CN109938406A - A kind of cigarette filter-tip additive agent, preparation method and application - Google Patents
A kind of cigarette filter-tip additive agent, preparation method and application Download PDFInfo
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- CN109938406A CN109938406A CN201910291004.2A CN201910291004A CN109938406A CN 109938406 A CN109938406 A CN 109938406A CN 201910291004 A CN201910291004 A CN 201910291004A CN 109938406 A CN109938406 A CN 109938406A
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- glyceryl triacetate
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Abstract
The present invention relates to technical field of tobacco, in particular to a kind of cigarette filter-tip additive agent, preparation method and application.The present invention is added to thorn containing hardship, Pu'er tea extract in cigarette filter rod for the first time, has the function of reducing tar and reducing harm to cigarette, cigarette smoking throat irritation can be significantly reduced, promote throat's refrigerant sense, has effects that significant ground pharynx-clearing throat-benefiting, the suction comfort of cigarette is greatly improved, it is deep to be liked by the majority of consumers.
Description
Technical field
The present invention relates to technical field of tobacco more particularly to a kind of cigarette filter-tip additive agents, preparation method and application.
Background technique
With the continuous improvement that consumer health realizes, cigarette product must more focus on being intended to low evil, safe and healthy
Etc. many aspects requirement.In cigarette new product process of innovation, the cigarette product of low tar, less harmful is developed, to meet
The diversified demands such as consumer psychology, physiology and health reduce cigarette smoke to the maximum extent and cause to consumer's health
Harmfulness, become the core content of cigarettes reduce coke damage.However, finding in production practices, cigarettes reduce coke damage is inevitable
Ground influences part aroma quality and loss perfume quantity in cigarette, causes original suction comfort of cigarette to decline, suction taste loses
Very.There is cigarette smoking throat comfort to a certain extent and slightly have deficiency in cigarette, dry sensation is prominent；Therefore, it is necessary to pass through phase
Pass technology makes up this defect, improves the suction comfort of cigarette.Currently, natural plant extracts can effectively be dropped as additive
Burnt harm reduction increases suction comfort.
Summary of the invention
In view of this, the purpose of the present invention is to provide a kind of cigarette filter-tip additive agent, preparation method and applications.It incite somebody to action this
Invention additive is added in cigarette filter rod, has the function of reducing tar and reducing harm to cigarette, can significantly reduce cigarette smoking to throat
Irritation, promote throat's refrigerant sense, there is obvious pharynx-clearing throat-benefiting effect, greatly improve the suction comfort of cigarette, it is deep by
The majority of consumers like.
In order to achieve the object of the present invention, the present invention adopts the following technical scheme:
The present invention provides a kind of preparation method of cigarette filter-tip additive agent, includes the following steps:
Step 1: taking bitter thorn, Pu'er tea, extracted with ethyl alcohol, obtain crude extract；
Step 2: taking the crude extract to add water dispersion, successively through ethyl acetate, extracting n-butyl alcohol, collect n-butanol and mutually extract
Object is dissolved in glyceryl triacetate, obtains the glyceryl triacetate solution containing bitter thorn, Pu'er tea extract, i.e. cigarette filter adds
Agent.
Step 1 of the present invention first pre-processes hardship thorn, Pu'er tea, obtains bitter thorn powder and Pu ' er tea powder, the pretreatment
For drying, crush.
In some embodiments, the drying is to dry at 40~60 DEG C, and the mesh number of the crushing is 50~100 mesh.
To bitter thorn powder and Pu ' er tea powder is obtained, is extracted with ethyl alcohol, obtain crude extract.Wherein, the ethyl alcohol that ethyl alcohol extraction uses
For edible ethanol, volume fraction of ethanol is preferably 95%.
In some embodiments, the extraction of ethyl alcohol described in step 1 impregnates for 24 hours~72h, Yu Wendu for 95% ethyl alcohol is added
It is extracted under conditions of being 0.5~3.0MPa for 20~60 DEG C, pressure.
In some embodiments, in terms of ml/g, 95% ethyl alcohol described in step 1 and hardship is peppery, the sum of Pu'er tea raw material
Volume mass ratio is 10~20:1.
In some specific embodiments provided by the invention, step 1 are as follows: take bitter thorn, Pu'er tea to clean, at 40~60 DEG C
Drying is crushed to 50~100 mesh, obtains bitter thorn powder and Pu ' er tea powder；Then be added 95% ethyl alcohol impregnate for 24 hours, in temperature be 20
~60 DEG C, pressure be 0.5~3.0MPa under conditions of extracted, obtain crude extract.
In some embodiments, crude extract described in step 2 adds in water dispersion, and the dosage of water is the 5 of crude extract weight
~10 times.
After the crude extract adds water dispersion, by the crude extract after dispersion successively through ethyl acetate, extracting n-butyl alcohol, collect just
Butanol phase extract, is dissolved in glyceryl triacetate.In some embodiments, the use of glyceryl triacetate described in step 2
Amount is bitter peppery, Pu'er tea quality sum 1~5 times.
In some embodiments, in step 2 obtain containing bitter thorn, Pu'er tea extract glyceryl triacetate solution it
Further include the steps that refining the glyceryl triacetate solution containing bitter thorn, Pu'er tea extract afterwards.
In some embodiments, the purification is that the thorn containing hardship, the glyceryl triacetate of Pu'er tea extract is molten
Liquid stands 3~8 hours under the conditions of -10~-20 DEG C, collects supernatant.
The present invention it has been investigated that, the glyceryl triacetate solution containing bitter thorn, Pu'er tea extract is carried out above-mentioned
It can make the performance of additive of cigarette filter stick more prominent after purification step, be made after cigarette and more can significantly reduce cigarette smoking to larynx
The irritation in portion promotes throat's refrigerant sense, has effects that become apparent from pharynx-clearing throat-benefiting, suction comfort is higher.
In some specific embodiments provided by the invention, step 2 are as follows: take crude extract to add the water dispersion of 5~10 times of weight,
Successively through ethyl acetate, extracting n-butyl alcohol, collects n-butyl alcohol phase extract and be dissolved in glyceryl triacetate, obtain and pierced containing hardship, is general
The glyceryl triacetate solution of Pu'er tea tea extract, by it is described containing bitter thorn, Pu'er tea extract glyceryl triacetate solution in -10
3~8 hours are stood under the conditions of~-20 DEG C, collects supernatant, obtains cigarette filter-tip additive agent.
The present invention also provides the cigarette filter-tip additive agents as made from preparation method of the present invention.
In a specific embodiment, the present invention is by test of smokeing panel test with gloss, fragrance, harmony, miscellaneous gas, irritation, remaining
Taste is evaluation index, is evaluated cigarette made of cigarette filter-tip additive agent of the present invention, the results show that being added by the present invention
For cigarette overall score made of agent between 93~95, overall score is apparently higher than cigarette made of control group additive.Show this hair
Cigarette made of bright additive can significantly reduce cigarette smoking to the irritation of throat, promote throat's refrigerant sense, have obvious clear
Sharp larynx effect is swallowed, improves the suction comfort of cigarette, effect is substantially better than control group.Therefore, the present invention also provides cigarette
Additives of filter tip is preparing the application in cigarette.
In some embodiments, sweet with triacetic acid when preparing cigarette using cigarette filter-tip additive agent provided by the invention
The cigarette filter-tip additive agent is diluted 5~20 times by grease, is then added in filter stick tow.Wherein, the cigarette filter after dilution
The additive amount of mouth additive is the 7~8% of filter stick tow quality.
The present invention provides a kind of preparation method of cigarette filter-tip additive agent, includes the following steps: step 1: taking bitter thorn, Pu'er
Tea is extracted with ethyl alcohol, obtains crude extract；Step 2: taking the crude extract, successively through ethyl acetate, extracting n-butyl alcohol, collect positive fourth
Alcohol phase extract, is dissolved in glyceryl triacetate, obtains the glyceryl triacetate solution containing bitter thorn, Pu'er tea extract, that is, rolls up
Cigarette filter tip additive.The present invention will be made additives of filter tip and be added in cigarette filter rod containing bitter thorn, Pu'er tea extract for the first time, pass through
Detection, can effectively reduce the harmful components in flue gas, such as nicotine, tar, carbon monoxide, have the work of reducing tar and reducing harm to cigarette
With.Test result of smokeing panel test, which shows that additives of filter tip provided by the invention adds, can significantly reduce cigarette smoking throat irritation, be promoted
Throat's refrigerant sense has effects that significant ground pharynx-clearing throat-benefiting, greatly improves the suction comfort of cigarette, deep to be liked by the majority of consumers
Love.
Specific embodiment
The invention discloses a kind of cigarette filter-tip additive agent, preparation method and application, those skilled in the art can be borrowed
Reflect present disclosure, is suitably modified realization of process parameters.In particular, it should be pointed out that all similar substitutions and modifications are to this field
It is it will be apparent that they are considered as being included in the present invention for technical staff.Method and application of the invention has passed through
Preferred embodiment is described, related personnel obviously can not depart from the content of present invention, in spirit and scope to described herein
Methods and applications be modified or appropriate changes and combinations, carry out implementation and application the technology of the present invention.
To the explanation of the disclosed embodiments, enable those skilled in the art to implement or use the present invention.To this
A variety of modifications of a little embodiments will be readily apparent to those skilled in the art, as defined herein general
Principle can be realized in other embodiments without departing from the spirit or scope of the present invention.Therefore, the present invention will not
It can be intended to be limited to the embodiments shown herein, and be to fit to consistent with the principles and novel features disclosed in this article
Widest scope.
The test material that the present invention uses is all common commercially available product, can all be bought in market.
Below with reference to embodiment, the present invention is further explained:
Embodiment 1
Bitter thorn, Pu'er tea wash clean are taken, dried in 60 DEG C and is crushed to 100 mesh.Bitter thorn, the Pu ' er tea powder crushed is taken,
Subcritical abstraction, immersion liquid are carried out with 95% edible alcohol immersion 24 hours, under the conditions of temperature is 25 DEG C, extracting pressure is 1Mpa
It is concentrated to give crude extract.5 times of water dispersions of crude extract use ethyl acetate, extracting n-butyl alcohol respectively, obtain n-butyl alcohol phase extract concentration
It is spare；After extraction, using glyceryl triacetate as entrainer, the triacetic acid glycerol of obtained thorn containing hardship, Pu'er tea extract
Ester solution.Hardship thorn, Pu'er tea glyceryl triacetate extract dilute 10 times with glyceryl triacetate again, keep it cold after completely dissolution
But it to room temperature, is transferred in -15 DEG C of refrigerators and freezes 10 hours, filter to isolate clear liquid, obtain cigarette filter-tip additive agent.
During cigarette filter tip shaping, additive obtained is added in cigarette filter rod by the 7.5% of tow weight,
Cigarette is made according to common process.
Embodiment 2
Bitter thorn, Pu'er tea complete stool wash clean are taken, dried in 45 DEG C and is crushed to 80 mesh.Take bitter thorn, the Pu'er tea crushed
Powder, was soaked for 3 times, extracted under the conditions of temperature is 35 DEG C, extracting pressure is 2Mpa with 95% edible alcohol immersion 12 hours
Liquid merging is concentrated to give crude extract.10 times of water dispersions of crude extract use ethyl acetate, extracting n-butyl alcohol respectively, obtain n-butanol and mutually extract
Take object concentration spare；After extraction, using glyceryl triacetate as entrainer, the three of obtained thorn containing hardship, Pu'er tea extract
Triacetin ester solution.Hardship thorn, Pu'er tea glyceryl triacetate extract dilute 10 times with glyceryl triacetate again, make it sufficiently
It is cooled to room temperature after dissolution, is transferred in -20 DEG C of refrigerators and freezes 10 hours, filter to isolate clear liquid, obtain cigarette filter addition
Agent.
During cigarette filter tip shaping, additive obtained is added in cigarette filter rod by the 7% of tow weight, is pressed
Cigarette is made in more solito technique.
Embodiment 3
Bitter thorn, Pu'er tea complete stool wash clean are taken, dried in 45 DEG C and is crushed to 80 mesh.Take bitter thorn, the Pu'er tea crushed
Powder, with 95% edible alcohol immersion 18 hours, 2 times, extracted under the conditions of temperature is 50 DEG C, extracting pressure is 1.5Mpa,
Immersion liquid merging is concentrated to give crude extract.8 times of water dispersions of crude extract use ethyl acetate, extracting n-butyl alcohol respectively, obtain n-butanol and mutually extract
Take object concentration spare；After extraction, using glyceryl triacetate as entrainer, the three of obtained thorn containing hardship, Pu'er tea extract
Triacetin ester solution.Hardship thorn, Pu'er tea glyceryl triacetate extract dilute 8 times with glyceryl triacetate again, make it sufficiently
It is cooled to room temperature after dissolution, is transferred in -18 DEG C of refrigerators and freezes 8 hours, filter to isolate clear liquid, obtain cigarette filter addition
Agent.
During cigarette filter tip shaping, additive obtained is added in cigarette filter rod by the 8% of tow weight, so
Cigarette is made using common process afterwards.
Embodiment 4
Using not adding, hardship is pierced, the cigarette of Pu'er tea additive is as blank control group.In addition, setting control group 1 and right
According to group 2, wherein control group 1 using bitter peppery extract as additive, control group 2 using Pu'er tea extract as additive, according to
The method of embodiment 1 prepares and adds the additive, and then routinely cigarette is made in technique.
It is carried out according to cigarette of the standard GB/T 5606.4-2005 to Examples 1 to 3, blank control group, control group 1~2
It smokes panel test, standards of grading are shown in Table 1, and evaluation result is shown in Table 2.
1 standards of grading of table
2 sample definite value of table and distribution
Embodiment 5
Filter tip prepared by Examples 1 to 3, control group 1~2 is rolled according to machine in technical requirements shown in table 3, and is carried out
Main flume tests and analyzes, and the results are shown in Table 4.
The requirement of 3 filter tip technology of preparing of table
The different sample cigarette main stream flue gas index testing results of table 4
The result shows that three kinds of Nicotine from Cigarette made of Examples 1 to 3 additives of filter tip, tar and carbon monoxide substances
Content it is 1~2 lower compared to the control group.Meanwhile machine coiling process quality is stablized on filter tip prepared by the present invention, and manufactured volume
Cigarette main stream flue gas index is stablized.
The above is only a preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, various improvements and modifications may be made without departing from the principle of the present invention, these improvements and modifications are also answered
It is considered as protection scope of the present invention.
Claims (10)
1. a kind of preparation method of cigarette filter-tip additive agent, which comprises the steps of:
Step 1: taking bitter thorn, Pu'er tea, extracted with ethyl alcohol, obtain crude extract；
Step 2: taking the crude extract to add water dispersion, successively through ethyl acetate, extracting n-butyl alcohol, it is molten to collect n-butyl alcohol phase extract
In glyceryl triacetate, the glyceryl triacetate solution containing bitter thorn, Pu'er tea extract, i.e. cigarette filter-tip additive agent are obtained.
2. preparation method according to claim 1, which is characterized in that in terms of ml/g, ethyl alcohol described in step 1 and hardship it is peppery,
The volume mass ratio of the sum of Pu'er tea raw material is 10~20:1.
3. preparation method according to claim 1, which is characterized in that the extraction of ethyl alcohol described in step 1 is 95% second of addition
Alcohol impregnates for 24 hours~72h, is extracted under conditions of temperature is 20~60 DEG C, pressure is 0.5~3.0MPa.
4. preparation method according to claim 1, which is characterized in that further include before ethyl alcohol extraction in step 1
Will be bitter peppery, Pu'er tea is dry, crushing the step of.
5. the preparation method according to claim 4, which is characterized in that the drying is to dry at 40~60 DEG C, the powder
Broken mesh number is 50~100 mesh.
6. preparation method according to claim 1, which is characterized in that the dosage of glyceryl triacetate described in step 2 is
Bitter peppery, Pu'er tea quality sum 1~5 times.
7. preparation method according to claim 1, which is characterized in that obtaining in step 2 containing bitter thorn, Pu'er tea extract
Glyceryl triacetate solution after further include that essence is carried out to the glyceryl triacetate solution containing bitter thorn, Pu'er tea extract
The step of processed.
8. preparation method according to claim 7, which is characterized in that described to refine as hardship thorn, Pu'er tea extraction described contained
It takes the glyceryl triacetate solution of object to stand 3~8 hours under the conditions of -10~-20 DEG C, collects supernatant.
9. cigarette filter-tip additive agent made from preparation method according to any one of claims 1 to 8.
10. cigarette filter-tip additive agent as claimed in claim 9 is preparing the application in cigarette.
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| CN201910291004.2A CN109938406B (en) | 2019-04-11 | 2019-04-11 | Cigarette filter tip additive, preparation method and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910291004.2A CN109938406B (en) | 2019-04-11 | 2019-04-11 | Cigarette filter tip additive, preparation method and application thereof |
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| CN109938406A true CN109938406A (en) | 2019-06-28 |
| CN109938406B CN109938406B (en) | 2021-08-06 |
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| US20120291793A1 (en) * | 2011-05-19 | 2012-11-22 | R.J. Reynolds Tobacco Company | Molecularly imprinted polymers for treating tobacco material and filtering smoke from smoking articles |
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