CN106858715A - A kind of preparation method and application of the additives of filter tip that can improve cigarette suction comfort - Google Patents
A kind of preparation method and application of the additives of filter tip that can improve cigarette suction comfort Download PDFInfo
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- CN106858715A CN106858715A CN201710197440.4A CN201710197440A CN106858715A CN 106858715 A CN106858715 A CN 106858715A CN 201710197440 A CN201710197440 A CN 201710197440A CN 106858715 A CN106858715 A CN 106858715A
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- additive
- purple perilla
- filter stick
- cigarette filter
- cigarette
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention discloses a kind of preparation method of additive of cigarette filter stick, purple perilla is raw material to the east of the additive of cigarette filter stick, and takes following steps:(1) prepared by raw material：Eastern purple perilla is dried at 50~80 DEG C, 50~100 mesh are crushed to；(2) subcritical abstraction：The eastern purple perilla powder that step (1) is crushed, with dimethyl ether as extractant, with glyceryl triacetate as entrainer, is 0~50 DEG C, is extracted under 0.5~3.0MPa in temperature；(3) preparation of filter stick additive：The dimethyl ether of recycling step (2), the glyceryl triacetate solution containing eastern purple perilla extract for obtaining is the additive of cigarette filter stick.The purposes that the additive of cigarette filter stick obtained the invention also discloses the preparation method is used in cigarette products.
Description
Technical field
The invention belongs to technical field of cigarettes, and in particular to a kind of filter tip addition that can improve cigarette smoking throat comfortableness
The preparation method of agent and its application in cigarette.
Background technology
With the continuous improvement that consumer health realizes, cigarette product must more focus on being intended to low evil, safe and healthy
Etc. the requirement of many aspects.In cigarette new product process of innovation, the cigarette product of low tar, less harmful is developed, to meet
The multiple demands such as consumer psychology, physiology and health, reduce that cigarette smoke is healthy to consumer causes to greatest extent
Harmfulness, the core content as Tar.However, being found in production practices, Tar is inevitable
Ground causes part aroma quality and perfume quantity loss in cigarette, causes original suction comfortableness of cigarette to decline, and suction taste loses
Very.There is cigarette smoking throat comfortableness and slightly have deficiency in cigarette, dry sensation is protruded to a certain extent；Therefore, it is necessary to pass through phase
Pass technology makes up this defect, improves the suction comfortableness of cigarette.
Eastern purple perilla (scientific name：Elsholtzia bodinieri Vant.) another name：Bodinier elsholtzia herb, small camellia, Yun Songcha, herbal tea
Deng, it is Labiatae perennial herb, high 25-30 centimetres, pyrene Long Circle is about 1.1 millimeters.Contain aromatic oil in eastern purple perilla；
All herbal medicine, control catch cold, cold, fever, headache bodily pain, sore-throat, toothache caused by fire of deficiency type, indigestion, diarrhoea, mesh pain, it is acute
The diseases such as conjunctivitis, renal shutdown and hepatitis.Its tender point can also work as tea-drinking use, there is clearing heat and detoxicating effect；Chafing dish is commonly used for Yunnan is among the people
The conventional herbal tea in shop, barbecue stand is drunk, it is soaked drink after can eliminate the dry sense of heat of the throat after eating barbecue, chafing dish, lift throat comfortable
Property.But the subcritical abstraction extracting method of eastern purple perilla and it is applied to not yet be had been reported that in cigarette.
The content of the invention
It is an object of the invention to use subcritical abstraction technology, there is provided it is a kind of it is simple to operate, be adapted to large-scale production, with
Eastern purple perilla is the preparation method of the mouth rod additive of primary raw material；Exist the present invention also aims to provide the mouth rod additive
Application in Cigarette processing；The additive can be such that throat's excitant of cigarette smoking substantially reduces, and throat's refrigerant sense is dramatically increased,
With obvious pharynx-clearing throat-benefiting effect.
Unless otherwise indicated, percentage of the present invention is mass percent.
The purpose of the present invention is achieved by the following technical programs.
First aspect present invention provides a kind of preparation method of additive of cigarette filter stick, purple to the east of the additive of cigarette filter stick
It is raw material to revive, and takes following steps:
(1) prepared by raw material：Eastern purple perilla is dried at 50~80 DEG C, 50~100 mesh are crushed to；
(2) extract：The eastern purple perilla powder that step (1) is crushed, is folder with glyceryl triacetate with dimethyl ether as extractant
Band agent, is 0~50 DEG C, is extracted under 0.5~3.0MPa in temperature；
(3) preparation of filter stick additive：The dimethyl ether of removing step (2), the triacetic acid containing eastern purple perilla extract for obtaining
Glycerine ester solution, as described additive of cigarette filter stick.
Preferably, it is further comprising the steps of：
(4) the glyceryl triacetate solution containing eastern purple perilla extract that step (3) is obtained is placed 5 at -10~-20 DEG C
~10h, is separated by filtration the clear liquid for obtaining, and is refined with to the additive of cigarette filter stick.
Preferably, the quality of the dimethyl ether is eastern 5~15 times of purple perilla quality, and the quality of the glyceryl triacetate is east
1~5 times of purple perilla quality.
Second aspect present invention provides the purposes of the additive of cigarette filter stick that described preparation method is obtained, and is added to
Cigarette excitant can be reduced in cigarette filter rod, increases the purposes of refrigerant sense.
Preferably, the additive of cigarette filter stick glyceryl triacetate that will be obtained is added to filter after diluting 5~20 times
In rod tow, addition is that the quality after the additive of cigarette filter stick dilution is the 7~8% of tow quality.
Beneficial effects of the present invention
1st, the present invention uses glyceryl triacetate as entrainer, because during glyceryl triacetate is molded for cigarette filter most
Conventional plasticizer, so the glyceryl triacetate in preparation method of the invention is served both functions, eliminates evaporation liquid
Obtain solid additive, and using when be dissolved in additional step in liquid, therefore preparation method process is simple of the invention,
Cost is relatively low, industrially easily realizes.
2nd, the present invention containing eastern purple perilla extract first being added in cigarette filter rod.Can containing eastern purple perilla extract additive
The requirement to Tar is played, while cigarette smoking throat excitant can be significantly reduced again, lifting throat refrigerant sense, tool
There is obvious pharynx-clearing throat-benefiting effect, improve the suction comfortableness of cigarette, satisfied product is provided to consumer.
3rd, additive of cigarette filter stick of the present invention freezes 5~10h of placement at -10~-20 DEG C, is separated by filtration the clear liquid for obtaining
Other solid impurities can be removed, the performance of additive of cigarette filter stick is more protruded.
Brief description of the drawings
Nothing.
Specific embodiment
The present invention is further described with reference to embodiment, but protection scope of the present invention is not limited to this.
Unless otherwise indicated, percentage of the present invention is mass percent.
Embodiment 1
Eastern purple perilla complete stool wash clean is taken, 80 mesh are dried and be crushed in 70 DEG C.The eastern purple perilla powder for crushing is taken, with dimethyl ether
Be subcritical abstraction agent, glyceryl triacetate is entrainer, temperature be 30 DEG C, extracting pressure be 2.5Mpa under the conditions of carry out Asia
Critical extraction；The amount of wherein extractant dimethyl ether is 10 times of eastern purple perilla weight.Entrainer glyceryl triacetate consumption is purple for east
4 times of Su Chongliang.After extraction terminates, extraction mixed liquor enters knockout drum, after extractant is separated by the way that principle is evaporated under reduced pressure
Can obtain the glyceryl triacetate extract of eastern purple perilla.The eastern purple perilla glyceryl triacetate extract after dimethyl ether is reclaimed to use again
Glyceryl triacetate dilutes 10 times, it is cooled to room temperature after fully dissolving, and is transferred in -15 DEG C of refrigerators and freezes 10h, filtering point
Clear liquid is separated out, the stillness of night can use as cigarette filter rod plasticizer.During cigarette filter tip shaping, the additive is pressed into tow
The 7.5% of weight is added in cigarette filter rod；The filter tip that with the addition of the additive is rolled into cigarette again.Cigarette sample is carried out
Sensory evaluating smoking, smoking result is shown in Table 1.
Embodiment 2
Eastern purple perilla complete stool wash clean is taken, 90 mesh are dried and be crushed in 75 DEG C.The eastern purple perilla powder for crushing is taken, with dimethyl ether
Be subcritical abstraction agent, glyceryl triacetate is entrainer, temperature be 25 DEG C, extracting pressure be 2.8Mpa under the conditions of carry out Asia
Critical extraction；The amount of wherein extractant dimethyl ether is 12 times of eastern purple perilla weight.Entrainer glyceryl triacetate consumption is purple for east
5 times of Su Chongliang.After extraction terminates, extraction mixed liquor enters knockout drum, after extractant is separated by the way that principle is evaporated under reduced pressure
Can obtain the glyceryl triacetate extract of eastern purple perilla.The eastern purple perilla glyceryl triacetate extract after dimethyl ether is reclaimed to use again
Glyceryl triacetate dilutes 10 times, it is cooled to room temperature after fully dissolving, and is transferred in -18 DEG C of refrigerators and freezes 10h, filtering point
Clear liquid is separated out, the stillness of night can use as cigarette filter rod plasticizer.During cigarette filter tip shaping, the additive is pressed into tow
The 7.8% of weight is added in cigarette filter rod；The filter tip that with the addition of the additive is rolled into cigarette again.Cigarette sample is carried out
Sensory evaluating smoking, smoking result is shown in Table 1.
Embodiment 3
Eastern purple perilla complete stool wash clean is taken, 95 mesh are dried and be crushed in 78 DEG C.The eastern purple perilla powder for crushing is taken, with dimethyl ether
Be subcritical abstraction agent, glyceryl triacetate is entrainer, temperature be 28 DEG C, extracting pressure be 2.9Mpa under the conditions of carry out Asia
Critical extraction；The amount of wherein extractant dimethyl ether is 15 times of eastern purple perilla weight.Entrainer glyceryl triacetate consumption is purple for east
5 times of Su Chongliang.After extraction terminates, extraction mixed liquor enters knockout drum, after extractant is separated by the way that principle is evaporated under reduced pressure
Can obtain the glyceryl triacetate extract of eastern purple perilla.The eastern purple perilla glyceryl triacetate extract after dimethyl ether is reclaimed to use again
Glyceryl triacetate dilutes 8 times, it is cooled to room temperature after fully dissolving, and is transferred to -20 DEG C of placement 8h, and centrifugation goes out clearly
Liquid, the stillness of night can use as cigarette filter rod plasticizer.During cigarette filter tip shaping, by the additive by tow weight
8.0% is added in cigarette filter rod；The filter tip that with the addition of the additive is rolled into cigarette again.Sense organ is carried out to cigarette sample to comment
Inhale, smoking result is shown in Table 1.
Embodiment 4
Eastern purple perilla complete stool wash clean is taken, 75 mesh are dried and be crushed in 72 DEG C.The eastern purple perilla powder for crushing is taken, with dimethyl ether
Be subcritical abstraction agent, glyceryl triacetate is entrainer, temperature be 28 DEG C, extracting pressure be 3.0Mpa under the conditions of carry out Asia
Critical extraction；The amount of wherein extractant dimethyl ether is 12 times of eastern purple perilla weight.Entrainer glyceryl triacetate consumption is purple for east
5 times of Su Chongliang.After extraction terminates, extraction mixed liquor enters knockout drum, after extractant is separated by the way that principle is evaporated under reduced pressure
Can obtain the glyceryl triacetate extract of eastern purple perilla.The eastern purple perilla glyceryl triacetate extract after dimethyl ether is reclaimed to use again
Glyceryl triacetate dilutes 5 times, it is cooled to room temperature after fully dissolving, and is transferred to -15 DEG C of placement 10h, and centrifugation goes out clearly
Liquid, the stillness of night can use as cigarette filter rod plasticizer.During cigarette filter tip shaping, by the additive by tow weight
8.0% is added in cigarette filter rod；The filter tip that with the addition of the additive is rolled into cigarette again.Sense organ is carried out to cigarette sample to comment
Inhale, smoking result is shown in Table 1.
Embodiment 5
Eastern purple perilla complete stool wash clean is taken, 95 mesh are dried and be crushed in 75 DEG C.The eastern purple perilla powder for crushing is taken, with dimethyl ether
Be subcritical abstraction agent, glyceryl triacetate is entrainer, temperature be 26 DEG C, extracting pressure be 3.0Mpa under the conditions of carry out Asia
Critical extraction；The amount of wherein extractant dimethyl ether is 10 times of eastern purple perilla weight.Entrainer glyceryl triacetate consumption is purple for east
4 times of Su Chongliang.After extraction terminates, extraction mixed liquor enters knockout drum, after extractant is separated by the way that principle is evaporated under reduced pressure
Can obtain the glyceryl triacetate extract of eastern purple perilla.The eastern purple perilla glyceryl triacetate extract after dimethyl ether is reclaimed to use again
Glyceryl triacetate dilutes 10 times, it is cooled to room temperature after fully dissolving, and is transferred to -12 DEG C of placement 8h, and centrifugation goes out clearly
Liquid, the stillness of night can use as cigarette filter rod plasticizer.During cigarette filter tip shaping, by the additive by tow weight
8.0% is added in cigarette filter rod；The filter tip that with the addition of the additive is rolled into cigarette again.Sense organ is carried out to cigarette sample to comment
Inhale, smoking result is shown in Table 1.
Using the cigarette without eastern additives enhanced by perilla as blank sample, carry out contrast with blank and smoke panel test, obtain
The overall organoleptic's result of the test for arriving is as shown in table 1 below.
Table 1：Eastern purple perilla additives of filter tip sensory evaluating smoking's result
Conclusion：Throat's excitant of the cigarette smoking that above-mentioned 5 materials can increase cigarette smoking is substantially reduced, and throat is clear
Cool feeling is dramatically increased, and with obvious pharynx-clearing throat-benefiting effect, can be made as the cigarette filter-tip additive agent for improving cigarette suction comfort
With.
Claims (5)
1. a kind of preparation method of additive of cigarette filter stick, it is characterised in that：Purple perilla is raw material to the east of the additive of cigarette filter stick,
And take following steps:
(1) prepared by raw material：Eastern purple perilla is dried at 50~80 DEG C, 50~100 mesh are crushed to；
(2) extract：The eastern purple perilla powder that step (1) is crushed, is entrainment with glyceryl triacetate with dimethyl ether as extractant
Agent, is 0~50 DEG C, is extracted under 0.5~3.0MPa in temperature；
(3) preparation of filter stick additive：The dimethyl ether of removing step (2), the triacetic acid glycerine containing eastern purple perilla extract for obtaining
Ester solution, as described additive of cigarette filter stick.
2. preparation method according to claim 1, it is characterised in that further comprising the steps of：
(4) the glyceryl triacetate solution containing eastern purple perilla extract for obtaining step (3) place 5 at -10~-20 DEG C~
10h, is separated by filtration the clear liquid for obtaining, and is refined with to the additive of cigarette filter stick.
3. preparation method according to claim 1, it is characterised in that the quality of the dimethyl ether is eastern 5~15 times of purple perilla quality,
The quality of the glyceryl triacetate is 1~5 times of eastern purple perilla quality.
4. the purposes of the additive of cigarette filter stick that a kind of preparation method according to claim 1 is obtained, it is characterised in that will
It can reduce cigarette excitant, increase the purposes of refrigerant sense in being added to cigarette filter rod.
5. purposes according to claim 4, it is characterised in that the additive of cigarette filter stick glyceryl triacetate that will be obtained
It is added in filter stick tow after 5~20 times of dilution, addition is that the quality after the additive of cigarette filter stick dilution is tow matter
The 7~8% of amount.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2016110473091 | 2016-11-21 | ||
| CN201611047309 | 2016-11-21 |
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| Publication Number | Publication Date |
|---|---|
| CN106858715A true CN106858715A (en) | 2017-06-20 |
| CN106858715B CN106858715B (en) | 2020-02-18 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201710197440.4A Active CN106858715B (en) | 2016-11-21 | 2017-03-29 | Preparation method and application of filter tip additive for improving cigarette smoking comfort |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109275956A (en) * | 2018-09-20 | 2019-01-29 | 云南中烟工业有限责任公司 | A kind of additives of filter tip and preparation method thereof based on the cool taste component of the eastern purple perilla of purification |
| CN109288125A (en) * | 2018-09-20 | 2019-02-01 | 云南中烟工业有限责任公司 | It is a kind of to refine the additives of filter tip and preparation method thereof based on snow mountain Radix Glycyrrhizae sweet ingredient |
| CN109317093A (en) * | 2018-09-18 | 2019-02-12 | 云南中烟工业有限责任公司 | A kind of fermentation carbonization phoenix tail tea granule and its preparation method and application |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109317093A (en) * | 2018-09-18 | 2019-02-12 | 云南中烟工业有限责任公司 | A kind of fermentation carbonization phoenix tail tea granule and its preparation method and application |
| CN109317093B (en) * | 2018-09-18 | 2021-07-09 | 云南中烟工业有限责任公司 | Fermented carbonized phoenix tail tea particles and preparation method and application thereof |
| CN109275956A (en) * | 2018-09-20 | 2019-01-29 | 云南中烟工业有限责任公司 | A kind of additives of filter tip and preparation method thereof based on the cool taste component of the eastern purple perilla of purification |
| CN109288125A (en) * | 2018-09-20 | 2019-02-01 | 云南中烟工业有限责任公司 | It is a kind of to refine the additives of filter tip and preparation method thereof based on snow mountain Radix Glycyrrhizae sweet ingredient |
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| CN106858715B (en) | 2020-02-18 |
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