CN104312725A - Perfume prepared by taking edible flowers as raw materials and used for featured cigarettes and application of perfume - Google Patents
Perfume prepared by taking edible flowers as raw materials and used for featured cigarettes and application of perfume Download PDFInfo
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- CN104312725A CN104312725A CN201410519810.8A CN201410519810A CN104312725A CN 104312725 A CN104312725 A CN 104312725A CN 201410519810 A CN201410519810 A CN 201410519810A CN 104312725 A CN104312725 A CN 104312725A
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- Prior art keywords
- perfume
- flower
- cigarettes
- cigarette
- featured
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Toxicology (AREA)
- General Health & Medical Sciences (AREA)
- Botany (AREA)
- Agronomy & Crop Science (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Seasonings (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a perfume prepared by taking edible flowers as raw materials and used for featured cigarettes and application of the perfume. The perfume disclosed by the invention is prepared from one or more of birchleaf pear flowers, sophora viciifolia hance, caragana sinica, azalea, mayodendron igneum, Japanese banana flowers and begonia by the following steps: adding an organic solvent to the raw material to perform microwave-assisted extraction, filtering an extract solution, concentrating and processing by an MCI reverse-phase chromatographic column to obtain a perfume extract for the cigarettes; and the extract is further added into the cigarettes. The featured perfume for the cigarettes has the effects of increasing fluid production sense, sweetness and moisture of the cigarettes, enriching the cigarette fragrance, reducing irritation, softening the fragrance, increasing comfort and effectively upgrading the smoking quality of the cigarettes, and is conductive to highlighting the style feature of the product. The perfume disclosed by the invention is conductive to improving the economic utilization value of featured plants, the process is simple, the industrialized production is convenient to implement, and the perfume has good development and application prospects.
Description
Technical field
The invention belongs to essence spice for cigarette technical field, specifically relate to a kind of characteristic tobacco aromatics using taking edible flower as raw material and prepare.Meanwhile, the invention still further relates to the application of described tobacco aromatics using in cigarette.
Background technology
Tobacco aromatics using is requisite material in production of cigarettes, is improving cigarette taste, and outstanding cigarette product style and features aspect has important effect.Along with people more and more pay attention to smoking and healthy problem, exploitation low tar Less harmful cigarette has become the long-term task of tobacco industry one.The insufficient fragrance on cigarette tobacco leaf formulation can be made up by the mode of flavoring and casing, assorted gas of forgoing, make the cigarette perfume (or spice) of cigarette product more abundant, sufficient, thus at suction taste, smell on perfume (or spice) there is individual style, strengthen the characteristic of cigarette product.Meanwhile, the exploitation that the plant resources making full use of region feature carries out characteristic tobacco aromatics using is the research direction highly paid close attention to.
The natural ecological environment of Yunnan uniqueness has bred very abundant plant species; 26 nationalitys with the process of getting along for a long time of periphery physical environment in define the cognitive knowledge system to wild plant and Land use systems that differ from one another; wherein; edible wild flower is the important component part that Yunnan's Ethnic folk tradition utilizes in plant, and its Land use systems, nutritive value, exploiting and protecting etc. have become the focus that association area investigator pays close attention to.
Birchleaf pear, bitter tattooing, Flower of Chinese Peashrub, rhododendron, baked wheaten cake flower, Flower of Japanese Banana, Flower of Evans Begonia are the Dai nationality of Yunnan Province, the Yi nationality, distributed over Yunnan, Sichuan and Guizhou, Bai nationality and the Han nationality flowers that tradition is edible for a long time.Birchleaf pear is the not open inflorescence of rosaceous plant birchleaf pear (Pyrus pashia Buch.-Ham.ex D.Don), tens kinds of mineral substance containing abundant VITAMIN, amino acid and needed by human body, there is unique fragrant, can stir-fry and eat, there is effect such as cleaning stomach, reducing blood-fat etc.; Bitter tattooing is the flower of the bitter tattooing (Sophora viciifolia Hance) of Papilionaceae plant, can stir-fry and eat, have the effects such as clearing heat and detoxicating, inducing diuresis and reducing edema; Flower of Chinese Peashrub is the flower of Papilionaceae plant Chinese Peashrub Root (Caragana sinica (Buchoz) Rehd.), stir-fry and eat or omelet eat, there is enriching yin and the effect such as blood, invigorating the spleen; Rhododendron is the petal of ericad sweetshell rhododendron leaf (Rhododendron decorum Fr.) and thick handle cuckoo (R.pachypodum Balf.f.et W.W.Sm.), has antibechic of reducing phlegm, the effect such as clearing heat and detoxicating; Burn the flower of flower for Bignoniaceae plant baked wheaten cake flower (Mayodendron igneum (Kurz) Kurz), the Dai nationality claims " burying glutinous ratio ", is the Dai nationality's tradition edible flower; Flower of Japanese Banana is not open inflorescence and the bract of Musaceae plant bajiao banana (Musa sapientum L.), has unique fresh and sweet taste, has effect of resolving phlegm and softening hard masses, flat liver and the stasis of blood; Flower of Evans Begonia is inflorescence and the rachis of (Begonia edulis Levl.).Scientific research shows, containing the multiple amino acids, electrolytes and minerals, carbohydrate etc. compared with horn of plenty in above-mentioned edible flowers, is conducive to HUMAN HEALTH.How to utilize these characteristic edible wild flowers to improve the suction quality of cigarette, in prior art, there is not been reported.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, a kind of characteristic tobacco aromatics using taking edible flower as raw material and prepare is provided; The cigarette enriching cigarette product is fragrant, promotes the smoking quality of cigarette.
The present invention also aims to provide the embody rule of described tobacco aromatics using in cigarette.
Object of the present invention is achieved by following technical proposals.
Except as otherwise noted, the percentage ratio adopted in the present invention is mass percent.
Take edible flower as a characteristic tobacco aromatics using prepared by raw material, this spices is prepared by following method:
(1) edible flower 50% ~ 95% ethanol of 10 ~ 30 times amount is carried out microwave radiation exaraction, microwave power 50 ~ 500W, extraction time 0.5h ~ 2h, extracted rear filtration, extracting solution is for subsequent use; Described edible flower is one or more in birchleaf pear, bitter tattooing, Flower of Chinese Peashrub, rhododendron, baked wheaten cake flower, Flower of Japanese Banana and Flower of Evans Begonia;
(2) extracting solution is concentrated into paste, upper MCI reverse-phase chromatographic column, first carries out wash-out repeatedly with water, removing pigment, then use 70% and 95% ethanol wash-out repeatedly successively, merging filtrate, concentratedly to obtain medicinal extract, be required tobacco aromatics using.
The application of described tobacco aromatics using in cigarette, is specially: after described tobacco aromatics using is diluted 100 times, with feed way, adds by 0.5% ~ 2% mass ratio, then rolls into cigarette in the usual way.
Compared with prior art, the present invention has the following advantages:
1, select Yunnan's Ethnic edible wild flower among the people to be raw material, such Special plant resource is introduced cigarette additive field, is conducive to the research and development of characteristic tobacco aromatics using;
2, be conducive to the economic use value improving Special plant, enrich its development and utilization measure;
3, develop the tobacco aromatics using shown unique characteristics, it applies in cigarette has the sense of promoting the production of body fluid increasing cigarette, sweet sense, enriches cigarette perfume (or spice), reduce to stimulate, submissive fragrance, increase comfortableness, the effect of effective lifting cigarette smoking quality, is conducive to highlighting of product style characteristic;
4, by microwave radiation exaraction and reversed phase column chromatography combine with technique, technique is simple, is convenient to realize suitability for industrialized production, has good development prospect.
Embodiment
In order to make object of the present invention, technical scheme and advantage clearly understand, below in conjunction with embodiment, the present invention is described in further detail.Should be appreciated that specific embodiment described herein only in order to explain the present invention, the protection domain be not intended to limit the present invention.
Embodiment 1
1. get birchleaf pear 1kg, extract with 95% ethanol of 10 times, microwave power is 50W, extracts 2h, has extracted rear filtration, obtained extracting solution;
2. extracting solution is concentrated into paste, upper MCI reverse-phase chromatographic column, first with water wash-out repeatedly, removes pigment, then use 70% and 95% ethanol wash-out repeatedly successively, merging filtrate concentrates and obtains tobacco aromatics using (medicinal extract);
3. the interpolation in cigarette and evaluation: after gained tobacco aromatics using is diluted 100 times, in reinforced mode, ratio according to 2% makes an addition to cloud and mist (purple) Ye Zuzhong, obtain treatment samples, and with the leaf group sample in contrast do not added, roll into cigarette and carry out sensory evaluating smoking, smoking result is as shown in the table:
Embodiment 2:
1. get bitter tattooing and Flower of Chinese Peashrub 1.5kg (bitter tattooing: Flower of Chinese Peashrub=1:2), extract with 75% ethanol of 15 times, microwave power is 100W, extracts 1.5h, has proposed rear filtration, obtained extracting solution;
2. extracting solution is concentrated into paste, upper MCI reverse-phase chromatographic column, first with water wash-out repeatedly, removes pigment, then use 70% and 95% ethanol wash-out repeatedly successively, merging filtrate concentrates and obtains tobacco aromatics using (medicinal extract);
3. the interpolation in cigarette and evaluation: after gained tobacco aromatics using is diluted 100 times, in reinforced mode, ratio according to 1.5% makes an addition to cloud and mist (purple) Ye Zuzhong, obtain treatment samples, and with the leaf group sample in contrast do not added, roll into cigarette and carry out sensory evaluating smoking, smoking result is as shown in the table:
Embodiment 3:
1. get bitter tattooing, rhododendron, baked wheaten cake flower 1.5kg (bitter tattooing: rhododendron: burn flower=1:2:2), extract with 75% ethanol of 20 times, microwave power is 300W, extracts 1h, has proposed rear filtration, obtained extracting solution;
2. extracting solution is concentrated into paste, upper MCI reverse-phase chromatographic column, first with water wash-out repeatedly, removes pigment, then use 70% and 95% ethanol wash-out repeatedly successively, merging filtrate concentrates and obtains tobacco aromatics using (medicinal extract);
3. the interpolation in cigarette and evaluation: after gained tobacco aromatics using is diluted 100 times, in reinforced mode, ratio according to 1% makes an addition to cloud and mist (purple) Ye Zuzhong, obtain treatment samples, and with the leaf group sample in contrast do not added, roll into cigarette and carry out sensory evaluating smoking, smoking result is as shown in the table:
Embodiment 4:
1. get Flower of Japanese Banana 1kg, extract with 95% ethanol of 10 times, microwave power is 500W, extracts 0.5h, has proposed rear filtration, obtained extracting solution;
2. extracting solution is concentrated into paste, upper MCI reverse-phase chromatographic column, first with water wash-out repeatedly, removes pigment, then use 70% and 95% ethanol wash-out repeatedly successively, merging filtrate concentrates and obtains tobacco aromatics using (medicinal extract);
3. the interpolation in cigarette and evaluation: after gained tobacco aromatics using is diluted 100 times, in reinforced mode, ratio according to 2% makes an addition to cloud and mist (purple) Ye Zuzhong, obtain treatment samples, and with the leaf group sample in contrast do not added, roll into cigarette and carry out sensory evaluating smoking, smoking result is as shown in the table:
Embodiment 5:
1. get Flower of Evans Begonia 1kg, extract with 50% ethanol of 30 times, microwave power is 100W, extracts 2h, has proposed rear filtration, obtained extracting solution;
2. extracting solution is concentrated into paste, upper MCI reverse-phase chromatographic column, first with water wash-out repeatedly, removes pigment, then use 70% and 95% ethanol wash-out repeatedly successively, merging filtrate concentrates and obtains tobacco aromatics using (medicinal extract);
3. the interpolation in cigarette and evaluation: after gained tobacco aromatics using is diluted 100 times, in reinforced mode, ratio according to 0.5% makes an addition to cloud and mist (purple) Ye Zuzhong, obtain treatment samples, and with the leaf group sample in contrast do not added, roll into cigarette and carry out sensory evaluating smoking, smoking result is as shown in the table:
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, all any amendments done within the spirit and principles in the present invention, equivalent replacement and improvement etc., all should be included within protection scope of the present invention.
Claims (2)
1. take edible flower as a characteristic tobacco aromatics using prepared by raw material, this spices is prepared by following method:
(1) edible flower 50% ~ 95% ethanol of 10 ~ 30 times amount is carried out microwave radiation exaraction, microwave power 50 ~ 500W, extraction time 0.5h ~ 2h, extracted rear filtration, extracting solution is for subsequent use; Described edible flower is one or more in birchleaf pear, bitter tattooing, Flower of Chinese Peashrub, rhododendron, baked wheaten cake flower, Flower of Japanese Banana and Flower of Evans Begonia;
(2) extracting solution is concentrated into paste, upper MCI reverse-phase chromatographic column, first carries out wash-out repeatedly with water, removing pigment, then use 70% and 95% ethanol wash-out repeatedly successively, merging filtrate, concentratedly to obtain medicinal extract, be required tobacco aromatics using.
2. the application of tobacco aromatics using described in claim 1 in cigarette, is specially: after described tobacco aromatics using is diluted 100 times, adds, then roll into cigarette in the usual way with feed way, mass ratio by 0.5% ~ 2%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410519810.8A CN104312725A (en) | 2014-09-30 | 2014-09-30 | Perfume prepared by taking edible flowers as raw materials and used for featured cigarettes and application of perfume |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410519810.8A CN104312725A (en) | 2014-09-30 | 2014-09-30 | Perfume prepared by taking edible flowers as raw materials and used for featured cigarettes and application of perfume |
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| Publication Number | Publication Date |
|---|---|
| CN104312725A true CN104312725A (en) | 2015-01-28 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410519810.8A Pending CN104312725A (en) | 2014-09-30 | 2014-09-30 | Perfume prepared by taking edible flowers as raw materials and used for featured cigarettes and application of perfume |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104946393A (en) * | 2015-06-17 | 2015-09-30 | 云南中烟工业有限责任公司 | Pyrus calleryana flower glycerol triacetate extract and application thereof in cigarette |
| RU2596115C1 (en) * | 2015-04-10 | 2016-08-27 | Федеральное государственное бюджетное образовательное учреждение высшего профессионального образования "Кубанский государственный технологический университет" | Method for production of hookah smoking composition |
| CN109938406A (en) * | 2019-04-11 | 2019-06-28 | 吉林烟草工业有限责任公司 | A kind of cigarette filter-tip additive agent, preparation method and application |
| CN115926887A (en) * | 2022-09-23 | 2023-04-07 | 云南中烟工业有限责任公司 | Spice capable of being subjected to color hiding, preparation method and application thereof |
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| CN102041173A (en) * | 2010-12-22 | 2011-05-04 | 华芳烟用香料有限公司 | Extraction and separation method of aromatic part in aromatic tobacco extract and application thereof to cigarettes |
| CN102389162A (en) * | 2011-08-04 | 2012-03-28 | 深圳烟草工业有限责任公司 | Method for preparing cornus officinalis extract, application in cigarettes and cigarette |
| CN103060095A (en) * | 2013-01-25 | 2013-04-24 | 安徽中烟工业有限责任公司 | Indocalamus leaf ethanol extract and application of indocalamus leaf ethanol extract in cigarette |
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2014
- 2014-09-30 CN CN201410519810.8A patent/CN104312725A/en active Pending
Patent Citations (4)
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| CN102041173A (en) * | 2010-12-22 | 2011-05-04 | 华芳烟用香料有限公司 | Extraction and separation method of aromatic part in aromatic tobacco extract and application thereof to cigarettes |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2596115C1 (en) * | 2015-04-10 | 2016-08-27 | Федеральное государственное бюджетное образовательное учреждение высшего профессионального образования "Кубанский государственный технологический университет" | Method for production of hookah smoking composition |
| CN104946393A (en) * | 2015-06-17 | 2015-09-30 | 云南中烟工业有限责任公司 | Pyrus calleryana flower glycerol triacetate extract and application thereof in cigarette |
| CN109938406A (en) * | 2019-04-11 | 2019-06-28 | 吉林烟草工业有限责任公司 | A kind of cigarette filter-tip additive agent, preparation method and application |
| CN109938406B (en) * | 2019-04-11 | 2021-08-06 | 吉林烟草工业有限责任公司 | Cigarette filter tip additive, preparation method and application thereof |
| CN115926887A (en) * | 2022-09-23 | 2023-04-07 | 云南中烟工业有限责任公司 | Spice capable of being subjected to color hiding, preparation method and application thereof |
| CN115926887B (en) * | 2022-09-23 | 2024-03-29 | 云南中烟工业有限责任公司 | Leuco-capable spice, preparation method and application thereof |
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Application publication date: 20150128 |