CN106858716A - A kind of subcritical abstraction prepares the method for tobacco this fragrant composition and the application in cigarette - Google Patents
A kind of subcritical abstraction prepares the method for tobacco this fragrant composition and the application in cigarette Download PDFInfo
- Publication number
- CN106858716A CN106858716A CN201710200522.XA CN201710200522A CN106858716A CN 106858716 A CN106858716 A CN 106858716A CN 201710200522 A CN201710200522 A CN 201710200522A CN 106858716 A CN106858716 A CN 106858716A
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- China
- Prior art keywords
- additive
- cigarette
- tobacco
- filter stick
- cigarette filter
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/062—Use of materials for tobacco smoke filters characterised by structural features
- A24D3/063—Use of materials for tobacco smoke filters characterised by structural features of the fibers
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/067—Use of materials for tobacco smoke filters characterised by functional properties
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention discloses a kind of preparation method of additive of cigarette filter stick, the additive of cigarette filter stick takes following steps with tobacco leaf as raw material:(1) prepared by raw material：Tobacco leaf is dried at 50~80 DEG C, 50~100 mesh are crushed to；(2) subcritical abstraction：The tobacco leaf powder that step (1) is crushed, with dimethyl ether as extractant, with glyceryl triacetate as entrainer, is 0~50 DEG C, is extracted under 0.5~3.0MPa in temperature；(3) preparation of filter stick additive：The dimethyl ether of recycling step (2), the glyceryl triacetate solution containing tobacco leaf extract for obtaining is the additive of cigarette filter stick.The purposes that the additive of cigarette filter stick obtained the invention also discloses the preparation method is used in cigarette products.
Description
Technical field
The invention belongs to technical field of cigarettes, and in particular to a kind of subcritical abstraction prepare tobacco this fragrant composition method and
Application in cigarette.
Background technology
Tobacco drafts a document Solanaceae, and tobacco is annual or limited herbaceos perennial, wherein being planted with tobacco N.tabacum L.
Training is most wide, and its ripe blade is the important source material of cigarette industry, is a kind of economic worth crop higher.Although harm of smoking
Health has been widely recognized, but tobacco still has powerful attraction to thousands of consumer, except nicotine into
Outside addiction, the fragrance matter enriched in tobacco is also played an important role.But with the continuous improvement that consumer health realizes,
Cigarette product must more focus on being intended to the requirement of many aspects such as low evil, safe and healthy.In cigarette new product process of innovation
In, the cigarette product of low tar, less harmful is developed, it is maximum to meet the multiple demands such as consumer psychology, physiology and health
Limit ground reduces the cigarette smoke harmfulness for causing healthy to consumer, the core content as Tar.So
And, being found in production practices, Tar inevitably causes part aroma quality and perfume quantity loss in cigarette, causes
Original aroma quality of cigarette declines, and aspirates taste distortion.Therefore, it is necessary to make up this defect by correlation technique, improve volume
The suction comfortableness of cigarette.
The content of the invention
It is an object of the invention to use subcritical abstraction technology, there is provided a kind of simple to operate, suitable large-scale production
Subcritical abstraction extracts the preparation method of tobacco this fragrant composition, and is added to cigarette filter rod in filter tip forming process, effectively
Lift the aroma quality of cigarette cigarette smoke, reduce miscellaneous gas and excitant, this perfume of prominent tobacco.
Unless otherwise indicated, percentage of the present invention is mass percent.
The purpose of the present invention is achieved by the following technical programs.
First aspect present invention provides a kind of preparation method of additive of cigarette filter stick, it is characterised in that：The cigarette filter rod
Additive takes following steps with tobacco leaf as raw material:
(1) prepared by raw material：Tobacco leaf is dried at 50~80 DEG C, 50~100 mesh are crushed to；
(2) subcritical abstraction：The tobacco leaf powder that step (1) is crushed, with dimethyl ether as extractant, with glyceryl triacetate
It is entrainer, is 0~50 DEG C, is extracted under 0.5~3.0MPa in temperature；
(3) preparation of filter stick additive：The dimethyl ether of removing step (2), the triacetic acid containing tobacco leaf extract for obtaining is sweet
Grease solution, as described additive of cigarette filter stick.
Preferably, it is further comprising the steps of：
(4) the glyceryl triacetate solution containing tobacco leaf extract for obtaining step (3) place 5 at -10~-20 DEG C~
10h, is separated by filtration the clear liquid for obtaining, and is refined with to the additive of cigarette filter stick.
Preferably, the quality of the dimethyl ether is 5~15 times of quality of tobacco, and the quality of the glyceryl triacetate is tobacco leaf
1~5 times of quality.
Second aspect present invention provides the purposes of the additive of cigarette filter stick that described preparation method is obtained, and is added to
The aroma quality of cigarette cigarette smoke can be lifted in cigarette filter rod, miscellaneous gas and excitant, this fragrant purposes of prominent tobacco is reduced.
Preferably, the additive of cigarette filter stick glyceryl triacetate that will be obtained is added to filter after diluting 5~20 times
In rod tow, addition is that the quality after the additive of cigarette filter stick dilution is the 7~8% of tow quality.
Beneficial effects of the present invention
1st, the present invention uses glyceryl triacetate as entrainer, and because glyceryl triacetate is in cigarette filter shaping
The most frequently used plasticizer, so the glyceryl triacetate in preparation method of the invention is served both functions, while eliminating steaming
Lotion body obtains solid additive, and using when be dissolved in additional step in liquid, therefore preparation method work of the invention
Skill is simple, and cost is relatively low, industrially easily realizes.
2nd, extract containing tobacco leaf of the invention is added in cigarette filter rod the aroma quality that can be obviously improved cigarette cigarette smoke
And amount, and miscellaneous gas and excitant are significantly reduced, and this perfume of tobacco is more protruded, make full aroma.Therefore it is of the invention containing tobacco leaf
Extract is added in cigarette filter rod the requirement that can be played to Tar, and the suction that cigarette can be lifted again is comfortable
Property, provide satisfied product to consumer.
3rd, additive of cigarette filter stick of the present invention freezes 5~10h of placement at -10~-20 DEG C, is separated by filtration the clear liquid for obtaining
Other solid impurities can be removed, the performance of additive of cigarette filter stick is more protruded.
Brief description of the drawings
Nothing.
Specific embodiment
The present invention is further described with reference to embodiment, but protection scope of the present invention is not limited to this.
Unless otherwise indicated, percentage of the present invention is mass percent.
Embodiment 1
Tobacco leaf used is the red big B2F in Yuxi, and tobacco sample is dried in 70 DEG C and is crushed to 80 mesh.The tobacco powder for crushing is taken,
Be subcritical abstraction agent with dimethyl ether, glyceryl triacetate is entrainer, temperature be 30 DEG C, extracting pressure be 2.5Mpa conditions
Under carry out subcritical abstraction；Wherein the amount of extractant dimethyl ether is 10 times of cigarette weight.Entrainer glyceryl triacetate consumption is
4 times of tobacco weight.After extraction terminates, extraction mixed liquor enters knockout drum, is separated extractant by the way that principle is evaporated under reduced pressure
The glyceryl triacetate extract rich in this fragrant composition of tobacco can be obtained afterwards.Reclaim after dimethyl ether rich in tobacco this fragrant composition
Glyceryl triacetate extract dilutes 10 times with glyceryl triacetate again, it is cooled to room temperature after fully dissolving, and is transferred to -15
10h is freezed in DEG C refrigerator, clear liquid is filtered to isolate, the stillness of night can use as cigarette filter rod plasticizer.In cigarette filter tip shaping
During, the additive is added in cigarette filter rod by the 7.5% of tow weight；The filter tip that with the addition of the additive is rolled up again
It is made cigarette.Sensory evaluating smoking is carried out to cigarette sample, smoking result is shown in Table 1.
Embodiment 2
Tobacco leaf used is Dali K326, and tobacco sample is dried in 75 DEG C and is crushed to 90 mesh.The tobacco powder for crushing is taken, with two
Methyl ether be subcritical abstraction agent, glyceryl triacetate is entrainer, temperature be 25 DEG C, extracting pressure be 2.8Mpa under the conditions of enter
Row subcritical abstraction；Wherein the amount of extractant dimethyl ether is 12 times of tobacco weight.Entrainer glyceryl triacetate consumption is cigarette
5 times of careless weight.After extraction terminates, extraction mixed liquor enters knockout drum, after extractant is separated by the way that principle is evaporated under reduced pressure
The glyceryl triacetate extract rich in this fragrant composition of tobacco can be obtained.Reclaim this fragrant composition rich in tobacco after dimethyl ether
Glyceryl triacetate extract dilutes 10 times with glyceryl triacetate again, it is cooled to room temperature after fully dissolving, and is transferred to -18
10h is freezed in DEG C refrigerator, clear liquid is filtered to isolate, the stillness of night can use as cigarette filter rod plasticizer.In cigarette filter tip shaping
During, the additive is added in cigarette filter rod by the 7.8% of tow weight；The filter tip that with the addition of the additive is rolled up again
It is made cigarette.Sensory evaluating smoking is carried out to cigarette sample, smoking result is shown in Table 1.
Embodiment 3
Tobacco leaf used is Red River cloud and mist -87, and tobacco sample is dried in 78 DEG C and is crushed to 95 mesh.The tobacco powder for crushing is taken,
Be subcritical abstraction agent with dimethyl ether, glyceryl triacetate is entrainer, temperature be 28 DEG C, extracting pressure be 2.9Mpa conditions
Under carry out subcritical abstraction；Wherein the amount of extractant dimethyl ether is 15 times of tobacco weight.Entrainer glyceryl triacetate consumption
It is 5 times of tobacco weight.After extraction terminates, extraction mixed liquor enters knockout drum, by the way that principle is evaporated under reduced pressure by extractant point
The glyceryl triacetate extract rich in this fragrant composition of tobacco can be obtained from rear.Reclaim dimethyl ether after rich in this perfume (or spice) of tobacco into
The glyceryl triacetate extract for dividing dilutes 8 times with glyceryl triacetate again, makes it that room temperature is cooled to after fully dissolving, and shifts
To -20 DEG C of placement 8h, centrifugation goes out clear liquid, and the stillness of night can use as cigarette filter rod plasticizer.In cigarette filter tip shaping mistake
Cheng Zhong, the additive is added in cigarette filter rod by the 8.0% of tow weight；The filter tip that with the addition of the additive is rolled again
Into cigarette.Sensory evaluating smoking is carried out to cigarette sample, smoking result is shown in Table 1.
Embodiment 4
Tobacco leaf used is Qujing cloud and mist 210, and tobacco sample is dried in 72 DEG C and is crushed to 75 mesh.The tobacco powder for crushing is taken,
Be subcritical abstraction agent with dimethyl ether, glyceryl triacetate is entrainer, temperature be 28 DEG C, extracting pressure be 3.0Mpa conditions
Under carry out subcritical abstraction；Wherein the amount of extractant dimethyl ether is 12 times of tobacco weight.Entrainer glyceryl triacetate consumption
It is 5 times of tobacco weight.After extraction terminates, extraction mixed liquor enters knockout drum, by the way that principle is evaporated under reduced pressure by extractant point
The glyceryl triacetate extract rich in this fragrant composition of tobacco can be obtained from rear.Reclaim dimethyl ether after rich in this perfume (or spice) of tobacco into
The glyceryl triacetate extract for dividing dilutes 5 times with glyceryl triacetate again, makes it that room temperature is cooled to after fully dissolving, and shifts
To -15 DEG C of placement 10h, centrifugation goes out clear liquid, and the stillness of night can use as cigarette filter rod plasticizer.In cigarette filter tip shaping mistake
Cheng Zhong, the additive is added in cigarette filter rod by the 8.0% of tow weight；The filter tip that with the addition of the additive is rolled again
Into cigarette.Sensory evaluating smoking is carried out to cigarette sample, smoking result is shown in Table 1.
Embodiment 5
Tobacco leaf used is Chuxiong cloud and mist 212, and tobacco sample is dried in 75 DEG C and is crushed to 95 mesh.The tobacco powder for crushing is taken,
Be subcritical abstraction agent with dimethyl ether, glyceryl triacetate is entrainer, temperature be 26 DEG C, extracting pressure be 3.0Mpa conditions
Under carry out subcritical abstraction；Wherein the amount of extractant dimethyl ether is 10 times of tobacco weight.Entrainer glyceryl triacetate consumption
It is 4 times of tobacco weight.After extraction terminates, extraction mixed liquor enters knockout drum, by the way that principle is evaporated under reduced pressure by extractant point
The glyceryl triacetate extract rich in this fragrant composition of tobacco can be obtained from rear.Reclaim dimethyl ether after rich in this perfume (or spice) of tobacco into
The glyceryl triacetate extract for dividing dilutes 10 times with glyceryl triacetate again, makes it that room temperature is cooled to after fully dissolving, and shifts
To -12 DEG C of placement 8h, centrifugation goes out clear liquid, and the stillness of night can use as cigarette filter rod plasticizer.In cigarette filter tip shaping mistake
Cheng Zhong, the additive is added in cigarette filter rod by the 8.0% of tow weight；The filter tip that with the addition of the additive is rolled again
Into cigarette.Sensory evaluating smoking is carried out to cigarette sample, smoking result is shown in Table 1.
Using the cigarette without this fragrant component additive agent rich in tobacco as blank sample.It is right to be carried out with blank
Than smokeing panel test, the overall organoleptic's result of the test for obtaining is as shown in table 1 below.
Table 1：This fragrant composition additives of filter tip sensory evaluating smoking's result rich in tobacco
Conclusion：Above-mentioned 5 materials can effectively lift the matter and the amount of fragrance of the fragrance of cigarette smoke, miscellaneous gas, excitant
Substantially reduce, this perfume (or spice) of tobacco is more prominent, and full aroma can be used as cigarette filter-tip additive agent.
Claims (5)
1. a kind of preparation method of additive of cigarette filter stick, it is characterised in that：The additive of cigarette filter stick with tobacco leaf as raw material, and
Take following steps:
(1) prepared by raw material：Tobacco leaf is dried at 50~80 DEG C, 50~100 mesh are crushed to；
(2) subcritical abstraction：The tobacco leaf powder that step (1) is crushed, is folder with glyceryl triacetate with dimethyl ether as extractant
Band agent, is 0~50 DEG C, is extracted under 0.5~3.0MPa in temperature；
(3) preparation of filter stick additive：The dimethyl ether of removing step (2), the glyceryl triacetate containing tobacco leaf extract for obtaining
Solution, as described additive of cigarette filter stick.
2. preparation method according to claim 1, it is characterised in that further comprising the steps of：
(4) the glyceryl triacetate solution containing tobacco leaf extract that step (3) is obtained is placed into 5~10h at -10~-20 DEG C,
The clear liquid for obtaining is separated by filtration, is refined with to the additive of cigarette filter stick.
3. preparation method according to claim 1, it is characterised in that the quality of the dimethyl ether is 5~15 times of quality of tobacco, institute
The quality for stating glyceryl triacetate is 1~5 times of quality of tobacco.
4. the purposes of the additive of cigarette filter stick that a kind of preparation method according to claim 1 is obtained, it is characterised in that will
It can lift the aroma quality of cigarette cigarette smoke, reduce miscellaneous gas and excitant, the sheet of prominent tobacco in being added to cigarette filter rod
Fragrant purposes.
5. purposes according to claim 4, it is characterised in that the additive of cigarette filter stick glyceryl triacetate that will be obtained
It is added in filter stick tow after 5~20 times of dilution, addition is that the quality after the additive of cigarette filter stick dilution is tow matter
The 7~8% of amount.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2016110473087 | 2016-11-21 | ||
| CN201611047308 | 2016-11-21 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106858716A true CN106858716A (en) | 2017-06-20 |
| CN106858716B CN106858716B (en) | 2020-07-21 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710200522.XA Active CN106858716B (en) | 2016-11-21 | 2017-03-29 | Method for preparing tobacco aroma component by subcritical extraction and application of tobacco aroma component in cigarettes |
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| CN (1) | CN106858716B (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109820235A (en) * | 2019-03-18 | 2019-05-31 | 云南中烟工业有限责任公司 | A kind of multi-functional pipe tobacco, preparation method and the usage |
| CN113638265A (en) * | 2020-05-11 | 2021-11-12 | 中国烟草总公司郑州烟草研究院 | Cigarette flavor for cigarette paper coating liquid and application thereof, cigarette paper coating liquid and cigarette |
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| CN101247739A (en) * | 2005-07-29 | 2008-08-20 | 菲利普莫里斯生产公司 | Extraction and storage of tobacco constituents |
| CN105132176A (en) * | 2015-09-28 | 2015-12-09 | 中国烟草总公司郑州烟草研究院 | Preparation method of Mao cigarette extract and application of Mao cigarette extract to cigarette filter stick |
| CN105146739A (en) * | 2015-07-28 | 2015-12-16 | 中国烟草总公司郑州烟草研究院 | Preparation method and application of Jin Tang tobacco essential oil |
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2017
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101247739A (en) * | 2005-07-29 | 2008-08-20 | 菲利普莫里斯生产公司 | Extraction and storage of tobacco constituents |
| CN105146739A (en) * | 2015-07-28 | 2015-12-16 | 中国烟草总公司郑州烟草研究院 | Preparation method and application of Jin Tang tobacco essential oil |
| CN105132176A (en) * | 2015-09-28 | 2015-12-09 | 中国烟草总公司郑州烟草研究院 | Preparation method of Mao cigarette extract and application of Mao cigarette extract to cigarette filter stick |
Non-Patent Citations (1)
| Title |
|---|
| 尉彭城 等: "《卷烟降耗工程》", 30 September 1999 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109820235A (en) * | 2019-03-18 | 2019-05-31 | 云南中烟工业有限责任公司 | A kind of multi-functional pipe tobacco, preparation method and the usage |
| CN109820235B (en) * | 2019-03-18 | 2022-03-11 | 云南中烟工业有限责任公司 | Multifunctional tobacco shred, preparation method and application thereof |
| CN113638265A (en) * | 2020-05-11 | 2021-11-12 | 中国烟草总公司郑州烟草研究院 | Cigarette flavor for cigarette paper coating liquid and application thereof, cigarette paper coating liquid and cigarette |
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| CN106858716B (en) | 2020-07-21 |
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