CN109758397A - A kind of application of feed with paper-mulberry leaf extraction process of active component and extract - Google Patents

A kind of application of feed with paper-mulberry leaf extraction process of active component and extract Download PDF

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Publication number
CN109758397A
CN109758397A CN201910209782.2A CN201910209782A CN109758397A CN 109758397 A CN109758397 A CN 109758397A CN 201910209782 A CN201910209782 A CN 201910209782A CN 109758397 A CN109758397 A CN 109758397A
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China
Prior art keywords
paper
feed
mulberry leaf
parts
extract
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Pending
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CN201910209782.2A
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Chinese (zh)
Inventor
田洋
周露
盛军
宋爽
陶亮
彭磊
解静
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Yunnan Agricultural University
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Yunnan Agricultural University
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Abstract

The present invention discloses the application of a kind of feed with paper-mulberry leaf extraction process of active component and extract, is related to plant extracts, technical field of phytochemistry.Feed with paper-mulberry leaf extraction process of active component of the invention, specifically include active constituent water mention with active constituent alcohol extracting, the active constituent in feed with paper-mulberry leaf is extracted by water extraction method and alcohol extracting method, impurity is removed with petroleum ether later, with active carbon decoloring;Extraction process is also relatively simple, and extracting cycle is obviously shortened, can be with industrialized production;The active component extract of acquisition is prepared into feed with paper-mulberry leaf active component extract moisturizing cream and everyday skincare simultaneously, skin aging situation can be improved, also have better inhibition effect to scytitis;New approaches are provided for the development and utilization of feed with paper-mulberry leaf.

Description

A kind of application of feed with paper-mulberry leaf extraction process of active component and extract
Technical field
The present invention relates to plant extracts, technical field of phytochemistry, it is specifically related to a kind of feed with paper-mulberry leaf active constituent and mentions Take the application of method and extract.
Background technique
Paper mulberry is Moraceae (Moraceae) paper mulberry category deciduous tree.Also known as paddy slurry tree, ancient name paper mulberry.Bark is paper making raw material. Important Arts for the People's Welfare are loaded with plantation and the papermaking process of paper mulberry.Sui Dynasty has mass production.It sets 6~16 meters high, there is milk.Bark is smooth In dark gray, branch is sturdy and open and flat.Leaf alternate, there is a long handle, and blade is wealthy oval or irregular 3~5 drastic crack, and there is rough sawn at edge Tooth, surface is dark green, and by coarse wool, the back side is grayish green, dense pubescence.Unisexual flower, dioecism, male flower Wei amentum are born in new Branches and leaves armpit;Female flower is capitulum.Collective fruits meat, it is spherical, there is long handle, it is red when ripe.Paper mulberry have fast-growing, it is adaptable, Distribution is wide, easily breeds, the feature that heat is high, the period of felling in turn is short.Its root system is shallow, and lateral root distribution is very wide, and growth is fast, rudiment power and tiller Power is strong, resistance to trimming.Resistance tocrocking is strong.Paper mulberry is a kind of small investment, the period is short, quick, be benefited long extraordinary economic forest, is had Ecology well, social and economic benefit, paper mulberry adaptability, resistance are strong, have at aspect of improving the ecological environment very big excellent Gesture;The tall and big grace of tree performance is outstanding Landscape Trees;Leaf, fruit, root, milk have very high medical value, can be used as Medicinal raw material;Fruit and leaf nutritive value are high, can develop new beverage and feed;Bark and limb are China's top grade paper Source, the huge market demand, therefore, reinforcement Broussonetia papyrifera is both protected to the development and utilization of Broussonetia papyrifera.
Currently, being concentrated mainly in the prior art for the development and utilization of paper mulberry: replacing grain using feed with paper-mulberry leaf as feed Food crop stock raising;Bark and limb are developed as high-grade paper making raw material;Broussonetia papyrifera seed is as medicinal material;Do not have also in the prior art Have and active constituent in feed with paper-mulberry leaf is applied in daily chemical products, there is presently no the shields developed with feed with paper-mulberry leaf active component extract Skin articles limit the development and utilization of paper mulberry.
Summary of the invention
In view of the above-mentioned problems existing in the prior art, it the present invention provides a kind of feed with paper-mulberry leaf extraction process of active component and mentions The application for taking object obtains extract by the extraction to feed with paper-mulberry leaf active constituent, and extract is applied to face cream and daily shield Skin product provide new approaches for the development and utilization of feed with paper-mulberry leaf.
To realize above-mentioned technical purpose and the technique effect, the present invention is achieved through the following technical solutions:
A kind of feed with paper-mulberry leaf extraction process of active component, including active constituent water mention with active constituent alcohol extracting, use petroleum later Ether removes impurity, with active carbon decoloring;
The extracting method that the feed with paper-mulberry leaf active constituent water mentions, comprising the following steps: shred feed with paper-mulberry leaf, 30-50 DEG C adds It is soaked in water after heat leaf 1-2 hours;Supernatant is extracted simultaneously to be concentrated, be concentrated to get water layer by petroleum ether extraction soluble pigment and Ester soluble components;Retain water layer passability carbon decoloring, freeze-drying obtains water-soluble active ingredient and extract;
The extracting method of the feed with paper-mulberry leaf active constituent alcohol extracting, comprising the following steps:
70%-75% ethyl alcohol extraction 2-3 times is used Step 1: feed with paper-mulberry leaf chopping is used at 50-60 DEG C of bath temperature, every time 2 hours, merges the ethanol solution of extraction and recycle ethyl alcohol acquisition feed with paper-mulberry leaf ethyl alcohol primary extract;
Step 2: being dissolved in water to feed with paper-mulberry leaf ethyl alcohol primary extract, with petroleum ether extraction, degreasing soluble components, pigment, water layer It decolourizes and is spray-dried;
Step 3: contact plate detects feed with paper-mulberry leaf active constituent and obtains feed with paper-mulberry leaf active component extract.
Another object of the present invention is to provide a kind of feed with paper-mulberry leaf active component extract answering in daily chemical products preparation With.
Another object of the present invention is to provide a kind of feed with paper-mulberry leaf active component extracts in face cream, lotion, facial mask preparation In application.
Another object of the present invention is to provide a kind of feed with paper-mulberry leaf active component extract face creams, including following parts by weight Raw material: 1-10 parts of paper mulberry leaf extract, 2-5 parts of butanediol, 2-3 parts of glycerol, 2-5 parts of rose (ROSA RUGOSA) flower extract, 2-3 parts of dimethyl silicone polymer, 3-6 parts of Jojoba (SIMMONDSIA CHINENSIS) seed oil, 2-5 parts of carbonic acid dioctyl ester, whale 3-5 parts of ceryl alcohol, 3-5 parts of Glyceryl stearate citrate, 3-5 parts of stearine, 2-3 parts of PEG-100 stearate, third Olefin(e) acid (ester) class/2-3 parts of C10-30 alkylol acrylamide acid esters cross-linked polymer, aloe barbadensis Miller (ALOE BARBADENSIS) leaf juice 2-3 parts of powder, 2-3 parts of Phenoxyethanol, 2-3 parts of Sensiva SC50,2-3 parts of triethanolamine, 20-30 parts of water.
Further, the feed with paper-mulberry leaf active component extract is mended Broussonetia extract (Paper mulberry) in face cream and is added Add and mentions as 1-10%.
Beneficial effects of the present invention: the application of feed with paper-mulberry leaf extraction process of active component and extract of the present invention is mentioned by water The active constituent extracted in feed with paper-mulberry leaf with alcohol extracting method is followed the example of, the active matter of higher degree can be obtained;Flavones, polysaccharide chemical combination Object;Extraction process is also relatively simple, and extracting cycle is obviously shortened, can be with industrialized production;The active constituent of acquisition is extracted simultaneously Object prepares feed with paper-mulberry leaf active component extract moisturizing cream and everyday skincare, can improve skin aging situation, to skin Inflammation also has better inhibition effect;New approaches are provided for the development and utilization of feed with paper-mulberry leaf.
Certainly, it implements any of the products of the present invention and does not necessarily require achieving all the advantages described above at the same time.
Detailed description of the invention
In order to illustrate the technical solution of the embodiments of the present invention more clearly, will be described below to embodiment required Attached drawing is briefly described, it should be apparent that, drawings in the following description are only some embodiments of the invention, for ability For the those of ordinary skill of domain, without creative efforts, it can also be obtained according to these attached drawings other attached Figure.
Fig. 1 is the process flow chart of feed with paper-mulberry leaf active constituent alcohol extracting described in the embodiment of the present invention;
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts all other Embodiment shall fall within the protection scope of the present invention.
Embodiment 1
A kind of feed with paper-mulberry leaf extraction process of active component, including active constituent water mention with active constituent alcohol extracting, use petroleum later Ether removes impurity, with active carbon decoloring;
The extracting method that the feed with paper-mulberry leaf active constituent water mentions, comprising the following steps: shred feed with paper-mulberry leaf, 30-50 DEG C adds It is soaked in water after heat leaf 1-2 hours;It extracts supernatant and is concentrated;Be concentrated to get water layer by petroleum ether extraction soluble pigment and Ester soluble components;Retain water layer and pass through active carbon decoloring, freeze-drying obtains water-soluble active ingredient and extract;
The extracting method of the feed with paper-mulberry leaf active constituent alcohol extracting, comprising the following steps:
70%-75% ethyl alcohol extraction 2-3 times is used Step 1: feed with paper-mulberry leaf chopping is used at 50-60 DEG C of bath temperature, every time 2 hours, merges the ethanol solution of extraction and recycle ethyl alcohol acquisition feed with paper-mulberry leaf ethyl alcohol primary extract;
Step 2: being dissolved in water to feed with paper-mulberry leaf ethyl alcohol primary extract, with petroleum ether extraction, degreasing soluble components, pigment, water layer It decolourizes and is spray-dried;
Step 3: contact plate detects feed with paper-mulberry leaf active constituent and obtains feed with paper-mulberry leaf active component extract.
The active constituent in feed with paper-mulberry leaf is extracted by water extraction method and alcohol extracting method, the active matter of higher degree can be obtained; Flavones, polysaccharide compound, extraction process is also relatively simple, and extracting cycle is obviously shortened, can be with industrialized production.
Embodiment 2
A kind of application of feed with paper-mulberry leaf active component extract in face cream preparation.
A kind of paper mulberry active component extract face cream, including following raw material: 1-10 parts of paper mulberry leaf extract, fourth 2-5 parts of glycol, 2-3 parts of glycerol, 2-5 parts of rose (ROSA RUGOSA) flower extract, 2-3 parts of dimethyl silicone polymer, Jojoba 3-6 parts of (SIMMONDSIA CHINENSIS) seed oil, 2-5 parts of carbonic acid dioctyl ester, 3-5 parts of cetanol, stearine lemon 3-5 parts of acid esters, 3-5 parts of stearine, 2-3 parts of PEG-100 stearate, acrylic acid (ester) class/C10-30 alkylol acrylamide 2-3 parts of acid esters cross-linked polymer, 2-3 parts of aloe barbadensis Miller (ALOE BARBADENSIS) leaf juice powder, 2-3 parts of Phenoxyethanol, second 2-3 parts of base hexyl glycerol, 2-3 parts of triethanolamine, 20-30 parts of water.
The feed with paper-mulberry leaf active component extract is mended Broussonetia extract (Paper mulberry) addition in face cream and is mentioned as 1- 10%.
The active component extract obtained in above-described embodiment 1 is subject to auxiliary material and prepares feed with paper-mulberry leaf active component extract face Frost, can improve skin aging situation, also have better inhibition effect to scytitis.
Embodiment 3
A kind of application of feed with paper-mulberry leaf active component extract in face cream, lotion, facial mask preparation and daily chemical products preparation.
In face cream, lotion, facial mask preparation process, add with the feed with paper-mulberry leaf active component extract of 1-10% parts by weight, Face cream, lotion, facial mask and the daily chemical products of preparation, can improve skin aging situation, also have to scytitis and preferably inhibit to make With;New approaches are provided for the development and utilization of feed with paper-mulberry leaf;
In specific implementation process, add with the feed with paper-mulberry leaf active component extract of parts by weight 1% or so, effect is preferable, can The effect of to play active matter.
In the description of this specification, the description of reference term " one embodiment ", " example ", " specific example " etc. means Particular features, structures, materials, or characteristics described in conjunction with this embodiment or example are contained at least one implementation of the invention In example or example.In the present specification, schematic expression of the above terms may not refer to the same embodiment or example. Moreover, particular features, structures, materials, or characteristics described can be in any one or more of the embodiments or examples to close Suitable mode combines.
Present invention disclosed above preferred embodiment is only intended to help to illustrate the present invention.There is no detailed for preferred embodiment All details are described, are not limited the invention to the specific embodiments described.Obviously, according to the content of this specification, It can make many modifications and variations.These embodiments are chosen and specifically described to this specification, is in order to better explain the present invention Principle and practical application, so that skilled artisan be enable to better understand and utilize the present invention.The present invention is only It is limited by claims and its full scope and equivalent.

Claims (6)

1. application of the feed with paper-mulberry leaf active component extract in daily chemical products preparation.
2. application of the feed with paper-mulberry leaf active component extract as described in claim 1 in face cream, lotion, facial mask preparation.
3. the application of the feed with paper-mulberry leaf active component extract as described in claims 1 or 2 any one, it is characterised in that: described Feed with paper-mulberry leaf extraction process of active component, including active constituent water are mentioned and being used with active constituent alcohol extracting later with petroleum ether removing impurity Active carbon decoloring.
4. the application of feed with paper-mulberry leaf active component extract as claimed in claim 3, it is characterised in that: the feed with paper-mulberry leaf activity at The extracting method for dividing water to mention, comprising the following steps: feed with paper-mulberry leaf is shredded, is soaked in water leaf 1-2 hours after 30-50 DEG C of heating.It mentions It takes supernatant and is concentrated;It is concentrated to get water layer and passes through petroleum ether extraction soluble pigment and ester soluble components;Retain water layer to pass through Active carbon decoloring, freeze-drying obtain water-soluble active ingredient and extract;
The extracting method of the feed with paper-mulberry leaf active constituent alcohol extracting, comprising the following steps:
It is extracted 2-3 times Step 1: feed with paper-mulberry leaf chopping is used at 50-60 DEG C of bath temperature with 70%-75% ethyl alcohol, 2 is small every time When, merge the ethanol solution of extraction and recycles ethyl alcohol acquisition feed with paper-mulberry leaf ethyl alcohol primary extract;
Step 2: being dissolved in water to feed with paper-mulberry leaf ethyl alcohol primary extract, with petroleum ether extraction, degreasing soluble components, pigment, water layer decoloration And it is spray-dried;
Step 3: contact plate detects feed with paper-mulberry leaf active constituent and obtains feed with paper-mulberry leaf active component extract.
5. a kind of feed with paper-mulberry leaf active component extract face cream, it is characterised in that: including following raw material: paper mulberry leaf extract 1-10 parts, 2-5 parts of butanediol, 2-3 parts of glycerol, 2-5 parts of rose (ROSA RUGOSA) flower extract, dimethyl silicone polymer 2-3 Part, 3-6 parts of Jojoba (SIMMONDSIA CHINENSIS) seed oil, 2-5 parts of carbonic acid dioctyl ester, 3-5 parts of cetanol, glyceryl stearate 3-5 parts of acid esters citrate, 3-5 parts of stearine, 2-3 parts of PEG-100 stearate, acrylic acid (ester) class/C10-30 2-3 parts of alkylol acrylamide acid esters cross-linked polymer, 2-3 parts of aloe barbadensis Miller (ALOE BARBADENSIS) leaf juice powder, Phenoxyethanol 2-3 parts, 2-3 parts of Sensiva SC50,2-3 parts of triethanolamine, 20-30 parts of water.
6. feed with paper-mulberry leaf active component extract face cream as claimed in claim 5, it is characterised in that: the feed with paper-mulberry leaf active constituent Broussonetia extract (Paper mulberry) addition mentions as 1-5% in extract face cream.
CN201910209782.2A 2019-03-19 2019-03-19 A kind of application of feed with paper-mulberry leaf extraction process of active component and extract Pending CN109758397A (en)

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