CN109700716A - A kind of application of paper mulberry, fresh fruit extraction process of active component and extract - Google Patents

A kind of application of paper mulberry, fresh fruit extraction process of active component and extract Download PDF

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Publication number
CN109700716A
CN109700716A CN201910075997.XA CN201910075997A CN109700716A CN 109700716 A CN109700716 A CN 109700716A CN 201910075997 A CN201910075997 A CN 201910075997A CN 109700716 A CN109700716 A CN 109700716A
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China
Prior art keywords
paper mulberry
fresh fruit
extract
parts
active component
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Pending
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CN201910075997.XA
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Chinese (zh)
Inventor
田洋
周露
盛军
宋爽
陶亮
彭磊
解静
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Yunnan Agricultural University
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Yunnan Agricultural University
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Priority to CN201910075997.XA priority Critical patent/CN109700716A/en
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  • Medicines Containing Plant Substances (AREA)

Abstract

The present invention discloses the application of a kind of paper mulberry, fresh fruit extraction process of active component and extract, is related to plant extracts, technical field of phytochemistry.Paper mulberry of the invention, fresh fruit extraction process of active component; active constituent water is specifically included to mention and active constituent alcohol extracting; pass through the active constituent in water extraction method and alcohol extracting method extraction paper mulberry, fresh fruit; new approaches are provided with the active component extract preparation paper mulberry of acquisition, fresh fruit active component extract facial mask and everyday skincare, the development and utilization for paper mulberry, fresh fruit.

Description

A kind of application of paper mulberry, fresh fruit extraction process of active component and extract
Technical field
The present invention relates to plant extracts, technical field of phytochemistry, be specifically related to a kind of paper mulberry, fresh fruit activity at Divide the application of extracting method and extract.
Background technique
Paper mulberry (Paper mulberry) is Moraceae (Moraceae) paper mulberry category deciduous tree.Also known as paddy slurry tree, ancient name paper mulberry. Bark is paper making raw material.Important Arts for the People's Welfare are loaded with plantation and the papermaking process of paper mulberry.Sui Dynasty has mass production.Set it is 6~16 meters high, There is milk.Bark is smoothly in dark gray, and branch is sturdy and open and flat.Leaf alternate, there is a long handle, and blade is wealthy oval or irregular 3~5 deep It splits, there is rough sawn tooth at edge, and surface is dark green, and by coarse wool, the back side is grayish green, dense pubescence.Unisexual flower, dioecism, male flower Wei rou sprout Inflorescence is born in shoot axil;Female flower is capitulum.Collective fruits meat, it is spherical, there is long handle, it is red when ripe.Paper mulberry has speed It is raw, adaptable, distribution is wide, easily breeding, the feature that heat is high, the period of felling in turn is short.Its root system is shallow, and lateral root distribution is very wide, and growth is fast, Rudiment power and tillering ability are strong, resistance to trimming.Resistance tocrocking is strong.Paper mulberry is a kind of small investment, the period is short, quick, be benefited long spy Kind economic forest has ecology well, and social and economic benefit, paper mulberry adaptability, resistance are strong, at aspect of improving the ecological environment With very big advantage;The tall and big grace of tree performance is outstanding Landscape Trees;Leaf, fruit, root, milk have very high medicine With value, medicinal raw material can be used as;Fruit and leaf nutritive value are high, can develop new beverage and feed;Bark and limb It is the source of China's top grade paper, the huge market demand, therefore, reinforcement had both protected paper mulberry to provide the development and utilization of Broussonetia papyrifera Source.
Currently, being concentrated mainly in the prior art for the development and utilization of paper mulberry: replacing grain using feed with paper-mulberry leaf as feed Food crop stock raising;Bark and limb are developed as high-grade paper making raw material;Broussonetia papyrifera seed is as medicinal material;Do not have also in the prior art Have and active constituent in paper mulberry, fresh fruit is applied in daily chemical products, there is presently no extracted with paper mulberry, fresh fruit active constituent The skincare product of object exploitation, limits the development and utilization of paper mulberry.
Summary of the invention
In view of the above-mentioned problems existing in the prior art, the present invention provides a kind of paper mulberries, fresh fruit active constituent extraction side The application of method and extract obtains extract by the extraction to paper mulberry, fresh fruit active constituent, and extract is applied to face Film surface frost and everyday skincare, the development and utilization for paper mulberry, fresh fruit provide new approaches.
To realize above-mentioned technical purpose and the technique effect, the present invention is achieved through the following technical solutions:
A kind of paper mulberry, fresh fruit extraction process of active component, including active constituent water mention and active constituent alcohol extracting, Zhi Houyong Petroleum ether removes impurity, with active carbon decoloring;
The extracting method that the paper mulberry, fresh fruit active constituent water mention, comprising the following steps: paper mulberry fresh fruit is shredded, It is soaked in water leaf 1-2 hours after 30-50 DEG C of heating.It extracts supernatant and is concentrated;Being concentrated to get water layer can by petroleum ether extraction Dissolubility pigment and ester soluble components;Retain water layer and pass through active carbon decoloring, freeze-drying obtains water-soluble active ingredient and extraction Object;
The paper mulberry, fresh fruit active constituent alcohol extracting extracting method, comprising the following steps:
Step 1: paper mulberry, fresh fruit flower chopping to be used at 50-60 DEG C of bath temperature and extract 2-3 with 70%-75% ethyl alcohol It is secondary, 2 hours every time, merges the ethanol solution of extraction and recycle ethyl alcohol acquisition paper mulberry ethyl alcohol primary extract;
Step 2: being dissolved in water to paper mulberry, fresh fruit flower ethyl alcohol primary extract, with petroleum ether extraction, degreasing soluble components, color Element, water layer decolourize and are spray-dried;
Step 3: contact plate detection paper mulberry, fresh fruit spend active constituent and obtain paper mulberry active component extract.
Another object of the present invention is to provide a kind of paper mulberry, fresh fruit active component extracts to prepare in daily chemical products In application.
Another object of the present invention is to provide a kind of paper mulberry, fresh fruit active component extracts in face cream, lotion, face Application in film preparation.
Another object of the present invention is to provide a kind of paper mulberries, fresh fruit flower active component extract benefit facial mask, including with Lower raw material: 1-5 parts of paper mulberry flowers and fruits extract, 30-50 parts of water, 3-5 parts of glycerol, 2-5 parts of butanediol, beta glucan 2-3 Part, 2-3 parts of tremella (Tremella fuciformis) polysaccharide, 2-3 parts of pomegranate (Punica granatum) pericarp extract, sea Algae sugar 3 parts, 1-2 parts of Argireline, glycol 1-2 parts pungent, ceramide × 1-2 parts, Radix Notoginseng (Panax notoginseng) 2-3 parts of extract, 1 part of decoyl hydroximic acid, 1 part of 1,2- hexylene glycol, 1 part of 1,3-PD, 1 part of Phenoxyethanol, ethylhexyl are sweet It is 1 part of oil, 1 part of carbomer, 0.5-1 part of sodium hydroxide, 1 part of dipotassium glycyrrhizinate, 1 part of collagen, 1 part of sorbierite, 1 part of xanthan gum, saturating Bright 1 part of matter acid sodium.
Further, the paper mulberry, fresh fruit spend Broussonetia extract (Paper in active component extract facial mask Mulberry) addition mentions as 1-5%.
Beneficial effects of the present invention: the application of paper mulberry, fresh fruit extraction process of active component and extract of the present invention passes through Active constituent in water extraction method and alcohol extracting method extraction paper mulberry, fresh fruit, can obtain the active matter of higher degree;It is flavones, more Saccharide compound.Extraction process is also relatively simple, and extracting cycle is obviously shortened, can be with industrialized production;Simultaneously by the activity of acquisition Component extract prepares paper mulberry, fresh fruit active component extract MASQUE APAISANT HYDRATANT and everyday skincare, can improve skin and decline Old situation also has better inhibition effect to scytitis;Development and utilization for paper mulberry, fresh fruit provide new approaches.
Certainly, it implements any of the products of the present invention and does not necessarily require achieving all the advantages described above at the same time.
Detailed description of the invention
In order to illustrate the technical solution of the embodiments of the present invention more clearly, will be described below to embodiment required Attached drawing is briefly described, it should be apparent that, drawings in the following description are only some embodiments of the invention, for ability For the those of ordinary skill of domain, without creative efforts, it can also be obtained according to these attached drawings other attached Figure.
Fig. 1 is the process flow chart of paper mulberry described in the embodiment of the present invention, fresh fruit active constituent alcohol extracting;
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts all other Embodiment shall fall within the protection scope of the present invention.
Embodiment 1
A kind of paper mulberry, fresh fruit extraction process of active component, including active constituent water mention and active constituent alcohol extracting, Zhi Houyong Petroleum ether removes impurity, with active carbon decoloring;
The extracting method that the paper mulberry, fresh fruit active constituent water mention, comprising the following steps: paper mulberry fresh fruit is shredded, It is soaked in water leaf 1-2 hours after 30-50 DEG C of heating.It extracts supernatant and is concentrated;Being concentrated to get water layer can by petroleum ether extraction Dissolubility pigment and ester soluble components;Retain water layer and pass through active carbon decoloring, freeze-drying obtains water-soluble active ingredient and extraction Object;
The paper mulberry, fresh fruit active constituent alcohol extracting extracting method, comprising the following steps:
Step 1: paper mulberry, fresh fruit flower chopping to be used at 50-60 DEG C of bath temperature and extract 2-3 with 70%-75% ethyl alcohol It is secondary, 2 hours every time, merges the ethanol solution of extraction and recycle ethyl alcohol acquisition paper mulberry ethyl alcohol primary extract;
Step 2: being dissolved in water to paper mulberry, fresh fruit flower ethyl alcohol primary extract, with petroleum ether extraction, degreasing soluble components, color Element, water layer decolourize and are spray-dried;
Step 3: contact plate detection paper mulberry, fresh fruit spend active constituent and obtain paper mulberry active component extract.
By the active constituent in water extraction method and alcohol extracting method extraction paper mulberry, fresh fruit, the work of higher degree can be obtained Property object;Flavones, polysaccharide compound.Extraction process is also relatively simple, and extracting cycle is obviously shortened, can be with industrialized production.
Embodiment 2
A kind of application of paper mulberry, fresh fruit active component extract in facial mask preparation.
A kind of paper mulberry, fresh fruit flower active component extract mend facial mask, including following raw material: paper mulberry flowers and fruits extract 1-5 parts of object, 30-50 parts of water, 3-5 parts of glycerol, 2-5 parts of butanediol, 2-3 parts of beta glucan, tremella (Tremella Fuciformis) polysaccharide 2-3 parts, 2-3 parts of pomegranate (Punica granatum) pericarp extract, 3 parts of trehalose, acetyl group six - 81-2 parts of peptide, glycol 1-2 parts pungent, ceramide × 1-2 parts, 2-3 parts of Radix Notoginseng (Panax notoginseng) extract, decoyl 1 part of hydroximic acid, 1 part of 1,2- hexylene glycol, 1 part of 1,3-PD, 1 part of Phenoxyethanol, 1 part of Sensiva SC50,1 part of carbomer, 0.5-1 parts of sodium hydroxide, 1 part of dipotassium glycyrrhizinate, 1 part of collagen, 1 part of sorbierite, 1 part of xanthan gum, 1 part of Sodium Hyaluronate.
Further, the paper mulberry, fresh fruit spend Broussonetia extract (Paper in active component extract facial mask Mulberry) addition mentions as 1-5%.
The active component extract obtained in above-described embodiment 1 is subject to auxiliary material preparation paper mulberry, fresh fruit active constituent mentions Object moisturizing cream is taken, skin aging situation can be improved, also has better inhibition effect to scytitis.
Embodiment 3
A kind of paper mulberry, fresh fruit active component extract answering in face cream, lotion, facial mask preparation and daily chemical products preparation With.
In face cream, lotion, facial mask preparation process, addition is mentioned with the paper mulberry of 1%-5% parts by weight, fresh fruit active constituent Object is taken, face cream, lotion, facial mask and the daily chemical products of preparation can improve skin aging situation, also there is preferable suppression to scytitis Production is used;Development and utilization for paper mulberry, fresh fruit provide new approaches;
In specific implementation process, addition with the paper mulberry of parts by weight 1% or so, fresh fruit active component extract, effect compared with Well, the effect of active matter being played.
In the description of this specification, the description of reference term " one embodiment ", " example ", " specific example " etc. means Particular features, structures, materials, or characteristics described in conjunction with this embodiment or example are contained at least one implementation of the invention In example or example.In the present specification, schematic expression of the above terms may not refer to the same embodiment or example. Moreover, particular features, structures, materials, or characteristics described can be in any one or more of the embodiments or examples to close Suitable mode combines.
Present invention disclosed above preferred embodiment is only intended to help to illustrate the present invention.There is no detailed for preferred embodiment All details are described, are not limited the invention to the specific embodiments described.Obviously, according to the content of this specification, It can make many modifications and variations.These embodiments are chosen and specifically described to this specification, is in order to better explain the present invention Principle and practical application, so that skilled artisan be enable to better understand and utilize the present invention.The present invention is only It is limited by claims and its full scope and equivalent.

Claims (6)

1. the application of paper mulberry, fresh fruit active component extract in daily chemical products preparation.
2. the application of paper mulberry as described in claim 1, fresh fruit active component extract in face cream, lotion, facial mask preparation.
3. the application of paper mulberry, fresh fruit active component extract as described in claims 1 or 2 any one, it is characterised in that: The paper mulberry, fresh fruit extraction process of active component, including active constituent water mention with active constituent alcohol extracting, removed later with petroleum ether Decontamination, with active carbon decoloring.
4. the application of paper mulberry as claimed in claim 3, fresh fruit active component extract, it is characterised in that: the paper mulberry, The extracting method that fresh fruit active constituent water mentions, comprising the following steps: paper mulberry, fresh fruit are shredded, use water logging after 30-50 DEG C of heating Bubble leaf 1-2 hours;It extracts supernatant and is concentrated;Be concentrated to get water layer by petroleum ether extraction soluble pigment and ester dissolubility at Point;Retain water layer and pass through active carbon decoloring, freeze-drying obtains water-soluble active ingredient and extract;
The paper mulberry, fresh fruit active constituent alcohol extracting extracting method, comprising the following steps:
70%-75% ethyl alcohol extraction 2-3 times is used Step 1: paper mulberry, fresh fruit chopping are used at 50-60 DEG C of bath temperature, often Secondary 2 hours, merges the ethanol solution of extraction and recycle ethyl alcohol acquisition paper mulberry, fresh fruit ethyl alcohol primary extract;
Step 2: being dissolved in water to paper mulberry, fresh fruit ethyl alcohol primary extract, with petroleum ether extraction, degreasing soluble components, pigment, water Layer decolourizes and is spray-dried;
Step 3: contact plate detection paper mulberry, fresh fruit spend active constituent and obtain paper mulberry active component extract.
5. a kind of paper mulberry, fresh fruit flower active component extract mend facial mask, it is characterised in that: including following raw material: structure Set 1-5 parts of flowers and fruits extract, 30-50 parts of water, 3-5 parts of glycerol, 2-5 parts of butanediol, 2-3 parts of beta glucan, tremella (Tremella Fuciformis) polysaccharide 2-3 parts, 2-3 parts of pomegranate (Punica granatum) pericarp extract, 3 parts of trehalose, acetyl group six - 81-2 parts of peptide, glycol 1-2 parts pungent, ceramide × 1-2 parts, 2-3 parts of Radix Notoginseng (Panax notoginseng) extract, decoyl 1 part of hydroximic acid, 1 part of 1,2- hexylene glycol, 1 part of 1,3-PD, 1 part of Phenoxyethanol, 1 part of Sensiva SC50,1 part of carbomer, 0.5-1 parts of sodium hydroxide, 1 part of dipotassium glycyrrhizinate, 1 part of collagen, 1 part of sorbierite, 1 part of xanthan gum, 1 part of Sodium Hyaluronate.
6. paper mulberry as claimed in claim 5, fresh fruit flower active component extract mend facial mask, it is characterised in that: the paper mulberry Flower, fresh fruit flower active component extract are mended Broussonetia extract (Paper mulberry) addition in facial mask and are mentioned as 1-5%.
CN201910075997.XA 2019-01-26 2019-01-26 A kind of application of paper mulberry, fresh fruit extraction process of active component and extract Pending CN109700716A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114053329A (en) * 2021-12-30 2022-02-18 广东药科大学 Application of broussonetia papyrifera in preparation of medicines or sunscreen cosmetics for preventing and treating ultraviolet injury

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CN102946894A (en) * 2010-06-18 2013-02-27 株式会社爱茉莉太平洋 Method for preparing broussonetia kazinoki extract
CN102970999A (en) * 2010-07-02 2013-03-13 株式会社爱茉莉太平洋 Skin-whitening composition for external application on skin containing extracts from paper mulberry flowers and fruits
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114053329A (en) * 2021-12-30 2022-02-18 广东药科大学 Application of broussonetia papyrifera in preparation of medicines or sunscreen cosmetics for preventing and treating ultraviolet injury

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Application publication date: 20190503