CN109699979A - The honey and preparation method and purposes of a kind of ingredient containing trollflower in trollflower flower source - Google Patents
The honey and preparation method and purposes of a kind of ingredient containing trollflower in trollflower flower source Download PDFInfo
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Abstract
The present invention relates to food processing fields, and in particular to the preparation method and purposes of a kind of honey of the ingredient containing trollflower in trollflower flower source.The honey of the ingredient containing trollflower in trollflower flower provided by the invention source, is made of: lily feet flower essential oil 0.1-1%, Flos Trollii extract 1-5%, honey 94-98.9% following components and its weight percent.The honey of the ingredient containing trollflower in trollflower flower provided by the invention source not only has the effect of good clearing heat and detoxicating, diminishing inflammation and clearing pharynx; can also it is anti-oxidant, protection enteron aisle, coordinating intestines and stomach, prevent constipation; take the honey of the ingredient containing trollflower in trollflower flower provided by the invention source; it is dry and astringent eye can effectively to be slowed down; alleviate eye strain, has a good application prospect.
Description
Technical field
The present invention relates to food processing fields, and in particular to the honey and system of a kind of ingredient containing trollflower in trollflower flower source
Preparation Method and purposes.
Background technique
Trollflower also known as golden lotus, globe-flower etc., happiness cool moist environment, be one kind be grown in heavy rainfall, height above sea level compared with
High, the biggish severe cold areas of day and night temperature herbaceos perennial, has high medical value and economic value.Trollflower
Golden yellow bright, clean taste has clearing heat and detoxicating, nourishing yin and lessening fire, and the effect of nourishing yin and clearing heat and the fire sterilization that disappears, long-term drinking can be clear
Throat soothing is swallowed, is refreshed the mind, clearly food eliminating greasiness, makes one to brace up, voice is limpid.To chronic pharyngitis, laryngitis, tonsillitis and sound
Hoarse person has anti-inflammatory, preventive and therapeutic action.Trollflower flower pattern is beautiful, and pattern is bright-coloured, and flower can be used as medicine.Trollflower is with its safety
Reliable antibacterial and anti-inflammatory effects are endowed the good reputation of natural antibiotics.
Trollflower is primarily used in the preparation of drug and herbal tea at present, wherein Chinese patent CN106420656B is disclosed
A kind of trollflower effervescent tablet, the trollflower effervescent tablet which provides is mainly by lily feet pollen, Coixol, syringic acid, sorb
Alcohol, xanthan gum, sodium citrate and sodium bicarbonate composition, have effects that good clearing heat and detoxicating, activating microcirculation and removing stasis medicinal and anti-inflammatory analgesic,
But in children's eliminating inflammation and expelling toxin pharmaceutical arts, the application of the effervescent tablet is very restricted.
Honey has the function of dual-purpose of drug and food.It is experimentally confirmed that honey removes from office orchid to streptococcus, staphylococcus, corynebacterium diphtheriae etc.
Positive bacteria has a stronger inhibiting effect, thus high-quality honey place at room temperature the several years will not corruption, show its antisepsis pole
By force.It is bowl spares emergency as its effect of drug, moisturizes, detoxifies.Suitable for the epigastric pain of deficiency-cold in spleen and stomach, cough caused by dryness caused by the deficiency syndrome of the lung
And intestinal dryness constipation, the detoxication of honey are suitable for the removing toxic substances of Aconitum poison.Honey or many nourishings in Chinese medicine
The common excipient of pill, paste can play flavoring and increase the effect of viscosity, in addition have many medicines all to adopt in the prepared slices of Chinese crude drugs
With honey process, also and its can take a tonic or nourishing food to build up one's health it is related with pharmacological property is mitigated.Modern doctor's research, there are also antibacterial, removing toxic substances, protection liver, rush for honey
Into the effect of wound healing.Honey can improve the ingredient of blood, promote heart and brain and vascular function, therefore often take in angiocarpy
Patient is very good；Honey has protective effect to liver, can promote liver cell regeneration, has certain inhibition to the formation of fatty liver
Effect；Honey at home and abroad all has good city as a kind of natural green food and medical and health-care products full of nutrition
?.Edible honey can regain one's strength of body rapidly, eliminate fatigue, build up one's resistance to disease；Various nutritional ingredients in honey and
Fresh Honey is applied on skin by the effect of collective effect of function factor makes it have beautifying face and moistering lotion, can play moisten and
Trophism, makes that skin is fine and smooth, smooth, high resilience.
Chinese patent application CN108125173A discloses a kind of preparation method of oat honey, this method by melon seeds powder and
What oatmeal decocted obtains being made in medicinal extract addition motherwort honey and being rich in dietary fiber, the richer oat honey of mouthfeel, but
The honey anti-inflammatory effects are general.
Therefore, a kind of with excellent anti-inflammatory effects, honey suitable for people of all ages is that current the urgent of honey manufacturing field is essential
It asks.
Summary of the invention
In view of the deficiencies of the prior art, the object of the present invention is to provide a kind of ingredients containing trollflower in trollflower flower source
Honey and preparation method and purposes.The honey of the ingredient containing trollflower in trollflower flower provided by the invention source not only has well
Clearing heat and detoxicating, diminishing inflammation and clearing pharynx effect, additionally it is possible to anti-oxidant, protection enteron aisle, coordinating intestines and stomach, prevent constipation, test is unexpectedly
It was found that take the honey of the ingredient containing trollflower in trollflower provided by the invention flower source, it is dry and astringent effectively to slow down eye, alleviates
Eye strain has a good application prospect.
The invention is realized by the following technical scheme:
A kind of honey of the ingredient containing trollflower in trollflower flower source, is made of following components and its weight percent:
Lily feet flower essential oil 0.1-1%, Flos Trollii extract 1-5%, honey 94-98.9%.
Further, the honey of the ingredient containing trollflower in trollflower flower source, by following components and its weight percent
Composition:
Lily feet flower essential oil 0.7%, Flos Trollii extract 3.8%, honey 95.5%.
Further, the honey is the honey using trollflower as nectariferous plant.
Further, the honey is that honeybee is adopted using one or both of trollflower nectar, pollen as plant nectar source
Collection obtains.
Further, the lily feet flower essential oil the preparation method comprises the following steps:
S1, it drains away the water, crushes after cleaning up trollflower, be sieved with 40-60 mesh sieve, obtain trollflower powder；
S2, supercritical CO2Refining: trollflower powder made from step S1 is sent into supercritical CO2In device, through for the first time
After extraction and second of extraction, extract liquor is collected, trollflower crude oil is obtained；
S3, refrigerated centrifuge: obtaining trollflower crude oil for step S2 and be placed in 8-11 DEG C of environment, freeze 30-35min,
The trollflower crude oil after freezing is placed in the high speed freezing centrifuge that revolving speed is 8000-10000r/min again and is centrifuged 20-
30min, remove impurity, be put into temperature be 45-50 DEG C, vacuum distillation purifying condensation to get.
Further, CO in the step S22The extracting pressure of supercritical extract is 30MPa, and extraction temperature is 40 DEG C, extraction
Taking the time is 2h.
Further, the Flos Trollii extract the preparation method comprises the following steps:
Crushing is dried in S1, selection trollflower, then infiltrates 12-24h in water, obtains immersion fluid；
S2, the immersion fluid that step S1 is obtained is subjected to reflux 1-2h with the ethanol water that volume fraction is 60-80%, returned
Flowing temperature is 75-80 DEG C, obtains ethanol extract；
S3, the ethanol extract for obtaining step S2 filter, and filter residue repeats the operation of a step S2-S3, merges two
Secondary filtrate；
S4, the step S3 filtrate obtained is concentrated into relative density for 1.05-1.10, obtains concentrate；
S5, the step S4 concentrate obtained is purified, 30-50% ethanol elution on adsorption resin column, obtains ethyl alcohol and returns
Receive liquid；
Cheng Fenmo after S6, the ethyl alcohol recovered liquid spray drying for obtaining step S5, obtains Flos Trollii extract.
A kind of preparation method of the honey of the ingredient containing trollflower in trollflower flower source, includes the following steps:
S1, pass through CO2Supercritical extract mode obtains lily feet flower essential oil, spare；
Crushing is dried in S2, selection trollflower, then infiltrates 12-24h in water, obtains immersion fluid；
S3, the immersion fluid that step S2 is obtained is subjected to reflux 1-2h with the ethanol water that volume fraction is 60-80%, returned
Flowing temperature is 75-80 DEG C, obtains ethanol extract；
S4, the ethanol extract for obtaining step S3 filter, and filter residue repeats the operation of a step S3-S4, merges two
Secondary filtrate；
S5, the step S4 filtrate obtained is concentrated into relative density for 1.05-1.10, obtains concentrate；
S6, the step S5 concentrate obtained is purified, 30-50% ethanol elution on adsorption resin column, obtains ethyl alcohol and returns
Receive liquid；
Cheng Fenmo after S7, the ethyl alcohol recovered liquid spray drying for obtaining step S6, obtains Flos Trollii extract；
S8, Flos Trollii extract made from lily feet flower essential oil made from step S1 and step S7 is weighed, is added in honey, stirs
Mix uniformly, tinning save to get.
Further, the adsorption resin column in the step S6 is AB-8 type adsorption resin column.
The honey of the ingredient containing trollflower in the trollflower flower source is preparing the application in diminishing inflammation and clearing pharynx health care product
Flos Trollii extract in the honey of the ingredient containing trollflower in trollflower flower provided by the invention source has heat-clearing solution
Poison, nourishing yin and lessening fire, the effect of nourishing yin and clearing heat and the fire sterilization that disappears, for treating chronic tonsillitis, otitis media acuta, acute conjunctiva
The diseases such as inflammation；Lily feet flower essential oil has throat-clearing throat-moistening, refreshes the mind, clearly food eliminating greasiness, makes one to brace up, the limpid work of voice
With having anti-inflammatory, preventive and therapeutic action, lily feet provided by the invention to chronic pharyngitis, laryngitis, tonsillitis and hoarseness person
Formula is scientific and reasonable for the honey of the ingredient containing trollflower of Hua Huayuan, and each component is mutually coordinated to be played clearing heat and detoxicating, diminishing inflammation and clearing pharynx, resists
Oxidation, coordinating intestines and stomach, prevents the effect of constipation at protection enteron aisle.
The honey of the ingredient containing trollflower in trollflower flower provided by the invention source is without any toxicity and side effects, suitable for people of all ages, is applicable in
In the diminishing inflammation and clearing pharynx product of children.
The honey of the ingredient containing trollflower in trollflower provided by the invention flower source in (28 ± 2) DEG C, relative humidity (60 ±
10) it is placed 36 months under conditions of %, character and quality are substantially unchanged, and stability with higher illustrates that the present invention mentions
The honey each component of the ingredient containing trollflower in the trollflower flower source of confession is mutually coordinated, the ingredient containing trollflower in enhancing trollflower flower source
Honey stability action.
In addition to this, it is dry can also to alleviate eye for the honey of the ingredient containing trollflower in trollflower flower provided by the invention source
Puckery, ocular pain alleviates eye strain, has good eyeshield effect.
Compared with prior art, technical solution of the present invention has the advantage that
(1) honey of the ingredient containing trollflower in trollflower flower provided by the invention source, using trollflower as plant nectar source, tool
The effect of having good raising appetite, promoting development.
(2) honey of the ingredient containing trollflower in trollflower flower provided by the invention source, lily feet flower essential oil, Flos Trollii extract
Addition has the function of good diminishing inflammation and clearing pharynx, while also having and promoting digestion, and coordinating intestines and stomach improves the effect of immunity.
(3) honey of the ingredient containing trollflower in trollflower flower provided by the invention source, can effectively slow down eye strain, delay
The dry and astringent feeling of pain of eye is solved, there is good eyeshield effect.
Specific embodiment
The specific embodiment of form by the following examples makees further specifically above content of the invention
It is bright.But the range that this should not be interpreted as to the above-mentioned theme of the present invention is only limitted to following embodiment.
Embodiment 1, a kind of trollflower spend the honey of the ingredient containing trollflower in source
The honey of the ingredient containing trollflower in trollflower flower source, is made of: lily feet following components and its weight percent
Flower essential oil 0.1%, Flos Trollii extract 1%, honey 98.9%.
The honey is the honey using trollflower as nectariferous plant.
The honey is that honeybee acquires acquisition using trollflower nectar as plant nectar source.
The lily feet flower essential oil the preparation method comprises the following steps:
S1, it drains away the water, crushes after cleaning up trollflower, be sieved with 40 mesh sieve, obtain trollflower powder；
S2, supercritical CO2Refining: trollflower powder made from step S1 is sent into supercritical CO2In device, extracting pressure
For 30MPa, extraction temperature is 40 DEG C, extraction time 2h, after first time extraction and second extract, collects extract liquor, obtains
To trollflower crude oil；
S3, refrigerated centrifuge: step S2 is obtained into trollflower crude oil and is placed in 8 DEG C of environment, freezes 30min, then will be cold
Trollflower crude oil after jelly is placed in the high speed freezing centrifuge that revolving speed is 8000r/min and is centrifuged 20min, removes impurity, puts
Enter temperature be 45 DEG C, vacuum distillation purifying condensation to get.
The Flos Trollii extract the preparation method comprises the following steps:
Crushing is dried in S1, selection trollflower, then infiltrates 12h in water, obtains immersion fluid；
S2, the immersion fluid for obtaining step S1 carry out reflux 1h, reflux temperature with the ethanol water that volume fraction is 60%
Degree is 75 DEG C, obtains ethanol extract；
S3, the ethanol extract for obtaining step S2 filter, and filter residue repeats the operation of a step S2-S3, merges two
Secondary filtrate；
S4, the step S3 filtrate obtained is concentrated into relative density be 1.05, obtain concentrate；
S5, the step S4 concentrate obtained is purified, 30% ethanol elution on adsorption resin column, obtains ethyl alcohol recycling
Liquid；
Cheng Fenmo after S6, the ethyl alcohol recovered liquid spray drying for obtaining step S5, obtains Flos Trollii extract.
The preparation method of the honey of the ingredient containing trollflower in trollflower flower source, includes the following steps:
S1, pass through CO2Supercritical extract mode obtains lily feet flower essential oil, spare；
Crushing is dried in S2, selection trollflower, then infiltrates 12h in water, obtains immersion fluid；
S3, the immersion fluid for obtaining step S2 carry out reflux 1h, reflux temperature with the ethanol water that volume fraction is 60%
Degree is 75 DEG C, obtains ethanol extract；
S4, the ethanol extract for obtaining step S3 filter, and filter residue repeats the operation of a step S3-S4, merges two
Secondary filtrate；
S5, the step S4 filtrate obtained is concentrated into relative density be 1.05, obtain concentrate；
S6, the concentrate that step S5 is obtained is purified on AB-8 type adsorption resin column, 30% ethanol elution obtains ethyl alcohol
Recovered liquid；
Cheng Fenmo after S7, the ethyl alcohol recovered liquid spray drying for obtaining step S6, obtains Flos Trollii extract；
S8, Flos Trollii extract made from lily feet flower essential oil made from step S1 and step S7 is weighed, is added in honey, stirs
Mix uniformly, tinning save to get.
Embodiment 2, a kind of trollflower spend the honey of the ingredient containing trollflower in source
The honey of the ingredient containing trollflower in trollflower flower source, is made of following components and its weight percent:
Lily feet flower essential oil 1%, Flos Trollii extract 5%, honey 94%.
The honey is the honey using trollflower as nectariferous plant.
The honey is that honeybee acquires acquisition using trollflower pollen as plant nectar source.
The lily feet flower essential oil the preparation method comprises the following steps:
S1, it drains away the water, crushes after cleaning up trollflower, be sieved with 60 mesh sieve, obtain trollflower powder；
S2, supercritical CO2Refining: trollflower powder made from step S1 is sent into supercritical CO2In device, extracting pressure
For 30MPa, extraction temperature is 40 DEG C, extraction time 2h, after first time extraction and second extract, collects extract liquor, obtains
To trollflower crude oil；
S3, refrigerated centrifuge: step S2 is obtained into trollflower crude oil and is placed in 11 DEG C of environment, freezes 35min, then will be cold
Trollflower crude oil after jelly is placed in the high speed freezing centrifuge that revolving speed is 10000r/min and is centrifuged 30min, removes impurity, puts
Enter temperature be 50 DEG C, vacuum distillation purifying condensation to get.
The Flos Trollii extract the preparation method comprises the following steps:
Crushing is dried in S1, selection trollflower, then infiltrates for 24 hours in water, obtains immersion fluid；
S2, the immersion fluid for obtaining step S1 carry out reflux 2h, reflux temperature with the ethanol water that volume fraction is 80%
Degree is 80 DEG C, obtains ethanol extract；
S3, the ethanol extract for obtaining step S2 filter, and filter residue repeats the operation of a step S2-S3, merges two
Secondary filtrate；
S4, the step S3 filtrate obtained is concentrated into relative density be 1.10, obtain concentrate；
S5, the step S4 concentrate obtained is purified, 50% ethanol elution on adsorption resin column, obtains ethyl alcohol recycling
Liquid；
Cheng Fenmo after S6, the ethyl alcohol recovered liquid spray drying for obtaining step S5, obtains Flos Trollii extract.
The preparation method of the honey of the ingredient containing trollflower in trollflower flower source, includes the following steps:
S1, pass through CO2Supercritical extract mode obtains lily feet flower essential oil, spare；
Crushing is dried in S2, selection trollflower, then infiltrates for 24 hours in water, obtains immersion fluid；
S3, the immersion fluid for obtaining step S2 carry out reflux 2h, reflux temperature with the ethanol water that volume fraction is 80%
Degree is 80 DEG C, obtains ethanol extract；
S4, the ethanol extract for obtaining step S3 filter, and filter residue repeats the operation of a step S3-S4, merges two
Secondary filtrate；
S5, the step S4 filtrate obtained is concentrated into relative density be 1.10, obtain concentrate；
S6, the concentrate that step S5 is obtained is purified on AB-8 type adsorption resin column, 50% ethanol elution obtains ethyl alcohol
Recovered liquid；
Cheng Fenmo after S7, the ethyl alcohol recovered liquid spray drying for obtaining step S6, obtains Flos Trollii extract；
S8, Flos Trollii extract made from lily feet flower essential oil made from step S1 and step S7 is weighed, is added in honey, stirs
Mix uniformly, tinning save to get.
Embodiment 3, a kind of trollflower spend the honey of the ingredient containing trollflower in source
The honey of the ingredient containing trollflower in trollflower flower source, is made of: lily feet following components and its weight percent
Flower essential oil 0.4%, Flos Trollii extract 2.3%, honey 97.3%.
The honey is the honey using trollflower as nectariferous plant.
The honey is that honeybee is acquired as plant nectar source and obtained using trollflower nectar, pollen.
Further, the lily feet flower essential oil the preparation method comprises the following steps:
S1, it drains away the water, crushes after cleaning up trollflower, be sieved with 50 mesh sieve, obtain trollflower powder；
S2, supercritical CO2Refining: trollflower powder made from step S1 is sent into supercritical CO2In device, extracting pressure
For 30MPa, extraction temperature is 40 DEG C, extraction time 2h, after first time extraction and second extract, collects extract liquor, obtains
To trollflower crude oil；
S3, refrigerated centrifuge: step S2 is obtained into trollflower crude oil and is placed in 10 DEG C of environment, freezes 30min, then will be cold
Trollflower crude oil after jelly is placed in the high speed freezing centrifuge that revolving speed is 9000r/min and is centrifuged 25min, removes impurity, puts
Enter temperature be 50 DEG C, vacuum distillation purifying condensation to get.
The Flos Trollii extract the preparation method comprises the following steps:
Crushing is dried in S1, selection trollflower, then infiltrates 18h in water, obtains immersion fluid；
S2, the immersion fluid for obtaining step S1 carry out reflux 1h, reflux temperature with the ethanol water that volume fraction is 75%
Degree is 75 DEG C, obtains ethanol extract；
S3, the ethanol extract for obtaining step S2 filter, and filter residue repeats the operation of a step S2-S3, merges two
Secondary filtrate；
S4, the step S3 filtrate obtained is concentrated into relative density be 1.05, obtain concentrate；
S5, the step S4 concentrate obtained is purified, 40% ethanol elution on adsorption resin column, obtains ethyl alcohol recycling
Liquid；
Cheng Fenmo after S6, the ethyl alcohol recovered liquid spray drying for obtaining step S5, obtains Flos Trollii extract.
The preparation method of the honey of the ingredient containing trollflower in trollflower flower source, includes the following steps:
S1, pass through CO2Supercritical extract mode obtains lily feet flower essential oil, spare；
Crushing is dried in S2, selection trollflower, then infiltrates 18h in water, obtains immersion fluid；
S3, the immersion fluid for obtaining step S2 carry out reflux 1h, reflux temperature with the ethanol water that volume fraction is 75%
Degree is 75 DEG C, obtains ethanol extract；
S4, the ethanol extract for obtaining step S3 filter, and filter residue repeats the operation of a step S3-S4, merges two
Secondary filtrate；
S5, the step S4 filtrate obtained is concentrated into relative density be 1.05, obtain concentrate；
S6, the concentrate that step S5 is obtained is purified on AB-8 type adsorption resin column, 40% ethanol elution obtains ethyl alcohol
Recovered liquid；
Cheng Fenmo after S7, the ethyl alcohol recovered liquid spray drying for obtaining step S6, obtains Flos Trollii extract；
S8, Flos Trollii extract made from lily feet flower essential oil made from step S1 and step S7 is weighed, is added in honey, stirs
Mix uniformly, tinning save to get.
Embodiment 4, a kind of trollflower spend the honey of the ingredient containing trollflower in source
The honey of the ingredient containing trollflower in trollflower flower source, is made of: lily feet following components and its weight percent
Flower essential oil 0.7%, Flos Trollii extract 3.8%, honey 95.5%.
The honey is the honey using trollflower as nectariferous plant.
The honey is that honeybee is acquired as plant nectar source and obtained using trollflower nectar, pollen.
The lily feet flower essential oil the preparation method comprises the following steps:
S1, it drains away the water, crushes after cleaning up trollflower, be sieved with 40 mesh sieve, obtain trollflower powder；
S2, supercritical CO2Refining: trollflower powder made from step S1 is sent into supercritical CO2In device, extracting pressure
For 30MPa, extraction temperature is 40 DEG C, extraction time 2h, after first time extraction and second extract, collects extract liquor, obtains
To trollflower crude oil；
S3, refrigerated centrifuge: step S2 is obtained into trollflower crude oil and is placed in 11 DEG C of environment, freezes 35min, then will be cold
Trollflower crude oil after jelly is placed in the high speed freezing centrifuge that revolving speed is 10000r/min and is centrifuged 20min, removes impurity, puts
Enter temperature be 50 DEG C, vacuum distillation purifying condensation to get.
The Flos Trollii extract the preparation method comprises the following steps:
Crushing is dried in S1, selection trollflower, then infiltrates 20h in water, obtains immersion fluid；
S2, the immersion fluid for obtaining step S1 carry out reflux 1.5h with the ethanol water that volume fraction is 75%, flow back
Temperature is 80 DEG C, obtains ethanol extract；
S3, the ethanol extract for obtaining step S2 filter, and filter residue repeats the operation of a step S2-S3, merges two
Secondary filtrate；
S4, the step S3 filtrate obtained is concentrated into relative density be 1.07, obtain concentrate；
S5, the step S4 concentrate obtained is purified, 45% ethanol elution on adsorption resin column, obtains ethyl alcohol recycling
Liquid；
Cheng Fenmo after S6, the ethyl alcohol recovered liquid spray drying for obtaining step S5, obtains Flos Trollii extract.
The preparation method of the honey of the ingredient containing trollflower in trollflower flower source, includes the following steps:
S1, pass through CO2Supercritical extract mode obtains lily feet flower essential oil, spare；
Crushing is dried in the first-class trollflower of S2, selection, then infiltrates 20h in water, obtains immersion fluid；
S3, the immersion fluid for obtaining step S2 carry out reflux 1.5h with 75% ethyl alcohol, and reflux temperature is 80 DEG C, obtain second
Alcohol extracting thing；
S4, the ethanol extract for obtaining step S3 filter, and filter residue repeats the operation of a step S3-S4, filtered
Liquid；
S5, the step S4 filtrate obtained is concentrated into relative density be 1.07, obtain concentrate；
S6, the step S5 concentrate obtained is purified, 45% ethanol elution on adsorption resin column, obtains ethyl alcohol recycling
Liquid；
Cheng Fenmo after S7, the ethyl alcohol recovered liquid spray drying for obtaining step S6, obtains Flos Trollii extract；
S8, Flos Trollii extract made from lily feet flower essential oil made from step S1 and step S7 is weighed, is added in honey, stirs
Mix uniformly, tinning save to get.
Embodiment 5, a kind of trollflower spend the honey of the ingredient containing trollflower in source
The honey of the ingredient containing trollflower in trollflower flower source, is made of: lily feet following components and its weight percent
Flower essential oil 0.9%, Flos Trollii extract 4.1%, honey 95%.
The honey is the honey using trollflower as nectariferous plant.
The honey is that honeybee is acquired as plant nectar source and obtained using trollflower nectar, pollen.
The lily feet flower essential oil the preparation method comprises the following steps:
S1, it drains away the water, crushes after cleaning up trollflower, be sieved with 45 mesh sieve, obtain trollflower powder；
S2, supercritical CO2Refining: trollflower powder made from step S1 is sent into supercritical CO2In device, extracting pressure
For 30MPa, extraction temperature is 40 DEG C, extraction time 2h, after first time extraction and second extract, collects extract liquor, obtains
To trollflower crude oil；
S3, refrigerated centrifuge: step S2 is obtained into trollflower crude oil and is placed in 9 DEG C of environment, freezes 30min, then will be cold
Trollflower crude oil after jelly is placed in the high speed freezing centrifuge that revolving speed is 8000r/min and is centrifuged 25min, removes impurity, puts
Enter temperature be 48 DEG C, vacuum distillation purifying condensation to get.
The Flos Trollii extract the preparation method comprises the following steps:
Crushing is dried in the first-class trollflower of S1, selection, then infiltrates 23h in water, obtains immersion fluid；
S2, the immersion fluid for obtaining step S1 carry out reflux 1.5h with 75% ethyl alcohol, and reflux temperature is 76 DEG C, obtain second
Alcohol extracting thing；
S3, the ethanol extract for obtaining step S2 filter, and filter residue repeats the operation of a step S2-S3, filtered
Liquid；
S4, the step S3 filtrate obtained is concentrated into relative density be 1.08, obtain concentrate；
S5, the step S4 concentrate obtained is purified, 45% ethanol elution on adsorption resin column, obtains ethyl alcohol recycling
Liquid；
Cheng Fenmo after S6, the ethyl alcohol recovered liquid spray drying for obtaining step S5, obtains Flos Trollii extract.
The preparation method of the honey of the ingredient containing trollflower in trollflower flower source, includes the following steps:
S1, pass through CO2Supercritical extract mode obtains lily feet flower essential oil, spare；
Crushing is dried in the first-class trollflower of S2, selection, then infiltrates 23h in water, obtains immersion fluid；
S3, the immersion fluid for obtaining step S2 carry out reflux 1.5h with 75% ethyl alcohol, and reflux temperature is 76 DEG C, obtain second
Alcohol extracting thing；
S4, the ethanol extract for obtaining step S3 filter, and filter residue repeats the operation of a step S3-S4, filtered
Liquid；
S5, the step S4 filtrate obtained is concentrated into relative density be 1.08, obtain concentrate；
S6, the step S5 concentrate obtained is purified, 45% ethanol elution on adsorption resin column, obtains ethyl alcohol recycling
Liquid；
Cheng Fenmo after S7, the ethyl alcohol recovered liquid spray drying for obtaining step S6, obtains Flos Trollii extract；
S8, Flos Trollii extract made from lily feet flower essential oil made from step S1 and step S7 is weighed, is added in honey, stirs
Mix uniformly, tinning save to get.
Comparative example 1, a kind of trollflower spend the honey of the ingredient containing trollflower in source
The honey of the ingredient containing trollflower in trollflower flower source, is made of: lily feet following components and its weight percent
Flower essential oil 2%, Flos Trollii extract 8%, honey 90%.
The honey is the honey using trollflower as nectariferous plant.
The honey is that honeybee is acquired as plant nectar source and obtained using trollflower nectar, pollen.
The colored source of the preparation method of the lily feet flower essential oil, the preparation method of Flos Trollii extract, trollflower contains trollflower
The preparation method of the honey of ingredient is same as Example 4.
Comparative example 1 is substantially the same manner as Example 4, and difference is, the component and its weight percent are by lily feet flower essential oil
0.7%, Flos Trollii extract 3.8%, honey 95.5% becomes lily feet flower essential oil 2%, Flos Trollii extract 8%, honey 90%.
Comparative example 2, a kind of trollflower spend the honey of the ingredient containing trollflower in source
The honey of the ingredient containing trollflower in trollflower flower source, is made of: lily feet following components and its weight percent
Flower extract 3.8%, honey 96.2%.
The honey is the honey using trollflower as nectariferous plant.
The honey is that honeybee is acquired as plant nectar source and obtained using trollflower nectar, pollen.
The preparation method of the Flos Trollii extract, trollflower flower source the ingredient containing trollflower honey preparation method with
Embodiment 4 is identical.
Comparative example 2 is substantially the same manner as Example 4, and difference is, the honey of the same composition of comparative example 2 replaces lily feet anthosin
Oil.
Comparative example 3, a kind of trollflower spend the honey of the ingredient containing trollflower in source
The honey of the ingredient containing trollflower in trollflower flower source, is made of: lily feet following components and its weight percent
Flower essential oil 0.7%, honey 99.3%.
The honey is the honey using trollflower as nectariferous plant.
The honey is that honeybee is acquired as plant nectar source and obtained using trollflower nectar, pollen.
Preparation method, the preparation method and reality of the honey of the ingredient containing trollflower in trollflower flower source of the lily feet flower essential oil
It is identical to apply example 4.
Comparative example 3 is substantially the same manner as Example 4, and difference is, the honey of the same composition of comparative example 3 replaces trollflower to mention
Take object.
Comparative example 4, a kind of jujube flower spend the honey of the ingredient containing trollflower in source
The honey of the ingredient containing trollflower in jujube flower flower source, is made of: trollflower following components and its weight percent
Essential oil 0.7%, Flos Trollii extract 3.8%, honey 95.5%.
The honey is the honey using jujube flower as nectariferous plant.
The honey is that honeybee is acquired as plant nectar source and obtained using jujube flower nectar, pollen.
Preparation method, the preparation method of Flos Trollii extract of the lily feet flower essential oil are same as Example 4.
Trollflower flower source contains gold in the preparation method and embodiment 4 of the honey of the ingredient containing trollflower in jujube flower flower source
The preparation method of the honey of lotus flower ingredient is identical.
Comparative example 4 is substantially the same manner as Example 4, and difference is, comparative example 4 is with same composition using jujube flower as the bee in nectar source
Honey is replaced using trollflower as the honey in nectar source.
Embodiment one, the test of pharyngitis clinical trial
1, test material: the honey of the ingredient containing trollflower in the trollflower flower source of embodiment 1-5 and comparative example 1-4 preparation.
2, subjects: coming from hospital and outpatient service totally 100 pharyngitis patients, wherein male 50, female 50, the age 20~60
In year, clinical diagnosis acpuei pharyngitis 50, chronic pharyngitis 50, wherein patient has the dry and astringent pain of different degrees of eye, digestion
Bad, insomnia.
3, experimental group: 100 pharyngitis patients are randomly divided into 10 groups, every group 10, wherein acpuei pharyngitis 5, chronic
Pharyngitis 5.
4, test method: patient sucks Caoshan Hu Hanpian daily, and 1 tablet once, three times a day, wherein one group is denoted as control group,
On this basis, the patient trollflower flower source that daily prepared by embodiment 1-5, comparative example 1-4 contains lily feet to remaining 9 groups of difference
The honey of flower ingredient, acpuei pharyngitis patient, 6 times a day, patients with chronic pharyngitis after taking 7 days, observe experimenter's 3 times a day
Clinical manifestation, and the dry and astringent pain relief of eye, indigestion alleviation, sleep improvement number are observed simultaneously.
Points for attention: Chinese and Western medicine mouth containing, for oral administration and injection anti-infectives should be deactivated during treatment.
Effect criterion:
Recovery from illness: symptom mitigates in consumable products 3 days, and clinical symptoms and sign disappear in 5 days.It is effective: in consumable products 5 days
Symptom mitigates, and most of sign disappears.Effective: symptom mitigates in edible product of the present invention 5 days, and part sign disappears.It is invalid: food
With clinical symptoms and sign cannot be made to disappear in product one week.
5, test result:
Test result is shown in Table 1.
1 pharyngitis clinic test data of table
As shown in Table 1, compared with comparative example 1-4 group and control group, 1-5 group of the embodiment of the present invention has pharyngitis higher
Cure rate and effective percentage, meanwhile, it is capable to alleviate, eye is dry and astringent, alleviates indigestion, and has certain alleviation to make insomnia
With.Wherein 4 groups of effects of embodiment are best, therefore embodiment 4 is highly preferred embodiment of the present invention, the results showed that, the present invention provides
Trollflower flower source the ingredient containing trollflower honey have good diminishing inflammation and clearing pharynx, alleviate eye strain, alleviate indigestion,
The effects of useful for sleeping.
The above-described embodiments merely illustrate the principles and effects of the present invention, and is not intended to limit the present invention.It is any ripe
The personage for knowing this technology all without departing from the spirit and scope of the present invention, carries out modifications and changes to above-described embodiment.Cause
This, institute is complete without departing from the spirit and technical ideas disclosed in the present invention by those of ordinary skill in the art such as
At all equivalent modifications or change, should be covered by the claims of the present invention.
Claims (10)
1. a kind of honey of the ingredient containing trollflower in trollflower flower source, which is characterized in that by following components and its weight percent
Composition:
Lily feet flower essential oil 0.1-1%, Flos Trollii extract 1-5%, honey 94-98.9%.
2. the honey of the ingredient containing trollflower in trollflower as described in claim 1 flower source, which is characterized in that by following components and
Its weight percent composition:
Lily feet flower essential oil 0.7%, Flos Trollii extract 3.8%, honey 95.5%.
3. the honey of the ingredient containing trollflower in trollflower flower as claimed in claim 1 or 2 source, which is characterized in that the honey
For the honey using trollflower as nectariferous plant.
4. the honey of the ingredient containing trollflower in trollflower flower as claimed in claim 3 source, which is characterized in that the honey is honey
Bee acquires acquisition using one or both of trollflower nectar, pollen as plant nectar source.
5. the honey of the ingredient containing trollflower in trollflower flower as claimed in claim 1 or 2 source, which is characterized in that the lily feet
Flower essential oil the preparation method comprises the following steps:
S1, it drains away the water, crushes after cleaning up trollflower, be sieved with 40-60 mesh sieve, obtain trollflower powder；
S2, supercritical CO2Refining: trollflower powder made from step S1 is sent into supercritical CO2In device, extracted for the first time
After being extracted with second, extract liquor is collected, trollflower crude oil is obtained；
S3, refrigerated centrifuge: obtaining trollflower crude oil for step S2 and be placed in 8-11 DEG C of environment, freezes 30-35min, then will
Trollflower crude oil after freezing is placed in the high speed freezing centrifuge that revolving speed is 8000-10000r/min and is centrifuged 20-30min,
Remove impurity, be put into temperature be 45-50 DEG C, vacuum distillation purifying condensation to get.
6. the honey of the ingredient containing trollflower in trollflower flower as claimed in claim 5 source, which is characterized in that in the step S2
CO2The extracting pressure of supercritical extract is 30MPa, and extraction temperature is 40 DEG C, extraction time 2h.
7. the honey of the ingredient containing trollflower in trollflower flower as claimed in claim 1 or 2 source, which is characterized in that the lily feet
Flower extract the preparation method comprises the following steps:
Crushing is dried in S1, selection trollflower, then infiltrates 12-24h in water, obtains immersion fluid；
S2, the immersion fluid that step S1 is obtained is subjected to reflux 1-2h, reflux temperature with the ethanol water that volume fraction is 60-80%
Degree is 75-80 DEG C, obtains ethanol extract；
S3, the ethanol extract for obtaining step S2 filter, and filter residue repeats the operation of a step S2-S3, and merging is filtered twice
Liquid；
S4, the step S3 filtrate obtained is concentrated into relative density for 1.05-1.10, obtains concentrate；
S5, the step S4 concentrate obtained is purified on adsorption resin column, 30-50% ethanol elution obtains ethyl alcohol recovered liquid；
Cheng Fenmo after S6, the ethyl alcohol recovered liquid spray drying for obtaining step S5, obtains Flos Trollii extract.
8. a kind of preparation method of the honey for the ingredient containing trollflower that source is spent such as the described in any item trollflowers of claim 1-7,
It is characterized by comprising the following steps:
S1, pass through CO2Supercritical extract mode obtains lily feet flower essential oil, spare；
Crushing is dried in S2, selection trollflower, then infiltrates 12-24h in water, obtains immersion fluid；
S3, the immersion fluid that step S2 is obtained is subjected to reflux 1-2h, reflux temperature with the ethanol water that volume fraction is 60-80%
Degree is 75-80 DEG C, obtains ethanol extract；
S4, the ethanol extract for obtaining step S3 filter, and filter residue repeats the operation of a step S3-S4, and merging is filtered twice
Liquid；
S5, the step S4 filtrate obtained is concentrated into relative density for 1.05-1.10, obtains concentrate；
S6, the step S5 concentrate obtained is purified on adsorption resin column, 30-50% ethanol elution obtains ethyl alcohol recovered liquid；
Cheng Fenmo after S7, the ethyl alcohol recovered liquid spray drying for obtaining step S6, obtains Flos Trollii extract；
S8, Flos Trollii extract made from lily feet flower essential oil made from step S1 and step S7 is weighed, be added in honey, stirring is equal
It is even, tinning save to get.
9. the preparation method of the honey of the ingredient containing trollflower in trollflower flower as claimed in claim 8 source, which is characterized in that institute
Stating the adsorption resin column in step S6 is AB-8 type adsorption resin column.
10. as the honey of the ingredient containing trollflower in claim 1-7 described in any item trollflower flowers source is preparing diminishing inflammation and clearing pharynx
Application in health care product.
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Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20020008333A (en) * | 2000-07-22 | 2002-01-30 | 최재문 | Manufacturing process for Jeongilpoom lacquer(ot) pork hock, Jeongilpoom lacquer(ot) pork hock soup, Jeongilpoom lacquer(ot) pork rib stew and Jeongilpoom lettuce-wrapped lacquer(ot) pork. |
| CN101172128A (en) * | 2006-10-31 | 2008-05-07 | 药都制药集团股份有限公司 | Globeflower tablet and preparing technique thereof |
| JP2015199713A (en) * | 2014-03-31 | 2015-11-12 | 日本メナード化粧品株式会社 | External and internal preparation for skin containing nasturtium extract irradiated with light having specific wavelength band to cultivate |
| CN106377599A (en) * | 2016-11-25 | 2017-02-08 | 广东大鹏医药科技有限公司 | Trollflower chewing gum and preparation method thereof |
| CN106420656A (en) * | 2016-11-25 | 2017-02-22 | 广东大鹏医药科技有限公司 | Trollflower effervescent tablet and preparation method thereof |
| CN106538779A (en) * | 2016-11-09 | 2017-03-29 | 辽宁佰福药业有限公司 | A kind of merceration legal system globeflower tea and preparation method thereof |
| CN106551056A (en) * | 2016-11-25 | 2017-04-05 | 广东大鹏医药科技有限公司 | A kind of Flos Trollii solid herbal tea beverage and preparation method thereof |
| CN106720727A (en) * | 2016-11-25 | 2017-05-31 | 广东大鹏医药科技有限公司 | A kind of trollflower herbal tea and preparation method thereof |
-
2019
- 2019-01-04 CN CN201910006070.0A patent/CN109699979A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20020008333A (en) * | 2000-07-22 | 2002-01-30 | 최재문 | Manufacturing process for Jeongilpoom lacquer(ot) pork hock, Jeongilpoom lacquer(ot) pork hock soup, Jeongilpoom lacquer(ot) pork rib stew and Jeongilpoom lettuce-wrapped lacquer(ot) pork. |
| CN101172128A (en) * | 2006-10-31 | 2008-05-07 | 药都制药集团股份有限公司 | Globeflower tablet and preparing technique thereof |
| JP2015199713A (en) * | 2014-03-31 | 2015-11-12 | 日本メナード化粧品株式会社 | External and internal preparation for skin containing nasturtium extract irradiated with light having specific wavelength band to cultivate |
| CN106538779A (en) * | 2016-11-09 | 2017-03-29 | 辽宁佰福药业有限公司 | A kind of merceration legal system globeflower tea and preparation method thereof |
| CN106377599A (en) * | 2016-11-25 | 2017-02-08 | 广东大鹏医药科技有限公司 | Trollflower chewing gum and preparation method thereof |
| CN106420656A (en) * | 2016-11-25 | 2017-02-22 | 广东大鹏医药科技有限公司 | Trollflower effervescent tablet and preparation method thereof |
| CN106551056A (en) * | 2016-11-25 | 2017-04-05 | 广东大鹏医药科技有限公司 | A kind of Flos Trollii solid herbal tea beverage and preparation method thereof |
| CN106720727A (en) * | 2016-11-25 | 2017-05-31 | 广东大鹏医药科技有限公司 | A kind of trollflower herbal tea and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 卫生部办公厅: "卫生部关于进一步规范保健食品原料管理的通知", 《卫生部文件》 * |
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