pool mouthful
More than, morbidity fingerling body surface has one to fester to several places, some festering wounds depths and internal organ, wound fester have development it is widened become
Gesture, microscopy also found that disease fish has serious gill rot symptom, and the treatment method provided is that every 5000kg fish uses embodiment 1 daily
Coating agent 200g., Sanhuang San 200g, the neomycinsulphate 40g of preparation prepare 2kg medicine slurry mix 40kg granular mixed feed and throw
Hello, it was even fed 5 from May 9 to May 13, it uses Autoamtic bait putting machine daily morning and afternoon each slow throwing 2 hours.It skimmed May 9 extremely
Fish more than 4000 tails skimmed more than 2200 tails of dead fish, skimmed more than 300 tails of dead fish on May 12, skimmed dead fish more than 30 May 13 on May 10
Tail.It is almost fished out less than dead fish within 15th to May, sampling of fishing of casting net, sick fish is without gill rot symptom, festering wounds newborn black flesh
Film is in ongoing healing status.Neomycinsulphate is aminoglycoside antibiotics, takes orally and seldom absorbs, is generally used only as controlling
Treat the endo-medicine of fish enteritis disease.According to the analysis, this for furunculosis is in severe systemic infection disease in this time diagnosis and treatment activity
The fish disease of shape, neomycinsulphate, the Sanhuang San effective component extracted can be with the phosphorus in coating agent of the present invention when making pharmaceutical chemistry
Rouge molecule forms a certain number of liposomes and phospholipid complexes, and disease fish on the one hand can be improved and ingest absorption of drugs after pharmaceutical chemistry
Utilization rate, the Some liposomes of molten mistake, phospholipid complexes can form dipping area in bait throwing in area after another aspect bait feeding, pass through
Multiple dipping, seriously ill fish are gradually recovered ingestion ability.Production practices prove coating agent of the invention can improve drug absorption rate,
The directed forces of bioavilability and drug to pathogen, synergy promotion disease cured.
The above embodiments surface coating agent green non-pollution has certain nutrition physiology isoreactivity, except auxiliary national standard
For veterinary drug outside, the aquatic animals such as fish shrimp crab can also individually mix for a long time takes coating agent or cooperation functional feed addition of the invention
Agent uses coating agent of the invention.
The present invention provides the thinking and method of a kind of emulsifiable natural oil coating agent applied to granular mixed feed,
There are many method and the approach for implementing the technical solution, the above is only a preferred embodiment of the present invention, it is noted that
For those skilled in the art, without departing from the principle of the present invention, several change can also be made
Into and retouching, these modifications and embellishments should also be considered as the scope of protection of the present invention.Each component part being not known in the present embodiment
The available prior art is realized.
Claims (10)
1. a kind of emulsifiable natural oil coating agent applied to granular mixed feed, which is characterized in that including following parts by weight
Component:
2. coating agent according to claim 1, which is characterized in that the natural animal-plant grease is from nature animals and plants
In directly extract lard, fish oil, rape seed oil, rice bran oil, soya-bean oil, peanut oil, in palm oil any one or it is two or more
Composition.
3. coating agent according to claim 1, which is characterized in that the concentrating soya lecithin oil is with soybean oil sediment
Conditioned for raw material, vacuum dehydration, hydrophilic-hydrophobic balance value is 3~5.
4. coating agent according to claim 1, which is characterized in that the emulsifier is hydrophilic-hydrophobic balance value greater than 11
Food additives sucrose ester, natural terpenoids Tea Saponin, in natural steroid compound hyodeoxycholic acid any one or
Two or more compositions.
5. coating agent according to claim 1, which is characterized in that the antioxidant is Vitwas E, tea polyphenols
Any one or two kinds composition；The vitamin be retinyl acetate, vitamine D3, menadione sodium bisulfite,
Thiamine mononitrate, riboflavin, puridoxine hydrochloride, chlorocobalamin, folic acid, D-Biotin, niacinamide, D-VB5 calcium, appointing in vitamin C
Meaning a combination of one or more object.
6. coating agent according to claim 1, which is characterized in that the chelating amino acids state microelement be iron, manganese,
Copper, zinc, iodine, selenium amino-acid chelate in any one or two or more compositions.
7. coating agent according to claim 1, which is characterized in that the probiotics is bacillus, saccharomycete, lactic acid
Bacterium, the solid-state of photosynthetic bacteria or any one in liquid formulation or two or more compositions.
8. coating agent according to claim 1, which is characterized in that the Chinese herbal medicine ultra-fine powder is folium cortex eucommiae, rheum officinale, Huang
Cypress, radix scutellariae, folium isatidis, Radix Isatidis, kuh-seng, any one or two or more compositions in rhizoma zingiberis ultra-micro powder.
9. coating agent according to claim 1, which is characterized in that the anti-mould fresh keeping agent is garlic extracting juice, garlic essence
Any one in oil, eucalyptus leaf essential oil or two or more compositions；The polar solvent is any one of dehydrated alcohol and water
Kind or two kinds of composition.
10. the preparation method described in claim 1 applied to the emulsifiable natural oil coating agent of granular mixed feed, feature
It is, after required raw material is mixed, sticky paste is made in agitated homogeneous dispersion to obtain the final product.
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| CN110583858A (en) * | 2019-10-23 | 2019-12-20 | 合肥五粮泰生物科技有限公司 | Glycolipid coated granular suckling pig feed and preparation method thereof |
| CN111184149A (en) * | 2020-02-12 | 2020-05-22 | 中国科学院兰州化学物理研究所 | Method for improving suspension property of granular fish feed |
| CN111248353A (en) * | 2020-03-17 | 2020-06-09 | 南宁市泽威尔饲料有限责任公司 | Micro-emulsion type liquid organic trace element feed additive and preparation method thereof |
| CN114010614A (en) * | 2021-12-01 | 2022-02-08 | 天津嘉汇捷瑞医药科技有限公司 | Antioxidant film coating agent for VC (vitamin C) product and preparation method thereof |
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Address after: 224246 No. 97, Fangong North Road, Dongtai town, Dongtai City, Yancheng City, Jiangsu Province Applicant after: JIANGSU OAK ANIMAL MEDICINE Co.,Ltd. Address before: 224200 No. 88, Dongjin North Road, Dongtai City, Yancheng City, Jiangsu Province Applicant before: JIANGSU OAK ANIMAL MEDICINE Co.,Ltd. |
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