CN109674724B - A kind of sleep mask and preparation method thereof containing dendrobium nobile - Google Patents
A kind of sleep mask and preparation method thereof containing dendrobium nobile Download PDFInfo
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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- A—HUMAN NECESSITIES
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
- A61K8/894—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone modified by a polyoxyalkylene group, e.g. cetyl dimethicone copolyol
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/895—Polysiloxanes containing silicon bound to unsaturated aliphatic groups, e.g. vinyl dimethicone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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Abstract
The invention discloses a kind of sleep masks containing dendrobium nobile, it in parts by weight include following component: 58-66 parts of deionized water, 6-9 parts of dimethyl silicone polymer, 2-3 parts of isopropyl myristate, 5-7 parts of butanediol, 7-9 parts of propylene glycol, 2-3 parts of glycine betaine, trimethylpentanediol/adipic acid/1-2 parts of glycerin crosspolymers, Polydimethylsiloxane PEG-10/15 Crosslinked Polymer/3-4 parts of dimethyl silicone polymer, 0.1-0.3 parts of PEG-10 Polydimethylsiloxane, ring five dimethyl silicone polymer (and) 1-3 parts of Dimethicone/Vinyl Dimethicone cross-linked polymer, 0.004-0.008 parts of citric acid, 0.2-0.4 parts of sodium citrate, 1-1.5 parts of sodium chloride, water/butanediol/purslane mentions Take 0.5-1 parts of object, Phenoxyethanol/1,2- hexylene glycol/0.4-0.6 parts of Chlorphenesin, 0.05-0.1 parts of hyaluronic acid, 0.08-0.1 parts of glucan, water/butanediol/2-3 parts of golden hairpin dendrobium extract and 0.01-0.03 parts of Tahiti cape jasmine flower extract.The present invention will have the ingredient of long-acting moistening effect in conjunction with Herba Dendrobii extract, improve skin itself repair ability, efficient moisture-retention moisturizing.
Description
Technical field
The present invention relates to cosmetic technical field, specially a kind of sleep mask formula and preparation method thereof containing dendrobium nobile.
Background technique
As the improvement of people's living standards, requirement of consumer's especially female consumer to skin nursing is increasingly
Height, " back to nature ", " green safe " consumption have become fashion；In addition, be added to the cosmetics of plant component, because its plant at
The effect of fractionated molecule amount is smaller, can rapidly permeate into skin and play its maintenance skin.Therefore, using Chinese medical extract as active constituent
" green medicine cosmetic " welcome unprecedented opportunity to develop.Night is that physiological function is restrained oneself the rest period nursed, at this moment
Time is maintenance damaged cell on daytime, supplements the nutrients, accelerates the golden age of cell metabolism.Sleep mask product has on the market
Many kinds, effect is different, wherein the sleep mask with functions such as moisturizing, whitening, nti-freckles was once pursued by people,
In order to efficiently be rapidly achieved these effects, most of facial mask is added to various harmful additives in the market, such as preservative, perfume (or spice)
Essence, alcohol, fluorescer, hormone and heavy metal etc., these harmful additives will lead to Skin pigmentation, skin allergy or even make
Immunity degradation leads to aberrant skin cell proliferation, or even canceration occurs.Most skin problem, such as the long acne skin of long spot
Skin is obscure, is all because of skin water shortage and caused by being damaged, and the most fundamental method of nursing skin is replenishing water and preserving moisture reparation,
Otherwise palliative.Moisturizing moisturizing is carried out, and can solve various skin problems and night repairs, better effect.Moisture-keeping functions
It is the most basic function of skin nursing class cosmetics and skin care product, and on the market various have the function such as moisturizing, conditioning
The product of effect declares that moisture preserving time is long, and moisturizing effect is obvious, in fact they be all by glycerol, urea etc. synthesis and it is semi-synthetic
Raw material reaches moistening effect, and such raw material moisture preserving time is short, is not easy to absorb, and safety is low, for a long time using easily to human body band
To injure.
HERBA DENDROBII is the traditional rare Chinese medicine in China, is classified as top grade in " Sheng Nong's herbal classic ".Modern medicine and Chinese medicine
It is apparent that pharmacological research shows that dendrobium nobile has in terms of improving human immunological competence, anti-aging, inhibiting tumour, tonifying five zang organs
Effect.HERBA DENDROBII is commonly called as medicine gold, has remarkable effect to women cosmetology in the civil title for having " help mesona ".Jin Chai
Chemical effective component alkaloid compound mainly has 24 kinds of dry measure used in former times alkali, HERBA DENDROBII alkali and dendrobium nobile pair alkali etc. in dendrobium nobile, these are effectively
Ingredient can dramatically increase the moisture-retaining capacity of skin, promote skin metabolism, restore skin barrier function.Glucan can be improved
Oxidation resistance of the Skin Cell when ultraviolet light irradiates is repaired ultraviolet light and is damaged caused by skin, effectively slow down skin
Light aging promotes fibroblastic proliferation, improves the phagocytic activity of macrophage, can accelerate human immunocyte to bacterium sense
The reaction of dye controls the position of bacterium infection, diminishes inflammation.
Chinese patent CN201610680977.1 discloses a kind of HERBA DENDROBII MASQUE APAISANT HYDRATANT, by weight ratio are as follows: gold
20-30 parts of hairpin dendrobe powder, 20-30 parts of HERBA DENDROBII extracting solution, 5-10 parts of amino acid, 20-30 parts of royal jelly, 30-50 parts of water.It should
Invention has used HERBA DENDROBII powder and HERBA DENDROBII extracting solution, and the dendrobine being rich in HERBA DENDROBII, which has, to relieve pain antipyretic and protect
It is wet and other effects；In addition, the invention joined amino acid and royal jelly, the vitality of epidermal cell can be promoted, effectively facilitate skin
Skin collagen quickly generates, and increases elasticity, and cutin-softening keeps skin more compact.But effective component is less in the invention, and
Royal jelly is difficult to be absorbed by the skin, and moisturizing moisturizing effect is weaker.
Chinese patent CN201710381055.5 discloses a kind of HERBA DENDROBII MASQUE APAISANT HYDRATANT and preparation method thereof, and raw material is pressed
Parts by weight are calculated as: 80-100 parts of Aqueous extracts of fresh of HERBA DENDROBII, and 1-5 parts of trehalose, 1-5 parts of ice crystal forming agent, glycerol 1-5
Part, 1-5 parts of propylene glycol, 1-2 parts of hyaluronic acid, 0.5-1 parts of citric acid, -2 parts of vitamin e1,0.5-1 parts of Phenoxyethanol.The skill
Art has used fresh Aqueous extracts of HERBA DENDROBII, by the fresh item of more than triennial golden hairpin and deionized water according to weight ratio 1:50-1:40
It is made, can completely retain effective component therein, in addition, the trehalose of addition, glycerol, propylene glycol, hyaluronic acid, lemon
Acid, vitamin E and hyaluronic acid are used cooperatively, and are formed layer protecting film in skin surface, are effectively lockked the moisture of skin, and
Damaged skin is repaired, the Transdermal absorption of nutritional ingredient is promoted.But the invention is not added with the effective component of maintenance skin effect,
Maintenance effect is weaker, and is added to propylene glycol, has it is demonstrated experimentally that propylene glycol often makes in cooperation locking agent (occlusion)
With when will appear irritant dermatitis, ratio is substantially in 12%-16%, therefore there is a certain security risk.
In the prior art, all without the effective component for being added with maintenance skin effect, maintenance effect is weak for major part；And it is existing
The moisturizing moisturizing effective component added in technology is few, is extremely difficult to the effect of good moisturizing moisturizing maintenance.Our invention needle
It to defect existing in the prior art, makes improvements, when not adding any specified risk material, utilizes dendrobium nobile, glucan etc.
The Overlay of effective component reaches better moisturizing maintenance moisturizing effect, and moisture preserving time is longer, and the shelf-life is longer, more pacifies
Entirely, has the function of good maintenance skin.
Summary of the invention
The purpose of the present invention is to provide a kind of sleep mask formula and preparation method thereof containing dendrobium nobile, it can effectively be solved
Certainly general facial mask moisture preserving time is short, is not easy to absorb, and safety is low, for a long time using easily injury is brought to human body the problems such as.
To achieve the above object, the invention provides the following technical scheme: a kind of sleep mask containing dendrobium nobile, described contains stone
The sleep mask of dry measure used in former times includes following component: deionized water, dimethyl silicone polymer, isopropyl myristate, butanediol, the third two
Alcohol, glycine betaine, trimethylpentanediol/adipic acid/glycerin crosspolymers, dimethyl silicone polymer PEG-10/15 cross-linked polymeric
Object/dimethyl silicone polymer, PEG-10 Polydimethylsiloxane, ring five dimethyl silicone polymer (and) dimethyl silicone polymer/
Vinyl dimethicone cross polymer, citric acid, sodium citrate, sodium chloride, water/butanediol/purslane extract,
Phenoxyethanol/1,2- hexylene glycol/Chlorphenesin, hyaluronic acid, glucan, water/butanediol/golden hairpin dendrobium extract, Tahiti
Cape jasmine flower extract.
Polydimethylsiloxane PEG-10/15 Crosslinked Polymer/dimethyl silicone polymer preparation method: it will weigh
Measure the Polydimethylsiloxane PEG-10/15 Crosslinked Polymer that number is 20-30 parts and the poly- diformazan that parts by weight are 70-80 parts
Radical siloxane mixes to obtain the final product.
The ring five dimethyl silicone polymer (and) Dimethicone/Vinyl Dimethicone crosslinking is poly-
Close object preparation method: by parts by weight be 20-30 part ring five dimethyl silicone polymer and parts by weight be 70-80 parts gather
Dimethyl siloxane/vinyl dimethicone cross mixed with polymers to obtain the final product.
The water/butanediol/purslane extract preparation method: water, parts by weight by parts by weight for 68 parts
It is mixed for 30 parts of butanediols and 2 parts of purslane extract to obtain the final product；The purslane extract is commercial product, is preferably purchased
It buys in Shanghai Shun Tuo scientific & trading Co., Ltd.: Purslane extract.
The Phenoxyethanol/1,2- hexylene glycol/Chlorphenesin preparation method: the benzene oxygen second for being 40 parts by parts by weight
The Chlorphenesin that the 1,2- hexylene glycol and parts by weight that alcohol, parts by weight are 40 parts are 20 parts mixes to obtain the final product.
The water/butanediol/golden hairpin dendrobium extract preparation method: water, weight by parts by weight for 58-68 parts
Number is that 30-40 parts of butanediol and 2 parts of golden hairpin dendrobium extract mix to obtain the final product；The golden hairpin dendrobium extract passes through quotient
Industry channel is bought, and preferably purchase is in Guangzhou Bo Teng trade Co., Ltd:DNE。
The Tahiti cape jasmine flower extract is bought by commercial channel, and preferably purchase has in the rich biotechnology of speeding in Guangzhou
Limit company: Tahiti gardenia extracting solution.
The sleep mask containing dendrobium nobile includes following component: 58-66 parts of deionized water, poly- diformazan in parts by weight
6-9 parts of radical siloxane, 2-3 parts of isopropyl myristate, 5-7 parts of butanediol, 7-9 parts of propylene glycol, 2-3 parts of glycine betaine, trimethyl
Pentanediol/adipic acid/1-2 parts of glycerin crosspolymers, Polydimethylsiloxane PEG-10/15 Crosslinked Polymer/poly dimethyl
3-4 parts of siloxanes, 0.1-0.3 parts of PEG-10 Polydimethylsiloxane, ring five dimethyl silicone polymer (and) polydimethylsiloxanes
Alkane/1-3 parts of vinyl dimethicone cross polymer, 0.004-0.008 parts of citric acid, 0.2-0.4 parts of sodium citrate,
1-1.5 parts of sodium chloride, water/butanediol/0.5-1 parts of purslane extract, Phenoxyethanol/1,2- hexylene glycol/Chlorphenesin 0.4-
0.6 part, 0.05-0.1 parts of hyaluronic acid, 0.08-0.1 parts of glucan, water/butanediol/2-3 parts of golden hairpin dendrobium extract and tower are uncommon
Mention 0.01-0.03 parts of cape jasmine flower extract.
Preferably, the sleep mask containing dendrobium nobile includes following component in parts by weight: 59-65 parts of deionized water,
7-8 parts of dimethyl silicone polymer, 2-3 parts of isopropyl myristate, 5-7 parts of butanediol, 7-9 parts of propylene glycol, 2-3 parts of glycine betaine,
Trimethylpentanediol/adipic acid/1-2 parts of glycerin crosspolymers, Polydimethylsiloxane PEG-10/15 Crosslinked Polymer/poly-
3-4 parts of dimethyl siloxane, 0.1-0.3 parts of PEG-10 Polydimethylsiloxane, ring five dimethyl silicone polymer (and) poly- diformazan
Radical siloxane/1-3 parts of vinyl dimethicone cross polymer, 0.004-0.008 parts of citric acid, sodium citrate 0.2-
0.4 part, 1-1.5 parts of sodium chloride, water/butanediol/0.6-0.9 parts of purslane extract, Phenoxyethanol/1,2- hexylene glycol/chlorobenzene
Sweet ether 0.4-0.6 parts, 0.05-0.1 parts of hyaluronic acid, 0.08-0.1 parts of glucan, water/butanediol/golden hairpin dendrobium extract 2-3
Part and 0.01-0.03 parts of Tahiti cape jasmine flower extract.
It is highly preferred that the sleep mask containing dendrobium nobile includes following component in parts by weight: deionized water 61-63
Part, 7-8 parts of dimethyl silicone polymer, 2-3 parts of isopropyl myristate, 5-7 parts of butanediol, 7-9 parts of propylene glycol, glycine betaine 2-3
Part, trimethylpentanediol/adipic acid/1-2 parts of glycerin crosspolymers, Polydimethylsiloxane PEG-10/15 Crosslinked Polymer/
3-4 parts of dimethyl silicone polymer, 0.1-0.3 parts of PEG-10 Polydimethylsiloxane, ring five dimethyl silicone polymer (and) poly- two
Methylsiloxane/1-3 parts of vinyl dimethicone cross polymer, 0.004-0.008 parts of citric acid, sodium citrate
0.2-0.4 parts, 1-1.5 parts of sodium chloride, water/butanediol/0.7-0.8 parts of purslane extract, Phenoxyethanol/1,2- hexylene glycol/
0.4-0.6 parts of Chlorphenesin, 0.05-0.1 parts of hyaluronic acid, 0.08-0.1 parts of glucan, water/butanediol/HERBA DENDROBII extract
2-3 parts and 0.01-0.03 parts of Tahiti cape jasmine flower extract of object.
Preferably, the preparation method of the sleep mask containing dendrobium nobile, comprising the following steps: step 1, raw material weigh；
Step 2 prepares aqueous phase solution；Step 3, cooling stirring；Step 4 prepares oil-phase solution；Step 5 prepares mixed solution；
Step 6, stirring, homogeneous；Step 7, finished product save.
According to above-described preparation method, specific steps are as follows:
In step 1, raw material is weighed according to formulation dosage；
In step 2, deionized water, butanediol, the propylene glycol, glycine betaine, trimethyl of formulation dosage is added in water phase pot
Pentanediol/adipic acid/glycerin crosspolymers, citric acid, hyaluronic acid, sodium citrate, sodium chloride, glucan, are warming up to 75
DEG C -85 DEG C, material stirring to uniform aqueous phase solution 1；
In step 3, the uniform aqueous phase solution 1 in step 2 is kept the temperature into 30min, stirring drop at a temperature of 75 DEG C -85 DEG C
Temperature forms uniform aqueous phase solution 2 to 40 DEG C -50 DEG C, spare；
In step 4, dimethyl silicone polymer, isopropyl myristate, five poly dimethyl silicon of ring are added in emulsion pot
Oxygen alkane (and) Dimethicone/Vinyl Dimethicone cross-linked polymer, dimethyl silicone polymer PEG-10/15
Cross-linked polymer/dimethyl silicone polymer, PEG-10 Polydimethylsiloxane, Tahiti cape jasmine flower extract, after mixing evenly,
Homogeneous 3-5min is mixed into uniform oil-phase solution；
In step 5, aqueous phase solution 2 uniform in step 3 is pumped into while stirring in the uniform oil-phase solution of step 4
(stirring of this process is opened to middling speed, and 1/3) Water-pumping valve is opened into, after aqueous phase solution exhausts, be stirred for 5-10min, mixed
Solution；
In step 6, into the mixed solution that step 5 obtains, remaining ingredient is added according to formula ratio, stirs evenly
Afterwards, homogeneous 2-3min, product inspection qualification to get.
Preparation method described in above-mentioned technical proposal, preferably, rising temperature to 76 DEG C -84 DEG C in the step 2；It is excellent
Selection of land rises temperature to 77 DEG C -83 DEG C；Preferably, temperature is risen to 78 DEG C -82 DEG C；More preferably 79 DEG C -81 DEG C, temperature is risen to 80
℃。
Preparation method described in above-mentioned technical proposal, preferably, stirring is cooled to 41 DEG C -49 DEG C in the step 3；
Preferably, stirring is cooled to 42 DEG C -48 DEG C；Preferably, stirring is cooled to 43 DEG C -47 DEG C；Preferably, stirring be cooled to 44 DEG C-
46℃；It is highly preferred that stirring is cooled to 45 DEG C.
Preparation method described in above-mentioned technical proposal, preferably, in the step 4, it is preferable that mixing when
Between be 4min-6min；It is highly preferred that the time being mixed is 5min.
The effect of each active constituent are as follows:
(1) effective component in HERBA DENDROBII can dramatically increase the moisture-retaining capacity of skin, promote skin metabolism, restore
Skin barrier function；(2) oxidation resistance of the Skin Cell in ultraviolet light irradiation can be improved in glucan, repairs ultraviolet light pair
It is damaged caused by skin, effectively slows down the light aging of skin, promote fibroblastic proliferation, improve the phagocytosis energy of macrophage
Power can accelerate reaction of the human immunocyte to bacterium infection, control the position of bacterium infection, diminish inflammation；(3) poly dimethyl
Siloxanes and its derivative are all the quality raw materials of cosmetics, have good skin-protecting function, nontoxic, stingless to skin and mucous membrane
Swash property, there is greasy property, anti-ultraviolet effect, good permeability usually can be all used in moisture retention product in skin care item, one
A little top grade skin care item also can all be applied；(4) isopropyl myristate can play the role of moisturizing and skin care, skin
It is preferable to the absorbability of this product, it can effectively be contacted in cortex with hair follicle, penetrate into cortex depths, and by the active group in cosmetics
Divide and bring into, gives full play to the effect of effective component, be good moisturizer and bleeding agent；(5) hyaluronic acid is natural moisturizing
Silver has special water retention, can also promote the Transdermal absorption of other nutriments while moisturizing；(6) purslane
Extract has anti-drying aging in winter, increases skin comfort degree and removes free radical, improves the comprehensive of skin comfort etc.
Performance is closed, the flavones and saponin contained in purslane, which has, removes free radical and antioxidation, can be with delay skin aging；(7)
Tahiti cape jasmine flower extract is spent moisturizing factor (sour (gradenlicacid) A, B and son acid) rich in natural gardenia, balance skin fat secretion,
Keep skin refreshing and vigor；(8) Chlorphenesin is a kind of preservative, compatible with most of preservatives；(9) 1,2- hexylene glycol generation
Have the function of promoting infiltration for propylene glycol, also there is certain antisepsis.
Compared with prior art, the beneficial effects of the present invention are: (1) is added to a large amount of safe high active ingredients, there will be length
The ingredient of moistening effect and core active ingredient, the glucan binding domian of Herba Dendrobii extract are imitated, skin immunity is improved, improves skin
Itself repair ability has extraordinary moisturizing moisturizing repairing effect；(2) addition of Tahiti gardenia, with other activity at
Divide and generate synergistic effect, so that while Whitening, spot moisturizing, second day facial edema can be effectively relieved in the invention；
(3) addition of glucan enhances Phenoxyethanol/1,2- hexylene glycol/Chlorphenesin antisepsis, and the facial mask shelf-life is longer；
(4) the invention all has the function of moisturizing moisturizing maintenance for all age group, for group it is more.By these effective components
It is used in combination, the performance of face permeability of the membrane, moisturizing moisturizing maintenance will be greatly reinforced, and the moisturizing moisturizing time is longer, the shelf-life
It is longer, it is safer, it can be used for a long time.
Specific embodiment
It describes in detail combined with specific embodiments below to technical method of the invention:
Embodiment 1: a kind of sleep mask containing dendrobium nobile includes following component: 58 parts of deionized water, poly- two in parts by weight
6 parts of methylsiloxane, 2 parts of isopropyl myristate, 5 parts of butanediol, 7 parts of propylene glycol, 2 parts of glycine betaine, trimethylpentanediol/oneself
1 part of diacid/glycerin crosspolymers, 3 parts of Polydimethylsiloxane PEG-10/15 Crosslinked Polymer/dimethyl silicone polymer,
0.1 part of PEG-10 Polydimethylsiloxane, ring five dimethyl silicone polymer (and) dimethyl silicone polymer/vinylpolydimethyl
1 part of Dimethicone Crosspolymer, 0.004 part of citric acid, 0.2 part of sodium citrate, 1 part of sodium chloride, water/butanediol/purslane mention
Take 0.5 part of object, Phenoxyethanol/1,2- hexylene glycol/0.4 part of Chlorphenesin, 0.05 part of hyaluronic acid, 0.1 part of glucan, water/fourth
0.03 part of 2 parts of glycol/golden hairpin dendrobium extract and Tahiti cape jasmine flower extract；Wherein, dimethyl silicone polymer PEG-10/15
The Polydimethylsiloxane PEG-10/15 Crosslinked Polymer that cross-linked polymer/dimethyl silicone polymer is 25 parts by parts by weight
The dimethyl silicone polymer for being 75 parts with parts by weight, which is uniformly mixed, to be prepared；Ring five dimethyl silicone polymer (and) poly- diformazan
Radical siloxane/vinyl dimethicone cross polymer by parts by weight be 25 parts ring five dimethyl silicone polymer and
Parts by weight be 75 parts Dimethicone/Vinyl Dimethicone cross-linked polymer be uniformly mixed preparation and
At；Water, the butanediol that parts by weight are 30 parts and 2 parts of the horse that water/butanediol/purslane extract is 68 parts by parts by weight
Sativa extract is uniformly mixed and is prepared；Phenoxyethanol/1,2- hexylene glycol/Chlorphenesin preparation method is by parts by weight
40 parts of Phenoxyethanol, the 1,2- hexylene glycol that parts by weight are 40 parts and Chlorphenesin that parts by weight are 20 parts are uniformly mixed system
It is standby to form.
The preparation method of the sleep mask containing dendrobium nobile, comprising the following steps:
Step 1: raw material is weighed according to formulation dosage；
Step 2 prepares aqueous phase solution: deionized water, butanediol, the propylene glycol, beet of formulation dosage is added in water phase pot
Alkali, trimethylpentanediol/adipic acid/glycerin crosspolymers, citric acid, sodium citrate, sodium chloride, glucan, are warming up to 80
DEG C, material stirring to uniform aqueous phase solution 1；
Cooling stirring: uniform aqueous phase solution in step 2 is kept the temperature 30min, stirring drop by step 3 at a temperature of 80 DEG C
Temperature forms uniform aqueous phase solution 2 to 45 DEG C, spare；
Step 4 prepares oil-phase solution: dimethyl silicone polymer, isopropyl myristate, ring five being added in emulsion pot
Dimethyl silicone polymer (and) Dimethicone/Vinyl Dimethicone cross-linked polymer, polydimethylsiloxanes
Alkane PEG-10/15 cross-linked polymer/dimethyl silicone polymer, PEG-10 Polydimethylsiloxane and Tahiti gardenia are extracted
Object, after mixing evenly, homogeneous 5min is mixed into uniform oil-phase solution；
Step 5 prepares mixed solution: the uniform aqueous phase solution to have cooled down in step 3 being pumped into step 4 while stirring
Uniform oil-phase solution in (this process stirring open to middling speed, 1/3) Water-pumping valve is opened into, after aqueous phase solution exhausts, be stirred for
10min obtains mixed solution；
Stirring, homogeneous: into the mixed solution that step 5 obtains, surplus stock is added according to formula, stirring is equal in step 6
After even, homogeneous 3min, product inspection qualification to get；
Step 7, finished product save.
Embodiment 2: a kind of sleep mask containing dendrobium nobile includes following component: 62 parts of deionized water, poly- two in parts by weight
8 parts of methylsiloxane, 2 parts of isopropyl myristate, 6 parts of butanediol, 8 parts of propylene glycol, 2 parts of glycine betaine, trimethylpentanediol/oneself
1 part of diacid/glycerin crosspolymers, 3 parts of Polydimethylsiloxane PEG-10/15 Crosslinked Polymer/dimethyl silicone polymer,
0.2 part of PEG-10 Polydimethylsiloxane, ring five dimethyl silicone polymer (and) dimethyl silicone polymer/vinylpolydimethyl
2 parts of Dimethicone Crosspolymer, 0.006 part of citric acid, 0.3 part of sodium citrate, 1.3 parts of sodium chloride, water/butanediol/purslane
0.8 part of extract, Phenoxyethanol/1,2- hexylene glycol/0.5 part of Chlorphenesin, 0.008 part of hyaluronic acid, 0.09 part of glucan,
0.02 part of water/2 parts of butanediol/golden hairpin dendrobium extract and Tahiti cape jasmine flower extract；Wherein, dimethyl silicone polymer PEG-
10/15 cross-linked polymer/dimethyl silicone polymer is crosslinked poly- by the dimethyl silicone polymer PEG-10/15 that parts by weight are 20 parts
The dimethyl silicone polymer that conjunction object and parts by weight are 80 parts, which is uniformly mixed, to be prepared；Ring five dimethyl silicone polymer (and) poly-
Five polydimethylsiloxanes of ring that dimethyl siloxane/vinyl dimethicone cross polymer is 20 parts by parts by weight
The Dimethicone/Vinyl Dimethicone cross-linked polymer that alkane and parts by weight are 80 parts is uniformly mixed preparation
It forms；Water that water/butanediol/purslane extract is 68 parts by parts by weight, the butanediol that parts by weight are 30 parts and 2 parts
Purslane extract is uniformly mixed and is prepared；Phenoxyethanol/1,2- hexylene glycol/Chlorphenesin preparation method is by parts by weight
For 40 parts of Phenoxyethanols, parts by weight be 40 parts 1,2- hexylene glycol and parts by weight be 20 parts Chlorphenesin be uniformly mixed
It is prepared.
The preparation method of the sleep mask containing dendrobium nobile, comprising the following steps:
Step 1: raw material is weighed according to formulation dosage；
Step 2 prepares aqueous phase solution: deionized water, butanediol, the propylene glycol, beet of formulation dosage is added in water phase pot
Alkali, trimethylpentanediol/adipic acid/glycerin crosspolymers, citric acid, sodium citrate, sodium chloride, hyaluronic acid, glucan,
85 DEG C are warming up to, material stirring to uniform aqueous phase solution 1；
Cooling stirring: uniform aqueous phase solution 1 in step 2 is kept the temperature 30min, stirring drop by step 3 at a temperature of 85 DEG C
Temperature forms aqueous phase solution 2 to 40 DEG C, spare；
Step 4 prepares oil-phase solution: dimethyl silicone polymer, isopropyl myristate, ring five being added in emulsion pot
Dimethyl silicone polymer (and) Dimethicone/Vinyl Dimethicone cross-linked polymer, polydimethylsiloxanes
Alkane PEG-10/15 cross-linked polymer/dimethyl silicone polymer, PEG-10 Polydimethylsiloxane and Tahiti gardenia are extracted
Object, after mixing evenly, homogeneous 3min is mixed into uniform oil-phase solution；
Step 5 prepares mixed solution: the uniform aqueous phase solution to have cooled down in step 3 being pumped into step 4 while stirring
Uniform oil-phase solution in (this process stirring open to middling speed, 1/3) Water-pumping valve is opened into, after aqueous phase solution exhausts, be stirred for
5min obtains mixed solution；
Stirring, homogeneous: into the mixed solution that step 5 obtains, surplus stock is added according to formula, stirring is equal in step 6
After even, homogeneous 2min, product inspection qualification to get；
Step 7, finished product save.
Embodiment 3: a kind of sleep mask containing dendrobium nobile includes following component: 66 parts of deionized water, poly- two in parts by weight
9 parts of methylsiloxane, 3 parts of isopropyl myristate, 7 parts of butanediol, 9 parts of propylene glycol, 3 parts of glycine betaine, trimethylpentanediol/oneself
2 parts of diacid/glycerin crosspolymers, 4 parts of Polydimethylsiloxane PEG-10/15 Crosslinked Polymer/dimethyl silicone polymer,
0.3 part of PEG-10 Polydimethylsiloxane, ring five dimethyl silicone polymer (and) dimethyl silicone polymer/vinylpolydimethyl
3 parts of Dimethicone Crosspolymer, 0.008 part of citric acid, 0.4 part of sodium citrate, 1.5 parts of sodium chloride, water/butanediol/purslane
1 part of extract, Phenoxyethanol/1,2- hexylene glycol/0.6 part of Chlorphenesin, 0.1 part of hyaluronic acid, 0.08 part of glucan, water/fourth
0.01 part of 3 parts of glycol/golden hairpin dendrobium extract and Tahiti cape jasmine flower extract；Wherein, dimethyl silicone polymer PEG-10/15
The Polydimethylsiloxane PEG-10/15 Crosslinked Polymer that cross-linked polymer/dimethyl silicone polymer is 30 parts by parts by weight
The dimethyl silicone polymer for being 70 parts with parts by weight, which is uniformly mixed, to be prepared；Ring five dimethyl silicone polymer (and) poly- diformazan
Radical siloxane/vinyl dimethicone cross polymer by parts by weight be 30 parts ring five dimethyl silicone polymer and
Parts by weight be 70 parts Dimethicone/Vinyl Dimethicone cross-linked polymer be uniformly mixed preparation and
At；Water, the butanediol that parts by weight are 30 parts and 2 parts of the horse that water/butanediol/purslane extract is 68 parts by parts by weight
Sativa extract is uniformly mixed and is prepared；Phenoxyethanol/1,2- hexylene glycol/Chlorphenesin preparation method is by parts by weight
40 parts of Phenoxyethanol, the 1,2- hexylene glycol that parts by weight are 40 parts and Chlorphenesin that parts by weight are 20 parts are uniformly mixed system
It is standby to form.
The preparation method of the sleep mask containing dendrobium nobile, comprising the following steps:
Step 1: raw material is weighed according to formulation dosage；
Step 2 prepares aqueous phase solution: deionized water, butanediol, the propylene glycol, beet of formulation dosage is added in water phase pot
Alkali, trimethylpentanediol/adipic acid/glycerin crosspolymers, citric acid, sodium citrate, sodium chloride, hyaluronic acid, glucan,
75 DEG C are warming up to, material stirring to uniform aqueous phase solution；
Cooling stirring: uniform aqueous phase solution in step 2 is kept the temperature 30min, stirring drop by step 3 at a temperature of 75 DEG C
Temperature is spare to 50 DEG C；
Step 4 prepares oil-phase solution: dimethyl silicone polymer, isopropyl myristate, ring five being added in emulsion pot
Dimethyl silicone polymer (and) Dimethicone/Vinyl Dimethicone cross-linked polymer, polydimethylsiloxanes
Alkane PEG-10/15 cross-linked polymer/dimethyl silicone polymer, PEG-10 Polydimethylsiloxane, Tahiti cape jasmine flower extract,
After mixing evenly, homogeneous 4min is mixed into uniform oil-phase solution；
Step 5 prepares mixed solution: the uniform aqueous phase solution to have cooled down in step 3 being pumped into step 4 while stirring
Uniform oil-phase solution in (this process stirring open to middling speed, 1/3) Water-pumping valve is opened into, after aqueous phase solution exhausts, be stirred for
8min obtains mixed solution；
Stirring, homogeneous: step 6 into the mixed solution that step 5 obtains, according to surplus stock is added in formula, stirs
Uniformly after, homogeneous 3min, product inspection qualification to get；
Step 7, finished product save.
Embodiment 4: a kind of sleep mask containing dendrobium nobile, the difference with embodiment 1 are only that the glucan containing 0.01 part.
Comparative example 1: a kind of sleep mask containing dendrobium nobile, the difference with embodiment 1 are only that without glucan.
Comparative example 2: a kind of sleep mask containing dendrobium nobile, the difference with embodiment 1 is only that be mentioned without Tahiti gardenia
Take object.
Comparative example 3: a kind of HERBA DENDROBII is prepared by embodiment 1 in prior art China patent CN201710381055.5 and is slept
Dormancy facial mask.
Experimental example 1: facial mask moisturizing moisturizing anti-senescence function experiment
100 kunming mices are selected, are provided by Military Medical Science Institute's animal center, wherein 50 aged rats, 50 childrens
Year mouse tests mouse skin moisture with Skin Moisture Test Pen, and it is about consistent to choose 50 aged rats moisture of skin, 50 childhood
Mouse moisture of skin is about consistent.Embodiment 1-3, comparative example 1 and comparative example 3 all take 10 aged rats and 10 young rats, will be real
It tests mouse back wool to cut, unhairing range about 4cm × 6cm, tests mouse skin moisture, young rat skin with Skin Moisture Test Pen
Water content average value is 25%, and aged rats moisture content of skin average value is 15%.1g product is taken to be directly applied to skin at night in daily
On skin, moisture content of skin average value (W is detected after massaging and absorbing1), morning next day detects moisture content of skin average value again
(W2), concrete outcome is as shown in table 1.
Table 1
The results show that compared with prior art, the present invention has good moisturizing moisturizing anti-aging function, and the present invention
Also there is good replenishing water and preserving moisture effect to aged rats, aged rats are moistened using the more compact water of skin after two weeks, restore elasticity, and show
There is invention substantially invalid to aged rats.Experiment discovery mouse skin is without allergic phenomenas such as red and swollen bubbles, it was demonstrated that product safety can
It leans on, to no skin irritation.
Experimental example 2: facial mask multiple-effect functional experiment
It needs to filter out 50 volunteers according to experiment, is classified as two groups of A, B, wherein the easy oedema of 25 human face of A group, hair
Hole is coarse, there is small pox and acne print；25 application on human skin of B group dries water shortage, and skin is obscure, there is different degrees of spot.Each embodiment
The people of 5 A groups and the people of 5 B groups are all selected with comparative example, and product is used before sleeping at night daily, it is one month on probation, as a result
As shown in table 2.
Table 2
It will thus be seen that provided by the invention sleep can achieve the effect of multiple-effect maintenance skin problem, and Tahiti Cape jasmine
The addition of sub- flower extract can effectively mitigate the skin problem of getting up early facial edema.
Experimental example 3: facial mask shelf-life experiment
50 kunming mices are selected, are provided by Military Medical Science Institute's animal center, are divided into totally 5 groups of A, B, C, D, E, by real
Test 1 shaving of example.The facial mask of embodiment 1-4 and comparative example 1 are put into the environment of high temperature and humidity profit, accelerate it rotten.3 months
Afterwards, it takes out facial mask to be applied to respectively on 5 groups of mouse skins, erythema redness rate occurs in observation mouse skin, and the results are shown in Table 3；6
It after month, takes out facial mask and is applied on 5 groups of mouse skins respectively, erythema redness rate occurs in observation mouse skin, and the results are shown in Table 4.
From the results, it was seen that the addition of glucan, extends the shelf-life of facial mask.
Table 3
| Grouping | Erythema redness rate (%) |
| A | 0 |
| B | 0 |
| C | 0 |
| D | 20 |
| E | 40 |
Table 4
| Grouping | Erythema redness rate (%) |
| A | 0 |
| B | 0 |
| C | 0 |
| D | 40 |
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto,
Anyone skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (9)
1. a kind of sleep mask containing dendrobium nobile, it is characterised in that:
It in parts by weight include following component: 58-66 parts of deionized water, 6-9 parts of dimethyl silicone polymer, isopropyl myristate
2-3 parts, 5-7 parts of butanediol, 7-9 parts of propylene glycol, 2-3 parts of glycine betaine, trimethylpentanediol/adipic acid/glycerin crosspolymers
1-2 parts, Polydimethylsiloxane PEG-10/15 Crosslinked Polymer/3-4 parts of dimethyl silicone polymer, PEG-10 poly dimethyl silicon
0.1-0.3 parts of oxygen alkane, ring five dimethyl silicone polymer (and) Dimethicone/Vinyl Dimethicone crosslinking is poly-
Close object 1-3 parts, 0.004-0.008 parts of citric acid, 0.2-0.4 parts of sodium citrate, 1-1.5 parts of sodium chloride, water/butanediol/dent
0.5-1 parts of amaranth extract, Phenoxyethanol/1,2- hexylene glycol/0.4-0.6 parts of Chlorphenesin, 0.05-0.1 parts of hyaluronic acid, Portugal are poly-
0.01-0.03 parts of 0.08-0.1 parts sugared, water/butanediol/2-3 parts of golden hairpin dendrobium extract and Tahiti cape jasmine flower extract.
2. the sleep mask according to claim 1 containing dendrobium nobile, it is characterised in that: in parts by weight include following component:
59-65 parts of deionized water, 7-8 parts of dimethyl silicone polymer, 2-3 parts of isopropyl myristate, 5-7 parts of butanediol, propylene glycol 7-9
Part, 2-3 parts of glycine betaine, trimethylpentanediol/adipic acid/1-2 parts of glycerin crosspolymers, dimethyl silicone polymer PEG-10/
15 cross-linked polymers/3-4 parts of dimethyl silicone polymer, 0.1-0.3 parts of PEG-10 Polydimethylsiloxane, five poly dimethyl silicon of ring
Oxygen alkane (and) 1-3 parts of Dimethicone/Vinyl Dimethicone cross-linked polymer, citric acid 0.004-0.008
Part, 0.2-0.4 parts of sodium citrate, 1-1.5 parts of sodium chloride, water/butanediol/0.6-0.9 parts of purslane extract, Phenoxyethanol/
1,2- hexylene glycol/0.4-0.6 parts of Chlorphenesin, 0.05-0.1 parts of hyaluronic acid, 0.08-0.1 parts of glucan, water/butanediol/gold
2-3 parts and 0.01-0.03 parts of Tahiti cape jasmine flower extract of hairpin Herba Dendrobii extract.
3. the sleep mask according to claim 1 containing dendrobium nobile, it is characterised in that: by weight number include below at
Point: 61-63 parts of deionized water, 7-8 parts of dimethyl silicone polymer, 2-3 parts of isopropyl myristate, 5-7 parts of butanediol, propylene glycol
7-9 parts, 2-3 parts of glycine betaine, trimethylpentanediol/adipic acid/1-2 parts of glycerin crosspolymers, dimethyl silicone polymer PEG-
10/15 cross-linked polymer/3-4 parts of dimethyl silicone polymer, 0.1-0.3 parts of PEG-10 Polydimethylsiloxane, the poly- diformazan of ring five
Radical siloxane (and) 1-3 parts of Dimethicone/Vinyl Dimethicone cross-linked polymer, citric acid 0.004-
0.008 part, 0.2-0.4 parts of sodium citrate, 1-1.5 parts of sodium chloride, water/butanediol/0.7-0.8 parts of purslane extract, benzene oxygen
Ethyl alcohol/1,2- hexylene glycol/0.4-0.6 parts of Chlorphenesin, 0.05-0.1 parts of hyaluronic acid, 0.08-0.1 parts of glucan, water/fourth two
Alcohol/2-3 parts of golden hairpin dendrobium extract and 0.01-0.03 parts of Tahiti cape jasmine flower extract.
4. a kind of preparation method of the described in any item sleep masks containing dendrobium nobile of claim 1-3, it is characterised in that: described
Preparation method the following steps are included:
Step 1, raw material weigh；Step 2 prepares aqueous phase solution；Step 3, cooling stirring；Step 4 prepares oil-phase solution；
Step 5 prepares mixed solution；Step 6, stirring, homogeneous；Step 7, finished product save；
In step 1, raw material is weighed according to formulation dosage；
In step 2, deionized water, butanediol, the propylene glycol, glycine betaine, trimethyl penta 2 of formulation dosage is added in water phase pot
Alcohol/adipic acid/glycerin crosspolymers, citric acid, hyaluronic acid, sodium citrate, sodium chloride and glucan, be warming up to 75 DEG C-
85 DEG C, material stirring to uniform aqueous phase solution 1；
In step 3, the uniform aqueous phase solution 1 in step 2 is kept the temperature into 30min at 75 DEG C -85 DEG C, stirring is cooled to 40
DEG C -50 DEG C, uniform aqueous phase solution 2 is formed, it is spare；
In step 4, dimethyl silicone polymer, isopropyl myristate, ring five dimethyl silicone polymer are added in emulsion pot
(and) Dimethicone/Vinyl Dimethicone cross-linked polymer, dimethyl silicone polymer PEG-10/15 crosslinking
Polymer/dimethyl silicone polymer, PEG-10 Polydimethylsiloxane, Tahiti cape jasmine flower extract, after mixing evenly, homogeneous
3-5min is mixed into uniform oil-phase solution；
In step 5, aqueous phase solution 2 uniform in step 3 is pumped into while stirring in the uniform oil-phase solution of step 4, water phase
After solution 2 exhausts, it is stirred for 5-10min, obtains mixed solution；
In step 6, into the mixed solution that step 5 obtains, remaining ingredient is added according to formula ratio, after mixing evenly,
Homogeneous 2-3min, examination and test of products qualification to get.
5. the preparation method according to claim 4, it is characterised in that: in the step 2, rise temperature to 79 DEG C -81 DEG C.
6. the preparation method according to claim 4, it is characterised in that: in the step 3, stirring is cooled to 44 DEG C -46
℃。
7. preparation method according to claim 4, it is characterised in that: in the step 4, the time of mixing is 5min.
8. preparation method according to claim 5, it is characterised in that: in the step 2, rise temperature to 80 DEG C.
9. preparation method according to claim 6, it is characterised in that: in the step 3, stirring is cooled to 45 DEG C.
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| CN111616983B (en) * | 2020-04-23 | 2023-06-27 | 安徽科昂纳米科技有限公司 | Tear-off mask containing aerogel and preparation method thereof |
| CN112494412A (en) * | 2020-11-27 | 2021-03-16 | 陈珲 | Skin tightening smearing type mask |
| CN112263492A (en) * | 2020-11-27 | 2021-01-26 | 天津郁美净集团有限公司 | Formula of jelly-like suspended oil drop high-moisture sleeping mask and preparation process thereof |
| CN115068381B (en) * | 2022-06-29 | 2023-08-25 | 杭州心悦化妆品有限公司 | Natural mild cleansing emulsion and preparation method thereof |
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| CN108451847A (en) * | 2018-03-30 | 2018-08-28 | 珠海美高美健康科技有限公司 | Facial mask liquid and its preparation method and application containing dendrobium candidum extract |
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