KR20110092721A - The composite make natural korean herb cosmetics from genseng saponin rg1 and polia coccos ferment - Google Patents

The composite make natural korean herb cosmetics from genseng saponin rg1 and polia coccos ferment Download PDF

Info

Publication number
KR20110092721A
KR20110092721A KR1020100012307A KR20100012307A KR20110092721A KR 20110092721 A KR20110092721 A KR 20110092721A KR 1020100012307 A KR1020100012307 A KR 1020100012307A KR 20100012307 A KR20100012307 A KR 20100012307A KR 20110092721 A KR20110092721 A KR 20110092721A
Authority
KR
South Korea
Prior art keywords
brown rice
ginseng
fermented
cosmetics
extract
Prior art date
Application number
KR1020100012307A
Other languages
Korean (ko)
Other versions
KR101238825B1 (en
Inventor
손동화
최향자
Original Assignee
대구산업정보대학 산학협력단
최향자
손동화
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 대구산업정보대학 산학협력단, 최향자, 손동화 filed Critical 대구산업정보대학 산학협력단
Priority to KR1020100012307A priority Critical patent/KR101238825B1/en
Publication of KR20110092721A publication Critical patent/KR20110092721A/en
Application granted granted Critical
Publication of KR101238825B1 publication Critical patent/KR101238825B1/en

Links

Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9728Fungi, e.g. yeasts
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/63Steroids; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/85Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine

Landscapes

  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Microbiology (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Mycology (AREA)
  • Dermatology (AREA)
  • Botany (AREA)
  • Biotechnology (AREA)
  • Engineering & Computer Science (AREA)
  • Gerontology & Geriatric Medicine (AREA)
  • Cosmetics (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

PURPOSE: A natural herb cosmetic product using ginseng saponin Rg1 and Poria cocos fermentation is provided to enlarge blood vessel and to supply enough nutrient. CONSTITUTION: A natural herb cosmetic product contains 0.8-1.5 weight% of Poria cocos fermentation and 0.3-0.8 weight% of ginseng saponin Rg1 as an active ingredient. The ginseng saponin is prepared by washing and drying ginseng leaves, and extracting and concentrating with 70-80% ethanol at 80°C. The fermentation is prepared by drying Poria cocos-fermented brown rice by hot wind at 40+/-5°C, pulverizing at 60-80 meshes, and extracting with 80% ethanol at 60-80°C for 3-5 hours.

Description

인삼사포닌Rg1과 복령발효산물을 이용한 천연 한방화장품{The Composite make natural korean herb cosmetics from genseng saponin Rg1 and polia coccos ferment}The composite make natural korean herb cosmetics from genseng saponin Rg1 and polia coccos ferment}

본 발명은 인삼사포닌Rg1과 복령발효산물을 이용한 화장품과 그 제조방법에 관한 것으로, 최적분리공정을 통해 인삼사포닌 성분이 강화된 혼합물을 생성하고, 이를 복령발효산물과 함께 첨가하여 천연물의 기능성을 구비할 수 있는 인삼사포닌Rg1과 복령발효산물을 이용한 천연 한방화장품에 관한 것이다.
The present invention relates to a cosmetic using the ginseng saponin Rg1 and Bokryeong fermented products and a method for manufacturing the same, to produce a mixture of enhanced ginseng saponin components through an optimal separation process, and added with the Bokryeong fermented products to provide the functionality of natural products The present invention relates to a natural herbal cosmetics using ginseng saponin Rg1 and Bokryeong fermented products.

최근의 친환경적, 자연적인 소비추세에 맞추어 식물유래 천연물의 효용성을 기반으로 여러 가지 형태로 화장품에 응용되고 있으며, 그 천연물의 기능성을 가져 여드름, 항염증, 피부개선, 보습 및 기타 화장품으로 널리 이용되고 있다.It is applied to cosmetics in various forms based on the effectiveness of plant-derived natural products in accordance with the recent eco-friendly and natural consumption trends, and has been widely used as acne, anti-inflammatory, skin improvement, moisturizing and other cosmetics because of its functionality. have.

국내에서 화장품 원료로 주로 사용되는 천연물에는 지역특산물과 밀접한 관계를 지니고 있으며, 천연물 화장품은 유효성분의 함량이 일정하지 않으며, 그 약리작용이 밝혀지지 않은 것이 단점이 있으며, 또한 제조시간이 길고, 저장성의 문제와 대량생산에 적합하지 않다는 문제점을 가지고 있어서 보편적으로 널리 이용되는 재료가 인삼과 홍삼이며, 인삼 및 홍삼을 함유한 화장료는 제형에 관계없이 다양하게 이용되고 있으며, 미백, 노화방지, 피부개선 등 복합기능성 효과를 나타내며, 인삼뿌리 추출물과 인삼과 홍삼에서 분리해 낸 다당체 및 진세노사이드 등이 이용되고 있으나, 특정 진세노사이드 성분이 강화된 제품으로 가장 잘 알려진 것은 일부 화장품에 한정되고 있다. Natural products mainly used as cosmetic raw materials in Korea have a close relationship with local specialty products, and natural cosmetic products have the disadvantage that the content of active ingredient is not constant and its pharmacological action is not revealed. Ginseng and red ginseng are widely used materials, and cosmetics containing ginseng and red ginseng are variously used regardless of the formulation. It shows a multi-functional effect, such as ginseng root extract and polysaccharides and ginsenosides separated from ginseng and red ginseng, but the best known as a product enhanced with a specific ginsenoside component is limited to some cosmetics.

수년간 국내의 피부 주름개선 화장품의 대명사처럼 사용되어 온 레티놀(비타민 A) 및 그 유도체들은 기존의 주름개선 원료들에 비해 주름완화 효과와 피부세포재생, 미백 등의 부가적인 효과가 있는 것으로 보고되고 있으나, 레티놀은 빛을 받았을 경우 빛에 의해 변성되면서 피부에 자극을 일으키는 광독성과 그 안정성이 끊임없이 문제제기 되어지고 있고, 강한 항산화효과로 가장 주목받고 있는 원료인 비타민 C의 경우는 강력한 항산화효과와 안정성과의 상관관계가 풀기 어려운 숙제로 남아있어 우수한 효과와 안정성을 두루 갖춘 새로운 원료에 대한 요구가 커지고 있다.
Retinol (vitamin A) and its derivatives, which have been used as a synonym for skin wrinkle improvement cosmetics in Korea for many years, are reported to have additional effects such as wrinkle relief, skin cell regeneration, and whitening, compared to existing wrinkle improvement ingredients. Retinol, which is denatured by light when exposed to light, is constantly questioned about its phototoxicity and its stability. In the case of vitamin C, which is the most notable ingredient due to its strong antioxidant effect, it has strong antioxidant effects and stability and Is a difficult task to solve, increasing the demand for new raw materials with excellent effects and stability.

본 발명은 상기와 같은 문제점을 해소하기 위한 것으로, 그 목적은 인삼사포닌Rg1과 복령발효산물의 정제효율을 증대시켜, 천연물질의 기능성을 구비한 천연 한방화장품을 제공하는 것이다. The present invention is to solve the above problems, the object is to increase the purification efficiency of ginseng saponin Rg1 and Bokryeong fermented products, to provide a natural herbal cosmetics with the functionality of natural substances.

본 발명의 또다른 목적은 인삼사포닌Rg1의 정제시, 진세노사이드의 함량을 일정하게 유지하면서 인삼내의 농약성분과 엽록소를 한번에 제거할 수 있는 천연 한방화장품을 제공하는 것이다. Another object of the present invention is to provide a natural herbal cosmetics that can remove the pesticide components and chlorophyll in ginseng at a time while maintaining the content of ginsenosides at the time of purification of ginseng saponin Rg1.

본 발명의 또다른 목적은 복령의 최적 발효를 통해 무기질, 아미노산, 비타민등의 유효성분을 최대로 유지할 수 있는 인삼사포닌Rg1과 복령발효산물을 이용한 천연 한방화장품을 제공하는 것이다.
It is another object of the present invention to provide a natural herbal cosmetics using ginseng saponin Rg1 and Bokryeong fermented products which can maintain the maximum active ingredients such as minerals, amino acids and vitamins through optimal fermentation of Bokryeong.

본 발명은 천연한방화장품에 있어서, 상기 한방화장품은 복령발효산물(Poria Cocos Extract) 0.8∼1.5wt%, 인삼사포닌 Rg1(Panax Ginseng Root Extract) 0.3∼0.8wt% 를 유효성분으로 포함하되,The present invention in the natural herbal cosmetics, the herbal cosmetics, but the active ingredient (Poria Cocos Extract) 0.8 ~ 1.5wt%, ginseng saponin Rg1 (Panax Ginseng Root Extract) 0.3 ~ 0.8wt% as an active ingredient,

상기 인산사포닌Rg1은 세척건조시킨 인삼잎을 70∼80% 에탄올에서 80℃ 추출하여 농축액을 생성하고, 생성된 농축액을 원심분리하여 엽록소와 살충제를 제거한 후 동결건조(Freeze-drying)시킨 다음, 분쇄하여 분말화하고,The saponin phosphine Rg1 was extracted by washing and drying the dried ginseng leaves at 80 ° C. in ethanol at 80 ° C. to produce a concentrate. The resulting concentrate was centrifuged to remove chlorophyll and pesticides, followed by freeze-drying and grinding. Powdered,

상기 복령발효산물은 복령발효현미를 40±5℃ 에서 열풍건조시킨 다음 60∼80mesh로 분쇄하고, 60∼80℃에서 80% 에탄올로 3∼5시간동안 진공감압법으로 추출하도록 되어 있다.
The fermented brown rice fermented product is dried by hot air drying at 40 ± 5 ° C., and then pulverized to 60 to 80 mesh, and extracted by vacuum vacuum at 60 to 80 ° C. for 3 to 5 hours with 80% ethanol.

이와 같이 본 발명은 인삼사포닌 Rg1 과 복령발효산물을 포함하도록 되어 있어, 피부에 혈관을 확장시켜 영양분을 충분히 공급하고, 항균 및 항산화 작용을 통하여 피부 트러블 방지와 노화방지효과를 구비하고 있다. As described above, the present invention includes ginseng saponin Rg1 and a fermented fermented product of Bokryeong, which expands blood vessels to the skin to sufficiently supply nutrients, and has anti-aging and anti-aging effects through antibacterial and antioxidant activities.

또한, 본 발명은 인삼사포닌 Rg1 의 추출시 농약성분과 엽록소를 한번에 제거하여 화장품 원료의 단가를 낮추고, 이익을 극대화하여 경제성을 향상시킬 수 있다. In addition, the present invention can remove the pesticide ingredient and chlorophyll at a time when extracting ginseng saponin Rg1 to lower the unit cost of the raw material of cosmetics, maximize the profit and improve the economics.

또한, 본 발명은 인삼사포닌 Rg1 의 최적추출에 의해 진세노사이드의 함량을 일정하게 유지하면서, 인삼잎 농축액보다 2∼3배 많은 함량의 원료를 생산할 수 있다. In addition, the present invention can produce a raw material having a content of 2-3 times more than the ginseng leaf concentrate while maintaining a constant ginsenoside content by the optimal extraction of ginseng saponin Rg1.

또한, 본 발명은 복령 발효를 통해 지용성 비타민 A, D, E 와, 천연 아미노산 등의 유효성분을 최대로 유지하도록 하여, 한방화장품의 기능성을 향상시킬 수 있는 등 많은 효과가 있다.
In addition, the present invention has a number of effects, such as to improve the functionality of herbal cosmetics by maintaining the maximum active ingredients such as fat-soluble vitamins A, D, E, and natural amino acids through the bokyeong fermentation.

본 발명은 천연한방화장품에 있어서, 상기 한방화장품은 복령발효산물(Poria Cocos Extract) 0.8∼1.5wt%, 인삼사포닌 Rg1(Panax Ginseng Root Extract) 0.3∼0.8wt% 를 유효성분으로 포함하되,The present invention in the natural herbal cosmetics, the herbal cosmetics, but the active ingredient (Poria Cocos Extract) 0.8 ~ 1.5wt%, ginseng saponin Rg1 (Panax Ginseng Root Extract) 0.3 ~ 0.8wt% as an active ingredient,

상기 인삼사포닌 Rg1 은 세척건조시킨 인삼잎을 70∼80% 에탄올에서 80℃ 추출농축하여 농축액을 생성하고, 상기 농축액을 원심분리하여 엽록소와 살충제를 제거한 후 동결건조(Freeze-drying)시켜 분쇄한 분말이고,The ginseng saponin Rg1 was extracted and concentrated by washing and drying the dried ginseng leaf at 80 ° C. in 70-80% ethanol, and centrifuging the concentrate to remove chlorophyll and insecticide, and then pulverized the powder by freeze-drying. ego,

상기 복령발효산물은 복령발효현미를 40±5℃ 에서 열풍건조시킨 다음 60∼80mesh로 분쇄하고, 60∼80℃에서 80% 에탄올로 3∼5시간동안 진공감압법으로 추출하도록 되어 있다.
The fermented brown rice fermented product is dried by hot air drying at 40 ± 5 ° C., and then pulverized to 60 to 80 mesh, and extracted by vacuum vacuum at 60 to 80 ° C. for 3 to 5 hours with 80% ethanol.

상기 인삼사포닌 Rg1 은 인삼잎을 세척 건조시키는 예비단계; 건조된 인삼잎을 70∼80% 에탄올에서 80℃ 추출하고 농축시켜 농축액을 생성하는 농축단계; 상기 농축액을 원심분리하여 엽록소와 살충제를 제거하는 제거단계; 상기 엽록소 및 살충제가 제거된 농축액을 동결건조(Freeze-drying)시키고 이를 분쇄하여 분말화하는 분말화단계를 통해 형성된다.
The ginseng saponin Rg1 is a preliminary step of washing and drying the ginseng leaves; Concentrating step of extracting the dried ginseng leaves in 70 ~ 80% ethanol and concentrated to 80 ℃ to produce a concentrate; Removing the chlorophyll and pesticide by centrifuging the concentrate; The concentrated solution from which the chlorophyll and pesticides are removed is formed through a powdering step of freeze-drying and pulverizing the powder.

상기 복령발효산물은 복령발효현미로부터 추출되는 것으로, 현미를 수침 및 세척하고, 멸균처리한 후 멸균처리된 현미를 상온으로 냉각하여 복령균사체를 접촉시킨 다음 복령균사체가 접종된 현미를 배양하여 복령발효현미를 생성하고, 이와 같이 생성된 복령발효현미를 40±5℃에서 열풍건조시킨 다음 60∼80mesh로 분쇄하며, 상기 분쇄된 복령발효현미를 60∼80℃에서 80% 에탄올로 3∼5시간동안 진공감압법으로 추출하여 복령발효산물을 생성한다. The fermented fermented product of Bokryeong fermented brown rice, soaked and washed with brown rice, sterilized, sterilized brown rice, cooled to room temperature, and then contacted with Baengryng mycelium, followed by culturing brown rice inoculated with Baeryeong mycelium. The brown rice is produced, and the produced Fuling fermented brown rice is hot-air dried at 40 ± 5 ° C. and then pulverized to 60 to 80 mesh, and the pulverized fermented brown rice to 80% ethanol at 60 to 80 ° C. for 3 to 5 hours. Extraction is carried out by vacuum decompression to produce a fermentation product.

이와 같이 형성된 복령발효산물은 고형분 함량 43∼50%를 구비한다. 즉, 진공감압법으로 추출한 80℃, 80%에탄올, 3시간 추출한 처리구의 고형분 추출함량은 약 49.1%였으며, 80℃, 80%에탄올, 5시간 추출한 처리구의 고형분 추출함량은 약 46.5%, 60℃, 80%에탄올, 5시간 추출한 처리구의 고형분 추출함량은 약 43.4% 이다.The fermented fermentation product thus formed has a solid content of 43-50%. That is, the solid content extraction of 80 ℃, 80% ethanol, 3 hours extraction treatment was 49.1%, the solid extraction content of 80 ℃, 80% ethanol, 5 hours extraction treatment was about 46.5%, 60 ℃ , 80% ethanol, the solids content of the extract was 53.4 hours was about 43.4%.

이때, 상기 에탄올은 복령발효현미 100 중량부에 대하여, 1000 중량부를 첨가하며, 1∼3회 진공감압법으로 추출하고, 추출하여 얻은 여과액을 24시간동안 4℃에서 정치, 40℃에서 감압농축(Rotary ebaporator N-1000, EYELA)한다.
At this time, the ethanol is added to 100 parts by weight of the Fuling fermented brown rice, 1000 parts by weight, extracted by vacuum pressure 1 to 3 times, the filtrate obtained by the extraction was left at 4 ℃ for 24 hours, concentrated under reduced pressure at 40 ℃ (Rotary ebaporator N-1000, EYELA).

상기 복령발효현미는 현미에 증류수를 가해 수침 및 세척하는 수침단계와, 상기 수침에 따라 수분이 함유된 현미를 일정온도로 가열하여 유해한 세균을 멸균하는 멸균단계와, 상기 멸균처리된 현미를 상온으로 냉각시키는 냉각단계와, 상기 현미에 복령균사체를 접종하는 접종단계와, 상기 복령균사체가 접종된 현미를 배양하는 배양단계를 통해 생성된다. The Boeryeong fermented brown rice is a soaking step of immersion and washing by adding distilled water to brown rice, and sterilization step of sterilizing harmful bacteria by heating the brown rice containing water according to the immersion to a certain temperature, and the sterilized brown rice at room temperature. Cooling step of cooling, the inoculation step of inoculating the baekrye mycelium on the brown rice, and the culture step of culturing the brown rice inoculated with the bokyeong mycelium is generated.

상기 수침단계는 현미의 이물질을 제거하고 수분을 함유하도록 하는 것으로, 현미에 대하여 약 1.3배의 증류수를 가하고, 15∼30분 동안 수침한다. The immersion step is to remove foreign matters of brown rice and to contain water, and about 1.3 times distilled water is added to brown rice and soaked for 15 to 30 minutes.

상기 멸균단계는 현미의 유해한 세균을 멸균하는 것으로, 약 110∼130℃에서 약 40∼60분동안 멸균처리하며, 바람직하게는 121℃에서 50분간 멸균한다. The sterilization step is to sterilize the harmful bacteria of brown rice, sterilization for about 40 to 60 minutes at about 110 ~ 130 ℃, preferably sterilization for 50 minutes at 121 ℃.

상기 접종단계는 상온으로 냉각처리된 현미에 복령 버섯에서 자체 분리한 균사체 중 가장 우수한 균주를 접종하는 것으로, 0.1%(v/w) 접종한다. 즉, 현미 100 g 에 대하여 균사체 0.1 ㎖ 가 되도록 접종한다.The inoculation step is to inoculate the best strain of the mycelium isolated from the Bokyeong mushroom in brown rice cooled to room temperature, inoculated 0.1% (v / w). That is, it inoculates to 100 ml of brown rice so that it may become 0.1 ml of mycelium.

상기 배양단계는 복령 균사체가 접촉된 현미를 배양하는 것으로, 20∼28℃, 상대습도 75∼85%에서 5∼9일간 배양하며, 바람직하게는 25℃, 상대습도 80%에서 7일간 배양한다.
The culturing step is to cultivate brown rice in contact with the Fukryeong mycelium, incubated for 5 to 9 days at 20 to 28 ℃, 75 to 85% relative humidity, preferably incubated for 7 days at 25 ℃, 80% relative humidity.

상기 한방화장품은 정제수 50∼65wt%, 부틸렌 글리콜(Butylene Glycol) 5∼10wt%, 하이드로지네이티드 폴리덴센(hydrogenated Polydecene) 3∼8wt%, 메도폼 시드 오일(Limnanenthes Alba Seed Oil) 2∼5wt%, 세틸알콜(Cetyl Alcohol) 2∼4wt%, 싸이클로메치콘(Cycolmethicone) 1.5∼3wt%, 카프릴릭/카프릭 트리글리세라이드(Caprylic/Capric Triglyceride) 1.5∼3wt%, 미소납(Microcrystalline Wax) 1.5∼3wt%, 광유(Mineral Oil) 1∼3wt%, 폴리글리세릴-3-메틸(Polyglyceryl-3-Methylglucose Distearate) 0.5∼2.5wt%, 이소프로필 미리스트산(Isopropyl Myristate) 0.5∼2.5wt%, 밀랍(Bees Wax)) 0.5∼2.5wt%, 부틸린 글라이콜 디카프릴레이트/디카프레이트(Butylene Glycol Dicaprylate/Dicaprate) 0.5∼1.5wt%, 차조기잎추출물(Perilla Frutescens Leaf Extract) 0.2∼0.4wt%, 은행잎추출물(Ginko Biloba Leaf Extract) 0.2∼0.4wt%, 멀베리추출물(Morus alba Root Extract) 0.2∼0.4wt%, 질경추출물(Platycodon Grandiflorum Root Extract) 0.2∼0.4wt%, 자목련눈추출물(Magnolia Liliflora bud Extract) 0.2∼0.4wt%, 천궁추출물(Cnidium Officinale Root Extract) 0.2∼0.4wt%, 디메칠콘(Dimethicone) 0.3∼0.8wt%, 아데노신(Adenosine) 0.03∼0.05wt%, 메칠파라벤(Methylparaben) 0.1∼0.3wt%, 페녹시에탄올(Phenoxyethanol) 0.05∼0.15wt%, 프로필파라벤(Propylparaben) 0.03∼0.08wt%, 트리에탄올아민(Triethanolamine) 0.15∼0.35wt%, 알란토인(Allantoin) 0.05∼0.15wt%, 칼보머(Carbomer) 0.05∼0.15wt%, 디소디움 EDTA(Disodium EDTA) 0.01∼0.03wt%, 잔탄검(Xanthan Gum) 0.2∼0.6wt%, 프래그런스(Fragrance) 0.05∼0.15wt% 를 포함하도록 되어 있다.
The herbal cosmetics are 50-65wt% purified water, 5-10wt% butylene glycol, 3-8wt% hydrogenated polydecene, 2-5wt% meadowfoam seed oil (Limnanenthes Alba Seed Oil) , Cetyl Alcohol 2 ~ 4wt%, Cyclomethicone 1.5 ~ 3wt%, Caprylic / Capric Triglyceride 1.5 ~ 3wt%, Microcrystalline Wax 1.5 ~ 3wt%, Mineral Oil 1-3wt%, Polyglyceryl-3-Methylglucose Distearate 0.5 ~ 2.5wt%, Isopropyl Myristate 0.5 ~ 2.5wt%, Beeswax (Bees Wax)) 0.5-2.5wt%, Butylene Glycol Dicaprylate / Dicaprate 0.5-1.5wt%, Perilla Frutescens Leaf Extract 0.2-0.4wt%, Ginko Biloba Leaf Extract 0.2 ~ 0.4wt%, Mulberry alba Root Extract 0.2 ~ 0.4wt%, Platycodon G randiflorum Root Extract) 0.2-0.4wt%, Magnolia Liliflora bud Extract 0.2-0.4wt%, Cnidium Officinale Root Extract 0.2-0.4wt%, Dimethicone 0.3-0.8wt% , Adenosine 0.03-0.05 wt%, Methylparaben 0.1-0.3 wt%, Phenoxyethanol 0.05-0.15 wt%, Propparaparaben 0.03-0.08 wt%, Triethanolamine 0.15 ~ 0.35wt%, Allantoin 0.05 ~ 0.15wt%, Carbomer 0.05 ~ 0.15wt%, Disodium EDTA 0.01 ~ 0.03wt%, Xanthan Gum 0.2 ~ 0.6wt % And 0.05 to 0.15 wt% of Fragrance.

이하 본 발명을 실시예에 의해 상세히 설명하면 다음과 같다. Hereinafter, the present invention will be described in detail by way of examples.

실시예 1Example 1

복령발효 전의 현미와, 복령발효현미의 성분을 분석하였으며, 그 결과는 [표1] 내지 [표4]와 같다. The contents of brown rice before the fermentation of Bokryeong and fermented brown rice were analyzed, and the results are shown in [Table 1] to [Table 4].

이때, 상기 복령발효현미는 현미에 대하여 1.3배의 증류수를 가하여 30분 동안 수침하고, 121℃에서 50분간 멸균처리하여 상온으로 냉각시키며, 상온 냉각처리된 현미 100 g 에 대하여 균사체 0.1 ㎖ 가 되도록 접종한 후, 이를 25℃, 상대습도 80%에서 7일간 배양하여 생성하였다. At this time, the fermented brown rice of Bokryeong fermented brown rice is 1.3 times distilled water, soaked for 30 minutes, sterilized at 121 ℃ for 50 minutes to cool to room temperature, inoculated so that the mycelium 0.1 ㎖ against 100 g of brown rice at room temperature cooling treatment Then, it was produced by incubating for 7 days at 25 ℃, 80% relative humidity.

[표1]Table 1

Figure pat00001

Figure pat00001

[표2][Table 2]

Figure pat00002
Figure pat00002

[표3][Table 3]

Figure pat00003

Figure pat00003

[표4]Table 4

Figure pat00004

Figure pat00004

상기 [표1]은 일반성분, [표2]는 무기질, [표3]은 비타민함량, [표4]는 아미노산함량을 측정한 것으로, 복령발효현미의 무기질, 비타민, 아미노산의 함량이 우수함을 알 수 있다.
[Table 1] is a general ingredient, [Table 2] is the mineral, [Table 3] is the vitamin content, [Table 4] is the amino acid content is measured, the contents of minerals, vitamins, amino acids of fermented brown rice is excellent Able to know.

실시예 2Example 2

인삼잎을 80% 에탄올에서 80℃ 추출하고, 추출액을 62brix 농축한 후, 상기 농축액을 원심분리하여 엽록소와 살충제를 제거한 다음, 이를 동결건조(Freeze-drying) 및 분쇄하여 인삼잎 파우더를 형성하였다. The ginseng leaves were extracted at 80 ° C. in 80% ethanol, the extract was concentrated to 62brix, and then the concentrate was centrifuged to remove chlorophyll and pesticides, which were then freeze-dried and ground to form ginseng leaf powder.

상기와 같이 형성된 인삼잎 파우더와 인삼뿌리 및 인삼잎에 대한 인삼사포닌 Rg1 의 함유량을 측정하였으며, 그 결과는 [표5]와 같다. The content of ginseng saponin Rg1 for the ginseng leaf powder, ginseng root and ginseng leaf formed as described above was measured, and the results are shown in [Table 5].

[표5][Table 5]

Figure pat00005

Figure pat00005

본 발명은 상술한 특정의 바람직한 실시예에 한정되지 아니하며, 청구범위에서 청구하는 본 발명의 요지를 벗어남이 없이 당해 발명이 속하는 기술분야에서 통상의 지식을 가진 자라면 누구든지 다양한 변형실시가 가능한 것은 물론이고, 그와 같은 변경은 청구범위 기재의 범위내에 있게 된다.The present invention is not limited to the above-described specific preferred embodiments, and various modifications can be made by any person having ordinary skill in the art without departing from the gist of the present invention claimed in the claims. Of course, such changes will fall within the scope of the claims.

Claims (4)

천연한방화장품에 있어서,
상기 한방화장품은 복령발효산물(Poria Cocos Extract) 0.8∼1.5wt%, 인삼사포닌 Rg1(Panax Ginseng Root Extract) 0.3∼0.8wt% 를 유효성분으로 포함하되,
상기 인삼사포닌 Rg1 은 세척건조시킨 인삼잎을 70∼80% 에탄올에서 80℃ 추출농축하여 농축액을 생성하고, 상기 농축액을 원심분리하여 엽록소와 살충제를 제거한 후 동결건조(Freeze-drying)시켜 분쇄한 분말이고,
상기 복령발효산물은 복령발효현미를 40±5℃ 에서 열풍건조시킨 다음 60∼80mesh로 분쇄하고, 60∼80℃에서 80% 에탄올로 3∼5시간동안 진공감압법으로 추출한 것을 특징으로 하는 인삼사포닌Rg1과 복령발효산물을 이용한 천연 한방화장품.
In natural herbal cosmetics,
The herbal cosmetics include 0.8 ~ 1.5wt% Poria Cocos Extract (Poria Cocos Extract), 0.3 ~ 0.8wt% ginseng saponin Rg1 (Panax Ginseng Root Extract) as an active ingredient,
The ginseng saponin Rg1 was extracted and concentrated by washing and drying the dried ginseng leaf at 80 ° C. in 70-80% ethanol, and centrifuging the concentrate to remove chlorophyll and insecticide, and then pulverized the powder by freeze-drying. ego,
The fermented saengin product of Bokryeong fermented brown rice is dried in hot air at 40 ± 5 ℃ and then pulverized to 60 to 80 mesh, extracted with vacuum reduced pressure for 3 to 5 hours with 80% ethanol at 60 to 80 ℃ Natural herbal cosmetics using Rg1 and Bokryeong fermented products.
청구항 1 에 있어서;
상기 복령발효현미는 현미에 증류수를 가해 수침 및 세척하는 수침단계와, 상기 수침에 따라 수분이 함유된 현미를 일정온도로 가열하여 유해한 세균을 멸균하는 멸균단계와, 상기 멸균처리된 현미를 상온으로 냉각시키는 냉각단계와, 상기 현미에 복령균사체를 접종하는 접종단계와, 상기 복령균사체가 접종된 현미를 배양하는 배양단계를 통해 생성되는 것을 특징으로 하는 인삼사포닌Rg1과 복령발효산물을 이용한 천연 한방화장품.
The method of claim 1,
The Boeryeong fermented brown rice is a soaking step of immersion and washing by adding distilled water to brown rice, and sterilization step of sterilizing harmful bacteria by heating the brown rice containing water according to the immersion to a certain temperature, and the sterilized brown rice at room temperature. Natural herbal cosmetics using ginseng saponin Rg1 and Fukryeong fermented products, characterized in that the cooling step, the inoculation step of inoculating the brown rice inoculated on the brown rice, and the culture step of culturing the brown rice inoculated with the bokryeong mycelium .
청구항 2 에 있어서;
상기 수침단계는 현미에 대하여 1.3배의 증류수를 가하고, 15∼30분 동안 수침하고,
상기 멸균단계는 110∼130℃에서 40∼60분동안 멸균처리하며,
상기 접종단계는 상온으로 냉각처리된 현미에 복령 버섯에서 자체 분리한 균사체를 0.1%(v/w) 접종하고,
상기 배양단계는 20∼28℃, 상대습도 75∼85%에서 5∼9일간 배양하는 것을 특징으로 하는 인삼사포닌Rg1과 복령발효산물을 이용한 천연 한방화장품.
The method according to claim 2;
In the immersion step, 1.3 times distilled water is added to brown rice, and immersed for 15 to 30 minutes,
The sterilization step is sterilized for 40 to 60 minutes at 110 ~ 130 ℃,
The inoculation step is inoculated 0.1% (v / w) of the mycelium isolated from the bokyeong mushroom in brown rice cooled to room temperature,
The culturing step is a natural herbal cosmetics using ginseng saponin Rg1 and Bokryeong fermented products, characterized in that culture for 5 to 9 days at 20 ~ 28 ℃, 75-85% relative humidity.
청구항 1 내지 3 항 중 어느 한 항에 있어서;
상기 한방화장품은 정제수 50∼65wt%, 부틸렌 글리콜(Butylene Glycol) 5∼10wt%, 하이드로지네이티드 폴리덴센(hydrogenated Polydecene) 3∼8wt%, 메도폼 시드 오일(Limnanenthes Alba Seed Oil) 2∼5wt%, 세틸알콜(Cetyl Alcohol) 2∼4wt%, 싸이클로메치콘(Cycolmethicone) 1.5∼3wt%, 카프릴릭/카프릭 트리글리세라이드(Caprylic/Capric Triglyceride) 1.5∼3wt%, 미소납(Microcrystalline Wax) 1.5∼3wt%, 광유(Mineral Oil) 1∼3wt%, 폴리글리세릴-3-메틸(Polyglyceryl-3-Methylglucose Distearate) 0.5∼2.5wt%, 이소프로필 미리스트산(Isopropyl Myristate) 0.5∼2.5wt%, 밀랍(Bees Wax)) 0.5∼2.5wt%, 부틸린 글라이콜 디카프릴레이트/디카프레이트(Butylene Glycol Dicaprylate/Dicaprate) 0.5∼1.5wt%, 차조기잎추출물(Perilla Frutescens Leaf Extract) 0.2∼0.4wt%, 은행잎추출물(Ginko Biloba Leaf Extract) 0.2∼0.4wt%, 멀베리추출물(Morus alba Root Extract) 0.2∼0.4wt%, 질경추출물(Platycodon Grandiflorum Root Extract) 0.2∼0.4wt%, 자목련눈추출물(Magnolia Liliflora bud Extract) 0.2∼0.4wt%, 천궁추출물(Cnidium Officinale Root Extract) 0.2∼0.4wt%, 디메칠콘(Dimethicone) 0.3∼0.8wt%, 아데노신(Adenosine) 0.03∼0.05wt%, 메칠파라벤(Methylparaben) 0.1∼0.3wt%, 페녹시에탄올(Phenoxyethanol) 0.05∼0.15wt%, 프로필파라벤(Propylparaben) 0.03∼0.08wt%, 트리에탄올아민(Triethanolamine) 0.15∼0.35wt%, 알란토인(Allantoin) 0.05∼0.15wt%, 칼보머(Carbomer) 0.05∼0.15wt%, 디소디움 EDTA(Disodium EDTA) 0.01∼0.03wt%, 잔탄검(Xanthan Gum) 0.2∼0.6wt%, 프래그런스(Fragrance) 0.05∼0.15wt% 를 포함하는 것을 특징으로 하는 인삼사포닌Rg1과 복령발효산물을 이용한 천연 한방화장품.
The method of claim 1;
The herbal cosmetics are 50-65wt% purified water, 5-10wt% butylene glycol, 3-8wt% hydrogenated polydecene, 2-5wt% meadowfoam seed oil (Limnanenthes Alba Seed Oil) , Cetyl Alcohol 2 ~ 4wt%, Cyclomethicone 1.5 ~ 3wt%, Caprylic / Capric Triglyceride 1.5 ~ 3wt%, Microcrystalline Wax 1.5 ~ 3wt%, Mineral Oil 1-3wt%, Polyglyceryl-3-Methylglucose Distearate 0.5 ~ 2.5wt%, Isopropyl Myristate 0.5 ~ 2.5wt%, Beeswax (Bees Wax)) 0.5-2.5wt%, Butylene Glycol Dicaprylate / Dicaprate 0.5-1.5wt%, Perilla Frutescens Leaf Extract 0.2-0.4wt%, Ginko Biloba Leaf Extract 0.2 ~ 0.4wt%, Mulberry alba Root Extract 0.2 ~ 0.4wt%, Platycodon G randiflorum Root Extract) 0.2-0.4wt%, Magnolia Liliflora bud Extract 0.2-0.4wt%, Cnidium Officinale Root Extract 0.2-0.4wt%, Dimethicone 0.3-0.8wt% , Adenosine 0.03-0.05 wt%, Methylparaben 0.1-0.3 wt%, Phenoxyethanol 0.05-0.15 wt%, Propparaparaben 0.03-0.08 wt%, Triethanolamine 0.15 ~ 0.35wt%, Allantoin 0.05 ~ 0.15wt%, Carbomer 0.05 ~ 0.15wt%, Disodium EDTA 0.01 ~ 0.03wt%, Xanthan Gum 0.2 ~ 0.6wt %, Fragrance (Fragrance) Natural herbal cosmetics using ginseng saponin Rg1 and Bokryeong fermented products comprising 0.05 to 0.15 wt%.
KR1020100012307A 2010-02-10 2010-02-10 The Composite make natural korean herb cosmetics from genseng saponin Rg1 and polia coccos ferment KR101238825B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
KR1020100012307A KR101238825B1 (en) 2010-02-10 2010-02-10 The Composite make natural korean herb cosmetics from genseng saponin Rg1 and polia coccos ferment

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
KR1020100012307A KR101238825B1 (en) 2010-02-10 2010-02-10 The Composite make natural korean herb cosmetics from genseng saponin Rg1 and polia coccos ferment

Publications (2)

Publication Number Publication Date
KR20110092721A true KR20110092721A (en) 2011-08-18
KR101238825B1 KR101238825B1 (en) 2013-03-04

Family

ID=44929525

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020100012307A KR101238825B1 (en) 2010-02-10 2010-02-10 The Composite make natural korean herb cosmetics from genseng saponin Rg1 and polia coccos ferment

Country Status (1)

Country Link
KR (1) KR101238825B1 (en)

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102657688A (en) * 2012-06-06 2012-09-12 吴伟銮 Traditional Chinese medicine composition capable of preventing cardiovascular and cerebrovascular diseases and application thereof
CN104154718A (en) * 2014-08-25 2014-11-19 济南康众医药科技开发有限公司 Drying method of cortex magnoliae officinalis
CN104180611A (en) * 2014-08-25 2014-12-03 济南康众医药科技开发有限公司 Application of freeze-drying technology in mangnolia officinalis
CN104197646A (en) * 2014-08-25 2014-12-10 济南康众医药科技开发有限公司 Drying method of magnolia officinalis and application of magnolia officinalis product
CN104434747A (en) * 2014-10-13 2015-03-25 金日制药(中国)有限公司 Face cream with anti-aging function and preparation method of face cream
CN104593178A (en) * 2014-11-19 2015-05-06 吉林农业大学 Multifunctional handmade soap containing rare ginseng saponins
KR20150104397A (en) * 2014-03-05 2015-09-15 배용태 Method for isolating and removing chlorophyll from natural material
KR20180038638A (en) 2016-10-07 2018-04-17 (주)스와니코코 Cosmetic herbal essence composition having excellent of antioxidant effect and skin improvement and a method for preparing it
KR102566925B1 (en) * 2022-09-20 2023-08-14 주식회사 단정바이오 A cosmetic composition comprising active ingredients of Magnolia Sieboldii, Magnolia Liliflora Flower, Cnidium Officinale Root, Benincasa Cerifera Seed, Prunus Persica (Peach) Kernel, and Poria Cocos

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101684433B1 (en) 2015-12-22 2016-12-08 주식회사 송이산업 Method of manufacturing a tablet cosmetic composition with corals and clusters
KR102176938B1 (en) 2020-08-20 2020-11-10 (주)브이에스신비 Cosmetic Composition Comprising Fermented Liquor of Natural Plant and Preparation Methods Thereof
KR102174660B1 (en) 2020-08-20 2020-11-05 (주)브이에스신비 Cosmetic Composition Comprising Fermented Liquor and Powder of Natural Plant and Preparation Methods Thereof
KR102303400B1 (en) 2021-04-06 2021-09-24 (주)브이에스신비 Preparation Methods of Fermentation Products Using JEJU Lava Seawater, JEJU Barley Yeast and Natural Plant and Cosmetic Compositions Having Thereof

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA2652308A1 (en) * 2006-05-17 2007-11-22 Bayer Consumer Care Ag Use of ginsenosides and extracts containing them
KR100962587B1 (en) * 2007-10-02 2010-06-11 동국대학교 산학협력단 A method for fermentation of natural plants and herbal medicines, a fermented product prepared therefrom and a paharmaceutical composition, a cosmetic compositon and a food composition comprising the product
KR20090128808A (en) * 2008-06-11 2009-12-16 최향자 The wrinkle improvement chinese medicine cosmetics which uses the ginseng saponin rg1 and the pack which uses this

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102657688A (en) * 2012-06-06 2012-09-12 吴伟銮 Traditional Chinese medicine composition capable of preventing cardiovascular and cerebrovascular diseases and application thereof
KR20150104397A (en) * 2014-03-05 2015-09-15 배용태 Method for isolating and removing chlorophyll from natural material
CN104154718A (en) * 2014-08-25 2014-11-19 济南康众医药科技开发有限公司 Drying method of cortex magnoliae officinalis
CN104180611A (en) * 2014-08-25 2014-12-03 济南康众医药科技开发有限公司 Application of freeze-drying technology in mangnolia officinalis
CN104197646A (en) * 2014-08-25 2014-12-10 济南康众医药科技开发有限公司 Drying method of magnolia officinalis and application of magnolia officinalis product
CN104434747A (en) * 2014-10-13 2015-03-25 金日制药(中国)有限公司 Face cream with anti-aging function and preparation method of face cream
CN104593178A (en) * 2014-11-19 2015-05-06 吉林农业大学 Multifunctional handmade soap containing rare ginseng saponins
KR20180038638A (en) 2016-10-07 2018-04-17 (주)스와니코코 Cosmetic herbal essence composition having excellent of antioxidant effect and skin improvement and a method for preparing it
KR102566925B1 (en) * 2022-09-20 2023-08-14 주식회사 단정바이오 A cosmetic composition comprising active ingredients of Magnolia Sieboldii, Magnolia Liliflora Flower, Cnidium Officinale Root, Benincasa Cerifera Seed, Prunus Persica (Peach) Kernel, and Poria Cocos

Also Published As

Publication number Publication date
KR101238825B1 (en) 2013-03-04

Similar Documents

Publication Publication Date Title
KR101238825B1 (en) The Composite make natural korean herb cosmetics from genseng saponin Rg1 and polia coccos ferment
KR101451981B1 (en) Compositions comprising fermentative extract of Orchidaceae for improving functions of skin
CN106667837A (en) Camellia oleifera component based body lotion and preparation method thereof
KR101321854B1 (en) Cosmetic composition containing fucus vesiculosus extract and prunella vulgaris extract for improving skin wrinkle and elasticity
KR101482873B1 (en) Fermentation metabolite of Dendropanax morbiferus produced by liquid-state fermentation and manufacturaring process for the same
KR101884660B1 (en) Cosmetic composition containing the enzymatic extracts of natural substances comprising propolis, royal jelly and honey
CN104306323A (en) Cordyceps-militaris-ingredient contained eye cream and preparing method of cordyceps-militaris-ingredient contained eye cream
CN108042436B (en) Anti-aging and moisturizing blue copper peptide essence cream
CN104434760A (en) Facial cream containing ingredient of cordyceps militaris and preparation method thereof
KR101582974B1 (en) Composition for improving skin condition containing the complex extracts of Hydrolyzed Manihot Esculenta Tuber and Chrysanthemum Parthenium
KR101167295B1 (en) A cosmetic composition for skin-antiaging effect comprising of oriental medical herbs' extracts fermened and method for preparing the same
KR102004366B1 (en) A cosmetic composition comprising centipeda minima extract
KR101769755B1 (en) A leuconostoc mesenteroides gfc 160704, cosmetic composition including the leuconostoc mesenteroides gfc 160704 or its culture fluid, and manufacturing method of the cosmetic composition
KR101794006B1 (en) Anti inflammatory comprising plant extract
KR102071218B1 (en) Anti-aging and anti-wrinkle of skin improving cosmetic composition comprising extracts of Moschus, Angelica gigas Nakai, Cornus officinalis, Cervi Parvum Cornu and Phellinus linteus, Ganoderma Lucidum, Inonotus obliquus, Grifola Frondosa, Sparassis crispa
KR20210026036A (en) Cosmetic Composition For Improving Skin Photoaging Comprising the Abeliophyllum Extract Fermented by Lactobacteria, And Manufacturing Method Thereof
CN110538123A (en) Preparation process and application of traditional Chinese medicine compound extract for whitening skin and removing freckles
KR101761771B1 (en) Method for fermenting Broussonetia plant or the extract thereof, the fermented extracts thereby and the cosmetic composition containing the same
CN104352422A (en) Eye cream containing cordyceps militaris component and preparation method of eye cream
CN113631227B (en) Anti-aging agent, antioxidant, anti-inflammatory agent, whitening agent, and cosmetic
KR20120096410A (en) A cosmetic composition for skin-antiaging effect comprising of oriental medical herbs' extracts fermened and method for preparing the same
CN113413336A (en) Whitening composition added with matsutake fermentation extract as well as preparation method and application of whitening composition
KR20210015491A (en) A cosmetic composition comprising papaw extract and stem cell such as rock samphire callus culture extract
CN104382836A (en) Stoste containing cordyceps militaris and preparation method of stoste
CN110693791A (en) Preparation of pure dew yeast essence toner (toning lotion)

Legal Events

Date Code Title Description
A201 Request for examination
E902 Notification of reason for refusal
E701 Decision to grant or registration of patent right
GRNT Written decision to grant
FPAY Annual fee payment

Payment date: 20160202

Year of fee payment: 4

FPAY Annual fee payment

Payment date: 20170223

Year of fee payment: 5

FPAY Annual fee payment

Payment date: 20180125

Year of fee payment: 6

FPAY Annual fee payment

Payment date: 20190808

Year of fee payment: 7

FPAY Annual fee payment

Payment date: 20200106

Year of fee payment: 8